Document e1eE89MZ1RGjLmRBO1qEQZ3LG

Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTI R X CAT" EE OR ANALYSIS Date: 1- Customer: September 10, 1992 Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: September 8, 1992 VKIA Product: 5265 Railcar No.: VIPX 45828 Order No.: 0014017-008 Property Test Method Specification Analysis Moisture, % ABR-1A 0.30 Max. 0.12 Bulk Density, gm/cc ABR-2A 0.520 Min. 0.542 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 17.2 % On Pan 5.0 Max. 3.6 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.050 Inherent Viscosity ABR-10 0.64 - 0.68 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202071 Vista Polymers ** Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date: Time Logged In: /(?P0 Ship Date: Product: Car No.: Logged In By: Co Order No: rf0/7-00S Silo(s): Customer: Ni\p<U) A/v Compartment A Sample From Bottom Moisture % . &2 BL Contain inat ion BR / Bulk Density 'W2. BD w/antistat CA Bottom 7 CB Bottom 22 JS /> B Bottom 6 Z Tappi Test 06 or less .07 . 15 .20 Contamination Composite .60 Screen Analysis Mesh \ Weight 40 <A o % 60 O fi 80 3'-/t 100 7' IS 120 140 2?? 200 Pan 17' 3*? Static Flow: /*?*> Color L: Avg. Microns: fQ*l a 0*7$ b Technician: /?t* ^ ^If wmm WPMV VAB.0001202072 f / Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 c ee re I R ICATE OR ANAL-YS X S A Date: September 10, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: September S, 1992 VBIA Product: 5265 Railcar No.: UTCX 46566 Order No.: 0014017-009 Property Test Method Specification Analysis Moisture, % ABR-1A 0.30 Max. 0.20 Bulk Density, gm/cc ABR-2A 0.520 Min. 0.544 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 15.0 % On Pan 5.0 Max. 3.0 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.052 Inherent Viscosity ABR-10 0.64 - 0.68 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. (^Bagwe 1K.J Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202073 Vista Polymers Highway 25 Aberdeen, MS $9730 A RAILCAR ANALYSIS Load Date: / ^ ^ ~ 1 Time Logged In d6 o Ship Date: AJt> /yr/H-~ Product: Logged In By: Order No : Car No 4(,rt> C Silo(s) ,G2l_ Customer: {\}{^D&& Compartment A Sample From Bottom Moisture % /* BL Contarnination BR Bulk Density 13 BD w/antistat CA Bottom ./? CB Bottom .20 B Bottom 20 11 3 Screen Analysis Mesh Weight % 40 04& OrO 60 QrOG 0.1 80 3.40 Static Flow: ^ / 7*/ Color L: 100 120 J0* 140 200 yj.rp 27.(3 ts.o Pan 3,0 Avg. Microns: /3^- / a QAl b * Technician: VAB.0001202074 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date 1992 Customer: Nibco, Inc 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: September 14, 1992 VIS1A Product: 5265 PLWX 44676 Order No.: 0014017-010 Test Method Soecification Analysis Moisture, % ABR-1A 0.30 Max. 0.23 Bulk Density, gm/cc ABR-2A 0.520 Min. 0.545 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 14.8 % On Pan 5.0 Max. 3.1 is 25.0% Max. for th 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.082 Inherent Viscosity ABR--10 0.64 - 0.68 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E\ Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202075 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS PcLO*f Load Date: S-Cf'2- Time Logged In: VM'DQ Ship Date: Product Car No. M- U (> 91 Logged In By: a Silo(s) Order No:. 0 l7"0/Onnflt.nBftr: 4 floytieMl-- Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density 0 6 A BD w/antistat Viscosity RVCM Zp> 3 o% z. CA Bottom .1# 3 .SH . 4>S7 .066, Tappi Test Contamination Composite . 06 or less .07 CB Bottom 33 lrSie> Dto-L . 15 B Bottom S' 3 / 20 .60 Screen Analysis Mesh Weight % 40 .6 60 Op 60 OjO 80 0 Static Flow: L Color L: 100 120 140 200 Pan ifeS Zf* 3.1 Avg. Microns a osf b /.4g Technician: mmm PRU mm mm VAB.0001202076 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601)369-8111 CERTIFICATE OF ANALYSIS A September 21, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: September 14, 1992 VK1A Product: 5265 Railcar No.: GACX 73400 Order No.: 0014017-011 Property Test Method Specification Analysis Moisture, % ABR-1A 0.30 Max. 0.22 Bulk Density, gm/cc ABR--2A 0.520 Min. 0.542 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 13.1 % On Pan 5.0 Max. 2.7 is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.133 Inherent Viscosity ABR--10 0.64 0.68 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy eY Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202077 Vista Polymers Highway 25 Aberdeen, MS 39730 V F>VO RAILCAR ANALY XS (>ACjL Load Date Time Logged In: Ship Date: ^^^ Product: Logged In By: Order No: Car No.: __ Silo(e): 11 Customer: /^l , ^A* /V\AO Compartment A Sample From Moisture % Bottom BL Contamination BR 9 Bulk Density ,S3(> BD w/antistat Viscosity RVCM (,<n ./53 CA Bottom .a/ j J7-. .537 .Asf& 4 Tappi Test Contamination Composite .06 or less 07 CB Bottom y u .05^ . 15 B Bottom .*o a f [osiT .20 .60 Screen Analysis Mesh Weight % 40 0.0*0 0.0 60 80 100 120 140 200 Pan S.Q3 9-3^ 1&.03 U.00 (,.$3 1M_ <?9.PLo Static Flow : 0 Avg. Microns Color L: n*s- a .34 b ITS. 2 Technician Co+ ^5 VAB.0001202078 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS A September 21, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: September 14, 1992 VIS1A Product: 5265 Railcar No.: VIPX 45866 Order No.: 0015895-000 Propertv Test Method Soecification Analvs Moisture, % ABR-1A 0.30 Max. 0.16 Bulk Density, gm/cc ABR-2A 0.520 Min. 0.543 Particle Size Distribution ABR--3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 16.8 % On Pan 5.0 Max. 2.4 is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.121 Inherent Viscosity ABR-10 0.64 0.68 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell (601) 369-3624 Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 i VAB.0001202079 Vista Polymers Highway 25 Aberdeen, MS 39730 A E>va RAILCAR ANALYSTS Load Date: <9 - 3-9X Time Logged In: Ship Date: ql/fh V Product: Logged In By: Order No : OO Car No. Silo(e): Customer: I\!\IQo . Compartment A Sample From Bottom Moisture % BL Contamination BR A Bulk Density BD w/antistat &LL Viscosity RVCM ,1 'Ll CA Bottom 3 .s</J . (ftp S .ooz Tappi Test Contamination Composite 06 or less .07 CB Bottom 3 7 M3 . 15 B Bottom a L Ms .11 .20 .60 Screen Analysis Mesh Weight % 40 O, OQ 0,0 60 P.Qg .SI 60 (.% <5W 100 7-.S3 is,/ 120 140 /3I 35SL 3o_ 200 In Pan /,v il.X 3.U Static Flow: (U. Avg. Microns Color L: 99-& a 0.&Q b Technician Ck VAB.0001202080 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE 07 ANALYSIS A September 23, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro. GA 30642 Attention: Steve Ryan Ship Date: September 21, 1992 VISHA Product: 5265 Railcar No.: VIPX 45793 Order No.: 0014631-001 Prooertv Test Method SDeoification Analys Moisture, % ABR-1A 0.30 Max 0.15 Bulk Density, gm/cc ABR-2A 0.520 Min. 0.541 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 14.0 % On Pan 5.0 Max. 3.3 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.032 Inherent Viscosity ABR--10 0.64 - 0.68 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202081 Vista Polymers Highway 25 RVC RAT LCAH ANALY \//fy Load Date: ^ Product: Car Ho. : f-S' 7 ?3 Time Logged In:_Z^_ Ship Date: uk Logged In Bv: At-tti Order No: 00 I(fl?3/ D& t Silo(s): Customer: A/tbcg jC? O' Compartment Sample From Moisture % Bottom Contamination Bulk Density BD w/antistat Bottom Bottom .11 Bottom ./s" RVCM Tappi Test Contamination . 06 or .07 .15 .20 .60 Screen Analysis Mesh 40 Weight 06 % 60 IL /.< 80 100 120 140 200 Pan 2.to A2.J4 /. 17*4 *7.4 j4.o Static Flow Avg. Microns : J3t* I Color L: fi~rj a ,, STV b / 7/ Technician: m T tin VAB.0001202082 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTIFICATE OF ANALYSIS A V September 23, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro. GA 30642 Attention: Steve Ryan Ship Date: September 21, 1992 VISIA Product: 5265 Railcar No.: VIPX 45718 Order No.: 0014631 000 Property Test Method Soecification Analysis Moisture, % ABR-1A 0.30 Max. 0.15 Bulk Density, gm/cc ABR-2A 0.520 Min. 0.550 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 10.9 % On Pan 5.0 Max. 2.4 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.061 Inherent Viscosity ABR-10 0.64 - 0.68 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E.`'''Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202083 Vista Polymers Highway 25 1/JOuaksJl Aberdeen, MS 39730 A RAILCAR YSI S Load Date: Time Logged In: / 2<>Q Ship Date =Muji Product: Car No. ^s?l? Logged In By: Silo(s): M7.LX Order No CD l4& 31- DOO :Customer All lob / N*?Kcf*C.___ Compartment A Sample From Moisture % Bottom BL Contamination BB / z .553Bulk Density BD w/antistat Viscosity RVCM W ( _____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________ CA CB Bottom Bottom ,/r 3t -- 1a .OW t Tappi Test Contamination Composite ..... .06 or less .07-----------.15 B Bottom Jr 1 VV .^7 .003 m . 20----------- . 60 Screen Analysis Mesh * 40 Weight d 00 % 0.0 60 0 /L 6,?~ 80 4^9- 140 200 Pan Static Flow: & / Microns: Color L: ab Technician: VAB.0001202084 I Vista Polymers A Division of Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS September 24, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: September 23, 1992 VISIA Product: 5265 Railcar No.: VIPX 45844 Order No.: 0014631-002 Property Test Method Specification Analysis Moisture, % ABR-1A 0.30 Max. 0.11 Bulk Density, gm/cc ABR-2A 0.520 Min. 0.548 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 12.5 % On Pan 5.0 Max. 3.4 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. 0.052 Inherent Viscosity ABR-10 0.64 - 0.68 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy W. Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 T VAB.0001202085 6m Vista Polymer Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged In: Ship Date: RAX LCAR ANALYSIS //A/ Product: Car No.: Logged In By: M<1 Silo(s): 2- Order No : 001 1~002- Customer: i f* i 7/7W l r? Mesh Weight % 40 Q,07> 0,0 60 72 LU 80 Am 100 121 ns: 120 Moo 2iiL 140 H<33 200 (? Pan ]t~)X 217 I_Asl 1MStatic Flow: o L Avg. Microns : HO,/ Color L: a uC b /JA Technician: VAB.0001202086 Vttta Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 OF ANALYSTS Date: June 19y 1992 Customer: NibcO} Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention Steve Ryan Ship Date June 15, 1992 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.17 0.548 0.0 11.6 3.0 0.064 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. / Amy E. Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202087 Vista Polymers \ Highway 25 A Aberdeen, MS 39730 Load Date: 6-9-92- Time Logged In: Ship Date RAILCAR ANALYSTS Product Car Ho. :v . Logged In By: /Q7 s Silo(e) Order Ho: 0010^^3^00^ Customer: Ai l\oC*0 */o `Vie**!--- Compartment A Sample From Bottom Moisture % ./k BL Contamination BR Bulk Density _Sl_ (9 S'iX BD w/antistat Viscosity n RVCM .ux '06*1 CA Bottom J5 / $ .JfS _ _ CB Bottom 3 /9 / ( .bb>l .064 o Ul B Bottom /7 ,H * .disr Tappi Test Contamination Composite .06 or less t .07----------- .15 .20----------- .60 Screen Analysis Mesh * 40 Weight 0<o0 % <&X>0 60 ozo 80 S'.Of JO.z 100 /t>2( 20 4 120 140 30 23.(d 200 sjf //,> Pan A 4# 3-0 Static Flow: ,7-g Color L : 99.2/ Avg. Microns: a oMl b ASJ Technician VAB.0001202088 Villa Polymers A Division of Vtsfci Chemical Company Highway 25 Post Office Box 91 CERT X F X OAT Aberdeen, Mississippi 39730 Phone (601) 369-8111 OF ANALYSX S h Date: June 19, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, 6A 30642 Attention: Steve Ryan Ship Date: June 15, 1992 .... VISIAProduct: Railcar No.: VIPX 45910 Order No.: 0012402-000 Property Moisture, % Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.15 0.544 0.00 3.9 2.1 0.056 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. tU /Amy E BaaweVl Amy e r J5agwe Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202089 Vista Polymers Highway 25 A Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date:_ Time Logged In: 0/o0 Ship Date: Product: Car No.:_ Logged In By:_ Silo(s) : / *7, iif Order No: C)00 Customer :AJlkC-b A/e 771-etn Mesh Weight % 40 AO 60 8.1,1 80 Static Flow: 0 JL g.9 Color L: 100 /t*o t "" S*9.G> 120 to 140 Vo /34- 200 LfS 3.1 Pan ------------------- Sl\ Avg. Microns: [^ b !? Technician VAB.0001202090 Vista Polymers A Divirion of Vista Chemical Company Highway 25 Poet Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-6111 A Date: June 19, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: June 15, 1992 .,-VISIAProduct: Railcar No.: GACX 73398 Order No.: 0010143-008 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.10 0.550 0.00 8.9 2.3 0.094 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E V BagwerT Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202091 Vista Polymers Highway 25 A Aberdeen, MS 39730 F>VO RAILCAR ANALYSTS Load Date Time Logged I n: &C&0 Ship Date: fell <b> Product: Car No. . V331S Logged In By: Order Ho: //O I 9<90H Silo(s) : Cuet-omer: H.P. Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density ,Ofr r CA Bottom ^Q%_ 2- CB Bottom 3 B Bottom . io 3 1 Tappi Test Contamination Composite less Screen Analysis Mesh 40 Weight 0*00 % 60 QJ2l. 0.3 80 5.35" ton 100 LUZ 2^3 120 140 ll.ol 2 2.0 200 13 Static Flow: o / 1A Avg. Microns: 14* Color L: itel a b (M Pan LA3 2.1 Technician: vmmmm wmmmm VAB.0001202092 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTX FICATE Aberdeen, Mississippi 39730 Phone (601) 369-8111 XS Date: June 19, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention Steve Ryan Ship Date June 15, 1992 Product 5265 Railcar No. GACX 73379 Order No. 0010143-007 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.16 0.544 0.00 8.4 2.4 0.192 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. ''Bagwe 1 Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202093 Vista Polymers Highway 25 A Aberdeen, MS 39730 PVC IRA X LCAR ANALYSTS Load Date: Time Logged In: .'bits Ship Date Product: Car No. : Logged In By: Order No: /0 / 43 DO "7 S i lo ( s ) : Customer Aliioco Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD w/antistat 6L 7 / sw Viscosity RVCM M3 m CA Bottom clL Y (o CB Bottom jl/4 dm . (%S' Tappi Test Contamination Composite .06 or less % .07----------- .15 ' *r B Bottom i // b7Y? .20----------- .60 Screen Analysis Mesh * 40 Weight %F OO &P 60 */ .3 80 S. b US' 100 /AT? J3.2 120 140 200 /o-Y-2 -4-Z! Jo.*} L Pan /-g2- Static Flow: 3> l3Z3f 1Avg. Microns: /Y\ Color L* ^ a &6>r'?ST b /-T'O Technician VAB.0001202094 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X FI CATE OF* Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: June 11, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: June 8, 1992 VIS1A Product: 5265 Railcar No.: PTLX 42236 Order No.: 0010143-005 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.15 0.538 0.00 6.4 2.5 0.058 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46615-1167 VAB.0001202095 Vista Polymers Highway 25 * M A Aberdeen, MS 39730 Load Date Time Logged In: Ship Date:_ b\%kz^ RAILCAR ANALYSIS Prof Product: Car No.: Logged In By: Silo(s) &><ZgP#1l Order No Ihi43-oo s Customer :Nl bCo M MJtsd. Compartment A Sample From Moisture % Bottom 1 /_ BL Contamination BR (iL Bulk Density BD w/antistat Viscosity RVCM - Ms .0$B CA Bottom ji Jt. s , D(#0 <v? 1 CB Bottom ./r ,<&Q> .&S3 .o Tappi Test Contamination Composite - 06 or less J/z- _______________________________________________________________________________ ______________________________________________________________________________________________________________________________________ .07----------- .15 B Bottom . / 7 S' .07 .bS'G' ,D6>T) .20----------- f .60 Screen Analysis Mesh ' 40 Weight % P 00 P-0 60 .zc #^ 80 7.C4- /fiV Static Flow: 0 / 7.1 100 27.JT 120 /f.U Si, t 140 t.u n.s 200 J.ai i.f- Pan t.xs JT Avg. Microns: t*?7 Color L: a ii b /.I7 Technician VAB.0001202096 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: June 11, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: June 8, 1992 VISIA Product: 5265 Railcar No.: GACX 73389 Order No.: 0010143-006 Property Moisture, X Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.12 0.533 0.00 5.6 2.3 0.151 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202097 Vista Polymers Highway 25 A Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: Time Logged In Ship Date : (f0 I 0C3O Product: Car No.: Logged In By: Order No: I 01*4?^ DOC? Silo(s) : Customer: su> AU&I Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density ,// & A BD w/antistat Viscosity - .iM RVCM .\**i CA Bottom jL_ ( .SS2. 1 .^5 0/'7 a0 -4 Tappi Test Contamination Composite .- .06 or less % Y Screen Analysis Mesh Weight % 40 0*OO o. 0 60 ,3 80 100 L.7Z* f IS.76 )3.+ 1 1 1 I CB Bottom JO $ 3 B Bottom ^ 2> 5" 1 IQ1} * yi .DZZ> .20----------- .60 1 120 33.3 140 r.zz /7.t 200 .2. to S'. 4 Pan /. /3 Z.3 Static Flow: ^ / 7'7 Avg. Microns: Color L: 7 9.V" a .7/ b 2-oi' Technician: VAB.0001202098 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 A OF ANALYSIS Date: June 8, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: June 1, 1992 VISIA Product: 5265 Railcar No.: UTCX 46419 Order No.: 0010143-002 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.13 0.530 0.00 7.9 3.3 0.031 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202099 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: Time Logged In: Ship Date : 1&A R A ILCAR ANALYSTS Product: Logged In By: Order No IQ 143 Car No.: Silo(s) : Customer: Screen Analysis Mesh ` 40 Weight % o.o 0.6 60 . /r . i4L 80 i.n 100 12. i* 2 120 }C>o* 3/* 4 140 9.rf 11.2- 200 3.97 7. 1 Pan /. a 3.3 Static Flow : o /7.1 Avg. Microns: IV3 Color L: a . *70 b 3.Q& Technician: VAB.0001202100 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: June 8, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, 6A 30642 Attention: Steve Ryan Ship Date: June 1, 1992 VIS1A Product: 5265 Railcar No.: ACFX 41135 Order No.: 0010143-001 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.16 0.536 0.00 5.3 2.5 0.049 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202101 Vista Polymers Highway 25 A Aberdeen, MS 39730 RVC RAILCAR ANALYSIS Load Date Time Logged In :Ship Date (e (l Product: Logged In By: Order No: / $I Car No.: Silo(6) : Customer: Screen Analysis Mesh ` 40 Weight 9-00 % Q.O _ 60 o.if 0- 3 80 L.tjl iZJ? 100 aw 274 120 n-rf SMz, 140 6.77 J7.S' 200 z-i-V jS- 3 Pan Le7 Z-sr Static Flow: 0 Avg. Microns: WS.*7 Color L : P9.JJ a b Technician: VAB.0001202102 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: June 8, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: June 1, 1992 VIS1A Product: 5265 Railcar No.: ACFX 41178 Order No.: 0010143-000 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 o -* 00 Analysis 0.543 0.00 6.0 1.7 0.059 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe-bF Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202103 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSTS Load Date: 92. Time Logged In: Ship Date: kll Product: Car No.: W7& Logged In By: Silo(s): Order No:. /DlU'3~t>CO . Customer: Ah beo /V P /n efj Compartment A Sample Prom Bottom Moisture % BL Contamination BR Bulk Density ,f O f BD w/antistat Viscosity RVCM US'! CA Bottom -/8 Tappi Test Contamination Composite 06 or less .07 CB Bottom ./S' jsgt . 15 B Bottom . <49 <> /? . OkZK .20 .60 Screen Analysis Mesh Weight %r 40 (&.> 60 /3 3 80 100 120 L , z*S 34,.o SiZ 140 /8-t 200 .2.00 & O Static Flow: & / y~Z> Avg. Microns ;4&-3 Pan Ll Color L: a n.fO b /-,7/ Technician: m mm mhhmr VAB.0001202104 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: May 22, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: May 15, 1992 Product: 5265 Railcar No.: ACFX 41163 Order No.: 0009092-008 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.07 0.547 0.00 10.3 2.7 0.050 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwerir Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202105 Vista Polymers Highway 25 Aberdeen, MS 39730 A RVC RAX LCAR ANALY3IS Load Date: $u*h 72 t Product: 4 HCar No. : Time Logged In: (3* : ' gfefr Ship Date Logged In By: Silo(s):_ C 7 9 ;Order No 90Qz-DCi 9! Customer: /Jo /7/<27$Z- Compartment Sample From V/a 3 ~(*7& AxUsy.f sep Bottom Bottom Moisture % BL Contamination BR .0 7 Bulk Density . ft 4 5 4 BD w/antistat CB Bottom .jgrt B Bottom .of <D Viscosity RVCM .os'o ,LSS J2L fOS'l i .D^b Screen Analysis Mesh Weight % 40 QJ) 0 <9 ., 60 ,/4 A 80 IM Static Flow: o L &o 100 //A7 3J 120 IS.Cj 3*3 140 /o .S<? l.2- 200 Pan .13 _uy_ is J?. 7 Avg. Microns: /4q.1 Color L: a b AdZ Technician VAB.0001202106 4 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601} 369-8111 OF ANALYSIS A Date: May 19, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: May 15, 1992 VKIA Product: 5265 Railcar No.: PLCX 43742 Order No.: 0009092-006 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.02 0.549 0.00 6.0 2.2 0.118 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Eiy Bagwell/ Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202107 Viata Polymers Highway 25 A Aberdeen, MS 39730 Load Date: 7*-^ Time Logged In: f\f Ship Date IRA I LCAR ANALYST S Product: Logged In By: Order No: Car No.: Silo(s): Customer:_AAJo(~0 Compartment N Sample From A Bottom Moisture % BL Contamination BR Bulk Density to BD w/antistat Viscosity RVCM Lgb j(e> CA Bottom . of /*J2L1 .(ebb .056> CB Bottom / <- MQ> B Bottom ( Ip4L , D(pf Screen Analysis Mesh 40 Weight % e><> 60 80 100 120 n.\o f3 tf(f 140 % 200 3-&Q Pan ,7 /<f 33-o Lho A- a. Static Flow & //**> Avg. Microns: Color L: a b /-2<P Technician: f VAB.0001202108 Ir * * Vista Polymers A Division of Vista Chemicol Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: May 19, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: May 13, 1992 VISTA Product: 5265 Railcar No.: VIPX 45748 Order No.: 0009092-007 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.13 0.540 0.00 11.3 3.4 0.076 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202109 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSTS Load Date:. Time Logged In: l(*3& Ship Date:___^ Product: Logged In By: Order No: Car No.: Silo(s): : Milo Customer /to j*&s( Compartment A Sample From Bottom Moisture % BL Contamination BR JO Bulk Density BD w/antistat ,r*j Viscosity RVCM JL CA Bottom o? 7 02 CB Bottom U. B Bottom ,/JS .rye .b> &> & Tappi Test Contamination Composite .06 or less .07---------- .15 .20----------- .60 Screen Analysis Mesh 40 Weight _JLi % 4*0 60 _ ,3 80 r.7* 17.4 Static Flow: / 7. i 100 120 140 200 //,* *57 3 ZZ.7 74.0 /J.3 Avff . Microns : ^ ^ Color L: ?/, rJ a . f? b A ro. Pan Technician: Ad 4*ft VAB.0001202110 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OE ANALYSIS A Date: May 6, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: May 4, 1992 VISIA Product: 5265 Railcar No.: PLCX 42999 Order No.: 0009092-004 Property Moisture, X Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.22 0.544 0.00 15.5 4.1 0.053 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202111 i Vista Polymers Highway 25 A Aberdeen. MS 39730 Load Date: LHrP'?d-~ Time Logged In: Ship Date: RAILCAR ANALYSIS Product: Logged In By: QoQl 'GQCp Car No. Customer L7X&8.6S71& / N\bto /?e> Compartment Sample From Moisture % Contamination Bulk Density BD w/antistat Viscosity RVCM Tappi Test Contamination Composite Screen Analysis Mesh * 40 Weight D.OO 60 p.oS % j - .*/ 80 S-s- 100 120 /S-? . 2*2- 140 /2.M 2^.P 200 Pan 7.7s- J?.c3 /.<S~ 4,/ Static Flow: 0 /7 Ave. Microns: /S/.Q Color L: a0 b Technician : Co VAB.0001202112 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFXCATE Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A ANALYSXS Date: May 6, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: May 4, 1992 VISIA Product: 5266 Railcar No.: UTCX 46552 Order No.: 0009092-003 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.23 0.536 0.00 15.0 2.8 0.051 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. BagweT-i Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202113 Vista Polymers Highway 25 Aberdeen, MS 39730 A IRA ILCAR ANALYST S Load Date: -iy-9z Time Logged In:. /boo Product: Logged In By: Ship Date: Order No: Car Ho.: Silo(6): 3 Customer: b)Q "htef* Compartment Sample From Moisture % A Bottom T CA Bottom BL Contamination BR .5 (* Bulk Density *523 5 7 BD w/antistat Viscosity RVCM V- MCI o& 4 Tappi Test Contamination Composite ___ ____ . .06 or less Screen Analysis Mesh * 40 Weight *0 1 1 j 1 1 % Ol 1 CB Bottom $ 10 **st2 B Bottom /<? 7 8 MU'! .0S& Ja&b .OS'gs .20----------- .60 Static Flow: ^ / o Color L: nsco Avg. Microns: A b mr Technician: VAB.0001202114 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date: May 6, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: May 4, 1992 VIS1A Product: 6265 Railcar No.: UTCX 46421 Order No.: 0009092-002 Property Moisture, % Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Apalysjs 0.09 0.540 0.00 15.8 3.2 0.097 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. agwe Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 mmmm m VAB.0001202115 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date:. 4-AI-91. Time Logged In: ^3 0 :Ship Date ^Af R AILCAR ANALYSIS Product: Car No . : o^% ( Logged In By: Ol (j~ Order No: 60 Silo(s) : U1&- Iq%Q~ \g .Customer Mb lOCi VVi&fA-I Compartment A Sample From Bottom Moisture % BL Contamination BR a Bulk Density BD w/antistat Viscosity RVCM ,on CA Bottom t QS f i( -i Tappi Test Contamination Composite .06 or less .07 CB Bottom O1 s 7 t^( .Oi/I . 15 B Bottom 3 ,te>bZ .20 .60 Screen Analysis Mesh Weight 40 o % 0.0 60 Q.OO 0.0 80 -Aid Static Flow: 0 t'J.S 100 -t.n /7.t 120 fool* 140 \L 200 Avg. Microns: /SO * I Pan /. 40 I. Color L: a U3 b Technician \ i' VAB.0001202116 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OE ANALYSIS A Date: May 1, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 27, 1992 Product: 5265 Railcar No.: VIPX 45810 Order No.: 0009788-000 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.08 0.540 0.00 15.3 3.5 0.056 0.67 Polyvinyl Chloride, Virgin Resin, Not Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202117 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date Time Logged In: Ship Date ilJl RAILCAR ANALYST S Product: Logged In By: Order No : Car No. : M'S IffD La Silo(s) &0Q Customer: t & Wc&h t------ Compartment A Sample From Bottom Moisture % .B BL Contamination BR / Bulk Density ,S^ BD w/antistat Viscosity RVCM .0*5(0 CA Bottom AltS" Tappi Test Contamination Composite .06 or less CB Bottom .us .DG6 B Bottom 09 . bio 2. .o&t Screen Analysis Mesh Weight % 40 A dC? OmO 60 5Zo3 80 BJ : d MStatic Flow l 100 120 fgfl 140 200 Pan /,* ('.3 Avg. Microns: /3*.f Color L: 973? a b i.w Technician;: Jxrrj-nt1-- VAB.0001202118 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Dates fatten Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: Product: 5265 Order No.: OOO tyrfOd? - &0 3 Cust. P0 No.: Trailer No.: Property * Moisture, 7. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR--10 Analvsis -/3 55! 0.0 >3.0. 3. ? Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora (Uj sor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202119 PVC BULK TRAILER ANALYSIS A Pate 4"* Z h f?- Customer If; 4 Technician Product S2.LC Silo___ 11 Trailer Number 7* 3^0 Time Order No. /Too COO tf&fa FRONT MOIST CONT. Top Bottom I Top Bottom ,/j I GEL I 2. 2. BULK DENSITY I ,ri / DRY TIME l I. I I l. l COLOR vise = ,4/ b - h7 L= RVCM MIDDLE i END I 2. l A= B L= A= B= Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. h on Mesh. 0. DO o. o .0^ ,/ /?,/ 14.1? U-lf 2.S~ A.t, Z. /.*r J.7 Screen Analysis Mesh Size Gross Wt. 40 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Tare Net Wt. % on Mesh Remarks Star 207A Revised 1/12/87 ---------------------------------- VAB.uuui^imzrr "" " Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERT I F I CCi^TE! OF AN AL_ YS I S A Date: Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: V/ -VBIAProduc t: Order No. DOO MSI- 00 3 Cust. P0 No. Trailer No. r 3&\ Property * Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM , ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana lysis .04 .U Polyvinyl Chloride, Virgin Resin, Not Rep cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202121 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERT I I CATE O R" ANALVS I S A Date: Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: 4(Zo/^Z- VISIAProduct: 5265 Order No.: OOQQ^^'J-OOT^ Cust. PO No Trai1er No.: f Propertv 9 Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR--1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana 1vsis . 13 .53/ D.D /4.3 3.1 .06% .67 Polyvinyl Chloride, Virgin Resin, Not Rep Labora cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202122 PVC BULK TRAILER ANALYSIS A fDlffllttp Customer Technician _______ Product A/1 ioC-o Silo(** Pt ^ Order No. jgjkA________ __ Time 13 o 9 OOP Trailer Number 13 o 9 T~ 3^jfl7O Particle Size Distribution: Screen Analysis /^ Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 4.00 o*o Screen Analysis Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb 60 80 100 120 140 200 Glassy Pan Part. 3.40 t.*t )4.it I3.1S 7./7 i.sL 0fo 7.S i M.3 J.J Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 VAD.0001202123 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 cert i F" i of analysis Date: 2^0 ^ Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: 2-0 /bfrt I ^2" Product: 5265 Order No.: 000 7 9 5"*7- 002- Cust. P0 No.: Trai1er No.: Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana 1ysis Q. 0 yr. 0 2, L .D&> , fo "7 Polyvinyl Chloride, Virgin Resin, Not Rep /Vt La bfi$rattoorryv Supe cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202124 PVC BULK TRAILER ANALYSIS Date 4-lo Customer AlA Technician ANi_ Product Silo___ i /7 MOIST Top Bottom l >/2*+*+ CON'T. TO Bottom I. * 0 GEL I FRONT 2. 2. I. I Trailer Number Time /73c Order No. BULK DENSITY I DRY TIME COLOR l * 94. /o A=* 1I B L- vise RVCM MIDDLE 2. I END i. i A= B= i L= A= B Particle Size Distribution: Screen Analysis /O Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 0, 0-0 0* 0 Mesh Size Gross Wt. Tare Net Wt. on Mesh 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Cart) 60 60 100 120 140 200 Glassy Pan Part. fi.OO PO Min. 60 J. 9,/1 J9.9T /,// 7.X/ 7.3____ /i. it.x Zt. z /sr.o On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 A3! Glassy Pan Part. Remarks -M Star 207A Revised 1/12/87 mmm T mmmm h Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I R" X CATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 XS Date: *fj*2^0 jtf Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: 4lzoki^ Product: 5265 Order No. : Cust. PQ No.: ------ Trailer No.: } - 3*7 Propertv Moisture, 7. Sulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana 1ysis O.D & Polyvinyl Chloride, Virgin Resin, Not Reprocessed. A ory cc: Nibco, Inc . 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202126 A Customer PVC BULK TRAILER ANALYSIS A Particle Size Distribution: Screen Analysts Mesh Size Gross Wt. /^Mln On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb 40 60 80 100 120 140 200 Glassy Pan Part. Tare Net Wt. % on Mesh 0.6 Screen Analysis 0.* f S.2S /o./S /ZB<f /2l // 0.2. /0.S 20.2k Jo.0 2+ Z ,2-Z Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. Pan 40 60 80 100 120 140 200 Glassy Part. % on Mesh Remarks * Star 207A Revised 1 /12/87 VAD.0001202127- Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 GERTX RICAT E OR ANALYSIS A Date: April 22, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 20, 1992 Product: 5265 Railcar No.: VIPX 45739 Order No.: 0007298-005 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis 0.11 0.545 0.00 15.6 4.1 0.120 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E.^BagwelD Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202128 * , ViBta Polymers Highway 25 Aberdeen, MS 39730 A RVC RAILCAR ANALYSIS Load Date:. Time Logged In: Ship Date: Product: Car No.: 73*} Logged In By: Order No Si lo (s ) : ~DC STCustomer: /Vib C& Compartment A Sample From Bottom Moisture % BL Contamination BR i oSL JL t. Bulk Density .5^/ BD w/antistat Viscosity RVCM 6^7 - . /io CA Bottom .o7 2 .070 CB Bottom . o (0 ? .073 Tappi Test Contamination Composite .06 or less .07----------- .15 B Bottom JL 3 S .20----------- .60 Screen Analysis Mesh ' 40 Weight 0.00 % O.'b _ 60 Q.Qtf 61 80 7.S 100 // 7 120 rf3( 3l8.L 140 200 /Z.S7 Vf/ / /S'. 4 Pan 4.0 7 Static Flow: 0 /?*> Avg. Microns: 13!/ Color L : 97 f/ a _0`>O b Technician: VAB.0001202129 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 O E R T I R I GATE: OR Aberdeen, Mississippi 39730 Phone (601) 369-8111 ANA l_YS X S 4 Date: April 22, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 20, 1992 VISIAProduct: 5265 Railcar No.: ACFX 41159 Order No.: 0009092-001 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.07 0.538 0.00 15.8 4.8 0.077 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. / Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202130 Vista Polymers Highway 25 A Aberdeen, MS 39730 RAILCAR ANALYSTS Load Date 12. Time Logged In: I Ship Date: *f|?P Product: Logged In By: Cb Order 9c/1Z-na Car No. y//^7 Silo(e): & 7S- & ft AJ<b to Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD w/antistat Viscosity RVCM .Mi >17 CA Bottom CB Bottom ,3* 67Z Tappi Test Contarnination Composite . 06 or less .07 - --------.15 4 B Bottom 3 Jll .20 .60 Screen Analysis Mesh * 40 Weight % ^ 60 *// A 80 3.0? 100 IZOl 120 0.<n h 140 /fizz t 200 Static Flow: / , mAvg. Microns Pan tfii Color L: ab Technician: VAB.0001202131 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone(601) 369-8111 4 Date: 20 ** Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: 2-0 A'pr^ ^2-- Product: 5265 Order No.: OOO J?~~7-0o) Cust. P0 No.: Trailer No. : 7^-J7 / Property * Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR--2A ABR--3 ABGC-26 ABR-10 Analysis / . CJO C. O /2. O 2..C *D2X) . && Polyvinyl Chloride, Virgin Resin, Not Reprocessed. cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja MM* MM mm VAB.0001202132 PVC BULK TRAILER ANALYSIS A Date 4~U0'"I'L Customer Technician FRONT Product Silo___ kl2 MOIST TO Bottom I. M CONT. Top Bottom GEL I 2. 2. I. i Trailer Number 7^37/ Time /Too Order No. flOOWSl- oof BULK DENSITY I , CIO DRY TIME I COLOR L =1%07 A =- *? vise RVCM B == /r* i L= MIDDLE 2. l END i 2. A= B= I L= A= B- Particle Size Distribution Screen Analysis /0 Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh fl- P ^ JL4 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Serb 60 80 100 120 140 200 Glassy Pan Part. . 2_ Min. 60 S'.ZI JO-2. t> J2joi Lot /0*<f 2o. JO*?-- z%l- n~c On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 A 2-7 z* c Glassy Pan Part. Remarks Star 207A Revised 1 /12/87 Y^CB.0001202133- Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date :. / 7- <7 Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: VISIAProduct: 5265 Order No ooo ocro Cust. P0 No.: Trailer No Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana1ysis .08 , sy 1-- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202134 Dale f I? Customer Mi beO Technician PVC BULK TRAILER ANALYSIS Product Silo___ &3S. Trailer Number _ Time /T*Q- Order No. 4 Particle Size Distribution Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh a 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 60 100 120 140 200 Glassy Pan Part. LU. b.^9 fO.SS tS7C3 <23 JL3. /p,<^ A6- Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 VAD.0001202135' Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen Mississippi 39730-0091 Phone (601) 369-81 11 CERTIFICATE F= ANALYSIS Date: *7 Customer: Nibco, Inc. 1900 Old Union Pt. Road Greensboro, GA 30642 Attention: Steve Ryan Ship `j VIS1AProduc t Order No 0&D Cust. P0 No.: -oof Trai1er No. : Propertv * Moisture, 7. Bulk Density, gm/cc Particle Si2e, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.0 (3.Q .m (p(p Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202136 PVC BULK TRAILER ANALYSIS A Dale Customer Technician FRONT Product o Silo___ 68% Trailer Number Time. a*. Order No. MOIST Top Bottom pa CONT. Bottom GEL i BULK DENSITY i DRY TIME i COLOR L = fjo 2. 2. A= Ii i B = 1+35 L= vise RVCM MIDDLE END A= ii i B= L= A= B= Particle Size Distribution: reen Analysis. Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 0^0 Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Min On Rotap abaker. 49 $fms. Resin |lus 1.0 grns. Carb 60 80 100 120 140 200 Glassy Pan Part. I0.2& f&(6 0.2- q.ip 20+zq.l! 2ff /3r0 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 /- Glassy Pan Part. Remarks Star 207A Revised 1 /12/87 VL Vista Polymers A Division of Vista Chemical Company Highway 25 Poet Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 OERTIFICATE OR ANALYSIS 4 Date: April 15, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 13, 1992 Product: 5265 Railcar No.: GACX 73379 Order No.: 0007298-003 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.05 0.551 0.00 12.3 3.2 0.192 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. BagweTl Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202138 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Logged In: Ship Date: a Product: 5265 Logged In By: PI Order No 3 Car No.: SLIoIb) : Customer: AlljoCo Compartment A Sample From Bottom Moisture % BL Contamination ___ BR Bulk Density ,of 7 BD w/antistat Viscosity RVCM Mb Tappi Test Contamination Composite or CA Bottom .o2> H j> .0b9s Bottom j 7 i .014 i S8^ Bottom .^53 V Screen Analysis Mesh 40 Weight %f 6>.0 00 60 80 of V- Static Flow: & / 3*3 100 2 / ^ 120 30.2 140 //'JTb 200 A-/3 / Avg. Microns: J S^>. *7 Pan /,<2_ 3-Sl. Color L: /^V ^ a &`S~0 b A3/ Technician: /ff^ 'ff VAB.0001202139 t Vista Polymers A Division of Vista Chemical Company Highway 25 Rost Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: April 10, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 1 -ULLH-u 111- -J --- -HimJ"| 8, 1992 . Product: 5265 Railcar No.: ACFX 41160 Order No.: 0009575-000 ......... -- ------i. .. -i- Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Test Method ABR-1A ABR-2A ABR-- 3 Analysis 0.15 0.549 0.00 15.8 Pan Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 3.6 0.023 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 i VAB.0001202140 v1 Viata Polymers Highway 25 Aberdeen, MS 39730 4 RAILCAR ANALYSIS Load Date:.21 Time Logged In: 4(<h7^ Ship Date: Product: Logged In By: Car No.:.AlUop Silo(s): Customer i loco Screen Analysis Mesh 40 Weight o,oo % C, o 60 O - 0/0 o 80 2 ,/e 4,2. Static Flow 0 / f ,C Color L: 100 LL U, I 120 /4*/Z- 32 ,4- 140 13SI 7, Z 200 ZAJL /s;s Avg. Microns: a ,/r b / 7d /27. U Pan /,7J JLA Technician: tE- VAB.0001202141 fa Villa Polymers A Division of Visla Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 V Date: April 10, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 6, 1992 ...VISIAProduct: Railcar No.: PLCX 42644 Order No.: 0007298-002 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.04 0.547 0.00 11.3 3.1 0.111 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E ,w Bagwe' Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202142 * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: April 10, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 8, 1992 VISIA Product: 5265 Railcar No.: ACFX 41160 Order No.: 0009575-000 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.15 0.549 0.00 15.8 3.6 0.023 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202143 Vista Polymers Highway 25 Cti lJ, Aberdeen, MS 39730 IP VC RAILCAR ANALYSIS Load Date: c? ~*/C ~'f3x Time Logged In: Ship Date: 4(thz^ Product: Car No.:. 4\\lr> Logged In By: Silo(8): #57Order No: ^6on Customer : A/lbCG A Compartment Sample From A --TM * Bottom Moisture % BL Contamination __ BR S' - CA Bottom ./r CB Bottom . / .4 Bulk Density BD w/antistat Viscosity _J/s4 RVCM ,015 .OZ% ,oitr L___________________________________________________________________________ Tappi Test Contamination .06 or less .07----------.15 Composite B Bottom S' , rsrj .Mr ,0&7 .20---------- .60 Screen Analysis Mesh 40 Weight % O.QQ 0, o 60 6 * 0/0 0J) 80 2 ./o 4,2- 100 /t" I 120 /4./Z- 12.4- 140 /j.r? -27. Z 200 2JJL /s:s Static Flow: 0/1.0 Avg. Microns: Color L: 11.03 a ,/r b / /27, Pan /, 7i Ul Technician: VAB.0001202144 hi Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 v Jt Date: April 10, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: April 6, 1992 VIS1AProduct: 5265 Railcar No.: PLCX 42644 Order No.: 0007298-002 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.04 0.547 0.00 11.3 3.1 0.111 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E y Bagwe' Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202145 Vista Polymers Highway 25 Aberdeen, MS 39730 A j RAILCAR ANALYSIS Load Date Time Logged In Ol'O o Ship Date mte. Product: Car Ho.: Logged In Bv: Silo(s) : Order No: 0.48 -oo - Customer : C r - -; .....~./~Q' f (- /y..- Compartment A Sample From Bottom Moisture % BL Contamination BR JP.t 3 Bulk Density BD w/antistat 'S3$ Viscosity RVCM .Ul> .ill CA Bottom . Of z. /Q ,<S1* MS .050, CB Bottom ,oZ JL_ y 017L B Bottom o'f 3 7 .010 Tappi Test Contarnination Composite Screen Analysis .06 or less 7 7 .07----------. 15 .20---------- .60 Mesh * 40 60 80 100 120 140 200 Pan Weight 0-0 ,^ 4-3^ f/.2$ /r.7g /f/z-- 5- /,S7 % <9,0 < 3-- 'S'7 8 3 Itf 3,9k-9- /1-3 3. ( Static Flow: 0 / *?* Color L: Avg. Microns: /c3C>- *? a ^ `33 b /&/ Technician: VAB.0001202146 Vista Polymers A Division of Vista Chemical Company Highway 25 Poet Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: April 10, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Product: 5265 Attention: Steve Ryan Railcar No.: UTCX 46419 Ship Date: April 6, 1992 Property * Test Method Order No.: 0007298-001 Analysis Moisture, % ABR-1A 0.02 Bulk Density, gm/cc ABR-2A 0.544 Particle Size, % on ABR-3 40 Mesh 0.00 200 Mesh 13.5 Pan 3.7 Residual VCM, ppm ABGC-26 0.064 Inherent Viscosity ABR-10 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202147 * Vista Polymers Highway 25 Aberdeen, HS 39730 A F>VO IRA. I LCAH ANALYST S Load Date: S~/J'9Z^ Time Logged In: o Ship Date: Product: 5265 Logged In By: Order No %-CDl Car No.: Sllof s') : *r?' Customer: AA ID&O Compartment A Sample From Bottom Moisture % -o/ BL Contamination __ BR (p> 9 Bulk Density -53' BD w/antistat Viscosity BVCM M CA Bottom r < Mo .Pal CB Bottom . of l J / 1^ <07Jt> Tappi Test Contamination Composite .06 or less y7 .07----------.15 B Bottom / t 7 , (p6>& ,17J .20---------- .60 Screen Analysis Mesh 40 Weight % oo 60 , >&> ./ 80 42/ /y 100 />-2^ 120 /S.[l 3L0-S' Jo 140 / A ^ E' 200 J3-2- /J^ Pan /Jj. 3-7 Static Flow: O //O 0 Avg. Microns: / 33-1 Color L: 9frS? a &,sz) b /sH Technician: VAB.0001202148 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: April 3, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 31, 1992 VISIA Product: 5265 Railcar No.: UTCX 46442 Order No.: 0009092-000 Property Moisture, % Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR--2A ABR-3 ABGC-26 ABR-10 Analysis 0.15 0.542 0.00 10.4 2.5 0.001 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202149 Vista Polymers Highway 25 Aberdeen, MS 39730 4 Load Date: Time Logged In: Ship Date: ILCAR ANALYSIS Product: Car No.: Logged In By: Silo(s) Order No: 7U--CrZTD Customer : /to Compartment Sample From Moisture % Contamination A Bottom ,,/3 CA Bottom ,/r CB Bottom -/ B Bottom c j/ Bulk Density BD w/antistat . SV/ Viscosity RVCM , [p S6? .Dbl Tappi Test Contamination Composite r /.DOI . LSI .13$ .q . (As 00 / Screen Analysis Mesh 40 Weight % 0. 00 40*10 60 . 0 2- ,0 o 80 a.,7 9V 100 f.ff zM 120 /I. Si 37- 3 140 12.13 25.1 200 /O.t/ Pan L Z.S~ Static Flow: 0 / Avg. Microns: /32.X Color L: 9f.23 a .70 b ,,../T Technician: flUf + /* VAB.0001202150 4 I. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: March 27, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 26, 1992 Product: 5265 Railcar No.: UTCX 46535 Order No.: 0007298-000 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.13 0.550 0.00 13.4 3.3 0.100 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. -------------BP----------- J-------------------------------- H.D. Lucas Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 mm T i VAB.0001202151 Vista Polymers Highway 25 Aberdeen. MS 39730 A Load Date: Time Logged Ship Date: RAILCAR ANALYSTS CL7ZX Product: Car No. Logged In By: Silo(e): Order No: O Q& "72. 7y~^^fcugtomer: /\Zf&^CS> Screen Analysis Mesh 40 Weight % 0'0 60 80 , *1 JA.I o v o 7.0 Static Flow > / /.0 Color L: 100 I0M^ 2/. 3 120 ISMo 140 /2, o<f 2./ 200 hth & /J.y Avg. Microns: 733,0 a .3* b 7*2 Pan A 7 Technician mmmmm mm VAB.0001202152 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601} 369-8111 A i* Date: March 24, 1992 Customer Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 23, 1992 VlSlA Product: 5265 Railcar No.: PLCX 43053 Order No.: 0007295-001 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.01 0.539 0.00 4 13.5 3.7 0.050 0.67 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 mm T mm MMM VAB.0001202153 mm- C. . Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date Time Logged In Ship Date: RAILCAR ANALYSIS Product: Logged In By: Order No: Car No.: Silo(s) : _ Customer: Nthcv ^ & Compartment A Sample From Bottom Moisture % BL Contarnination BR Bulk Density l (O BD w/antistat Viscosity RVCM .DSD CA Bottom O( (2- .53^ .7 CB Bottom -of B Bottom L. .o'^ 33 634- ,&74- ,!3*f Tappi Test Contamination Composite .06 or less .07----------.15 .20---------- .60 Screen Analysis Mesh 40 Weight % IO 0.0 o, 60 ; Q(e> .) 80 /C> $3 100 S0-70 !-<f 120 TOA 140 //-& 2S>-7 200 &?? I7 .5 Pan /-2- 3-7 Static Flow: & / % *9 Avg. Microns: /JV / Color L: 99' a <9Q"f b Technician: VAB.0001202154 i^HiiNi Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 RTIFIGATE OF Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 ANALYSIS A Date: March 18, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 17, 1992 VISIA Product: 5265 Railcar No.: VIPX 45921 Order No.: 0007295-000 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.17 0.538 0.00 6.6 2.1 0.182 0.66 Polyvinyl Chloride, Virgin Resi^\ i, Not Reprocessed. L Amy EY Bagwe Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202155 1 w Vista Polymers Highway 25 Aberdeen, MS 39730 A! t>VC RAILCAR ANALYSIS Load Date: Time Logged In: Ship Date: Product: Logged In By: Order No:, Car No.: Silo(s): Customer: Mb jrtaZM Compartment A Sample From Bottom Moisture % BL Contamination BR ,/3 Bulk Density BD w/antistat ,5* 7 Viscosity RVCM 3 CA Bottom n S -7 So . Me i .no CB Bottom *jC 3 S -O'? MS' .&PI Tappi Test Contamination Composite .06 or lest5 */t .07 ---- - .15 - B Bottom ./? S* 1 .SJS~ .0T^> .20---------- .60 Screen Analysis Mesh * 40 Weight % 0i 6 60 .22- 80 7. IS.Q 100 iZ~*S0 z+x 120 /ST ~70 31. 1 140 /I r 200 jr. Pan /. *6 ZJ Static Flow: 0 / 2. Avg. Microns: W7% 3 Color L: a. b /<i Technician: mm ^T * VAB.0001202156 T mmmm* Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIEX CATE Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 ANALYSIS A Date: March 16, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 16, 1992 VIS1A Product: 5265 Railcar No.: PLWX 44567 Order No.: 0006964-002 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR--2A ABR-3 ABGC-26 ABR-10 Analysis 0.05 0.547 0.00 7.4 2.4 0.100 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202157 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date: *3 ~~ fi- Time Logged In: ISoo Ship Date: Product: Car No. : ? Logged In By: LSQ. L 87 (f% <-003- Customer Nibto fj6 A Compartment Sample From A Bottom CA Bottom CB Bottom Moisture % BL Contamination BR Bulk Density /$ 3 .6 t5 JL BD w/antistat Viscosity RVCM ,}b0 -65 .051 aon Tappi Test Contamination Composite .06 or less 1 .07----------.15 B Bottom 45" g s .(ok> dll .20---------- .60 Screen Analysis Mesh Weight 40 & oO % 60 6>.2( 0>*h 80 Gz.93L ms_ Static Flow: 0 /L& 100 120 140 200 \0.eo Avg. Microns: Color L ft a b Pan Technician: apPMMlPffPHiPinmp WP VAB.0001202158 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date: March 12, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 9, 1992 VISIA Product: 5265 Railcar No.: GACX 73409 Order No.: 0005590-005 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.05 0.547 0.00 12.2 2.7 0.081 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202159 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged In: Ship Date: IRA ILCAR ANALYST S Product: Logged In By: Order No: Car No.: Silo(s): Customer: C Compartment A Sample From Bottom Moisture % i BL Contamination BR Bulk Density 5 % BD w/antistat Viscosity RVCM M. M\ CA Bottom t (o(oS .Ma CB Bottom ,5 &57 .DU) Tappi Test Contamination Composite .06 or less .07----------.15 B Bottom .(a(&(p ,4| .20---------- .60 Screen Analysis Mesh * 40 Weight 02>O % 60 e. /? G.+ 80 //f 100 /o.sf 2./.0 120 21.3 140 /f.3--f(" 200 4./o /2. z Pan /. 35 *7 &LStatic Flow: 6 L Avg. Microns Color L: a m bm Technician m VAB.0001202160 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 RTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (6011369-8111 ANALYS A Date: March 10. 1992 Customer Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 9, 1992 VIS1A Product: 5265 Railcar No.: UTCX 46511 Order No.: 0006964-001 Property Moisture, X Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.11 0.545 0.00 13.0 2.9 0.021 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H.D. Lucas Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202161 Viata Polymers Highway 25 Aberdeen, MS 39730 A IP VC IRA I LCAR ANALYSIS ucrc^ Load Date Time Logged In: 3 Ship Date: iSdq Product Logged In By: Order No Car No. msn Sllof e1) : C> 7 ,N\bto Customer m jfcf Compartment Sample From A Bottom CA Bottom CB Bottom Moisture % BL Contamination BR .07 , ol Jo Bulk Density BD w/antistat Viscosity RVCM mi Ml ,061 Tappi Test Contamination Composite .06 or less .07----------.15 B Bottom . // Ml .(ML .20---------- .60 Screen Analysis Mesh 40 Weight % OiOO P, o 60 >X)Z f>. I 80 5-2 100 120 140 200 /8.o 32.7 2*U /3o Static Flow: o / r.i Avg. Microns Uo, 7 Color L: 49X2, a ,62. b Pan / Technician #4+Pi~ wmmmmmm mm VAB.0001202162 Vista Polymers Highway 25 A Division of Post Office Box 91 Vista Chemical Company CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date: March 9, 1992 Customer: NibcO) Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 6, 1992 VISIA Product: 5265 Railcar No.: VIPX 45811 Order No.: 0007295-002 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.14 0.543 0.00 8.6 1.6 0*028 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H.D. Lucas Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 imapHP turn VAB.0001202163 Viata Polymers Highway 25 Aberdeen, MS 397SO A Load Date: Time Logged In Ship Date: 3/ 'J?2, o HA I L.C A!R ANALYST S V/M Product: Car No.: V8il Logged In By: Silo(8): Order No: &QD 7^^^"^fl^Histomer: A)lbcC> Sample From Bottom Moisture % BL Contamination BR Bulk Density t s BD w/antistat Viscosity RVCM ,Dt% Bottom // S H ,odl Tappi Test Contamination Composite .06 or less .07 Bottom ,/3 3 f -JT4(, ML <DOS' . 15 Bottom 1 /d ,D0S .20 .60 Screen Analysis Mesh 40 Weight % 0. o 60 80 4.37 in Static Flow: 0 / *3 100 j/.jf AM 120 a 23 111 140 ILIA 21- 200 m Avg. Microns: /39.0 Pan 6. ft I.L Color L: ?f.// a b/ Technician VAB.0001202164 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSI A Date: March 9, 1992 Customer: Nibco, Inc* 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 6, 1992 VISIA Product: 5265 Railcar No.: VIPX 45812 Order No.: 0007295-003 Property Moisture, X Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC--26 ABR-10 Analysis 0.05 0.543 0.00 9.6 1.9 0.072 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H.D. Lucas Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 fH mmmmmmmmmrnmmmm mm VAB.0001202165 i Vista Polymers t Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged Ship Date R AILCAR ANALYST3 \/!fX IL,3C> Product: Logged In By: Car No.: Silo(e): bflfZj &&br&8!8 -0$3 Customer locO L /H Compartment A Sample From Bottom Moisture % <oS~ BL Contamination BR JL_ /f Bulk Density .S4( BD w/antistat Viscosity RVCM , bb! cm CA Bottom S' (C . S~M .ttff CB Bottom ? /A .LES" .DOS Tappi Test Contamination Composite .06 or less % .07----------.15 B Bottom /* LS .SSI .DoS' .20---------- .60 Screen Analysis Mesh * 40 Weight O.0& % 0,0 60 . of ./ 80 ;,4i> 7. Static Flow: * / 0 100 /0.v 2/0 120 n.4t 3si 140 12.ot ^2 200 .tt 1*4 Avg . Microns: / (* Pan Color L: a , 72 b 2_ Technician: . mmm mam VAB.0001202166 * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601) 369-8111 A O ERT X F" X OX e: O P~ AN *=% L YS I S Date: March 5, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: March 2, 1992 Product: 5265 Railcar No.: UTCX 46416 Order No.: 0006964-002 P|tWHrIIopertyfliVlMi Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 O tt (M Analysis 0.18 0.542 0.00 8.5 0*040 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. / Cburt 'Amy E.MBagwellU Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 mmmmmm mm 4 VAB.0001202167 Vista Polymers t Highway 25 Aberdeen, MS 39730 A 3PVC TRA X L.C AR ANALYSTS Load Date: Time Logged In: o&t><o Ship Date: Product: Car No.: Logged In By: Silo(s) : 4> $i*\ L 8$ 6? A/tOrder No: ^(o {4'~Cr&L) Customer: lo Cb hto `TriefoL-- Compartment A Sample From Bottom Moisture % 7* Contamination BL BR Bulk Density , j5^> BD w/antistat Viscosity RVCM CA Bottom . 4f ,53. .Dbb CB Bottom .*5" /Q Ml .D7 Tappi Test Contamination Composite .06 or less .07---------- .15 B Bottom . 0 c^~ 7 g .<513 .20---------- .60 Screen Analysis Mesh * 40 Weight && O, O Static Flow: Color L: Microns: a M b 4 Technician: VAB.0001202168 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 C EI R T X F I C2 A T El O F A N AI__'Y' S I S * Date: Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: Order No.: CCOcM-oog Cust. PO No.: 3I-2&39J Trailer No.: Property Moisture, '/. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO Ana 1vsis 0-0 <0.9 2.1 ,0%0 .7^ Polyvinyl Chloride, Virgin Resin, Not Reprocessed cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja wmmmmmm fMM VAB.0001202169 T lto J? - JtA - 92. PVC BULK TRAILER ANALYSIS Product S3o J ______ Trailer Number /-- Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare Net Wt 46 on Mesh Screen Analysis 40 Mesh Size Gross Wt Tare Net Wt 46 on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gnu. Carb 60 100 120 140 200 Glassy Pan Part. &.Q Min. 60 22.. / 3- X<? f2.<?2 3-<47 s o afc-6> f- n.8 2 On Rotap shaker 49 gms. Resin plui 1.0 gms. Carb 80 100 120 140 200 4 a Glassy Pan Part. Remarks VAB.0001202170 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I R" I CATE OF ^l\l^L_V'S I S A Date: February 19, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, 1 30642 + Attention: Steve Ryan Ship Date: February 17, 1992 Product: 5265 Railcar No.: GACX 73379 Order No.: 0006963-000 Propertv Moisture, V. Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 553 oo iz.i Jl* 3 .036, ____ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 MMMVM MUM VAB.0001202171 Vista Polymers Highway 25 Aberdeen , MS S9730 A RVC RAILCAR ANALYSIS Load Date: 2. -/i"-9 Time Logged In: 7*0-00 Ship Date: Product: Logged In By : 0Order No: Car No.: 7 S3 7 1 Silo(s): CIS (.80 Customer: m.../n Compartment A Sample From Bottom Moisture % BL Contamination BR ,/J V Bulk Density BD w/antistat . S74> Viscosity RVCM An <d6o CA Bottom . to CB Bottom .if 9 &itb' 3 S5W , C+g .051 ' 036? Tappi Test Contamination Composite .06 or less .07----------.15 B Bottom ,7 7 Y Dl2~ .20---------- .60 Screen Analysis Mesh * 40 Weight % e.** 6. 0 60 , oC ,/ 80 3. If C.4 100 q.zc lt.<t 120 n.io 140 13. 07 200 C, Of* 12 J Pan A 17 3.3 Static Flow: 0 / f* l Avg. Microns: f3 3.2- Color L: fft a ,7^ b / ^ Technician: VAB.0001202172 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: February 19, 1992 Customer Nibco, Inc. 1900 Old Union Point Road . GA 30642 Attention: Steve Ryan Ship Date: February 17, 1992 wnA Product: 5265 Railcar No.: PTLX 42336 Order No.: 0005590-004 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .os .f&i 0.0 n.iL Jo4 . Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E . "Bagwe 11^ Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202173 Vista Polymers Highway 25 Aberdeen, MS 39730 & 1? V G RAILCAR ANALYSIS Load Date: -/& -f 2- Time Logged In: /Tco Ship 8Date ajnh Product: Logged In By: Order No: Q80& Car No. Silo(a): C?t tfo. it6, Customer: Mo 7yt^faL_____ Compartment A Sample From Bottom Moisture % .6-9- BL S'Contamination __ BR 7 Bulk Density ,337 BD w/antistat Viscosity RVCM ,09L CA Bottom 3- s ' 6S& Jo4 Tappi Test Contarnination Composite .06 or less CB Bottom .oS (* 8 .001 B Bottom # f 7 M*k> 7)0! .20 .60 Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight > at? O.pS *7.7/ 17.7% (3iS 7!?o /p/ % 0.0 M' ys'.i S.&f? II.9^ Static Flow: 0 Avsc. Microns: Color L: TL17 _ a $.7 b f.W Technician VAB.0001202174 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601} 369-8111 CERTIFICATE OF ANALYSIS Ai Date: February 19, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention Steve Ryan Ship Date February 13, 1992 VB1A Product: 5265 Railcar No.: UTCX 46423 Order No.: 0007115-000 Property Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh A 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ' !(d 53i D-D /.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Hr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515--1167 VAB.0001202175 ViBta Polymers Highway 25 Aberdeen, MS 39730 A Load Date: a ^-<n. Tine Logged In Ship Date: -- Product: Logged In By: Order No: Q&fff Car No . : V ^ 3 Silo(s): Customer: Compartment A Sample From Bottom Moisture % .10 BL Contamination BR Bulk Density BD w/antistat Viscosity RVCM ,C>81 CA Bottom . Ik . , CB Bottom J4 632. B Bottom , 2.0 s II .3? .Lnt> Tappi Test Contarnination Composite i ! .06 or less .07----------.15 . 20---------- . 60 Screen Analysis Mesh 40 Weight OtOQ % 0-0 60 0. o & *<0 60 Ml 8. o 100 120 l IRS If.33 33. <T It?.S' 140 JlH ^.0 200 S.f 3 Ml Pan LR Static Flow: 0 / Avg. Microns: Color L: 97 a /.<?> b A 77 Technician: VAB.0001202176 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A i Date: February 14, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: February 11, 1992 visnA Product: 5265 Railcar No.: GACX 73409 Order No.: 0005590-002 Property Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.11 0.547 0.00 11.5 2.1 0.001 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E.VQagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 m mrm ppm VAB.0001202177 Vista Polymers Highway 25 QenUL* Aberdeen. MS 39730 FVG HAILCAR ANALYSIS Load Date: Time Logged In: :_ctklh Ship Date Product: Logged In By: Order No: Car No.: '73 Silo(s): Customer: k Compartment A Sample From Bottom Moisture % BL Contamination BR C Bulk Density BD w/antistat Viscosity RVCM LL1 CA Bottom .of // .(oQ,\ CB Bottom ,C 7 J 9 B Bottom r// H 10 Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % 0,0 06 or less Ul 60 P.GS 80 J'.HO L.o Static Flow: 0 / 7T Color L: .07 - -------.15 .20 .60 100 Do.le 120 3V.Z 140 /Xt>? 200 Pan s~,7s_ ns 5./ Avg . Microns: / a b /-S9 Technician: VAB.0001202178 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CC EE R ~T X R X CATE CD R~ ANAI_V' S I S A Date: * February 14, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: February 10, 1992 Product: 5265 Railcar No VIPX 45921 Order No 0005590-003 Propertv Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.23 0.540 0.00 11.7 2.1 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202179 * Vista Polymers Highway 25 Aberdeen, MS 39730 A rvc RAILCAR ANALYSIS Load Date: it-*} Product: Time Logged In D4?ocj> Logged In By: Ship Date : t&f(0Order No: Car No , t+Sct 2-/ do Silo(e): *62 LSI Customer: m ni jUJ Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density j 7 BD w/antistat Viscosity RVCM .m CA Bottom . // t < .ASS' Tappi Test Contamination Composite .06 or less ______?A_______________ 0 "-3 1 t 1 1 1 4 tr CB Bottom . /7 7 rs? B Bottom jt S / ^2- 6 IS l&L m4 .20---------- .60 Screen Analysis Mesh * 40 Weight e.o _ % 60 G't> 0.0 80 z.o f 4`0 100 /.I7 /?. 7 120 it on 140 27.7 200 S. *7 /A 7 Pan /. 0 7 Static Flow: 0 /? / Avg. Microns: A?/, 0 Color L: 9tSZ a .77.. b A7& Technician: Airfare W mm v VAB.0001202180 r Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS Date: February 12, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: February 7, 1992 VKIA Product: 5265 Railcar No.: PLCX 43944 Order No.: 0006903-000 Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 0.15 0.538 0.00 10.0 2.2 0.055 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Et Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202181 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSTS Time Logged In: PC0T$ Ship Date: Product: 5265 Logged In By: Order Ho: 0@Q(Zrf> Car Hn : _ Sllofs): OOP Customer: LI? /VO /? Compartment A Sample From Bottom Moisture % BL Contamination BR .// _ 3 A? Bulk Density .tj4> BD w/antistat Viscosity RVCM d `0<Ss' CA Bottom .Li . ;f 3 7 .6/1 CB Bottom /t> .(& ,6// - Tappi Test Contamination Composite .06 or less .07----------.15 ^V 1 1 B Bottom ./r .OS? .on 0 CO m 1 i i i t o ft Screen Analysis Mesh 40 Weight % 0*0 60 0. 00 C.6 80 J. /*2- 100 //, o</ ZZ 120 17,31 140 IZ'^O z&r 200 /o< o Pan /.A *7 Static Flow: ^ ^ Avg. Microns: / -2- Color L: 7$(* $ a . 7/ Technician: VAB.0001202182 w Visto Pblymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 Aberdeen Mississippi 39730-0091 Phone (601) 369-811 1 CEIR TIFICATE OF ^M#=L_V'SIS & Date: February 6, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention Steve Ryan Ship Date February 3, 1992 Produc t Railcar No.: VIPX 45871 Order No.: 0005590-000 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.23 0.525 0.00 8.0 2.1 0.141 0.66 Polyvinyl Chloride, Virgin Resin, Not Rep Amy E. (-Bagwell Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 *** mrnmm VAB.0001202183 4 # VUU. Mimts HiftaMT2S: * Load Date:xi Product; Time Logged In: Logged In Ship Date: Silot s): Car Mo. Customer fho Moisture Contamination Bulk Density w/antistat 1 *st I 2nd 1 UVT.*&-J 1st 1 2nd J 1st J^pkJ T<Jj 1 ~ ,27 m HEMS Hf I -- & 3 1 .T>7 1 ,r*7 1 . S'SS 1 11 Viscosity RVCM 2nd Mirrex Shipments ONLY Screen Analysis Mesh Welght X 40 >00 0,0 60 0.00 0,0 80 r. io 100 11,10 Z2-2. 120 HO k. ?r /3.2i -?2,Z *tT 200 <Jf f.f Pan 2.J Static Flow: Avg. Microns: 1*1.0 Color L: a ,0 b Technician 1' II mm VAB.0001202184 1 Load Date: Product Car Time Logged In Logged In By: Ship Date: Silo(s} Cuatoaer: A Screen Analysis Mesh 40 Weight ___ 60 80 100 120 140 200 Pan _> 1 --__ __ - I Static Flow: / Avg. Microns: Color L; Technician: VAB.0001202185 Visto Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X F" X OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 __VS X S A Date: February 6, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention: Steve Ryan Ship Date: February 3, 1992 Product: 5265 Railcar No.: PLCX 42984 Order No.: 0005590-001 Property Moisture, 7, Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.28 0.538 0.00 11.6 2.3 0.004 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Ev Bagwell Laboratory Supervisor H (601) 369-3624 cc: Nibco, Inc. Nr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 wHvpmvee wmmmmmmrn m VAB.0001202186 Vista Polymers Highway 25 Aberdeen. MS 39730 A IP VC RAILCAR ANALYSIS Load Date: Time Logged In: Ship Date I*' Product: Logged In By: Order No: 0 Car No.: Silo(8): / Customer: l Compartment Sample From Moisture % Contamination Bottom Bottom Bottom no Bottom Bulk Density BD w/antistat Viscosity RVCM Tappi Test Contamination Composite ,(do(q .Old . OfiO or .07 .15 .hbD .60 Screen Analysis Mesh 40 Weight % 0. p 9.0 60 . ot> W 80 "7,c> 100 7.7 7 /ir 120 /*/</ 32 J 140 /J.J? tin 200 6". 3* Q Jt.L Pan L/C 2. 3 Static Flow: A / 7-f Avg. Microns: /J. O Color L: 1f.fi a .7/ b Technician flf 2$ xb T* VAB.0001202187 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I F1" X Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 OF ANALYS X S & Date: January 29, 1992 Customer: Nibco, Inc. 1900 Old Union Point Road Greensboro, GA 30642 Attention Steve Ryan Ship Date January 27, 1992 VISIA Product: 5265 Railcar No.: VIPX 45805 Order No.: 0005589-000 Property Moisture, V. Bulk Density, gm/cc Particle Size, '/. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.21 0.00 13.8 2.6 0.016 0.65 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy EL/ Bagw^lJ/ Laboratory Supervisor/Lead (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202188 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date: Time Logged In Ship Date : t )43o Product: Car No.: Logged In By: Silo(s) : Order No: 0^O&Q Customer: A/o 7Vef+(-- Compartment A Sample From Bottom Moisture % 6JZ BL Contamination Jp BR sty/Bulk Density BD w/antistat Viscosity RVCM Ml CA Bottom 7 -W CB Bottom B Bottom .2/ MSI Tappi Test Contarnination Composite .06 or less .07----------.15 .20---------- .60 Screen Analysis Mesh 40 Weight % 60 D/t 80 3.6,0 7.2 100 9,0o /$ 0 120 30 140 2V.3 200 /2* Pan III 2.L Static Flow: ^ 7 Avg. Microns Color L: Cf/-Zf a QM(c b /?/ Technician: VAB.0001202189 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone {601)369-8111 C EE F? T IFI OF ANALYSIS A January 13, 1992 Customer: Nibco, Inc. Route 2 Greensboro, GA 30642 Attention: Ron Greene Ship Date: January 11, 1992 VKIA Product: 5265 Railcar No.: VIPX 45812 Order No.: 0004556--005 Property Moisture, V. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.15 0.00 10.4 1.9 0.001 0.66 my t.^uagwel Laboratory rv] (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202190 Vista. J I * ML * Load Date: Product: 5265 Car ito..- Q&81& Tine Logged In: Ship Date: Silo(s): Logged In By: .Custoner Alike Moisture Contamination Bulk Density 1st 2nd 1st 1st | 2nd 1 1st 2nd i-to-1 jr j 2- 1 1 \ , 12, J~ / ^ ^ 2--1 Lfjo w/antistat Viscosity RVCM OOl Mirrex Shipments ONLY Screen Analysis Mesh 40 Weigh t X 0^0 0,0 60 80 Z ,3 % + Static Plot#: Color L; 100 oXf 2,/./ 120 U.00 140 a. 200 /0.<t Avg. Microns: /3S.I b /. 3 & Pan /.? T^chnicimn: VAB.0001202191 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTIFICATE OF V' SIS A Date: January 13, 1992 Customer: Nibco, Inc. Route 2 Greensboro, GA 30642 Attention: Ron Greene Ship Date: January 10, 1992 VIS1A Product: 5265 Railcar No.: VIPX 45811 Order No.: 0004556-006 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.25 0.531 0.00 15.4 3.3 0.015 0.65 Amy E. Hague Laboratory Supervisor/Lead (601) 369-3624 cc : Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202192 nm. Mimt* triitwr 28.' %J* mb.: A Load Date; Tine Logged In: Ship Date: Product: 5265 Car No ... (ist/f 70o Logged In Bp; : h/Jj-CC Mirrex Shipments ONLV Screen Analysis Mesh Weight 40 <2 , X? 60 80 100 120 140 { jL /L.9 Static Flow: Color L: Avg. Microns: ?7 * >-?' b /-19 200 7-^ Pan 3-3 Technician: VAB.0001202193 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTIFICATE OF ANALYSIS A Date: January 10, 1992 Customer: Nibco, Inc. Route 2 Greensboro, GA 30642 Attention: Ron Greene Ship Date: January 8, 1992 Product: 5265 Railcar No.: UTCX 46419 Order No.: 0004556-004 Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.09 0.539 0.00 8.9 2.1 0.020 0.65 .# Laboratory Supervisor/Lead (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. 0. Box 1167 Elkhart, IN 46515-1167 VAB.0001202194 I ** K A > * Vista* MLfNrs ML 3.1T3IX Load Data: Product: 5265 Car No*; Ti.se Logged In: Ship Date: SLlo(s): Logged In By: ; A/lkdO . Cuatoaer /i/p Moisture Contamination Bulk Density w/antistat Viscosity RVCM 1st 2nd 1st 2nd 1 1St 2nd 1 1st , e> 1 1i 7f 1 . 0*9 __________________ 1 1 '<0/ I I -- IX J_1 _______________________ I y l><7 1 Is<7jT 2nd Mirrex Shipments ONLY Screen Analysis Mesh 40 so so Weight * -p c>~ o Static Flow: Color L: 100 120 140 200 Pan 7.63 7 Avg. Microns: ab Technician: M v-* &rr VAB.0001202195 Vista Polymen A Division of Vista Chemical Company Highway 25 Post Office 8ox 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: / /0/4Z- Customer: Nibco, Inc. Rt. 2 Greensboro, GA 30642 Attention: Ron Greene Date of Shipment: i/e/iz- VISIA Product: 5265 Order No. : 2 '002- Trailer No.: 7" tyiS' Property Moisture, X Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana 1vsis ,/6 , 630 0-OQ H.& Zb lr,< upe a/ r/Lead cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja Mft PMNM VAB.0001202196 Date. Customer Nik Technician. PVC BULK TRAILER ANALYSIS Product Trailer Number Time f^ Order No. COLOR A vise RVCM FRONT MIDDLE END a = o5 B L= A= & rtf B= L= A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt H on Mesh <p,0 g>4>P Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 0.0fa >/ u_ /Q.2.Q AgJ)3 + X0.[ &>. $ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 60 100 120 140 200 Glassy Pan Part. / Glassy Pan Part. Remarks Star 207A Revised 1 /12/87 4H* AB.0001202197 mmm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I R" X OF ANALYSIS Date; A Customer: Nibco, Inc. Rt. 2 Greensboro, GA 30642 Attention: Ron Greene Date of Shipment; A$"^2 Product: 5265 Order No.: OOOSS>2* '00^ Trailer No.: Property Moisture, V, Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.00 15.0 ('o Labor sor/Lead cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT; Louis Macakanja mmi IP mmmmmmmmmmmrnmm VAB.0001202198 PVC BULK TRAILER ANALYSIS A Date Customer Technician. Product Silo___ m. Trailer Number (Of-g-Uoo Time Order MOIST T0 Bottom I CONT. Bonom GEL i BULK DENSITY i DRY TIME COLOR 9fg! vise RVCM FRONT i MIDDLE 2. ii A= B Xi L A= B= I l i i i L* END A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh > 60 s>wr a Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap ithaker. 49 gms. Resin plus 1.0 gmii. Carb 60 80 100 120 140 200 Glassy Pan Part. ^S 1i to $ i 0. 6S SfCe 7/5 is.s ts.o 29 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1 /12/67 vmM m T .0001202199 t Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 A CERTIFICATE OF ^Y S I S Customer: Nibco, Inc. Rt. 2 Greensboro, GA 30642 Attention: Ron Greene Date of Shipment: Product: 5265 Order No.: 00O*D3i-to2- ailer No.: 7^-72-Z- Property Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-iO Analysis .os' ,S4z D'OQ H-3 L3_ cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja f wmmmmmm wmmrnmmmmmmmmm VAB.0001202200 PVC BULK TRAILER ANALYSIS A Date ^* ... Customer M lO^O Technician ptF+ftP1-- Product Silo Trailer Number Time Order No. 7*"^^ 3 / ~OCTZ^ Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 6.00 &> Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap sitaker. 49 <gms. Resin plus 1.0 gins. Carb 60 80 100 120 140 200 Glassy Pan Part. >. o& P. fp- lo.3f e>.> f;SL 20/7 ss:g 7?6.l //? /7 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks i VAB.0001202201 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I I CATE OF ^fM^L_VSIS Date: Customer: Nibco, Inc. Rt. 2 Greensboro, GA 30642 Attention: Ron G Date of Shipment Product Order No. Trailer No. Property Moisture, V, Bulk Density, gm/cc Particle Size, V, on 40 Mesh 200 Mesh Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.60 fHs7 0% Laboratory Supe isor/Lead cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mmmmmmmmmmmmmMmmrn mmmm mmm mm VAB.0001202202 Customer Technician PVC BULK TRAILER ANALYSIS A Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt % on Mesh 0. 0D Ot On Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 60 100 120 140 200 Glassy Pan Part. zm. _125 /t jjM. / /IS 23,2- g(*: 2- j+j_ Min On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. Remarks VAB.0001202203 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 CERTIFICATE OF ANALYSIS Date.: Customer: Nibco, Inc. Rt. 2 Greensboro, GA 30642 Attention: Ron Greene Date of Shipment: I ~ VISIA Product: 5265 Order No.: OOO *0t> i- OO O Trailer No.: ~7~~~'3'7S Property Moisture, X Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm n Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana1vsis 0.00 Z. 5 .017 or/Lead cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja MM* wmmmmmm m VAB.0001202204 r PVC BULK TRAILER ANALYSIS * Date. Customer Hi b<?o Product Silo___ Technician MOIST Tod Bottom CONT. Bottom '.M GEL I Trailer Number Time Order No._ OoO 5V3/ -OCO BULK DENSITY I. DRY TIME I COLOR vise RVCM FRONT 2. MIDDLE 2. 2. =<0.77 B -2./ I II L= \y A= `ip B= i i i L= END A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt 0 &G % on Mesh Screen Analysis .1 .i Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. e e>! o,C /of# Zb# **.3 /3S& T7)7 L 13 //? Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A ........ "*........... Revised 1/12/87 nm ....................... .. ................... Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601)369-8111 CERTIFICATE OF Date: / ~ 6? " Customer: Nibco, Inc. Rt. 2 Greensboro, GA 30642 Attention: Ron Greene Date of Shipment: Product: 5265 Order No.: OQC&S^I Trailer No.: 'T"2- / Property Moisture, 7. Bulk Density, gm/cc Particle Size, 'A on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ,23 n.DO 2-6 Super r/Lead cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja m VAB.0001202206 PVC BULK TRAILER ANALYSIS Date A A ^ Customer AV b^-O TechniciaPr/Tf-HP*-- Product Silo___ Trailer Number 7^7(s> Time IPS* U36 Order No. CDOSS^Z -6Of FRONT MOIST CON'T. Top Bottom | Top Bottom \2$ m I GEL I BULK DENSITY I 2. 2. DRY TIME I \i i MIDDLE 2. COLOR vise RVCM a =<0.7 2 B =2 L= A- 1+ P.ls I. i B= 1 L= END 2. A= B= Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare Net Wt. h on Mesh Screen Analysis 40 6.0 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap sitaker. 49 gims. Resin pHus 1.0 gims. Carb 60 80 100 120 140 200 Glassy Pan Part. &>f ksa. ft35' fsrus: //*/ /*?<? 1 &(s> 3LZ a-z.S IQ.H- Zb Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Glassy Pan Part. 60 80 100 120 140 200 Remarks Star 207A Revised 1/12/87 ................... Vista Polymers A Division of Vista Chemicol Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601} 369-8111 CERTIFICATE OF Date.: ^__ Customer: Nibco, Inc. Rt. 2 Greensboro, GA 30642 Attention: Ron Greene Date of Shipment: 2_ Product Order No. Trailer No. 7~<S? Property Moisture, V, Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis O .f)DZ K 00/ Laboratory Supervisor/Lead cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mm VAB.0001202208 PVC BULK TRAILER ANALYSIS A Dale Zr Customer Technician FRONT Product Silo___ MOIST CONT. \Top Bottom Top Bottom t 05. I i 2. II GEL Trailer Number Time Order No. C>> o J "3 ? jL-eo / BULK DENSITY DRY TIME l COLOR vise L = 9 7-9? RVCM 7A - O./ I b - /-xt 7-i lI L= Miwi inni f A= B= l l l l L- END A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Jl1p Net Wt. % on Mesh 0*00 0,,e>6 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap sihaker. 49 gms. Resin 1plus 1.0 gms. Cart) 60 80 100 120 140 200 Glassy Pan Part. o. >4 t> . O Min. 4.i(o u,n /s-.K ILLt `LSI /. 1 23.S 311 23S u'r 1 - - 2S On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12A87 mmmmmmmrnm w wmmmmm pmm AB.0001202209 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS Date : / S "2-- Customer: Nibco, Inc. Rt. 2 Greensboro, 6A 30642 Attention: Ron Greene Date of Shipment: /*"2 Property Moisture, X Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR--IO Product Order No. ailer No. 3? / Analysis >.Q f. 2. A &a Laboratory Supervisor/Lead cc:Nibco 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202210 % PVC BULK TRAILER ANALYSIS Date / Customer Technician a/* Jo /** . Product Silo___ SJ Jo Trailer Number Time <222. Order No. FRONT MOIST CON'T. Top Bottom | Top Bottom I of 1/ 2. GEL I. 2. BULK DENSITY l . sr7 DRY TIME I COLOR L* = O' B = /&} i I I1 I L= MIDDLE 2. l END i. i A* B= LA= B- A / vise RVCM Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0.0 #.o bj Screen Analysis \< d' V Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 \gms. Resin plus 1.0 gnrts. Carb 60 80 100 120 140 200 Glassy Pan Part. 0.02^ 9-2 / /^ // bL 23 7 31-1- ZJ 2> Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 /. (Jf Gtaasy Pan Part. Remarks Star 207A Mmmv Revised 1 /12/87 mrnrnmmmmm 3/AB.00Q12Q2211 1:11..........I' I11" . i I I' I " 11 111 1111! 11III' I'''' 111' II!'''' II !11' 'Til1' II !TI ri nl 1111 PI ' 11 I' ! 111 n 11 l r-1111 !. II11! : I " 111! 111111,11 - 11" 1111 : III 1111 III n... ill- III . : I -1 - - I I' H v. i t f i * . * % t j 4 i t i- . i i 4 i i Cu-' f- } i > i i i * VAB.0001202212 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Fax # 219-534-1079 Date: Customer: January 4, 1993 Nibco, Inc. 701 Eisenhower Drive Goshen, IN 46526 VISIA Product: 5265 Attention: Pat Forrest Railcar No.: GACX 73411 Ship Date: December 31, 1992 Order No.: 0019801-002 Property Test Method Specification Moisture, % ABR-1A 0.30 Max. Bulk Density, gm/cc ABR-2A 0.520 Min. Particle Size Distribution ABR-3 % On 40 Mesh 01 Max. % On 200 Mesh *NDS % On Pan 5.0 Max. *Specification is 25.0% Max. for the 200 Mesh plus Pan Residual VCM, ppm ABGC-26 2.0 Max. Inherent Viscosity ABR-10 0.64 - 0.68 Analysis 0.18 0.543 0.00 20.9 2.0 0.007 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwel it Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202213 Vista Polya Highway 25 Aberdeen, MS 39730 A RAILCAH ANALYSIS Load Date: ^ Product: Car No. : *?3 7 H Time Logged In Logged In By:rtzir Silo(s): Ship Date : tlizf Order No: AX) / 002^ Customer: (=&& Compartment * Sample From Moisture % A Bottom BL Contamination ___ BR ? Bulk Density .r*f BD w/antistat Viscosity RVCM .ool CA Bottom 3 t m 02i' J CB Bottom ./7 S 9 .Uh 1 .001 B Bottom ./t - .6s'? DC) Tappi Test Contarnination Composite .06 or less 4 .07----------.15 .20 :---------- .60 Screen Analysis Mesh * 40 60 80 100 120 140 200 Pan Weight C.60 . /A to Jl. S'o /a 4fcf ^ % 0`Q W U i?.Q 21.7 22.0 2>*1 o Static Flow: 6 / f.t- Avg. Microns: 7 Color L: /T a > 7/" b / Technician: VAB.0001202214 Vista Polymers A Division of Vista Chemical Company >1 Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERT IEICATE OE ANALYS X S Date: Customer: 12/22/92 Nibco, Inc. 701 Eisenhower Drive Goshenf IN 46526 VlSlAFax # 219-534-10 Product: 5265 Attention: Pat Forrest Railcar No.: VIPX 45872 Ship Date: 12/21/92 Order No.: 0019801-001 Property Test Method Specification Moisture, % ABR-1A 0.30 Max. Bulk Density, gm/cc ABR-2A 0.520 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. % On 200 Mesh *NDS % On Pan 5.0 Max. Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. Inherent Viscosity ABR-10 0.64 - 0.68 Analvs 0.18 0.550 0.00 20.0 2.4 0.128 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H. D. Lucas Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 noiiture x BL Contamination BR r* 3 | Bulk Density BD w/antistat m Viscosity .SSj RVCH *S 7 ,ss0 \>!J .SSI .o%- // n <* - .u<r m Tappi Test Contamination Composite .06 or less * .07----------.15 ____________________________________ _________________________________________________________________________________________ .20 :---------- .60 Screen Analysis Mesh * 40 Weight O.o % 60 0<e 80 l.te 3.*7 100 t-u 120 51*},% 140 87*0 200 I8.&0 5(iD' (3Static Flow: o L Avg. Microns: / * "7 Color L 2HZ .si a b Pan / z-Z. <5 / Technician: VAB.0001202215 TRANSMISSION CONFIRMATION REPORT No.-001191 DATE/TIME DURATION TRANSMITTER C FROM1 26s U1STA QC LAB 601 369 3642 RECEIUER CTO) PAGES XMITTED 01 PAGES ERRORED RESULT OK COMM. MODE G3 RESOLUTION NORMAL 2195341079 A VAB.0001202216 55-0000349 TRANSMISSION CONFIRMATION REPORT No.-001268 DATE/TIME DURATION TRANSMITTER CFRQM) JAN 2Bs 6, 1993 -1 * * 1 UISTA QC LAB 601 369 3642 2:35PM rf i* RECEIUER CTO) PAGES XMITTED PAGES ERRORED RESULT COMM. MODE RESOLUTION i^M^B | 2195341079 01 OK G3 NORMAL VAB.0001202217 55-0000349 Vista. Polymers Highway 25 Aberdeen, MS 39730 A RAI Load Date 2-/0 ^90- Product : ANALYSTS V\PK Tine Logged In: Ship Date: /X-/-2-t/fy Logged In By: Order Ho: Silo(6): ustoner Ahbdo t Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD w/antistat .SSI Viscosity RVCM * CA Bottom rtf 4 uhi I2S CB Bottom /J 2zL_ .SSI 0C .o9sr Tappi Test Contamination Composite .06 or less Hj> .07----------.15 B Bottom s .SS'O * .DSt? .20---------- .60 Screen Analysis Mesh 40 60 Weight .0(e 80 L5A % &*() t3Static Flow: o L Color L 100 120 140 200 MSI fJ*S^ MM Ibt 37*0 3 qjo> Avg. Microns: /2 ~7 .si ab Pan 22=. Technician: VAB.0001202218 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Fax # 219--534--1079 Date: December 17, 1992 Customer: Nibco, Inc. 701 Eisenhower Drive Goshen, IN 46526 VISIA Product: 5265 Attention: Pat Forrest Railcar No.: UTCX 46419 Ship Date: December 15, 1992 Order No.: 0019801-000 Property Test Method Specification Moisture, % ABR-1A 0.30 Max. Bulk Density, gm/cc ABR-2A 0.520 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max % On 200 Mesh *NDS % On Pan 5.0 Max. is 25.0% Max. for the 200 Mesh plus Pan Residual VCM, ppm ABGC-26 2.0 Max. Inherent Viscosity ABR--10 0.64 0.68 Analysis 0.23 0.548 0.00 13.2 2.3 0.113 0.66 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 cc: Nibco, Inc. Mr. Louis Macakanja P. O. Box 1167 Elkhart, IN 46515-1167 VAB.0001202219 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged In: Ship Date: iziid RAX 4 ANALYSIS uW Product: Car No. f^t/f Logged In By: Silo(s): 87 +(=88 Order No: Cf) I/"'OOQ Customer: A^l loCo , No -- Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density /<g s BD w/antistat * Viscosity RVCM CA Bottom f .6gb 4 * ./4-JT7 CB Bottom .2/ ? A3 , 432. *S^7 .m Tappi Test Contarnination Composite .06 or less .07----------.15 N f\ i B Bottom ,33 cH>o .20---------- .60 Screen Analysis Mesh ' 40 Weight a co % 0,0 60 q <?/ 80 3.7+ 7 100 MAh d&A 120 L6Z!S JM 140 f 200 IS&. Pan U7 Static Flow: 0 /fUf Avg. Microns: Color L: 77 ^O a b LS7 Technician: terT-HtpL' VAB.0001202220 I A NIBCO - KENTUCKY : i \ VAB.0001202221 Vista Polymers A Division of Vista Chemical Company A H Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 5^2- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: VISIAProduct: 5305 Order No.: Cust. PO No.: Trailer No.: yes/y=w> 'owj 3/- 7o <9 & '7~-3EO Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. ./* Bulk Density, gm/cc ABR-2A 0.510 Min. . S3<f Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max % On 200 Mesh *NDS % On Pan 5.0 Max. 3 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. .vk> Inherent Viscosity ABR-10 0.71 - 0.76 .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202222 PVC BULK TRAILER ANALYSIS Date 9'll Customer flJ 1 bC a Technician Product Silo___ .P 0 * MOIST Top Bottom I CONT. Toe Bottom li-a GEL FRONT 2. 2. I. Trailer Number o $e> Time / A'^fT Order No. QO/47 ~O BULK DENSITY I .SJ4- DRY TIME i COLOR L = ko, * o = 4.ZS vise B == /.Cl L- Tv V Urnfl % l/^| J o 7, A MIDDLE 2. END l 2. A= B= l 1 L= A= B= Particle Size Distribution: Screen Analysis \O Mesh Size 40 Gross Wt. Tare Net Wt. $\ % on Mesh * O *> 0-0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 6..15- 7 ,U 19. 9? /, n ts-i V.o 3X.o too llf-0 4-.S Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 1.(3 1.3 ( Pan Part Remarks Star 207A Revised 1/12/87 *4* 4. VAB.0001202223 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTX FICATE OF ANALYSTS A : blgLl/l Date Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: Q}Si7 VIS1AProduct: 5305 Order No. : QQI3&ZZ -00^7 Cust. PO No . : J?/- 36 3 3 Z- Trailer No. : Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. .02- Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.0 % On 200 Mesh *NDS % On Pan 5.0 Max. -^JL Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. .Do! Inherent Viscosity ABR-10 0.71 - 0.76 .1^ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory ervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202224 Date. Customer itjib CjQ PVC BULK TRAILER ANALYSIS Product Silo___ ?62 /Trailer Number Time & 9 '/j Order No. A Particle Size Distribution: Screen Analysis i& Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. H on Mesh Screen Analysis o.& 60 80 100 120 140 200 ;/ O >& jay /(.S7 %3sT asY 33-3 121 -3-V7 A3 __ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 80 100 120 140 200 _________ _________ __________ __________ _________ _________ ______ _________ _________ _________ _________ __________ _________ __________ _________ ___________ ____________ _________ _________ _ _________ _________ Glassy Pan Part. 2d. Glassy Pan Part. p Remarks 4 ft Star 207A Revised 1/12/B7 - * \ -*v < + * w\ 'h mmrnmmmmtmmmmmmmm m VAB.0001202225 Vista Polymers 4 A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 OERTXFXOATE OE ANALYSX S A Date : 4 j(O Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: ^ j( 0 Product: 5305 Order No.: Cust. PO No.: Trailer No.: 7^ 3&C> D&'Z*' Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. 0.0! Bulk Density, gra/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0*0 % On 200 Mesh % On Pan *NDS 5.0 Max. / A fh Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. ___* 60 Inherent Viscosity ABR-10 0.71 - 0.76 7- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Su visor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202226 PVC BULK TRAILER ANALYSIS 4 Date______ ^-/O * 9 Customer /C**A ee Technician *! H -- Product ^?QJ~ Silo_______ 7 Time Order No. _________ /H-'lO Trailer Number / " 3> O0 !*j: '0 A Particle Size Distribution: Screen AnalysisLMin fO On Rotap shaker. 49 gms. Resin plus 1.0 gms. Garb Glassy Mesh Size Pan Part. 40 60 80 100 120 140 200 Gross Wt. Tare /o T Net Wt. % on Mesh /'/* U7 M3 IS. OS' 7US' ji.Sj o-h C>.p e?-,3 [13 M.o Jo.3 IS.3 A/ Screen Analysis Mesh Size Gross Wt. 40 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Tare Net Wt. a1 % on Mesh Remarks Star 207A Revised 1/12/87 v -*. 'J*', vm wan VAB.0001202227 mrnmm o Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 RTIFX CAT OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 ANALYSIS A Date: 7 Se?*- 12, Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 7 Sejrt* ^ *- Product: 5305 Order No.: o o /yr?6-o o J Oust. PO No.: Trailer No.: 7" Property Test Method Specification Analysis Moisture, % Bulk Density, gm/cc ABR-1A ABR-2A 0.3 Max. 0.510 Min. . /I Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0. o % On 200 Mesh *NDS % On Pan 5.0 Max. Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. Inherent Viscosity ABR-10 0.71 - 0.76 -7Z Polyvinyl Chloride, Virgin Resin, Not Reprocessed. #/. jds oratory Supervrsor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202228 Dale Customer Technician ;k /H*i PVC BULK TRAILER ANALYSIS Product ^ j^>r Silo. LZ.3 Trailer Number Time fjoo Order No. oo ^ / A Particle Size Distribution Screen Anelysis 10 Mesh Size Gross W1. Tare Net Wt. % on Mesh Screen Analysis 40 0 AO Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min shaker. gms 1.0 gms. Carb Glassy Pan Part. 60 80 100 120 140 200 . vS* 1*30 // I3'*1 ir.sO t.<o S.ia zt.z. n.e Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 L31 Glassy Pan Part. |> Remarks Star 207A Revised 1/12/87 I* Mi VAB.0001202229 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: &[ - 3 -i Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: ^ ^ Product: 5305 Order No.: DO/*/S7-OOO Oust. PO No.: Trailer No.: Property Moisture, % Test Method ABR-1A Specification 0.3 Max. Analysis . op. Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. GlO g>. o 3-0 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 2.0 Max. 0.71 - 0.76 ,73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202230 Dale_____ Customer fO \ & Technician____ fHt PVC BULK TRAILER ANALYSIS Product vS3 QJ Silo& ?7 Trailer Number _____ Time Order No. 7~~~ / - Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh Screen Analysis 40 OO 0D Mesh Size Gross Wt Tare Net Wt % on Mesh Remarks 40 M Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. i2.or /o./i* tgz. & j<a u 3 fro Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 /o f 3- o Glassy Pan Part. Star 207A Revised 1/12/87 - " - *'-i *- SeV ' ^ ^ C -f THE* iMsmuMimi^ r wmmmm VAB.0Q01202231 L Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTIFICATE OF ANALYSIS A Date: -- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: $*^30 **-- Product: 5305 Order No.: --Go8 Cust. PO No.: 30X3^-- Trailer No.: "A-*' Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. Bulk Density, gm/cc ABR-2A 0.510 Min. , jT/5" Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. &O % On 200 Mesh *NDS Z^./ % On Pan 5.0 Max. 1. </ Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. . IQ.Q Inherent Viscosity ABR-10 0.71 - 0.76 <75 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc, (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 wmm VAB.0001202232 PVC BULK TRAILER ANALYSIS Datea "qw -*7 Product________53^________ Customer t\J b^o _ Silo______ fci&D: Time Technician_______ Order No. Trailer Number_____ T ____________ h Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare ^ Net Wt. % on Mesh Screen Analysis 40 * o.Z> & o Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 0,0 b ./ Y-t2- P'UL 3? a t-3 31- 1L. > 7 JA Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. l Glassy Pan Part. Remarks Star 207A Revised 1/12/87 W VAB.0001202233 *i*. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: | ^ Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 8 {'Zofoi, Product: 5305 Order No.: Cust. PO No.: 3/-^q332^ Trailer No.: 1^383 S Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. . bCo Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. >.D <?.7 3. o Specification is 25.0% Max. for the 200 Mesh plus Pan, Residual VCM, ppm ABGC-26 2.0 Max. .02*1 Inherent Viscosity ABR-10 0.71 - 0.76 *73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. visor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202234 4 Date Customer Technician - n-9 M iltO (V\ PVC BULK TRAILER ANALYSIS Product SiIo___ 5JoS Trailer Number. T~ Order No. 0 h ^ Particle Size Distribution: Screen Analysis / Mesh Size 40 Gross Wt. Tare T Net Wt. % on Mesh /P.O <0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. * 0 ^7 _q S.l Kp-^4- /2.3S -?n l.tf* 3a. 8 *1-1 f.*7 3-o Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Pan Glassy Part. Remarks VAB.0001202235 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen,, Mississippi 39730-0091 Phone (601)369-8111 h Date: S^/do ~9 Customer: Nibco, Inc. 2929 W, Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: Product: 5305 Order No. C>o / J -ooy Cust. PO No. Trailer No. JI-30 33X. Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. ></ Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max 6>. O % On 200 Mesh *NDS 7JT % On Pan 5.0 Max. S7 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. . DOl Inherent Viscosity ABR-10 0.71 - 0.76 73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 mrnmrnimmmmmmmm mrnmmmmmmmmm VAB.0001202236 mmmm it Date 2 Customer _ fUi b Co Technician M *T PVC BULK TRAILER ANALYSIS Product Silo J5~3 3 Trailer Number _/" ^ Time Order No. T A Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare Net Wt.' % on Mesh Screen Analysis 4 Mesh Size Gross Wt. Tare Net Wt. % on Mesh -------40 o Q.O- 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 f Min. f.OZ AS.fo to*) aS.4 1 Ifi2 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. LSI 3,7 Glassy Pan Part. Remarks VAB.0001202237 I 1^ * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYST A Date: *3/*? Customer: Nibco, Inc. 2929 W. Mag ine Louisville, KY 40201 Attention: Sandy Money Ship Date: VIS1AProduct: 5305 Order No. OOtSColz-OoS Gust. PO No. : 5/- ^0532- 1 Trailer No. : j ---,^^7*7 Property Moisture, % Test Method ABR-1A Specification 0.3 Max. Analysis ool Bulk Density, gm/cc ABR-2A 0.510 Min. 0.53/ Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. o.o to. 5 3.1 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 2.0 Max. 0.71 - 0.76 OZS" 72- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. pervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202238 * PVC BULK TRAILER ANALYSIS Customer aX. I c,e> Product Silo___ sS"3o &> pi Technician JH FRONT MOIST Top I of Bottom 2. COTNT. Top Bottom 1y i GEL 2. II Trailer Number 7~-3?7 Time TO'.20 Order BULK DENSITY l DRY TIME COLOR vise RVCM L = r?,sz> S'3 / A =0 b= I L= MIDDLE 2. I I l. END A= B= L= A= B= Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare Net Wt 44 on Mesh Screen Analysis 40 &.Q 00 Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. /<*3 7 /&>.bO .<?</ J.fC Mi . / t i-i 3^-U 4.3 3.7 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369*8111 ANALYSXS A Date A 92^ Customer: Nibco, Inc. 2929 W. Mag ine Louisville, KY 40201 Attention: Sandy Money Ship Date: $--9''"*? Product: 5305 Order No. : 0O(Z(0*f^L -- OO'Z. Oust. PO No. : 3/-30332 Trailer No . : f ~ 3 77 Property Moisture, % Bulk Density, gm/cc Test Method ABR-1A ABR-2A Specification 0.3 Max. 0.510 Min. Analysis j? , S37 Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. Q^ 56 ^9 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. .038 Inherent Viscosity ABR-10 0.71 - 0.76 .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202240 U-T PVC BULK TRAILER ANALYSIS A Date Customer FRONT Product Silo___ to Trailer Number__/ J' 77 Time OtoO Order M 0 0 17 ^-OCT^ MOIST CON'T. Top Bottom | Top Bottom I 4r 2. GEL I. 2. BULK DENSITY i L ??7 DRY TIME i I I II I COLOR L =n A= B `<2.IL L= vise RVCM ^7 MIDDLE 2. l ll END A= B= L= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh p<po 0,0 t. Screen Analysis 4 l' Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. .// (r 1SJ U.ld Z7 J.g2 L32 ,2. iM 3.7I ,7.?. -2. 17.1 .L 3,7 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Glassy Pan Part. 60 80 100 120 140 200 Remarks VAB.0001202241 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone {601) 369-8111 Date : - L - /L? Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: P , Product: 5305 Order No.: O O / %C>a\ 2 ~ O O j Cust. PO No.: Trailer No.: T'" 2 17 Property Moisture, % Test Method ABR-1A Specification 0.3 Max. Analysis -// Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 6. o % On 200 Mesh *NDS 7 % On Pan 5.0 Max . Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max . #Do~ Inherent Viscosity ABR-10 0.71 - 0.76 .7? Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202242 PVC BULK TRAILER ANALYSIS A Date Customer Technician FRONT Product 5Joi MOIST Top Bottom CON'T. Top Bottom I. A GEL I 2. 2. I. I Trailer Number / Time (JQ'< 3 Order BULK DENSITY I DRY TIME COLOR -nv - ,7<f B - 2-0 f II L= MIDDLE 2. l i A= B i L= J?7 Co | vise 79 ,<S(4 END A= R= Panicle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt. % on Mesh O Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. oa6.01 22 /l.yy 0-1 II-4 2L(e-X 116 U3 Sto Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFIC Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSX S l Date: Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: Product: 5305 Order No.: Oo/3^Si-oc/ Cust. PO No. : 3b 3033 Trailer No.: ~[~~307'7 Property Moisture, % Bulk Density, gm/cc Test Method ABR-1A ABR-2A Specification 0.3 Max. 0.510 Min. Analysis . iU> .53Co Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. o. o % On 200 Mesh % On Pan *NDS 5.0 Max. &/ z.s Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. .on Inherent Viscosity ABR-10 0.71 - 0.76 .13 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory dj rvisor/Lead (601) 369-8111 (' FAX To^Ester Saldiva: v"----------Nibco. Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202244 PVC BULK TRAILER ANALYSIS A Date Customer A/t&CO Product Silo___ 22 Trailer Number Time Technician Order FRONT MOIST I CON'T. I Top Bottom I Top I Bottom ' GEL '<./(0. 1 J bulk DENSITY 1 b 2. DRY TIME I 11 l COLOR A = d).4f . -2./Z L= Oof vise RVCM MIDDLE 2. 1. 1 1 1 END A= B= L= A= AA, B- Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh a 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 A 00 0X> Min On Rotap shaker. 49 <gms. Resin |dIus 1.0 gims. Carb 60 80 100 120 140 200 Glassy Pan Part. 6. Min. 1333 fot *7 to S(*z fS.3 20, Sb ' J5l3 TM 2+ On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 I 80 Pan 100 120 140 200 Glassy Part. o,f 9.13 (3& 1343 ass ftS Z9+ 3/jO *03 4f Remarks VAB.0001202245 o Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date : 7&/12- Customer Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date : VIS1AProduct: 5305 Order No. : Oust. PO No. : 3/~ Trailer No.: ~/~37? Property Moisture, % Test Method b ABR-1A Specification 0.3 Max. Analysis Bulk Density, gm/cc ABR-2 A 0.510 Min. . 570 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. % On 200 Mesh % On Pan *NDS 5.0 Max. 2.1 Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. . P22 Inherent Viscosity ABR-10 0.71 - 0.76 .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 ster Saldivar Nibco Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202246 PVC BULK TRAILER ANALYSIS A Date Customer Technician Product Silo 7/ C 75 MOIST CON'T. Bottom | Top Bottom l. i GEL FRONT 2. 2. 1. i I MIDDLE 2. !. i l END Trailer Number ~37$ Time (?:Sr Order No jOO /24+S DRV TIME 1. COLOR vise - II PS 11^ 3 * *> * B = 4?/ I L= A= RVCM <&/ D28 B= L= A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh tf'O Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 . Min On Rotap ishaker. 49 gms. Resin p>1us 1.0 g ms. Carb 60 80 100 120 140 200 Glassy Pan Part. 03'3 (.1 /?.*/ axt 13--"31f 1-13 W 2Li liJ 7,1 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 133 3.1 Glassy Pan Part. Remarks VAB.0001202247 Vista Polymers A Division of Vista Chemical Company o Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: g~ >-72- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: % VK1AProduct: 5305 Order No.: &o/3 - OO o Cust. PO No.: 3>/-3033>; Trailer No.: Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. . e>3 Bulk Density, gm/cc ABR-2A 0.510 Min. S/I Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. ___o o___ <7. / 3J Specification is 25. 0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. Inherent Viscosity ABR-10 0.71 - 0.76 .76 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 Ester Saldivar Nibco, Inc. (502) 778-0603 To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202248 PVC BULK TRAILER ANALYSIS k Date 3/-U Customer Product Silo___ SJoJ 021 Technician FRONT MOIST ISSL Bottom \c>3 2. CONT. Ttip Bintom i3 L GEL I 2. i tI Trailer Number _ Time /# <f Order No. >0/3 BULK DENSITY l .SbC f fietsSff DRY TIME I COLOR L = me A = ti B= L* 37? ooo vise 7(TV T6 /.? MIDDLE 2. I END I. I A= B= l L= A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. on Mesh 6,0 0<O Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh Remarks 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. Min. 60 &J2 UJU IZZJ tl3 V-fl Hi 2L2 Jo. 4 LLSL la On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 ISY Glassy Pan Part. Visto Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSX S k Date: 7|ze>|^z- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 7 Product: 5305 Order No. : QC>I Cust. PO No.: 31-300 </</ Trailer No . : ~T~` <370 Property Test Method Specification Analysis Moisture, % Bulk Density, gm/cc ABR-1A i ABR-2A 0.3 Max. 0.510 Min. . t! . 530 Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. 0 .o *NDS 3.6 5.0 Max. 3.C? Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 2.0 Max. 0.71 - 0.76 .0S! . 7Z- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor visor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202250 PVC BULK TRAILER ANALYSIS Date 7- 2 77- Customer Mil Technician Product 0 Silo___ Lil, Lti Trailer Number. Time /f& o Order Nn. O FRONT MOIST CON'T. Top I. ,// Bottom | Top I Bottom GEL i. . SO Hi BULK DENSITY I 2. 2. DRY TIME I I I II I COLOR L = 4% 77 A = .LI b = 2*o3 L MIDDLE 2. I END A= B= l I I l L= A= B 3 7? OO vise RVCM oof Particle Size Distribution: Screen Analysis_______ / &_______ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Pari. Gross Wt. Tare Net Wt. H on Mesh 6<0o 0*0 ///? /7-3-a- 4,/<t_____/*/ /. If /./ zz.- jy. i z7.o r.3 3.(, Screen Analysis Mesh Size 40 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. Gross Wt. ______ - _________ _________ _________ _________ _________ _________ Tare __________ __________ _________ _________ _________ _________ Net Wt. __________ _________ _________ _________ _________ _________ _________ _________ ____ % on Mesh __________ ______ __ Remarks Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTXFI Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date: / ^ Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 7--^^ *" ^ Product: 5305 Order No.: 012.4^3-007 Cust. PO No. : 3 I- 30 Trailer No. : J _ 3 7 7 Property Moisture, % Bulk Density, gm/cc Test Method ^m^^^^^*****i ............... ii -- ABR-1A ABR-2A Specification 0.3 Max. 0.510 Min. Analysis , oi . 521 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. n.o % On 200 Mesh *NDS % On Pan 5.0 Max. Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 2.0 Max. Inherent Viscosity ABR-10 0.71 - 0.76 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 mmmmm p VAB.0001202252 V PVC BULK TRAILER ANALYSIS Date Customer Technician. Cr\^A- -5 Product Silo___ 177 MOIST Top Bottom :0? CONT. Bottom GEL i FRONT 2. 2. I. I. Trailer Number Time 4-T Order No. BULK DENSITY l .saf DRY TIME l COLOR - *7* -M iI L= vise RVCM MIDDLE 2. i END l l A= B= L= A= B* Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. on Mesh 0.0 o 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 <gms. Resin |plus 1.0 gims. Carb 60 80 100 120 140 200 -3 7.13 JH52 lf.yo .7 )U 35.8 3- j&a. Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 cr in i Glassy Pan Part. 1 * to ^ Glassy Pan Part. Remarks VAB.0001202253 mmm / Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSX S A : 7/2 Z l4Z- Date Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: *7j'ZT^j VIS1AProduct: 5305 Order No. : 00(2-4*43 -DOO Cust. PO No. i 3(- 300*7*4 Trailer No.: Property Moisture, % Test Method ABR-1A Specification 0.3 Max. Analysis .OS Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.0 % On 200 Mesh *NDS % On Pan 5.0 Max. 3. & Specification is 25.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 2.0 Max. 0.71 0.76 .065" .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-8111 FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 mmmmm mmmmmmmmmmm mrnmmmmm mm VAB.0001202254 Date Customer Technician. tsnfrHPi- PVC BULK TRAILER ANALYSIS A Product Silo___ 4*7 Trailer Number 'TZ'31? Time Order DO! 9.4^5-00^ Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. 4k on Mesh V-&Q 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. 4k on Mesh 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. ao 2. //.2f _/Lt3 ?.6>(d o.r is,z r 3Z. 5 /S.z Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 /.2Q 2-4> Glassy Pan Part. Remarks VAB.0001202255 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTI I CAT Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 SIS (<n.Date: ?//& Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 'f/fofaZ' Product: 5305 Order No. : Oust. PO No. : <3 / - 3 Trailer No . : "JZ Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .07- 0-0 n.x 3.1 .o4n .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. A Labor ervisor/Lead ster Saldivar ibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 IPMMMMIP m MMNMMWPPP mmmm IPPMM VAB.0001202256 Date 7 Customer Technician ri /L/, & m. PVC BULK TRAILER ANALYSIS h Product Silo___ '5"3o-/ Trailer Number Time //SXO Order no. Do i-m4*>-oo4 Particle Size Distribution: Screen Analysis------- _____________Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Gross Wt. Tare o r Net Wt. % on Mesh t> . 0.(3 . .3 C.ZS U.L IZlo. li'i. h /C.JC 33.1 111 %2 Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh * 40 60 80 100 120 140 200 - Glassy Pan Part. /S7 3.1 Glassy Pan Part. Remarks % VAB.0001202257 TRANSMISSION CONFIRMATION REPORT No.-001134 DATE/TIME DURATI ON , -.* &?*JUL 20 1992 11:10AM ..... . - - .. . . . ____ 28s ........ TRANSMITTER CFROM) OMNIFAX 0123456709 RECEIUER CTO) 502 778 0603 PAGES XMITTED 01 PAGES ERRORED RESULT OK COMM. MODE G3 RESOLUTION NORMAL r- | VAB.0001202258 55-0000349 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601} 369 81 1 1 A Date: /X Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: /Z ^ Order No.: 00 J $ 3 Oust. PO No.: J Trailer No.: 7^^^ Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis . /j *V7 A0 // +. z- .o4z~ ,73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. boratory Superv r/Lead FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202259 TRANSMISSION CONFIRMATION REPORT No.=001100 DATE/TI ME DURATION JUL 14* 1992 28s 3U9PM TRANSMITTER CFROMD OMNIFAX 0123456789 RECEIUER CTOD PAGES XMITTED PAGES ERRORED RESULT COMM. MODE RESOLUTI ON 502 770 0603 01 OK G3 NORMAL VAB.0001202260 55-0000349 PVC BULK TRAILER ANALYSIS k Date 7-/2 >7 m Customer Product S'3 cS Silo___ i2 Technician mm FRONT MOIST Bottom i * /3 ** 2. CONT. I2P Bottom i t VV* * # * * # /(? GEL I 2. t. i I Trailer Number Time Order No. BULK DENSITY I .S/7 DRY TIME I COLOR L ~??.77 A == acf7 b= /.7J l L= vise RVCM MIDDLE 2. I i ii END A= B= L= A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. a.po H on Mesh 0,0 t Screen Analysts 4' IP Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 h Min On Rotap shaker. 49 igms. Resin f>lus 1.0 g ms. Carb 60 80 100 120 140 200 Glassy Pan Part. /./<P Min. S.z 7 to. SL !o.sn S. 7/ /O.s M.7 3/J s HA On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 H 80 100 120 140 200 a.// V-a Glassy Pan Part. Remarks mm m VAB .0001202251 * Vista Polyman A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date : '7/V( Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: vhfaz. Product: 5305 Order No . : Oo Cust. PO No.: 3f'-30O<f(/ Trailer No. : 3*77 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 * ABGC-26 ABR-10 Analysis .13 * > 0 n. (0 S- */" OIU .75 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory S sor/Lead FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 mRMRMP I T mmmmm T VAB.0001202262 PVC BULK TRAILER ANALYSIS Date Customer ^3l Product k15Silo___ Trailer Number Time 10 to Technician Order No. FRONT MOIST CONT. Too Bottom | Top Bottom I .13 1. r 2. I GEL I 2. I BULK I DENSITY l IK DRY TIME I i i i. i COLOR L = nsi A = I 37 - I, S3 L= vise RVCM 0 MIDDLE 2. I END i A= B= I L= A= B* Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh O.>0 0,eo Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 , Min On Rotap shaker. 49 gms. Resin pthis 1.0 cpms. Carb 60 60 100 120 140 200 Glassy Pan Part. OZ 9 /2.79 0-L JSJ 2S.L 2ll J7.S Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Pari. Remarks VAB.0001202263 Vista Polymers A Division of Vista Chemical Company Highiway t25 Post Office Box 91 FtT I FI CAT Aberdeen, Mississippi 39730 Phone (601) 369-8111 * Date: 7h hx Customer: Nibco, Inc. 2929 W. Mag me Louisville, KY 40201 Attention: Sandy Money Ship Date: VB1AProduct: 5305 Order No . : <50/^5 -OOO Cust. PO No.: 31- 30044- Trailer No.: 'T'- Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .13 .5n o.o /o.o xn .073 J3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed at Laboratory Supervisor/Lead FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202264 PVC BULK TRAILER ANALYSIS A Date Customer Technician V the-* r>\JCi Product Silo___ CSO MOIST Top Bottom l .13 CON'T Top Bottom iy* FRONT 2. l. 1. GEL I Trailer Number Time /WO Order No. r-3&? BULK DENSITY l ,S7/ DRY TIME COLOR L = ff. a-- > vise B= I L* RVCM MIDDLE 2. I. END . 1. I 1 A= B= L= A= B= Particle Size Distribution: Screen Analysis /0 Mesh Size Gross Wt. PTare Net Wt 46 on Mesh Screen Analysis 40 0*0 Mesh Size Gross Wt. Tare Net Wt 46 on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. , OS' J. Min 60 12*00 iCoo jO.OO 431 /.i r S3.1 2^.0 JO* i Zc. c /O, o 2.7 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. Remarks VAB.0001202265 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: ?-S~ Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: VIS1AProduct: 5305 % Order No. : >0/<W3-Oo/ Cust. PO No.: 5/'jOoyy Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis . O3 &<? Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 wmrnmmmmmmmmmmm VAB.0001202266 mm m Date Customer Technician zb PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number. Time /<>// Order No. &$>/ & f Particle Size Distribution: Screen Analysis / P______ Min Mesh Size Gross Wt. Tare Net Wt. H on Mesh Screen Analysis 40 60 go l0 _____________ Min. Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 60 ______ ________ _________ ________ _________ ________ _________ ' On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 100 120 140 200 Glassy Pan Part. 9%<q /3.F) /;Z<~ 7-77 3-Y7 / 7.7 37-S 2%n rsS 4-7 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. Remarks VAB.0001202267 Vista Pblymers A Division of Vista Chemicol Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 h Date: Customer: Nibco, Inc. 2929 W Mag ine Louisville, KY 40201 Attention: Sandy Money Ship Date: VB1AProduct: 5305 Order No.: OOI9S-4-/-0&7 Cust. PO No. : 3/ Trailer No.: r Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ,/3 >-<> G ri 001 J73 Polyvinyl Chloride, Virgin Resin, Not Laboratory Supervisor/Lead FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 M mmmmmmmmmmmmmmmmmmmm mm VAB.0001202268 * Date (r - &L-9Z Customer s?/J>c o Technician o PVC BULK TRAILER ANALYSIS Product Silo___ k72 Trailer Number ov? Time Order Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh a. o o 0tQ Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Q.&o Q<& Min On Rotap shaker. 49 gms. Resin plus 1.0 5|ms. Carb 60 80 100 120 140 200 Glassy Pan Part. .13 I) 09 ts.i/j t/.o S.OO AS 22. a 30.4- lAo f.z /O.o Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 b 80 Pan 100 120 140 200 Glassy Part. o. / J.2Z> 19-91 9. St H 0.3 14.+ 2H- 'l 3o.o ft.le _LS. Remarks V AB .0001202269 TRANSMISSION CONFIRMATION REPORT DATE/TIME t- JUL 1, 1992 *3=571P. M DURATION 28s TRANSMITTER CFROM3 OMNIFAX 0 1 23456789 No,-001033 RECEIUER CTQ} PAGES XMITTED PAGES ERRORED RESULT COMM. MODE RESOLUTION 502 778 0603 01 OK G3 NORMAL h j r* 't Vista Polymers A Division of Vista ChemicaJ Company Highway 25 Rost Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERTIFICATE OE ANALYSIS A Date: (sfz.S-JliL Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: te/zz^faz' Product: 5305 Order No. OOIOQ^-OOCo Oust. PO No.: 3l-Jl%3cP Trailer No.: 'T'3'77 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .i4 0.0 Polyvinyl Chloride, Virgin Resin, Not Labo ory _____________ ipervisor/Lead Ester Saldivar Nibco Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202271 *': d* TRANSMISSION CONFIRMATION REPORT N o .-0 0 1 0 0 ? IaE; CM S) cn 44 CD CD 5> U3 cCrM> cn in cn rvi xn u<_r PJ i^ D- CM a is m e: |mw| j 1-- \ LU 4 CC Q L z a K'*4 V- ce DC ! ) Q ID H -N t/3 z: za C CL CL U_ n USD3 S3 gDr-o- i t6n3 ( I cl ID S3 fe 4 iII----D X QLU aCL gonc ID oX | UID IOD' ai-- if) I1D3 X CL to , IC1DC3 3D if) LU CL vAB.0001202272 PVC BULK TRAILER ANALYSIS k A Date. (, Customer Technician 9Z. Af i i> ML! Mr Product Silo___ US Trailer Number. T-J77 Time Order No 06/6&`J/-CO(s FRONT MOIST | CONT. Top Bottom | Tup | Bottom I , J4- i GEL I. 2. BULK DENSITY I .r.2? DRY TIME I i i. i COLOR L= A = . 0 B = / 74 L= vise RVCM 7^ Qsy MIDDLE 2. I. END I A= B= L= A= B= Particle Size Distribution: Screen Analysis/ O______________ Min Mesh Size 40 60 Gross Wt. _________ ________ Tare ^ Net Wt. H on Mesh _________ __________ a* &Q . <3. a 2- Screen Analysis Min. Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 ______ ________ _________ ________ _________ ________ _________ ________ On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 //. f /Jjo 27.2. ^ 3X7 t.fo /7. / 3.4h> X2 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 100 120 140 200 Glassy Pan Part. A 0 2.^ Glassy Pan Part. Remarks wmmmmmmmm mmmmmm m --VAB.0001202273 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: /A? /?2^ Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: (p/tffaZ, Product: 5305 Order No. : OOlD&^bOOS^ Oust. PO No.: Trailer No. : 'T-~$rJr7 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis Q.O L.Z */3Q -72- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202274 PVC BULK TRAILER ANALYSIS A Date Customer Technician /? ^ ^/CfT Product Silo___ S3^S Trailer Number 3?-? Time / o. vJ Order No OOlOMl FRONT MOIST CO NT. I I BULK Top Buuom Top f Bottom 1 GEL I DENSITY ox A7 II 2. 2. DRY TIME l COLOR L vise = & fl' B = /'? I i Il L= RVCM {10 MIDDLE mmm m m END I ii A= B= L* A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt d>Q J2. % on Mesh Screen Analysis Mesh Size Gross Wt Tare Net Wt H on Mesh 40 Remarks Min On flotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. dZ. fl. 3% / .2? -? SO 3-27 2*2* Un-s ak.s 39. 7 /S&> (e>5 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. VAB.0001202275 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 0>/(b/<jz^ Product: 5305 Order No.: CO/OQ^I-OO^ Cust. PO No. : Trailer No.: 3*7*7 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ./3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. utiy ervisor/Lead FAX To: Ester Saldivar Nibco, Inc. (502) 778-0603 MAIL To: Nibco, Inc. Louis Macakanja 500 Simpson Avenue Elkhart, IN 46515-1167 VAB.0001202276 Date 74-* Customer Technician A/ PVC BULK TRAILER ANALYSIS A Product Silo___ 53or 47* Trailer Number Time Order No. /3c o D0l0%4-)-66f /oa Particle Size Distribution: Screen Analysis to Mesh Size Gross Wt Tare Net Wt % on Mesh Screen Analysis 40 Mesh Size Gross Wt Tare Net Wt % on Mesh Remarks 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. Min. 60 t-t'l HA 14-Zl /*74 7.rr 2,rt Lo\ JSJt ISL*L _ao_ On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Glassy Pan Part. 80 100 120 140 200 VAB.0001202277 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601J 369-8111 A - I \Cl*'"'11 1 1 * XRXGATIE OR ANALYSX S Date: (s? Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: VIS1AProduct: 5305 Order No. : $ > Cust. P0 No. 31 Trailer No.: O p-- Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR- 3 ABGC -26 ABR- 10 Analvsis .si o A SO Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202278 PVC BULK TRAILER ANALYSIS A Date Customer Technician FRONT Product MOIST Top Bottom I CON'T Bottom 1., GEL I 2. 2. Trailer Number Time !7*o Order No. BULK DENSITY I .S'/o DRY TIME I COLOR L= A= vise RVCM l. I MIDDLE 2. Ii END I L= A B= i L= A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt % on Mesh 6.00 0. 0 tp Screen Analysis s* \ V Mesh Size Gross Wt Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 4>'.3/ OCo Min 60 ltS3 7 go L&9- a/U Kr.7 . 3!> (.(*> a On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. Remarks VAB.0001202279 - T' Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A C EE R X R I G A AMA LYSIS :Date 7^ Okh Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date : bluin' VIS1AProduct: 5305 Order No.: Do /0%4/ - OO t Cust. P0 Mo..: 3l-a%34- Trailer No Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis on . /</- o.o ID 32 ML 32^ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. visor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202280 PVC BULK TRAILER ANALYSIS & Date > -s 22 Product O Customer Silo___ Technician FRONT MOIST Top Bottom I 2. CONT. Top Bouam > C GEL l 2. I. I Trailer Number / '3X1 Time '3 Order Nn. 6 > ^ / BULK DENSITY I DRY TIME I COLOR L - V2 vise -JT/4 A= B = I.U I L= Rr> tT(/C>>irir f Jo.o MIDDLE i END i i. A= B= i L= A= B= Particle Size Distribution: Screen Analysis Min On Rotap sitiaker. 49 <gms. Resin iplus 1.0 <jms. Carb Glassy Pan Part. Mesh Size 40 60 80 100 120 140 200 Gross Wt. Tare Net Wt. t % on Mesh />'OQ && 7 <00 / HI i. ft J.99 /- o . 5' A HI J(.0 3.2 i. Screen Analysis Min. On flotap shaker 49 gms. Resin plus 1.0 gms. Carb fc-l Mesh Size Gross Wt. Pan 40 60 80 100 120 140 200 _________ _________ _________ _________ _________ _________ Glassy Part. Tare _________ _________ _________ _________ _________ _________ Net Wt. _________ _________ _________ _________ _________ _________ _________ % on Mesh _________ ___ _ Remarks VAB.0001202281 T H Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 G EE R X R X CA ANA LYSX 3 Date : (.ftfa zu Customer: Nibco, Inc. 2929 W. Magazine Louisville. KY 40201 Attention: Sandy Money Ship Date: Cpji VISIAProduct: 5305 Order No. : 001034/"0O& Cust. PO No.*: 3h Trailer No.: ~T-'33>I Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis , to 0.0 7ft Z.b ov4 ,72- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202282 Date Customer Technician PVC BULK TRAILER ANALYSIS Product &yJ* Silo Trailer Number Time Order No. #C) /08&/ 0C& <> Particle Size Distribution: Screen Analysis /O Mesh Size 40 Gross Wt Tare Net Wt. 0- % on Mesh Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. ^-5c> / o n-o /J.j, 7 ,d qj S&-3 Jin n. 6 3. S'1 ( 31 'P. 8 J. (i Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001202283 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 C EE R I R X O A AN A L_ YS X S Date: h 2- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy, Money Date: VIS1AProduct: 5305 Order No.: Oust. PO No.: St- T railer 0 Property Moisture, % Bulk Density, gm/cc Particle Size, 516 on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A V ABR-3 ABGC-26 ABR-10 Analysis .0& .530 o. 0 3-3 lOCs .'K' Polyviny1 Chloride, Virgin Resin, Not Reprocessed. cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202284 PVC BULK TRAILER ANALYSIS k 291 Customer CO Product 30 S Silo__ Technician. MOIST Top Bottom I CON'T. IlIE Bottom iI k GEL I FRONT 2. I. I Trailer Number. T- 37/ Time. /3W Order QOQQH'73 -067* BULK DENSITY l 'S'bo DRY TIME COLOR L A = 6-31 vise RVCM f/ot+> )Z- II B - 107 L= ID LmI^E 2. END II A= B= I L- A= B Particle Size Distribution: Screen AnalysisMin Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 60 .2 Min. Mesh Size 40 60 Gross Wt. Tare Net Wt. % on Mesh On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 Glassy Pan Part. S', "t# ft.97 1.70 1-27 f.L3 J\.g aw 31;i ilsr tx 3.3 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. Remarks VAB.0001202285 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CER I R I C A Date: s!sl -hz~ Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: AM A L.YS X S VISIAProduct: 5305 Order No. Cust. PO No. T rai ler No. OOoqtfj^oo') 3hSL1300 T- 37/ Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A % ABR-3 ABGC-26 ABR-10 Analvsis dh 0. D S'-7 *f.o .511 7A Polyvinyl Chloride, Virgin Resin, Not Reprocessed. * i sort/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja Ml mmm VAB.0001202286 WlMli mmm PVC BULK TRAILER ANALYSIS h Date Customer Technician FRONT Product Silo___ 22 MOIST CON'T. Top Bottom I Top Bonom !I V'ty GEL I. 2. 2. 1I Trailer Number 371 Time DL IS* Order No. fro?#i BULK DENSITY I DRY TIME COLOR L = <fB^o vise RVCM A = 47 b = /<77 &Yin l L= MIDDLE 2. A= B= l i ii i L= END A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh Lj>0 0.0 ft Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap sihaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. o-fc/ 9J>7 13.91 13.T7 7J3 A.ssr ?oz /i2 if.l .37. f A7.9 s3T.l y. 0 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001202287 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 & C EE R X f= I C A ANA LYS Date: S/is'faz, Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: VK1AProduct: 5305 Order No.: DDOQ^73"0OS~ Cust. P0 No. : s?/-- 3$ 30 O Trailer No Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Anal .0& .3^ o.o 9.o A.O .o/g ,7ft Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor visor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mm mmm VAB.0001202288 mm f PVC BULK TRAILER ANALYSIS Datp S'"IS-9^. Customer Ac a Technician. & Product Silo___ k> 79 MOIST CONT. Top Bottom Bottom 1l GEL 1 Trailer Number Time Order No. OCOWZ-Qt^ BULK DENSITY I DRY TIME I COLOR L= vise RVCM FRONT 2. I 2. I1 A= BL= MIDDLE I END A= B= i i L- A= B- Particle Size Distribution Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt H on Mesh 0-00 JLO Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 ftejA iryvh lie Glassy Pan Part. 12M /6-T/ /039 4So __QiL l/.o 32. Z 9.o Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 /.DO Glassy Pan Part. Remarks VAB.0001202289 Harp /5** ^ Customer /7/6ao Technician. PVC BULK TRAILER ANALYSIS Silo 79 Trailer Number Time S/0* Order No. A Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0 po oo Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 &\DO 0.0 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. O.of 0.2 Min. 60 3. ft/ U.3 JS 30 // 4(a 3.9/ 7.1 2Q. 7 29.2 22.1 //.! On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 /./*/ Glassy Pan Part. <j,e>Z JO.if2. fSjft, ntg 333 > 1 8.0 (2.1 6.7 Remarks VAB.0001202290 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 A CERTI FRIGATE OR ANALYST S Date : A Customer: Nibco, Inc. W. Magazine Louisvilie, KY 40201 Attention: Sandy Money = 5/Ship Date /z. VISIAProduct: 5305 Order No Cust. PO No Trailer No 0009*4-1SrOO <4 3l--15oo ~P 3&/ Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2i A ABR-3 ABGC-26 ABR-10 Analvsis . / ^2. 5Vg o.o /S..5 3.1 . \(ol .7Jk Polyvinyl Chloride, Virgin Resin, Not Reprocessed. rvisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mm m f wmmmm VAB.0001202291 m Date Customer Technician -5P AJfl PVC BULK TRAILER ANALYSIS Product Silo__ Trailer Number Time 1^3O ~~ Order No OOP ^75-00 A Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare Net Wt. 4k on Mesh Screen Analysis 40 0.0 Mesh Size Gross Wt. Tare Net Wt. 4k on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. d.of k-31 Ioffe- fSVo 10-43 &J3 0.1 213. 01.1 tP.3 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001202292 Vista Polymers A Division of Vrsta Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601} 369-8111 A X I CA ANA l_YS X S frkz. Date: S' Customer: Nibco, Inc. 2929 W. Magazine Louisvilie, KY 40201 Attention: Sandy Money Ship Date: VISIAProduct: 5305 Order No.: 00074-73-602' Cust. PO No TraiTer No.: Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis . Of . If 4. % . 73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202293 * Date -7 Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ ^3ojT Trailer Number. Time / . YS Order No. 2^ A Particle Size Distribution: Screen Analysis <o Min On Rotao shaker. 49 ams. Resin olus 1.0 ams. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare YO Net Wt. % on Mesh 0.0 o, o O,o -J&-0 3.73 Jp.of )</.&> f //2L 7-SU J?.3X i.* 2Q1, if.9 tfji? l JS' t ?.2 I Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 Pan 200 Glassy Part. Gross Wt. _________ _________ _________ _________ _________ _________ _________ _________ Tare _________ _________ _________ _________ _________ _________ _________ Net Wt. % on Mesh _________ _________ __________ _________ _________ l-F***-**^_____ _____ Remarks. * .4^107 VAR00017.027.94 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OR ANALYSIS Date : 5// A Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date : t/ffo VIS1AProduct: 5305 Order No.: OOO Oust. PO No.: 3I~<?300 Trai1er No T'3&4 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis , It . 55/ f}. Q *1 ,/>/ , Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: ATT: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ,. Louis Macakanja wmmmm VAB.0001202295 w mm PVC BULK TRAILER ANALYSIS A Date /- 9Z Customer Technician Product Silo___ Trailer Number Time Order No. FRONT MOIST CON'T. I Too Bottom I Top Bottom * GEL II 2. 2. j BULK I DENSITY I I DRY TIME I. COLOR A - a5/ b = /.2S I I I. I I L MIDDLE 2. I i i. i A= B= L- END 2. A= B- vise RVCM y^OoJ Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0.00 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 (ims. Carb 60 80 100 120 140 200 Glassy Pan Part. o./7 0.3 Min. 4*0*7 JOJ On Rotap shaker IS. 2? f?W 3c. f 9//. 4. pc 49 gms. Resin plus 1.0 gins. Carb 60 80 100 120 140 200 2-9 Glassy Pan Part. Remarks. A A :+ A/OT mmmmmmmrnmmmmmmmm mm mmm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CER IFICATE OR AM A L_ YS X S Date: Customer Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: VISIAProduct: 5305 Order No 0000^43-067 Cust. PO No.: Trailer No.: /^ Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis o. o // - 3.ZL oocf Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labo rvisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mrnmmmm mm VAB.0001202297 Date Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number Time lo^ts Order No. A 7 Panicle Size Distribution: Screen Analysis_ Mesh Size 40 Gross Wt. Tare Net Wt. >. OC> % on Mesh __ Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap sibaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. U-So AS3 IOM7 28 ISX 69- <7.2 2^0 ZL7 /t.2 3^ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks 4 Star 207A Revised 1/12/87 VAB.0001202298- Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 G ER~T I R I G AT R OR ANALYSIS Date: /q -y Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: c/^/o~9 7^ VK1AProduct: 5305 Order No. Cust. PO No. Trailer No. 7^391 -OD3 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis . 03 S~f O Q /9 / ^7 0/3 . Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202299 Date. V-fO -?2- Customer /V. A Technician PVC BULK TRAILER ANALYSIS Product Silo___ JT3 o A Trailer Number Time / Q o o Order 3' Particle Size Distribution Screen Analysis L& Mesh Size Gross Wt. PTare Net Wt % on Mesh Screen Analysis 40 >,> On Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 40 gms. Resin plus 1.0 gms. Carto 60 80 100 120 140 200 Glassy Pan Part. i2jO 0.0 Min. 60 J.fU 7-7^ H70 7*53 ^jlT_2x 2g- ml _ .1. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 VAB.0001202300" Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 G EE F? IFI C A E= OR AM A L_YS X S A Date A&ril 7, m Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date:/^pyri ) *7, VISIAProduct: 5305 Order No.: 000@^3-D02,, Cust. P0 No.: 37 Trailer No.: 7^3'?/ Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 15 .527 O. O US -M2. Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Csfyu/y rfa-So^ tif Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202301 PVC BULK TRAILER ANALYSIS ntp 4~~ 7- f __________ Product-ST 1 & ^_______________ Trailer Number / ? / Customer _________ Silo(r"7f Time /J+1" Technician __________. Order No. @GQ A Particle Size Distribution: Screen AnalysisL.Min Mesh Size Gross Wt. Tare N9VeVt% wVftt.i 9k on Mesh Screen Analysis 40 6*0-0 0s O Mesh Size Gross Wt. Tare Net Wt. 9k on Mesh 40 On Rotap shaker. 49 gms. Resin plus 1.0gms. Carb 60 80 100 120 140 200 ,p\ 341 1* ,*to M/l iX* to t*Z S 6*0 itA 2aT. io /l.S~ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. _X^** /r_ #.3 Glassy Pan Part. Remarks________ __ ________ _ \ Star 207A Revised 1/12/87 VAB.0Q01202302- Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CRF?~TXRICATE OR ANALYSTS h Date: -- 3 Customer: Nibco, Inc. 2929 W. Magazine Louisvilie, KY 40201 Attention: Sandy Money Ship Date: VKIAProduct: 5305 Order No.: &00&f Cust. P0 No.: 3i~ &?00? Trailer No. / -77 7 Property Moisture, % Bulk Density, gm/cc Particle Size, 515 on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis , >2 0.0 /*-7 .//& 7A Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202303 PVC BULK TRAILER ANALYSIS A Date Customer Technician Z-9z 0 $Q ^ Product MOIST Top Bottom L.0? CON'T. Top Bottom l~?. GEL I Trailer Number Time ///> Order Nn. 0 BULK DENSITY 1 DRY TIME COLOR -9Uf FRONT 2. I. 2. 2. I 1. I ^ o.z9 B= L= / vise RVCM MIDDLE END A= B= I Il l L- A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. H on Mesh D.0O Q'OO Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap aihaker. 491gms. Resin plus 1.0 \gms. Carto 60 80 100 120 140 200 Glassy Pan Part. O.Q# Q-Z Min. 60 L.9s~ /9 Jtf.9 zS 9.3f 2S-3. ML S.1L /.7 On Rotap shaker 49 gms. Resin plus 1.0 gins. Carfa 80 100 120 140 200 , uz Glassy Pan Part. Remarks Star 207A Revised 1/12/87 A6.0001202304~ Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369*8111 CERT X E I GATE OR ANALYSIS A Date: 3/3/fa Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 3/3/ Hsl- Product: 5305 Order No. : OQOQ3.45-OCO Oust. PO No. : SZ-olrfOO f Trailer No.: Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .05 D .O (p. H 34^ - O^t .'IT-- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ___ '(jUL rvisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202305 naif 3-J7-y2- Customer Technician PVC BULK TRAILER ANALYSIS ft Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. H on Mesh 0. O Screen Analysis Mesh Size Gross Wt. Tars Net Wt. % on Mesh 40 Min On Rotap sitaker. 49 gms. Resin pilus 1.0 g ms. Carb 60 80 100 120 140 200 Glassy Pan Part. 1 j 0,0 Cp 9<?f- 33`f-' (. 7 /5Tf (*,7 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks \ Star 207A Revised 1/12/87 VAB.QQQ12Q23Qir Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIR X CATE OR ANALYSIS A Date: 3/2 7 Customer: Nibco, Inc. 2929 W. Magazine Louisvilie, KY 40201 Attention: Sandy Money Ship Date : 3/^7f?Z- VISIAProduct: 5305 Order No. : Q0 0 73 7*^ Oust. PO No Trailer No.: Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis - OJL . S/2- (p _ & o f yy .t(A Polyviny1 Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanj a VAB.0001202307 PVC BULK TRAILER ANALYSIS Date 3 ~1 ?-<9 Customer /v*' 4 c*o Product Silo___ 35 3 Trailer Number Time off-Sl' Technician // Order FRONT MOIST Top Bottom I CJ 2. CONT. Top Bottom *> i GEL l BULK DENSITY I .'fg? 2. L2*6 DRY TIME I COLOR L =V?./d A = -0-of b~ /.of i L= vise RVCM ftfll 1D Ln E END i A= B= L= A= B Particle Size Distribution: Screen Analysis. Mesh Size Gross Wt. Tare /P Net Wt. % on Mesh Screen Analysis 40 5>-D Mesh Size Gross Wt. Tare Net Wt. % bn Mesh Remarks. 40 Min On Rotap sitaker. 49 gms. Resin plus 1.0 gims. Carb 60 60 100 120 140 200 Glassy Pan Part. .f Min. // On Rotap shaker / r ?z- /dSl? 3/- ? p'- / A?.<? 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Star 207A Revised 1/12/07 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 C EE R T I RIGA Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 AM A L_ YS I S Date Customer: Nibco, Inc. W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: fa 4/2 VIS1AProduct: 5305 Order No.: 0001604- DOG Oust. P0 No. : Trailer No 7-J77 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A % ABR-3 ABGC-26 ABR-10 Analysis 1*7 * ?// Q.Q 3 - 7a Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory rvisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202309 * Date Customer Technician PVC BULK TRAILER ANALYSIS Product_______ t}>i>ilo______ fc ^ Trailer Number Time /Z/0 Order No. Particle Size Distribution: Screen Analysis /o Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 >.0O 0*0 Mash Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. , o7 ./ 6,73 /J.sT /J / M7V g. tf /7.7 <P.J Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 2.+0 Glassy Pan Part. Remarks Star 207A Revised 1 /12/07 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS Date: 3- 3 0 -- i *** Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: J3 -- io VIS1AProduct: 5305 Order No. Cust. PO No. Trailer No. 7 5 ?y, cx>S U>SS Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .n .S3? 0.0 n.s~ 3. S -mi .15 Polyviny1 Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja 4 VAB.0001202311 PVC BULK TRAILER ANALYSIS Date 3~&Q ~&2> Customer Product Silo___ 6> 79 Technician MOIST Top Bottom (/. CON'T. Top Bottom '$5. GEL l Trailer Number Order coontnHr BULK DENSITY 1. DRY TIME I COLOR L vise FRONT 2. i 2. I 1. A = *.// B == .2.3/ L= RVCM %r MIDDLE END i. i i 2. A= B= L* A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt. % on Mesh Pt$* Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh Remarks 40 o-o 6.0 Min On Rotap shaker. 49 ams. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. S.7o 8-2* _ J*.43 //.3f Zf /></ 22-1 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 BO 100 120 140 200 4.tg Glassy Pan Part. If t ?3 1.90 .3 m at,-)&.5~ 2S.W ns 3.8 Star 207A Revised 1/12/87 ~" VAB.0001202312 "1 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CEERTI FICATE OR ANALYSTS h Date: 3/ I 3/?^ Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: gl/g/qZ- Product: 5305 visiA Order No. : OCO '73'?4'-OC 3 Cust. PO No.: Trailer No.: Propertv Moisture, % Bulk Density, gm/cc Particle Size, as on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis .46 0.0 .DU .7Z. Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora Supe sor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202313 PVC BULK TRAILER ANALYSIS Dale. 3 ~/2 - 92 Customer Technician Product Silo__ Trailer Number Time Order No 7 FRONT MOIST CONT. Top Bottom I Top Bottom I .of I 2. GEL i 2 BULK DENSITY l .5/0 DRY TIME I lI COLOR 99'rt A -= 0-2! B = Jko/ L= vise RVCM Wo CcJ 3 MIDDLE I END i i A= B= L= A= B= Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 90 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. H on Mesh 0.0 0 il I XU !(/io iSZ Q -IS 1sL 0.0 ,x_ tCf, | 17.0 S.g 3-* Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 _________ 60 90 _________ _________ 100 _________ 120 140 _________ _________ 200 _________ Pan Glassy Part. Tare _________ _________ ________ _ _________ _________ _________ _________ Net Wt. _________ _________ ___________ ___________ _________ _________ _________ H on Mesh _________ _________ _______ Remarks VAB.0001202314 Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601)369-6111 __V'S I S A Date: Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: Product: 5305 Order No. Cust. P0 No 4 31- 2$7~7j Trailer No.: Propertv Moisture, V. Bulk Density, gm/cc Particle Size, on 40 Mesh 200 Mesh Residua 1 VCM, ppm Inherent Viscosity Test Method ABR--1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana 1ysis . // 0.6)0 /& (o 3-1 M~L- ,?z- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. i Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202315 Date 3-/0 "9^ Customer Af ? oc^o Technician MS PVC BULK TRAILER ANALYSIS Product S* 3 Silo 6 7 ? Trailer Number T"" Time /4>Jo Order No. 007374-62-~ Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare Net Wt. H on Mesh Screen Analysis 40 0<OQ Q~0 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 ____ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. .0t> ,/ Min. 60 S-.Ll? //. 3 2,3.0 /r./? Je. 2/, 3 S'. 32. />.C On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 3.3 Pan Glassy Part. Remarks VAB.0001202316 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF IS A Date: Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date Produc t Order No Cust. PO No Trailer No 3/- 28777 // Propertv Moisture, Bulk Density, gm/cc Particle Size, '/. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR--10 Analysis IS 0.0 3.6 .051 Polyvinyl Chloride, Virgin Resin, Not Rep twit? Supei'visor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202317 Customer Technician PVC BULK TRAILER ANALYSIS A Particle Size Distribution: Screen Analysis Min On Rotap heker. *19 gms. Resin plus 1.0 gims. Carb Glassy Pan Part. Mesh Size 40 60 80 100 120 140 200 Gross Wt. Tare Net Wt. % on Mesh Ojdo o.t) 0-0 <9.t) /0.3C IV. 7f 11.78 4/7-2. 7.40 <?>1 JeO 23.U JlM Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gins. Carto Mesh Size Glassy Pan Part. 40 60 80 100 120 140 200 Gross Wt. _________ _________ _________ _________ _________ _________ _________ _________ Tare _________ _________ _________ _________ _________ _________ _________ NetWl. _________ _________ _________ _________ _________ _________ _________ _________ ____ H on Mesh _________ _________ Remarks a^ f VAB.0001202318 t Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: Q- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: Q _ Q.) - <=9 Product: 5305 Order No . : Crf (Ff , Cust. P0 No.: 3/ Trailer No.: Propertv Moisture, V. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 iz. . stu G'O I a.3 .1,1... Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202319 * Customer PVC BULK TRAILER ANALYSIS Particle Size Distribution Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt % on Mesh S. Screen Analysis l.*> ' Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Remarks Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. Q.tr> Min. 60 <*77 /t-io 1LZ9M32 iI3 16.0 33-1/ 35 1*3 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 3 hi Glassy Pan Part. VAB.0001202320 uriHi m Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERT X X CATE OF ANALYS I S A Date: 2, - / 9 * ^ 2- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 2 Product: 5305 Order No. : 0C 0 / o 9 - &o 4 Cust. P0 No. : Jj - Zm 1 Trailer No.: Propertv Moisture, V. Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO Analysis . /2 . S'JJ JUA____ ,D*>& . 7^ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. oratory Superv<ysor/Lead cc: Nibco, Inc . 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202321 i 4 n.t. Z-/S1ZCustomer N ^ c-^ ...... Technician PVC BULK TRAILER ANALYSIS Product Silo 6X3 Trailer Number T~. 3?_7..... Time Z-o exo Order No. o* 06/c7- c> os~ Particle Size Distribution: Screen Analysis to Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 O' 0*0 0. o Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. .01 . / 7. O IL4Z- / 7.33 // IL 22. i JV. 7 23.3 4,7C /.*/ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001202322 Visto Polymers A Division of Vista Chemical Company Highwoy 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 CERT IFI CATE OF ANALYS X S Date: fU* {QQ l Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: db- H( VIS1AProduct: 5305 Drd No Occ&loQ-ocd Cust. PO No.: 31-2.85*11 Trai1er No //3 Propertv Moisture, */. Bulk Density, gm/cc Particle Size, '/. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ,oe> < \X2st D.O . DOC? ^33 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202323 PVC BULK TRAILER ANALYSIS Date Customer Technician At FRONT Product Silo___ MOIST CONT. Top Bottom I Top Bottom I. oS I/S A3 2. GEL I 2. I I I. Trailer Number T-//J Timgg J V__________________ s. Order No BULK DENSITY I / DRY TIME I COLOR L* A= vise RVCM II B= L= MIDDLE 2. A= B= I. i ii i END A= B= Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh Screen Analysis 40 Mesh Size Gross Wt Tare Net Wt. % on Mesh pu> Remarks 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Garb 60 80 100 120 140 200 Glassy Pan Part. .f Z47 Mm'77 >Z.oK /<ft42/S.r %S L S7 US 9XL AfL S*Q Min. On Rotap shaker 49 gnus. Resin plus 1.0 gms. Carb Pan 60 100 120 140 200 Glassy Part. . d% s'yp /,?. xo 3.an _A loji 27 (* 377, /% 7 3 VAB.0001202324 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X Fr X CATE QF Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 A Date 4 fa Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date : fafa^. VIS1AProduct: 5305 Order No. s 00O(i>IC/1-OO{ Cust. P0 No.: 31-OQ T railer No- !//3 / Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ?/ i 0-0 5.Z I -(o /75 Polyvinyl Chloride, Virgin Resin, Not Reprocessed (laboratory isor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202325 PVC BULK TRAILER ANALYSIS A Date Customer Technician FRONT Product Z2Silo___ MOIST 1st Bottom I of 2. MHMI CONT. Bottom GEL I 2. I II Trailer Number Time Order No. ObOfnlOq-O0 1 BULK DENSITY I ,00 DRY TIME I COLOR L *9F.76 A vise RVCM .57/ II b = <3-/3 L= / wo. 7 MIDDLE A= B 1. i i i i L = END *> 4M1 * 2. i r A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 O.oo Tare Net Wt. Mi on Mesh Q'PO Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gims. Carb eo 80 100 120 140 >J 233 a%/ 3a(, /Y-3 200 Glassy Pan Part. /O O.S'T 6.o7 /4,ez. /7.3o 2.LI /3V ML /7.i L-2. Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 0.7? ___________ Glassy Pan Part. Remarks VAB.0001202326 r**. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 CERTIFICATE OF ANALYSIS Date: Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: /fc/fTJ, Product: 5305 Order No.: QOOG Cust. P0 No . : Trailer No.: / dOQ / Propertv Moisture, V. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Anal vsis , 02. 554 Q.O HO S.Q .O'JP ,7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. rvisor/Lead cc : Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mm mm mmm ffm VAB.0001202327 * Date /- JV- ? Customer * Technician 4L FRONT MIDDLE END PVC BULK tRAILER ANALYSIS A Product SUo___ o4 Trailer Number. 7^37/ Time /a'.trO Order No. 0Q& 2 /^ COLOR L vise RVCM A= * B -_ A ?* L= A= B= L= A = B= Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Te _p Net Wt. H on Mesh Screen Analysis 40 (9^0 on Mesh Size .6Gross Wt Tare Net Wt. 4* on Mesh 40 a>.o Min On Rotap shaker. 40 gms. Resin pius 1.0 gmi. Carto 60 60 100 120 140 200 Glassy Pan Part. os Min. y.fs 1 ZlA iLoi 4 / Lo On Rotap shaker 49 gms. Resin pius 1.0 gms. Carto 60 60 100 120 140 200 .7 /3. 2. f jp.? fo.z. LiH Glassy Pan Part. Remarks VAB.0001202328 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 CERTIFICATE OF ANAI__V' S X S Date: 22, Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Ship Date: 2%. 144Z Product: 5305 Order No.: D0O5/ ~ 0&2 Cust. P0 No.: 31-2^1 (O Trailer No.: j ^ Proper tv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm * Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ,// n. o /S'./ B.D .d6Q> 19s Polyvinyl Chloride, Virgin Resin, Not Rep uf sor/Lead cc : Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202329 e# Date Customer Technician `72- PVC BULK TRAILER ANALYSIS Product 3 OS Trailer Number Time / 3/o Particle Size Distribution: Screen Analysis__ Jo Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carto Mesh Size Gross Wt. 40 60 80 100 120 140 200 Glassy Pan Part. Tare Net Wt. % on Mesh Screen Analysis Mesh Size Gross Wt. Tare Net Wt. OiQO 0*0 0, / ____ Min. t. 9r E-Z(* IL.ol !4'U 7.!>> 3 . *7 U.& 32-1 -29,3 15-1 On Rotap shaker 49 gms. Resin plus 1.0 gms, . Carb ___________ 60 0-0 80 IS 100 u.g 120 140 200 Zi-'t //* /*? ^. o Glassy Pan Part. 2. yC % on Mesh Remarks VAB.0001202330 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A CERTIFICATE OF ANALYSIS Dates //z.//?2* Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Date of Shipment: ilzihz- VISIA Product: 5305 Order No.: 00OS/4-Z-~CGCo ailer No.: /--VZ'S Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABSC-26 ABR-10 Analysis .12.__ .55% o.o Z .L .oon n\ cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202331 PVC BULK TRAILER ANALYSIS Date Customer fa AJ/A Product Silo___ Technicia FRONT MOIST m Top Bottom '.{S> * I * * * 2. CON'T. ISB. Bottom # ij a GEL I 2. I. I Trailer Number rune Order BULK DENSITY I DRY TIME I COLOR L= . A = *17 B= II L= MIDDLE I. I l I END A= B* L= A= B= A vise RVCM J Particle Size Distribution: Screen Analysis Mesh Size 40 Min On Rotap sitaker. 49 <gms. Resin pilus 1.0 gims. Carto 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. 1 I Tare Net Wt. H on Mesh 0A 0.09 3.70 0* 0 0.2 7/ /QOO C-7/ 11/ Zt-2 12.4 9.9 Screen Analysis Min. On Rotap shaker 49 gms. Resin plus Mesh Size Gross Wt. 100 120 1.0 gms. Carto Pan 140 200 Glassy Part. Tare Net Wt. % on Mash C- //?& &.*7 L*A &tJ zo* as.f fcS IL/a Remarks VAB.0001202332 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-6111 CERTIFICATE OF ANALYSIS A Date: /Vj Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Date of Shipment: 3U. . /( /W VIS1A Product: 5305 Order No.: 0005lLPz-Go4 Trailer No.: Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh . 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO Analvsis .o4 .sn 0-00 12-4 b3 .o/y 73 Labor __ lU sor/Lead cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mMmpai PH* W VAB.0001202333 m A 0 PVC BULK TRAILER ANALYSIS Date/ - / ^ ________ Product______ ^ ^________ Trailer Number Customer A/ < ^ _______ Silo^ ^-3 Time / Technkian__^L^_______________ _______________________ Order No. 7 _______ ^^ ^ ^OOt Particlc Size Distribution: Screen Analysis________ UL______ Min On Rotsp shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 0.00 0.0 60 80 100 120 140 200 .o'? ./ Min. 3.3 0 fl.1V U* /%r __________ IZ.4 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 60 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. AS Glassy Pan Part. * Remarks. VAB.00012Q2334 Vista Polymers A Division of Vista Chemical Compony Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTIFICATE OF ANALYSIS A Date: /-- Customer: Nibco, Inc. 2929 W. Mag a z i ne Louisville, KY 40201 Attention: Sandy Money Date of Shipment: /" i0 - VISIA Product: 5305 Order No.: D0O5l4z-O63 Trailer No.: Propertv Moisture, '/. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis * /tT~ .S/fr p.o 3. ^ /-Y ,008 .n$ Super or/Lead r A cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja wtmmm mmmmmm mm VAB.0001202335 4. PVC BULK TRAILER ANALYSIS & Date /0-&Z Customer Product Silo FRONT MOIST liJE Bottom l ,/jf. 2. CONT. Tj Bottom 1/' Pzi GEL I. 2. I. t I Trailer Number y/r _____ Time //3o Order No.. OOObl<4'l-OD2r BULK DENSITY I DRY TIME I. COLOR l * <93% vise RVCM .slL Il a = Q'3T b = a.a-f L= uJ fs.7 MIDDLE 2. l END A= B= I. I I l L = A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh Q.OO Q *0 Screen Analysis Mesh Size Grots Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin pthis 1.0 grns. Carb 60 80 100 120 140 200 Glassy Pan Part. .Hr .3 Min. 60 *J* jL ism C 3 ^ l H Itl 32.V 311 123* --*- -f-- On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 m w PM VAB.0001202336 Vista Polymers A Division of Visto Chemical Company Highway 25 i Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601} 369-8111 CERTIFICATE OF ANALYSIS A Date: /khz- Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Date of Shipment VISlA Product: 5305 Order No.: Trailer No.: / Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO Analysis ,03 .576 d.qQ 4.1 IS .DM .13 Labo sor/Lead t cc: Nibco, Inc. 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja mmm p VAB.0001202337 * PVC BULK TRAILER ANALYSIS A Dale /-J Customer Technician U Product a/ * y Silo A4 9^/-re <S> MOIST CONT. Top Bottom | Top Botlom l1-3 GEL i. FRONT 2. c 2. i i i. /Trailer Number. Time /X?J order Pol BULK DENSITY I SlP DRY TIME I i COLOR vise =L 2- a = a* sz 8 = /.?/ L= /*/ RVCM MIDDLE 2. i END A= ii i B= LA= B= Particle Size Distribution Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt H on Mesh O,O t Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. LAI Min. 60 1.6 A /4.U }L.tA $Jo 2. AS LH'Q J/J /LA. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 6.73 LA Glassy Pan Part. Remarks Star 207A Revised 1/12/87 "M8MIMM @233$ Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F I CATE OF ANALYS I S Date: 2, Customer: Nibco, Inc. 2929 W. Magazine Louisville, KY 40201 Attention: Sandy Money Date of Shipment: Z, VTSJIA Product: 5305 Order No.: OOOSl<4%, Trailer No.: 7^* Propertv Moisture, '/. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis ,0& .3b n.oo o.o /f .00^ .06 cc: Nibco, Inc . 500 Simpson Avenue Elkhart, IN 46515-1167 ATT: Louis Macakanja VAB.0001202339 PVC BULK TRAILER ANALYSIS Date / ( Product K* Customer Silo___ Technician FRONT MOIST CONT. Top I* 8 2. Bottom I Top i 7 Bottom GEL I Trailer Time Order BULK DENSITY 1 DRY TIME I COLOR I MIDDLE I. I END 1I L= A= B= A RVCM Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. TTare O Net Wt. >**P__ % on Mesh 0s * Screen Analysts Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On flotap sttaker. 49 <9ms. Resin |plus 1.0 gmis. Card 60 80 100 120 140 200 Glassy Pan Part. 6.1 0*4 Min. 60 3-Uy.2r /j .// /7.I? tb.i9 J. <r As'.v 3sr.i 7-1 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carto 80 100 120 140 200 fiJA JJl. Glassy Pan Part. t Remarks Star 207A Revisad 1 /12/87 .... 1 w^wiwais----iswwph--i----wsMw--wdmiw^^ii i ................ . ................ .....>wwaMi*iiMMni^iiHa8MnMnnMnivvnHiniiMi