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_ + CBaigloennidaalrRYeepaorrst offor20th0e2Maannduf20a0c3ture ofAPFO DuPont Com--pFayaettneviylle Work ARZ Page old 1876 Biennial Report for the Manufacture of APFO Calendar Years of 2002 and 2003 DuPont Company -- Fayetteville Works Naontdel:orTmhodeiifnicfaotrimoant.ion contained inthisdocumenitssubmitied voluntarily and may be subject tofuture revision CONFBUI SINED SS INEFORN MATT IONIISREA DACL TED o"TfhiIsntreenptor(tLiOsI)sutbomSittetepdhepnurLs. uJaonhtntsoonc,omAmssiitsmteannttsAdmmaindiestbryatDourP,oUnStEiPnAa,Meanrtcithle1d4", V2o0l0u3n,taLretyter Actions to Evaluate and Control Emissions of Ammonium Perfluorooctanoate (APFO)" PbuergsiunannitngtoiAn dtdheenydeaurmaIfItIoerftphriosduLcOtLi,onprcoovmimsieonnc5e,sa, faancidlictyonmtainnuufiancgtufrorinfgivAePcFoOnsiescurteqiuviereydeatros, following, for the prior calendar year, report to EPA biennially the following information on a calendar year basis: 1. Annual production volume of APFO; 2. Emissions per facility (air, water, waste); 3. Summary reportofgroundwater monitoring results; 4. Summary reportof surface water monitoring results; 5. Workplace industrial hygiene monitoring; and 6. Summary data on employee blood monitoring results. "ATPhiFs Oreipsorttheprsouvbisdteasnctehepraobdouvceeidnfatortmhaetfiaocnilfitoyr,ctahleensduabrstyaenacresm2e0a0s2uraendd b20y03a.nalNytoitcealthtaetcwhnhiiqluees is the perfluorooctanoate anion (PFO), which is reported herein as perfluorooctanoic acid (PFOA). General Facility Information Company Name: ~~ E. I. du Pont de Nemours and Company Site Location: Site where APFO is manufactured: DuPont Company ~ Fayetteville Works 2Fa2y8e2tt8evNiClleH,iNgChwa2y838076-W7332 Confidential Business Information Redacted 2 Company Sanitized CBiaclaennidaalrRYeepaorrstoffo20t0h2e Maannduf20a0c3tureof APFO DuPont Company ~ Fayetteville Works Page2of4 1. Annual production volume of APFO TprhoeduDcutiPoonntinCloatmep2a0n0y2. TFhaeyetftoelvliolwliengWotrabklse'shAoPwFsOthMeatnoutfalacptruordiuncgtioFancivloiltyumceomofmeAnPcFeOd for calendar years 2002 and 2003. Calendar Year "APFO Production [ 2003 2 T| T (0 3 | Soren | an ww | 2. Emissions per facility (air, water, waste); TfahceilietsytiatmaFtaeydetqtueavnitlilteywoafsaidreteemrimsisnieodnsutsointgheenagtimnoeseprhienrgecaflrcoumlattihoensA.PFIOn amdadniutifoanc,tusrtiancgk edestteicntgiopnelrifmiotr.medAnninua2l0ly03a showed sample oPfFtOheAsiatier's esmuirsfsaicoenswattoerbdeislcehsasrgtehatno the the analytical Cape Fear RquiavnetrifiiscaatniaolnyzleidmiftorofPFthOeA;anahloywtiecvaelr mtehtahtomdo.nitTohreinwgasshtoewesmitshesiPonFsOAaretothbee less than quantities the of PFOA, streams otnraansdfreyrrbeadsifs,rotmhatthaereFeaysettitmeavtieldletoWhoarvkesbesieten. present The fionltlhoewivnagritoaubslesogliivdewsastthee estimated emissions of PFOA to specific media from the Fayetteville Works during the subject years: eeeT 0 ET 323 b. Note 1: tDhueesthoortthedulraatteisotnarotf-utpheof2t0h0e2ApPrFodOucMtainounfraucnt,urniongsuFrafcaicleitywaatnedr monitoring occurred in 2002. NQ = less than the practical analytical quantification limit of 0.05 g/L 3. Summary report of groundwater monitoring results dInet2e0r0m2i,nethteheDumPoosnttpCroobmapbalenylo--caFtaiyoentstefvoirllteheWoartmkossppheerrfiocrmdeedpoasiirtidoinspeorfsiPoFnOmAodferloimngthtoe `ew manufacturing facility. New monitoring wells were installed in the surficial aquifer at Confidential Business Information Redacted 3 CBaielnennidaalrRYeepaorrst foofr2t0h0e2Maannduf2a0c03tureofAPFO DuPont Com--pFayaettneviylle Works Page3ord the two locations predicted by the modeling. ITnhe20m0o3n,itthoeriFnagyetitnevvoillvleedWtohrektswsoitneebwelgyaninasntnalulaeld mwoenliltsodreisncgroibfetdheabgorvoeu,ndawnadteirncflourdPedFOtwAo existing monitoring wells. GlervoeulnsdowfatPeFrOAm.oniintotrheintgwoconndeuwctweedllisnaJnadnutaheryexainsdtinMgarweclhl 2a0t0t3hesOhlodweBdionsoluqdugaentLiafgiaobolne (SMU-01, of PFOA SWM-02, above the aqnudanMtiWfi-ca1tiorenspleicmtiitvelayt).theTheexsiestmionngitwoerllingloecvaetnetds did indicate upgradient levels of the Nafion Common Sump. gForloluonwdiwnagtedrismcounsistioornisngwiwtahstheexpNaonrdtehdCtaoroilnicnlaudDeivtihsreieonexoifstWiangstweelMlsandaogwenmgernadti,enttheo2f0t0h4e Ninaf2i0o03n, aCnodmtmhoenthSreuemapboarveea-.meTnhteio2n0e0d4dmoownnigtroardiinegnrteswuelltslswesrheowveirdtuPalFlyOiAdecnotniccaelnttroatthioosnes of 0.303 PFOA is pg/L, 1.530 a resultof a pg/L, and 0.123 historical release pg/L respectively. originating from the It is believed that the detected Nafion manufacturing area's common process wastewater sump. That source has been eliminated from the site. `The following table shows the groundwater monitoring analytical results for 2003 and 2004: `Confidential Business Information Redacted CBaielnennidaalrRYeepaorrst offor2t0h0e2Maanndu2f0a0c3tureofAPFO DuPont Company - Fayetteville Works Pagedofd (SMaomnpilteorNiangmeWell Description) `MoDnaittoering PFOA ug (SNMeUw-0w1ell on River Pump Road; 0013/72277/0033 East of APFO Facility) 02/04/04 (SNMeUw-0w2ell at Construction Gate entrance; Southwest |[ 0327o 03 |Tp __<<oos 0101|| of APFO Facility 0204/04 (MEWx-is1tSing well a1 Od Biosludge Lagoon SWMU by 0O12s8/o03 00s | Central WWTP; SouthofAPFO Facility) 0327/03 22/0404 (NEAxiFst!ing well upgradientof Nafion Common [032702003|00006 68 s| Sump; SoutheastofAPFO Facility) [opis [oo o2o40a 0062| N(EAxFi-st0i2ng well downgradient of Nafion Common 020404 0303 Sump: Southeast ofAPFQ Faciliy (NEAxiFs-ti0ng well downgradientofNafion Common 0204004 1530 Sump: Southeast of APFO Facil (NEAxFis-t0i4ng well downgradientofNafion Common 020404 0123 Sump; Southeast of APFO Facility 4. Summary report of surface water monitoring results As for reported in Item 1 above, the PFOA in the site's surface DuPont Company water discharge to -- Fayetteville Works annually monitors the Cape Fear River. The monitoring conducted in both 2003 and 2004 shows the the analytical method, or less than 0.0 g/L. PFOA to be less than the quantification No surface water monitoring occurred limit of in 2002 due to the late start-up of the APFO Manufacturing Facility and the short duration of the 2002 production run. 5. Workplace industrial hygiene monitoring The DuPont Company -- Fayetteville Works began workplace monitoring for PFOA with the start up of the APFO Manufacrtyurarienag mFoanciiltiotrysitnha2t0s0a2m.plTehdethweorbukiplldaicneg maiornistpoarcienfgorintw2e0l0v2e and 2003 consisted of stationa (12) continuous hours. These sampled locations are. limited access restricted areas in which Confidential Business Information Redacted . CBaiglaennidaalrRYeepaorrst offor20th0e2Maannduf2a0c03tureofAPFO DuPont Company -- Fayetteville Works PageSof4 personnel wear reported in the both respiratory following table and are dermal personnel the 12-hour time protection. weighted The analytical average (TWA) results PFOA concentration values. Minimum| Maximum| Average [vo20r02 |pAree alPzh[r | omp_ les|| _ 0(0mmg0/4 e8mrT | e m0g./02m4'] (mg/m | 0.017 Twa [10s| oo |ox | ooo] mg/m' = milligrams per cubic meter 6. Summary data on employee blood monitoring results At the DuPont measured since Company 2002. A s--umFmayaertytevoiflrleesuWlotrskosf,embploloodyeseesrwuimthleivdeelnstioffiedPFAOPAFOhaevxepobseuerne potential in 2002 and 2003 is presented in the table below. The entire data setofblood concentrations is available upon request. Minimum Maximum Average oameples! ppm) ppm ppm) [Zoe| 17 | ood | oo Toor | C2005| 44[0008| 2280 ppm = partspermillion Confidential Business Information Redacted