Document dnpgMk9Lb2d5vD1dEo1mwyan0
A R f t S -0331
ACUTE TOXICITY TO FISH
TEST SUBSTANCE
Identity:
N-Ethylperfluorooctanesulfonamide; may also be referred to as U1464, EtFOSA, EtPOSA, F-6309, or FX-12. (1Octanesulfonamide, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-N-ethyl-, CAS #4151-50-2)
Remarks: Material is a white solid, lot 505 (cc842-3, F6309, L-1089). Sample purity was not recorded.
The following summary is abbreviated due to the fact that this study has been superceded by a more recent test.
M E T H O D ________________________________________________________
Method: Not provided Type: Acute static GLP: No Year completed: 1984 Species: Pimephales promelas
RESULTS____________________________________________________
96-hour LC50: 34 (27-44) mg/L (Probit analysis)
DATA QUALITY__________________________________________________
* Reliability: Klimisch ranking = 3. This study was tested in excess of solubility (individual weights above solubility limits) and actual concentrations were not measured. Results were based on nominal concentrations. Additionally, sample purity was not adequately characterized.
REFERENCES__________________________________________________
This study was conducted by the 3M Company, Environmental Laboratory, 1984.
O T H E R _________________________________________________________
Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133
Last changed: 5/16/00
006058
BEST COPY AVAILABLE
ENVIRONMENTAL LABORATORY CHEMICAL ENVIRONMENTAL EFFECTS EVALUATION
TOXICITY TEST SUMMARY REPORT
Chemical Tested-F -X L ? I ^ 5 ^BC5o/IC5o/GR5o w ~ =
5 ) Teat Type.;
}
C
Test Speciesi P ^ n J F A h M /fC K b u r * ,.
7 i< .\
Test Date:.
L.R. :___ ,^
Analyst(sTT ~ ______________________
(Exposure/Test Conditions)
Exposure Type:
Static y / t 4 & 7 Static Recirculatory Diluent:
Static/Continuous Orbital Shaking
Static Renewal
Flow-Through
Aerated Well Water (Initial D.O, f, Z jn g /1 1 pH f i , 2 j 1 Temp.
C( / ^ F ) )
Water Hardness: L * * //! ppm Hardness Classification: ^ W tM
J
Dissolved Oxygen % Saturation:
Control(s)
Lowest Experimental Dose 15 Highest Experimental Dose ^
48-hr
W W
PZ)
96-hr
P. 'IP
Extended Exposure
pH Levels:
48-hr
96-hr
Extended Exposure
Control(s) Lowest Experimental Dose Highest Experimental Dose
o ff
.I fl.L 8.1
@)\1 8 lL
Test Temperature C (F):
48-hr
96-hr
Extended Exposure
scan . c < j 0 0 6 0 5 9
Photoperiod: Sixteen hours light with a 15-30 minute transition period.
ENVIRONMENTAL LABORATORY .AQUATIC TOXICITY DATA SHEET DEFINITIVE (FULL-SCALE TEST)
rx ^ tfy Z.
TYPE TEST
*5 *1 0 7 7 ^ s
MATERIAL TESTED A T
x n -,< W C f r / W ? tS)
TEST ORGANISM te frU & S W ty f/A r tT M ?
BEST CO
X -/O X 9
PEST RUNS
2 4 HOURS
RUN
1
REPLICATE
COMBINED LCgo's
?EST RUNS 24 HOURS RUN
\
LC50's (95% CONFIDENCE LIMITS)
* PROBIT ANALYSIS
4 8 HOURS
r
72 HOURS
96 HOURS .
vZ w
(k .4 ' -- 4 4 ) Z t jM li/f'
C z ^ -s s ) ;
( z .1 - ^ 4 )
MOVING AVERAGE ANGLE METHOD
48 HOURS
72 HOURS 96 HOURS
.COMMENTS
REPLICATE
COMBINED i LC3o 's
( /S - 4 9 )
fx 4 ~ 4 4 )
006060
ENVIRONMENTAL LABORATORY D t C T r n p v JKHJIII ADI rAQUATic t o x i c i t y d a t a s h e e t
" W l u u r i AVAILADIX,d e f i n i t i v e (f u l l -s c a l e t e s t )
lr ~7F>/ZZ21
'p Test-y^ 4 ^ y h r r c '^ /W ' * * a te r ia l st Qcganism^^^ /i/f //V M ,^ ) Source ^ p ^ ,
_______ . Date Rec'd ^ A / / ? / Batch * ^ 5 - r V
g.Wt.^ ^ ^ g rams Avg. Size^g, ^ # a n No. Organisms per dose //Q Loading Factor /9, /y , g/i
sh Disease Treatment; A f r f / f f z , ___________________________________
'
st Solution Volume / Liters/All-Glass Tkrik Tank Dimensions;
25 an^e^ ^ ^ eCf
" e ta ^ - U 2 J Z D p ( J * * * Started .
Date Quieted /fr /fty L
iution Water Carbon-filtered well water (Tenp. Z O C-, D.O.
ppm, pH ^ , 7 / )
vestiga ull Si
' `M oe & y
<95% Confidence Limits)
____________
T '/ ^ s / r - k s /^ <5V f . 2 - V < ? )*< * 4 ?
M v 'A fir *jK **G e 4 M rC C 5
y 6 ) ^ y _____________
o.
Cone. mg/1
Amount Aided
Total No. pH Dead
D.O. Total No. pH D.O. Total No. pHD.O. Total No. pH D.O.
ppm Dead
pgn Dead
ppn Dead
ppm
X Control ^VKCj - J 3 fit
o ft! 7 / .0 ?.i
<o fl y ,x
1 _ \ s liK)
o ft I
-O. ft I ft? ......1 fit
\ R/
zr> 200 O ft I yy
1X _ ->Zj zzc
2,0 Y ^
ft7a r 7 0 /LJ ftt
v*> 8f(! h '/
"/X X5>
y 2)0 SCO ... j ftO
Y fi,r
Iftf , //? 7ii / . r-*
5 y<7 *iQ() Y 8if $4- ft 14 Y f t
7 Y.P:
Test Temo. C Initials &Date
- ^ A T W /j W - ' ~vr ^ v/ a / pc/
zzr, v//,/>,/_
condary Effects (other than Mortality);
EC50
'ank No. Symptoms or Reactions
>ntrol
-T -L_
|/
\
24-Hr.
M yU K A f/'f
?/ )
4 X
\
V
'/
Z)
/ -5
.
Total Number Affected
48-Hr.
y
72-Hr.
A f/iA 'e . A / a .
/A/C'
!
f/fV G
/
3 ..
.
2J
-3 1
96-Hr. A /4 s ____ A fm U F -___ _ _ i _______ ____ L l
/ G0G'
BEST COPY AVAILABLE
ENVIRONMENTAL LABORATORY
AQUATIC TOXICITY DATA SHEETraw u r \ XX V-- Xl JA 11. I I I I IM 1 M Tn T. T. 1 DEFINITIVE (FULL-SCALE TEST)
***
,. . 7
XrrtT,/' .Material fested ,ty/7 f o s t g - X )
Iot a s '
*=~~^
P O & O l , ~ / W',
*3
gr ans Avg. S iz e ^ Q Q a a No. Organisms per dose / f l Loading Factor 4 ) ,.Z ln f/7 g/1
ish Disease Treatment: A f/O A fP .__________________________________ ____ ___________
Solution Volume / f ) Liters/All-Glass Tank Tank Dimensions: 35x20*^ M >d 25
ime Started /J Z J O ^ ^ / ^ D ate Started
_Date Completed
Llution Water Carbon-filtered well water (Tenp. 2 P C., D.O. ? ,J L ppn, pH f\,2 L
ivestigapsf e ^ ^ g T ^ g g
till signai)
/
.. ....^
------- ---
~n7cMg crrrr T iA frM fir^ t*>(/ ^S--jSs_33A n A ffS
)
'to.
5:
24 Hours
48 Hours
72 Hours
96 Hours
Gone. mount !Total No. pH D.O. Total No. PH D.O. Total No. pH D.O. Total No. pH D.O.
rog/1 1Added Dead
ppn Dead
FE*n Dead
PP" Dead
ppti
Control
vnq ..o
11d i (9 fill V o __ o
SJ M
n Si w
M_
l*>0 j n
Ih ? o
=?.(
o Si f o l i / Si H
L 2.0 y?
2-00 - o
.^JZ 4
75>5Q Q
v w -Tf
(M Y 6
n . ?,0 y<9 0
fi( f l
ffl maJUya
fiio 1 ,1 , V . f*C 1 $
4
(41.5".. Jj
w
ajj
?,r1
1 e ,1 i
* h i Y
p 7,1SJ. 1 ,1
f ai
ft
Id SJ 1 1
!
Test Ten. C1 Initials & Date
-k^LUt&A-Klf
1
2 J P s
1____2 P E -____ -. Z J L '
1___ __________
7 7 7 ^ r r ^ T 3 <// ^ JR U I
J i/ /H /.VY
, /,.W/7C H i y ^ r/J /j./A
xxmdary Effects (other than Mortality):
7ank No. Symptoms or Reactions
24-Hr.
>ntrol X
/ ffl-AJp
1A /
\ Af/LrAjf.
- - - - - - - - - - - - - - - - - - - - - - - " A ha K
Y A 40?&7<r/Afc..
4 A v~ '
;
V- :
BCso_
Total Number Affected
48-Hr.
72-Hr.
/A m C A fro r
1_ .
/
/
Z j.-
^_
Zj Zj
05
-- M i_ _ _ _
96-Hr.
/ 7 7 --------^ 006062
- *-
