Document dpnJVkyEy472gD4RBJ3zzgZ6

4448* LBS. < EST WT > PROCESSES < ) YE-721--D <M> APPROVED BY: FWP 11/08/82 COMTYP JOB NAME: 01YE721DMM <CODE) <LOT) <POUNDS) EQUIP MENT PREP 1 351 7 Am & Vv'j yCi i\ NAME: MOLYBDATE OBTAIN FOR S-12 OBTAIN FOR S-34 OBTAIN FOR S-38 OBTAIN FOR S-40 OBTAIN FOR S--44 OBTAIN FOR S-47 1 RED -----......--1| /\/oT-~---- --A, I 1 1 ^| Sa JL- 1 USE LBS 68 600 120 195 61 WEIGH IN: OPTR >*Z_, MtfMTjf T-ljjk, ^^7, OPTR 33.2., MK T- .___% i I ACCT 1 N-CODE 1------- ------ | LBS 1 108-A I 63 1 4-A 1 600 1 3-A | 120 1 32-D 1 195 1 3-A 1 1 711-BD 1 61 10-D 1509 359 WEIGH IN: OPTR____ , MK , T~24.?-, 32*?J_% 3 OPTR___ MK _______ , T- ...,____,,,,% 423-D 243 358 N 10* <500 G) WATER INTO V-358 4 RUN V-359 INTO V-351 & PUMP IN V-351 ADJ TO 55* <2600 G) SIFT IN N-108-A FROM S 1 TIR 5 MIN 6 RECORD: PH__fc51^<9.0-10.0) ADJ TO PH 9.8-9.9 & RECORD: PH____ _ ASSUME 50% ASSUME 66% RUN INTO V-351 FROM BADGER MEIER . OPTR___________ MK_______, ZUL&hkX Jjkk 28-D IMP FROM V-351 TO V-358 ' FLUSH V-351 6 PUMPING LINES WITH 1000G # JATER INTO V-358 ADJ TO 74* <3530 G) AT 67-69*F RECORD: VGL_l_* 6 _,,Al*F 1 STIR 5 MIN 6 RECORD: PHJ&*T?.2-7.4) 6 I G/ML 1.055-1 .058) I NOTE IF G/ML OUT OF LIMITS FILL CW CHECK I LIST & ATTACH. TAKE 1 QT SAMPLE. SV I RUN 20* <996 G) WATER INTO V-_iL^gl_ 5 RE|^PHB-N-44^D STORAGE TANK TO PUMP FROM. I (Cir c l e o n e_i>402 410 411 420 424 425 'h eBK W"iL CU SUPV: *STQRAGE TANK MUST CONTAIN AT LEAST 1900 GAL: 402-39*, 410=20", 411=38", 420=20", 424=20*, 425=25" *STORAGE TANK MUST HAVE STIRRED AT LEAST 20 MIN SINCE LAST ADDITION OR ADJUSTMENT *STQRAGE TANK MUST BE ISOLATED UNTIL ALL PUMPING FOR THIS BATCH IS COMPLETE |2f | SET METER FOR 300 G 6 PUMP TO SV LOT:____ EQUIP MENT [ | COMTYP JOB NAME: 01YE721DMM PAGE 02 BATE PRINTED:11/08/82 USE N~ ACCT LBS CODE LBS AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH 6 DENSITY* RECORD BELOW* IF NOT IN RANGE, STOP PUMPING & SEE SUPV. * PH :_*#. (2*2-3*7) DENSITY: G/ML (1 *270-1 *328) IF S-23 OK & WHEN S-22 COMPLETE, RECORD DENSITY /JLtJZ G/ML ON TRAPPED SAMPLE ?0M END OF S-22 PUMPING* USING DENSITY FROM S-24, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-22. CIRCLE DENSITY 6 SETTING IN TABLE BELOW* *#** TABLE ***# G/ML 1.270 1.271 1 *272 1.273 11 1.274 1 1 .275 1 1.276 1 1 *277 1 1.278 1 1.279 1 1.280 1 1.281 1 1.282 1 1.283 1 1.284 1 1.285 1 1.286 1 1 .287 1 1 .288 1 1.289 1 1.290 SETTING 1 G/ML 1259 1 1.291 1253 1 1.292 1248 1 1 ,293 1242 1 1.294 1236 1 1 *295 1 231 1 1,296 1225 1 1 .297 1219 1 1.298 1214 1 1 .299 1208 1 1.300 1203 1 1 .301 1198 1 1 .302 1193 1 1.303 1187 1 1 .304 1182 r 1 .305 1177 i 1.306 1171 i 1 1307 1166 i 1 *308 1161 i 1 .309 1155 i 1 .310 1151 i 1 .311 SETTING 1 G/ML SETTING 1146 1 1.312 1049 1141 ! 1.313 1045 1136 1 1.314 1040 1131 1 1.315 1036 1126 1 1.316 1032 1121 1 1.317 1027 1116 1 1.318 1023 1112 1 1.319 1019 1107 1 1.320 1015 1103 1 1.321 1010 1 098 1 1.322 1006 1094 1 1.323 1003 1089 1 1.324 999 1084 1080 1076 1 1.325 995 -9-21. 101^27 TT987J 1070 I 1.328 983 1066 1 1.329 979 1061 1 1.330 975 1057 1 1.331 971 1053 1 1.332 967 J#t*TsET METER 6 PUMP JL7__& (RECORD FROM TABLE) ` FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 30 SECONDS ADJ LEAD NITRATE TO 3244 G (68'-242/245 6 66.5* 247) AT 67-69*F I___ RECORD: *F & ICE CONSUMED (3304/BLOCK) STIR 5 MIN 6 RECORD PH: (2*2-3.7) 330X_*_ I USE TITRIMETER TO ADJUST N-41-D PH *#* L*T IF NECESSARY ADJ TO PH 3*0-3.1 ASSUME 66% T 6 RECORD PH: ASSUME 50% I J^NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING pSO RECORD: b3&J G/ML (1.128-1.129) IF OUT OF SPEC \^A FILL OUT CHECK LIST 6 ATTACH* mi STIR AT 67-69*F FOR S-33* TAKE 1 QT SAMPLE. 41 -D 57-A 33-D 7-D 4094 DUP050059753 t.v^PS& LOT= MENU ,, | _ COMTYP JOB NAME: 01YE721DMM PAGE 03 DATE PRINTED:11/08/82 USE N- | USE LBS CODE I LBS SV 5I CONTI OBTAIN i QT SAMPLES OF S-19 t, S-31 SOLUTIONS 6 TITRATE TWICE NOTIFY SUpV IF ML N-IO-D IS NOT IN RANGE 9.5-9*9 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN 0*10 ML N-10-D (IF YES, FLUSH ALL EQUIPMENT 6 REPEAT TITRATIONS). DO NOT PROCEED IF N-10-D TITRATION IS OUT OF RANGE ADJUST V-35S FOR A TITRATION PH OF FROM FINAL IN-LINE TITRATION, RECORD LOWEST PH ZP4- & ML N-IO-D 4VgHjQXLO /.fo-p'Qd | | | | 1 | I lI^SCsT 1 "svr^jjsr WHEN S-32 TITRATION OK, STRIKE V-358 THRU BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN 44-46 MIN | RECORD: START TOTAL MIN I NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS U 6 BUBBLES APPEAR IN SIGHT GLASSES 34j IMMEDIATELY DUMP IN N-4-A FROM S 2 & SET TIMER FOR 15 MINUTES 3DURING S 34, WASH IN V-358^ | STIR 2 MIN & RECORD PH J_\_%,,(1 .7-1 .8) j.-- pBxs,__drr_(MusT b e + ) 571 STIR TOTAL OF 15 MIN_FR0M S-34 6 RECORD: TEMP<67-73F> DUMP N-3-A FROM S-3 STIR 3 MIN POUR IN N-32-D FROM S-4 STIR 2 MIN I RUN IN LIQUID ALUM USING BADGER METER I STIR 3 MIN 6 FLUSH ALUM LINE WITH WATER DUMP IN N-3 FROM S-5 STIR 4 MIN FOR S-49 604 33-D 7-D 11 5-D /4T1 302 RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOUL . CONTROL PANEL MK ___ _ 4-51. MK _______ ____ LJ7, | DURING S-45 SIFT N-711-B FROM S-6 INTO V-390 WITH AGITATOR ON IN 1-2 MIN nriR 1-2 MIN TO MILKY SOLUTION 28-D 28-D 6. / WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP UNTIL FOAM SUBSIDES. X DUMP IN BLANC FIXE N ] 275 128-A WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON I TOP OF PAGE 1 ' RECORD: CODE ..mZT, LOT STIR 20 MIN.-- 4 .^RECORD: PH_Jj ,,'JL .(5.8-6.0) IF NECESSARY, ADJ TO PH 5.8-6.0 ASSUME 50% 6 RECORD: PH-___ tnASSUME 66% 7-D 33-D IS*'' FLOOD TO 153* <7298 G) 6 STOP AGITATOR 275 START I I ____ i\ DUP050059754