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r% 01 CODE YE-698-D Mjjm 7 PATE 7 L2H24 5527* LBS. 7"l o t > ( EST WT ) nL ( PROCESSES ) YE-698-D (T) APFi&V^D BY: FWP f/i5/82 A COMTYP JOB NAME: 1YE698DMT iLENDED CG 1, PC QUNDSJ EQUIP i MENT | NAME: MOLYBDATE ORANGE PREP 1 lJ<a^0TSTAIN SODIUM SULFATE FOR S-13 l<Sr'l CALCULATE 6 SET ON BADGER METER FOR.Sjl 6 | i (NITRIC ACID WEAK) -J&ikgSL % I 3 ! OBTAIN SODIUM CHLORIDE FOR S-33 I 4>T OBTAIN. SODA ASH FOR S-37 I 5 J>pTAIN SODIUM SILICATE FOR S-39 ` I 6M/0BTAIN SODA ASH FOR S-43 I It/] OBTAIN ANTIMONY TRIOXIDE FOR S-46 1 usi 7 \ ACCT 1 LBS | N-CODE 1 LBS .j -j | 1 84 j 1 08-A I . 84 iJTJ 33-D 1 i 41 > t i 4-A i 734 1 146 | 3-A 146 1 237 | 32-D 23? 1 35 | 3-A 35 I 7 | 711 -B 7 331 I WEIGH SODIUM CHROMATE INTO V-351. j 1 -D 1885 o OPTR 3ZO-, MK____, % II OPTR _____ , MK 'Ji ii 359 jJ^I WEIGH IN SODIUM MOLYBDATE SOLUTION 3II II OPTR OPTR MK 4_, T~S4$L,vS4 MK ;, T-__________, i i 423-D 303 358 <UN 1* (500 G) WATER INTO V-358 |>rn^RUN V-359 INTO V-351 & PUMP IN V-351 M-Jfj. ADJ TO 55* (260 G) Itrt^SIFT IN N-1G8-A FROM S 1 IHT I SJIR 5 MIN & RECORD : PH_ Adi(9.0-1 .) |ll^HSl)J t o PH 9.8-9.9 & RECORD: PHf^L- !' l (CAUSTIC SODA SOLUTION) ASSUME 5% I . ASSUME 66'/. tJ^L^ADD N-33-D FROM S 2 USING BADGER METER 4*T\ ADJ TO 6'6" (3121 G) AT 67-69*F RECORD: VOlZA-- * 6 Jfe2LF 18 I STIR 5 MIN 6 RECORD: PHJL^ (7.4-7.6) h. I G/ML (1.08-1.83 > I NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK 1 LIST 6 ATTACH. TAKE 1 QT SAMPLE i?T RUN 2* (996 G) WATER INTO V-_ SV 5 RECORD N-41-D STORAGE TANK TO PUMP FROM. CIRCLE ONE: 42 41 411 42 424 425 CHECK WITH CU SUPV: ^STORAGE TANK MUST CONTAIN AT LEAST 2376 GAL: 402-49*, 410-25*, 411=48*, 420=25 *, 424=25*, 425=31* ^STORAGE TANK MUST HAVE STIRRED AT LEAST 2 MIN SINCE LAST ADDITION OR ADJUSTMENT STORAGE TANK MUST BE ISOLATED UNTIL ALL PUMPING FOR THIS BATCH IS COMPLEJE | SET METER FOR 30 G 6 PUMP TO SV 7-D 3 3-D NOV 5 1982 N40884 LOT :* EQUIP KENT I SV 122 3I CONT i I i 123 124 GOMTYF JOB NAME: 01YE698DMT PAGE 02 DATE PR IN TED : 10/1 5.'32 I USE | N~ IACCT LBS CODE LBS AT APPROX 10O G WHILE CONTINUING TO PUMP, CHECK PH 6 DENSITY * RECORD BELOW. IF NOT IN RANGE, STOP PUMPING & SEE SUPV. * PH:___ <2.2-3.7) * DENSITY: _______ G/ML (1 .270-1.328) IF S-22 OK & WHEN S-21 COMPLETE, RECORD DENSITY G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING. USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21. CIRCLE DENSITY 6 SETTING IN TABLE BELOW. * TABLE #*** G/ML 1.270 1.271 1.272 1.273 1.274 1.275 1 .276 1.277 1 .278 1.279 1 .280 1 .281 1 .282 1.283 1.284 1.285 1 .286 1 .286 1 1 .287 1 .288 1 .289 1.290 SETTING 1 G/ML SETTING | G/ML 1678 1 1.291 1534 | 1 .312 1670 1 1.292 1527 | 1 .313 1663 I 1.293 1521 | 1 .314 1656 I 1.294 1515 | 1 .315 1649 1 1.295 1509 I 1 .316 1641 1 1.296 1503 | 1 .317 1634 1 1.297 1497 | 1 .313 1 627 1 1.298 1490 | 1 .319 1620 I 1.299 . 1484 | 1 .320 1614 1 1.300 1478 | 1 .321 1 607 1 1.301 1473 | 1 .322 1600 1 1.302 1467 1 1 .323 1593 1 1.303 1461 | 1 .324 1 586 I 1.304 1455 | 1.325 1580 1 1.305 1449 | 1 .326 1573 I 1.306 1444 | 1 .327 1566 1 1.307 1438 | 1 .328 1 566 1 1.307 1438 | 1 .328 1559 1 1.308 1432 I 1.329 1553 1 1.309 1427 | 1 .330 1546 1 1.310 1421 | 1 .331 1540 t 1.311 1415 1 1 .332 SETTING 1410 1404 1399 1394 1388 1383 1378 1 372 1 367 1 362 1 357 1351 1 346 1341 1 336 1331 1326 1326 1543 1 537 1532 1526 i 25 I 26 1271 1281 1i II 1291 II 1301 SET METER 6 PUMP _______G (RECORD FROM TABLE) FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 30 SECONDS ADJ LEAD NITRATE TO 76' (3625 G) AT 67-69WF. RECORD: __________F STIR 5 MIN 6 RECORD PH:____ _ (2.2-3.7) IF NECESSARY ADJ TO PH 3.0-3.i ASSUME 66% 6 RECORD PH: ______ ASSUME 50% NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING RECORD: _______ G/ML (1.143-1.144) IF OUT OF SPEC FILL OUT CHECK LIST & ATTACH. STIR AT 67-69*F FOR S-31. TAKE 1 QT SAMPLE. 41-D | 5110 57-A t____ 33-D |______ 7-0 I______ > \ jm. DUP050059686 CQMTYP JOB NAME: 01YE698DMT PAGE 02 . - -t 'c - ; :bu . APPROX 1001G WHILE CONTINUING TO PUMP, 'CHECK PH &/DENSITY. RECORD "BELOW * IF NOT IN RANGT, 'STOP PUMPING6SEE SUPV.* I LBS I CODE I LBS DENSITY': :%2&2L . G/ML (1^270-1^328) IF S-22 OK & WHEN S-21 COMPLETE, RECORD SITY Jj 3.2J? G/ML ON TRAPPED SAMPLE ROM END OF S-21 PUMPING* USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW* NOTE: TABLE ACCOUNTS FOR 3O0 G ALREADY PUMPED IN S--21 * CIRCLE DENSITY 6 SETTING IN TABLE BELOW* ** TABLE ***# I G/ML 1 1*270 1 1*271 f 1.272 i 1.273 1 1.274 1 1*275 i 1 .276 I 1*277 1 1,276 I 1.279 I 1 * 28 .1 1*281 1 1.282 I 1-283 I 1.284 1 1*285 1 1-286 i 1*287 i 1*288 1 1*289 1 ITT? SETTING l G/ML SETTING 1 G/ML 1 644 I 1.291 1504 i 1*312 1637 : 1 1*292 1487 1 1*313 1630 | 1-293 1491 1 1*314 1623 i 1*294 1485 1 1-315 1616 I 1.295 1479 1 1*316 1609 1 1.296 1473 1 1*317 1602 1 1*297 1467 1 1 .318 1 595 i 1*298 1461 1 1*319 1 588 [ 1*299 1455 1 1.320 1 582 1 1*300 1443 I 1*321 1 575 1568 fJ-aSLL- 1 1-322 1Cl*302 1 438} 1 1*323 1562 I 1*303 1432 1 1*324 1555 1 1-304 1426 i 1*325 1549 1 1.305 1420 1 1.326 1542 I 1*306 1416 1 1*327 1535 1 1*307 1410 I 1.328 1528 ' -...i 1*308 1 404 1 1*329 1522 r -1 *309 1399 I i-330 1515 ! 1*310 1393 1 1*331 1510 I 1.311 1387 I 1*332 SETTING! 1382 1376 1 371 1367 1361 1356 1351 1345 1 340 1335 1330 1324 1319 1315 1310 1305 1 300 1295 1 290 1285 1 280 I .SET METER & PUMP /4fg&C (RECORD FROM TABLE) FLUSH.LINE WITH WATER INTO SV FOR APPROXIMATELY ICONDS ADJ LEAD NITRATE TO 3625 G (76"-242/245 & 74*5 247) AT 6T-69*F 41-D ! 5110 ECORD:___.feL_*F 6 ICE CONSUMED (330S7BLOCK) STIR 5 MIN & ^RECORD PH: 2er*JO? (2 *2-3 *7) 33X= -5-A- ** USE TITRIMETER TO ADJUST N-41-B PH *** IF NECESSARY ADJ, TO PH 3.0-3*1 'RECORD PH: 3^y~ ASSUME 66% ,,^__l 33--D |______ ASSUME 50% .Jfcflj 7--D I 3TE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING RECORD: A/M.y~ G/ML (1 *143-1 *144) IF OUT OF SPEC TILL OUT CHECK LIST 6 ATTACH* I STIR AT 67-69KF FOR S-31. TAKE 1 QT SAMPLE. DUP050059687 LOT:. ssajjAi MENT SV~" CONT CQMTYP JOB NAME: GiYE698DMT PAGE 03 DA TE PRINTED: 10/J5/82 USE I N- ACCT LBS I CODE LBS OBTAIN 1 ST SAMPLES OF S-18 & S-30 SOLUTIONS 6 TITRATE TWICE NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE 7*1-7.4 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN 0,10 ML N-10-D (IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS), DO NOT PROCEED IF N-10-D TITRATION IS OUT OF RANGE l> '' ADJUST V-358 FOR A TITRATION PH OF 2*4^ 2f#Y FROM FINAL IN-LINE TITRATION, RECORD LOWEST PH f ML N-10-D jtP ~ 0[t, ,firr-- 0^ ti&zr'iA 33-D 7-D WHEN S-31 TITRATION OK , STRIKE? V-358 THRU SV I BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN 6 I 16-18 MIN ^ I RECORD: START O TOTAL MIN_,,Jl 1____ ! NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS ___l 6 BUBBLES APPEAR IN SIGHT GLASSES 33 I IMMEDIATELY DUMP IN N-4-A FROM S 3 6 SET TIMER U<1 FOR 15 MINUTES ^ DURING S 33, WASH IN V-358 I STIR 2 MIN & RECORD PH_1 .8-2.5) fBXS,__^__(MUST BE + ) re 1 STIR TOTAL OF 15 MIN FROM S-33 & RECORD: TEMP_?/___wF <67-73#F) DUMP N-3-A FROM S-4 STIR 3 MIN POUR IN N-32-D FROM S-5 STIR 2 MIN RUN IN LIQUID ALUM USING BADGER METER , STIR 3 MIN & FLUSH ALUM LINE WITH WATER AS'-j^DUMP IN N-3 FROM S-6 44PH STIR 4 MIN FOR S-48 Lr?t RUN IN HYDROCHLORIC ACID USING WEIGHT & BLOW . 390 | | CONTROL PANEL MK_3~, MK ___ _____ % 6 | DURING S-44 SIFT N-711-B FROM S-7 INTO V-390 L- WITH AGITATOR ON IN 1-2 MIN IJ>tr\ STIR 1-2 MIN TO MILKY SOLUTION 734 I 115-D i I 367 XML! 28-D .1 28-D I 105 SV WHEN S--44 COMPLETE, IMMEDIATELY RUN IN N-711-B 8 | SOLUTION GRADUALLY OVER 5,MIN PERIOD INTO SV I WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP W . UNTIL FOAM SUBSIDES. i#<Ki)UMP IN BLANC FIXE N 5<r i WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON I yrOP'OF PAGE 1 - RECORD : CODE_____LOT_________________ _________* STIR 20 MIN r Re c o r d . p h __JL_ (5,8-6.0 > IF NECESSARY, ADJ TO PH 5.8-6.0 ASSUME 50% 6 RECORD: PH-__ ASSUME 66% FLOOD TO 153" <7298 G) 6 STOP AGITATOR 330 | 128-A 330 I I _____ .1 7-D _>3_. 33-D START FINISH OPTR ISS Z~2fl7LA DUP050059688