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DISPOSAL OF SOLID "HEFLON".WASTES CONTAINING C-8 APFeG .: . "+ ..i-
Introduction
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:" DoifspFeoxrisciopneSroAfmrleeuaoorfoofctahtrehbeoSxo"ylTliellfidlsconwd"aisstppelsarnstifnrgocmonatgtehaenitnsF.isnmeaAlPlocwhademeaorpuna atmsdndd:eFos
} . aaTbcilc1e1e,'p1t6apvbrelolev.imdeetdShiontdchaetotfthhedei.dstipwmaxpsieircnsgiangogefnttashgeesenertessoraleriedduscveodlisattioilneaan-atalcacnidept= :
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mnoedceersastaerytetompbearkaeturtehse,reWsetinsgettoouta tnoon-dteotxeircminteatteh.e condition: s trCoe
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Summary and Conclusions:
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1. Toe Sisperaing agent loved oF the golnd vaste
oF ili
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a{tbreelaonw i2spprme)dubcyedbatokinagquatite17a5cCcepftoarbl5eholuervse.l GrFera a
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2. pWeirtfhiouuotroaceprrbeotxryelaltimcenatc,idadissmpaelrlsianmgounatgenotf Wtohueld'
| be leached into the ground water.
"Discussion:
EGaRn a
Eh
Ll
2 DChirsepne.rsiTo+hnAisansdyisnFtvieonmlevefdoPorwtdhceeorl:lulsAeercetaiofnwgassutnheppsrospoaolnsdieddsweabtsyttleiAsnngdefbrrasosominntshaemedto =|
:n ' ei 7 vi I`
vCaoxncefnitlrtaetres athned in this system.
vsaoAxlifiwdpsb.ersaShtieooelrtidsosfeittnthletihnepgrofwpoeorrsmeedofaslsycoosatgteuomluihsme
cforlolmected' attached.
i.
ii' :
Tahtecutrortaelntamoopuenrtatofngscoolniddisltiisonse.stimated at.ca. 768 pounds mer: day' oT Ge
. croelplreecs. teinotnaStapimovpielnetossf moifnatthse0erl.i1adpllrowtpoaosstbeeedspwbsetyraseitenmeo.dbta`fiTrnhoeemdsethfersoammfipnltee.hsepwoewrdee.s
:
.
Sump, the wax trap, the boittom of the wax separator and the...
. sump from the Dispersion Alfea: The make-up of these sarples.''
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Was EN
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foSllEoCwstA C .. .R \.. Eoof
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Ae EET re TM R. F. ANDERSON
LAE RY 2RR AA ee AEERESAREE
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August 81, 1966
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"_conFciotnnateiannPioenwdadteer3d6,S.,l2u%wmeptw,a-teTrrhiinseandpmoawt1d3ee0rri.paplmTlhpoeeokrsfmlautloeirrkoie.al SL rT LL
carbon dispersing agent caloulated as C-b AFF.
Le
*'e WonaxheTaratping- taop)pe1a7r5sC.likeCownatxa,insLocsa.t 83%0 pbypmveC-8i.gme " DE
: Bpooptdteorn oanfdWacxo:mtSaeipnaeraatboorut- 6a5p%pewaartserlikaendwe2t40ipmpem: = .L. en| c-8.
DobitsapienresdionfroAmr:veatheSumbpatt-oTmhiosf .stahmeplsetawbaislizaacttiuoanlly Cael
Ttlhaienqkumsiadtaenardnidawalas:1w8oa0n1tm1aidixntceuodrnetsaaio.nfi.na3g0060ap%bonudtiwsap3te0errs,wiaotneIrn'..
VEU Wh
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mtohset11ofquitdheawnocrksodliddnephwaisteh twheirse mainxatluyrsee,d.bo=th
psiy
1. Leaching
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As a first `step, it was desernined that the dispiersing a) -+ `* agw1ea0t0netrgracimnosuladoWfabretihnelgeasBcalhmepenlddeofrfr.m.oommAtfhthteese-erdisbfollfeiendrdsei.nntg Tfshooirusrc5ewsamsintuodtoen1se0,0bmiytlhaeod.fding~..~. ii"7
WttahiattterrattvhiaeosnCm-fe8itldhtioesdrpeed(rsseaisnndgbaealnmomwel)ny:tsecdoTuhfelo.drdaidnitdseepeesdrhsoiwbenngiexnatgrTeanatclteebdyTbhysiiehwowater| ':Laionii: mTehnti)i.se the conclusion remched by Crandell in 1964 (see attaT ch n "
a
Table T
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: . The Efrxotmra"gTteifofnionof CS-a8mplDeisspeirnsWiantgerAgent .
ciaEtse o
.
Sample Source wUi IE l Extper M cad Ec-xtzt rnadci tEexdtoramnti,on, SRE 2
2 Pine Powder Susp L A UBLgLe PEat - "a
"Wax Separator
03.
L218) p So
. Wax Trap
, ol - EL)
Ca
NE iy
: 2. Baking
:
2
Analy| sis oTfhethessaem.plseasmpwleesre(sbhaokweedd aaltm.o1s7t50comfpolret3e,. r5emaonvdal20ofmfoutsh.e dsperaing agent at 5 or 2(0hours; after 3 hours treatment onl:
SAi -
the saaple frou the fine piowdar sump contained any residual Gof i" i.
Po
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ERE edi
BURGE
Rle e DL SIG
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000075
CF020542
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Ton EEE La TL augues 31, 1966 |
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ANALYSIS OF PERIPLUOROCAREON DISPERSING AGENT.
HE
IN "TIEFLON" SOLIDS WASTE
NAT
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SampleSource2
1H
Lol kT
riHoouurssfHeeaatt=eedd8A1g R17052 C
eycre
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aono
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Pine Powder Sump BESAEE) Goat 2g Toa
7
Bottom of Wax Trap Li [200 Gi <0 C24 Teme UC 4
Wax Trap #8 sb EON 0 L073 mmm
Tr
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Sanitation
- Sofia
TankSETRTUE
460 i3 viaao.pan Co :
Ta30 Tee 0.77 oul
CL
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A TRA Le Tage
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Se
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CTPTn epHERE eT blHh en
SRTTe
: Som Ceant eE H TIERRe RSE aEfER eh
Eine
Fer BERL SR
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: Com AES ah
I Sl TE
Cu ARR EEE RE RE DA A
T . s e y Re LE
JURA
ACE ME
a CT Aa SwRihfe BAT ENIN RR fr mei rn EID1B3616 000076 croz0s43
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August 311, 1966 Lis
| bAyPPCm.ostThoeventsempaendratbuerceausoef 1it75isC wbaeslowchtohseenflasashonepoienatsiolfy rtiehaechweadx Lhi
+. used (20590), )
ChE
I 3. analysts
EA
of perfluorTowcoamrebtohnoddsisopferasnianlgysaigsentwsereinustehed wfaosrtethestdreeatmesr.minaTthieon we
-+-
.
wptihrteohcperwdoauptreeerrstyafrreotmhaitnacplsuetdrrefodlnugholemyroceaacrifbdooirnficedodimsplpseelturersnriyen.sgs.gTehniOtsnsedicmsaatndielbleu:iiassdeeisotcfialnled
Ae .*~: -/-t!
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tohoetnanobieo taictirdate(CdrFt)osCZd0gH fer--miMnWe procedure was folldRed:
t43h1e).ano`uInnt thoefse`acsitd ud:(iaesspethrefi:mofoaorlerl-o.wing oC
'.wl,
7-
"1. a21s00cutgrainm asaWiaprlieing(+B2l0e0nd1or.of Tdhiestisllluerdrywwaatser)
i Li 3 yn
aPdhdoesdphotroica 5a0c0i-dnlmladfelda.sk and 25 ml of concentrated.' ; Tii . li.
:
2. Tchoendefnlsaesrk.wasThefistltuerdrywiwtahsahedaitsetdilltionbgoihleiadnganadnd TPEU A E: R
x
tchoentacionndienngsa5t0e'-mlcololfecdtiesdtilinledanwaErtleyrmmtehyaetrhafdlabseken.. `Girel.
.
pchaerneoflupllhythanleuetirnalilnidziecdattoor.a pDiinsktielnlda-tpeoinstamwpiltehs* WRIT T R
e1/r2e00cNollseocdtieudn ehymdcrhox5idmei.nutes and titrated with . ha ni:
" "3. Wwahsenbethiengtdiitsrtaitilmlnesd i(cnad.ics3tetdittrhaatitonnso sorddi15timoinnaultewse)l.d t"~i~ |. 7;is
. athgeenttitcraelcwualsateadddlaecdcoarnddintghetmootuhnetfoolflodwiisnpge.rsing
FwiTe
i
ppm C8 = ml x 43.1
wt
* TahmiosuntmsethoofdCc-8heickmedtheversylurwreyl.l with known spiked
eH
bbleutewee1sn mnoe"tTthheyelxetonrteahcetbrelmdueetfharonoddm!l itashceibdadsisesodpleurtoisnoinntgheinatgfoeonrtmc.ahtlioWorhonfiolorefm,maefcittohhymelpe=lnee..x. ..% =.
TM,
f.,
occfoomnpctlheeenxtrciaostlioporaantritooifntidoiinnsepdtehreisnictmhogloatrghoeefntocrhmlinorloathfyeoerramq1usleaoryueesrl.aptheaTdsheet.oitnNtheeeonnsiiotnyto.. ..a . .,"H: A
:
dThdespmeertahiondg 1a8genstesn,iitsiuvceh tamw. 0".T0r5itponp"n Xd-i1s0p0e,raidnognoatgenitnteirnfetrheeee:aqueous
phase.
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In this method, the following procedure was useds:'.
i
+ 1. "bTyheosuatmbpilneg waas10p0regpraermedsum(palsinintsheWamreitnhgodBlaebnodveo)r, ;~... -%' .. .
Lo fF e ooR e h e e oy) d wdfi a feasn)s Bvaigdong aE TeshAY r TA Fr * eT ERaTIRE e FT L AEET TEnega
000077 cro2054s
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3/ o Re Po AND:ERSON .
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EREETO EEE : Aug.ust 31, 1966 odol
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wFiotrhtwhaitsert,esta,cld5i(i0f-nylingofwidtihstHilPlOayteawnadsdicsotlillelcitnegd.. .-. " "=a: '1Y
2;
. 2. 2TAhme1e0a0mseumarlseudrveo`ldpuomaretmtioicwronintcodffelpateshnkeddaeindsdtonidlillthauett.eedawmawosiuntthadwdoeafdtCetr-o,8y "Ii.i . xin%ri..ll
. + A"nsamtphlees,diast2i5llmalte.porFtoiorn,indsitalnuctee,d itno t1h0e0 mbla,kedwas
MEENLIST
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uwzsaaestdi;ounsefdot.arnkt,heaas0...-2remcleisveemdpls: ea,mpldeiluftreodm ttohe10st0a-bmillil-'
e li.y,i
= 3. Tthoea10205-0m-lnlfrsoempairtahteindgilfuutninoenlofandste1p.02mwlasofad1d-9ed <i'. =:
E"N
:
K(C0L.50s0olgumtsi/o1ni,te1r.!0)0,ulanodf1m0e.0thmyllenoef bcihuleorosfoolrumtiwoenre: <. gE;
..
wmaiidtndhueddtr.easw,nT.halelomwiexdt.iurteo wsaesttlsehakaennd vthiegorcohulsolryofofromr l2ayrer' Ciirai''frliF
J. : 7
wi" 8.
pT7hh0e0otmocymhelttooerorf6oi0r0nmmayli-aluy-seoirmnwggalsacshslaonracolefyllosrebmdyiinnscatahnesnipnergecfterfrore-onmcis'1
|.
rl
Ae
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.
c65e0ll.my Twhaes mpeeaaksuwrbesdo.rbande for the sample at H no T7
Co
5. For these studies, it had been.shown that 0.0057 i. i. i
.
uC-n8i.ts oFnrotmhethespaemtoruontp.hootfomaebtseorrba=nc1ex10a-n5d gtrhaemsfaocftow < i n i {"iiiim
.\
cfarlocmulsatteepd.2, the amouLnteof C-8 iSneethe sample was Ni = /':f to,
separator Tshaempltew,o m+. ethods cBhoei:cked wgiothiwnav10% for the S wax e~~,
n iNY
i
eT DRE TGeT
. Hye Tl
epaa ren ATTRSRlTHgAONEa A VALINEet A A Sl ele
ROAtse
Attachment
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