Document deZ0V4OyLxzB6qoZRgVbgZLG
CG 46 '
CODE YT-3Q8-D PKG ___ '
PROCESSES
' APPROVED BY '
< .) YT-80S-D < .)
' V J?'* V . J&G A6
c:v, 105,(106
CODE YC-11-A PKG ___
JiU2/j&. i DATE )
(LOT NUMBER)
EST, WT. 2126* LBS
DATE PRINTED: 12/22/81 D.V./300^|St5) 317, 322, &3\\'
PROCESSES (C)YC-11-A < )
\
TYPED BY: JMH ' TANDARD HRS;___________
APPROVED BY JJG 6/10/81 EWK 10/21/81
TIME
EQUIP !> I MENT | 1
- .. , NAME: DALAMAR YELLOW
PREP | 1 I OBTAIN 5-NITR0-2-AMIN0ANISQLE FOR S6
i USE . | LBS
|
I N-CODE | ACCT I VLB'S
| 557-C \~
1 I 2 I OBTAIN ACETO ACET ORTHO ANISIDIDE FOR S22 |
.13! CLEAN, DRESS, CLOSE 24* CLARIF PRESS -
1
1 }15 FRAMES
' * ' :
'
1
I1
'' . -
I
| 46-C J |I ||
11
~DV 2
T~4~T_RUN~T77"7595~G)'"WAfER~INTO"vIIiriIZ~ -----
151 WEIGH IN HYDROCHLORIC ACID FROM V-324
!
1
j
II
M_____,2__ ,_____ _____%
I 6 1 DUMP & RINSE IN .5-NITRO-2-AMINQ,' ANISOLE
I_______ 1 28-D j
I1
1
I 1 DRUMS FROM SI
II 557-C |
1 1 LOT * 1002:
%
II
I
-- 458 974
1I
I_______ 1 i______
i______
I 7 I STIR 10 MIN OR LONGER TO WET
I
I 8 I'ADJ TO 33* (1155 G) AT 28-32 DEG F* (ICE) 110X330
I 9 1 SIPHON IN SODIUM NITRITE IN`12-15 MIN
|
I1
- M______________________ Y.\_______
110 1 STIR 30 MIN AT 28-32 DEG F MAINTAINING
I
I + CR, + KI FOR S 12
I
I RECORD : TIME START,____ CR____________ (+),
|
1
KI_
(+)
I
1 NOTE:(1) IF CR-, KI-, ADD 20* 'AS^IS*
I
I
` INCREMENTS HYDROCHLORIC ACID
f
1 ASSUME 32% j
I RECORD: CR________ ( + ), KI______ ,(+)
1
1 (2) IF CR+,KI-, ADD 20* "AS IS" INCREMENTS 1
1 SODIUM NITRITE
ASSUME 33% |_______
1 RECORD: CR________ ( + ), KI______ ( + )
1
57-A 1______ I
725-A 1 405
28-D 1._____ I I
725-A |____
DUP050061291
nni\ x iiu jL-pt.* i nuu i x ui'co- - on i wn urt x t
Eq u ip
me n t
MISC 3
II
I USE | N-CQDE l ACCT
I I PAGE 2 OF 3 CG 46 CODE YC-i1-A
<C) I LBS I
| LBS
i -- | ---- ----------------- ------------ -------------- ------------- ------- --- i.----------------1.----------------1 --
III I SLURRY IN 40 GAL WATER IN DRUM & PRECOAT I
|
I
1 I CLARIF PRESS WITH DICALITE FILTER AID
| 5 | 777-A. j
5
DV 12 WHEN S10 STIR COMPLETE, DUMP IN ACTIVATED 4 CARBON n' DUMP IN DICALITE FILTER AID 14 -STIR 30 MIN At 28-32 DEG F MAINTAINING
15 | 113-B I . 15
J1
10 1 777-A 1f 1
10
+ CR, + KI FOR S 20
..... i 57-A I
RECORD: TIME START_______ , CR____
i
KI_______< + )
. ..
!
NOTE: <1) IF CR-, KI-, ADD 20* "AS IS"
11
INCREMENTS HYDROCHLORIC ACID
i1
ASSUME 32%
_____i . 28-D 1
RECORD: CR__ __< + >', KI . ( + >
11
<2> IF CR+,KI-, ADD 20* "AS IS" INCREMENTS
1
1
` SODIUM NITRITE
' ASSUME 33%
1 725!~A
RECORD: CR___ ____ < + >, KI,,_____( + )
CV 115 J RUN 10" (970 G> WATER INTO V____ &
1I
S' 1 I INSTALL TEMP CHART
1
f 1 6 1 POUR IN SODIUM HYDROXIDE . M___ _I__,____ ,,__%!.
... 117 1 ADJ -TO 40" <3904 G) AT 66-70 DEG F
1 3X3301
118 CLOSE STACK'DAMPER
1
119 1 STIR FOR S 22
1
I
DV 20 "WHEN~S~?4''sTIR"cOMPLETl7~:risT"Dv"^"RicORD""T
6 CR_____..< + >, KI< + > TEMP:___________ ___(28-32 F) i
NOTE: <1> IF CR-, KI-, ADD 20* "AS IS"'
|
INCREMENTS HYDROCHLORIC ACID
I
ASSUME 32% |______
RECORD: CR___ ;< + ), KI________ ( + >
I
<2) IF CR+,KI-, ADD 20* "AS IS" INCREMENTS!
SODIUM NITRITE
ASSUME33% I_____ !
RECORD: CR
._< + > , KI ___ ( + )
I I
21 AT TURN ON V-____ AGITATOR, CHOP & ADD ICE, I 2X3301
I THEN SHUT OFF AGITATOR, 21B1 PUMP DV THRU CLARIF'PRESS INTO DV
iI !I
MAINTAINING TEMP AT 28-32 DEG F
}]
RECORD: TIME START___TOTAL
MIN____ _____I
I
II
CV 122.| DUMP ?&T0 CV FROM S2 ACETO ACET ORTHO
7 l | ANISIDIDE. ' LOT
*100%
%
I -I NOTE:
________ ________
I I BREAK UP
-___ :____________
II
LUMPS
______
I-23. I STIR 3 MIN TO DISSOLVE 124 I OPEN"STACK DAMPER
125 | RUN IN UNDERSURFACE IN 20-25 MIN. ACETIC
I i ac id .
m;___ _________ ______%
. * 126 I STIR 5 MIN & RECORD: PH________ <5.8-6.3)
127 I IF NECESSARY, ADJ TO PH 5.8-6.3
II
SODIUM HYDROXIDE
ASSUME50%
*> I
ACETIC ACID
ASSUME70%
I 1 RECORD: PH______ <5.8-6'.3)^
7-D 466 57-A 1
2S-D
f 725-A |_____,
I 57-A |_______
I I . I. \ `I I
' y46-C 1.1265-
1 . I r ( r i' i
30-D | 713
7-D 30-D
DUP050061292
NAKJ&& INSTRUCTIONS:BATCH UNIT
DATE PRINTED: MM/DD/YY
EQUIP MENT
CV . 5'
I USE j N-CODE ACCT
OF 3 CG 46 CODE YT-808-D < ) | LBS J ..
LBS
- --------------- ---------- j-------------- 1-------------- --I ---------- --
t97^6) WATER INTO
&'
}
TEMP CHART
.... ' _ f
.J
SODIUM HYDROXIDE
. 7-D I 466
*30* <3904 0 AT 6.6-70 j )EG''- F STACK DAMPER .
| 3X330 J . 57-A U,,___
| / , j . ... \ !
. ;
S 17.
| |- : I v .
: i- . /r. ' . L.
DV /J1S J WHEN S 9 STIR COMPLETE,, TEST DV G RECORD ,| I f ,CR____,,<, . KlU_7__< + )'. TEMP(28-32 F) J I .| NOTE: CD IF CR-/ KX-*, ADD 204/*AS IS* : j
j "" .. 'ji:
/}
l ~~'
v/;-/'/.v
II \I
INCREMENTS HYDROCHLORIC ACID '
|
. ( '
. ' ! -
/.A
ASSUME 32% !_____.^.j 2R-D |_____ ,,
J. I
RECORD: ' CR___< + >, KI^,,___ < + > .
I
: J-v
/.
j * | (2) IF CR*,KI-Y ADD 20* "AS. IS8 INCREMENTS! ' '
| : 7'/ I '
(i
SODIUM NITRITE
- ASSUME 33% i
_;{/, 725-A !;_/-,
i1
RECORD: CR_______ < + >, KI
)J !
i
ji6 | ADJUST TO 60* <20540 WITH WATER AND ICE !_
.1 S7-A Ul U
I I TO 2S-32#F.
I
CV<.
DUMP INTO CV FROM S2 ACETO ACET ORTHO
AN I SID IDE*
LOT 3L0%
..NOTE:
. ;ZQ4<2iU '
BREAK UP
' ZZP..2C2&L
LUMPS
EM44Qft{ ....
STIR 10 MIN TO DISSOLVE"
,PEN STACK DAMPER'
IN UNDERSURFACE IN 20-25 ^N, AC
I ' ACID
i STIR 5 MIN h RECORD: PH____<5.8-6.3)
I IF NECESSARY, ADJ TO PH 5.8-6.3
1
I
SODIUM HYDROXIDE
ASSUME 50%
| ; ACETIC ACID
ASSUME 70%
! RECORD : PH____ ;,,,,/ <5.8-6.3)
!' /' 46-C K 1-265
'- T
i;
. .!
30-D I. 71.3
7-D !. 30-D 1.
!
DV . 123 | STIR 5 MIN 6 RECORD-. TB1P.,..._,,_<28-32 DEG
8' | F) & IF NECESSARY, ADJ TO 28-32 DEG F
j. RECORD: ______DEG F
12* i" tmmmmtsmmmsSxmaSm
!
125
]26 I
IF NECESSARY, ASDaJPTnOJ-4fX* 1As6s, uRreEsCs tLl.?.,, , ...3.__*_%_
127 tettrBSrawnj
57-*-A i____ J
HISC 9
V-
128 ! WEIGH SODIUM HYDROXIDE'IN- DRUMS FOR^aJ.
II
:h _,A2_____&&2s a .~
129 I DISSOLVE ICEPAL C0630 IN 2 GAL WATER IN
I i DRUMS FOR Sd# '
!1
7 i 7-D i 296 62 97?-D ! 62
I
DUP050061293
t *sg| S*V-' '
. . C.V* 105, 106
BATE PRINTED: 12/23/81 B.V. 300, 315/ 317/ 322, 323
/G 46
CODE YC-11-A
PKG
"d a t e ")"" ~<l 6t ~n u mb e r >''
EST. WT. 2126* LBS* f.
;
PREPARATION NOTES:__LLl /.:._.L___
PROCESSES (C)YC-i1-A < )
w-V* ^ TYPED BY: JMH
STANDARD HRS*
___
APPROVED BY JJG 6/10/81 EWK 10/21/81
TIME *______M
BLEEDING
EQUIP MENT
NAME: DALAMAR YELLOW
I USE 1 N-CQDE I ACCT
. I LBS I
I LBS
-I -----
PREP
1 OBTAIN 5-N ITR0-2-AMIN0ANI SOLE FOR S6
I
557-C I
1 2 OBTAIN ACETO. ACET ORTHO ANISIDIDE FOR S22 I
46-C
3 CLEAN, DRESS, CLOSE 24* CLARIF PRESS -
15 FRAMES
DV 4 RUN 17* (595 G> WATER. INTO V________
5 WEIGH IN HYDROCHLORIC ACID FROM V-324
M_____^__,_____ '_____%
DUMP & RINSE IN .5-NITRQ-2-AMINQ ANISOLE
DRUMS FROM Si
. LOT
* 100%
%*
28-D 557-C
458 974
7 STIR 10 MIN OR LONGER TO WET 8 'ADJ. TO 33* (1155 G) AT 28-32 DEG F* (ICE) 10X330 9 SIPHON IN SODIUM NITRITE IN 12-15 MIN
'10 STIR 30 MIN AT 28-32 DEG f "mAINTAINING"""
+ CR, + KI FOR S 12
RECORD: TIME START____ CR,,__________ ( + ),
KI_____ ( + )
NOTE; (1 > IF CR-/ KI-, ADD 20# *AS/'lS* '
INCREMENTS'HYDROCHLORIC ACID
ASSUME 32%
RECORD: CR .._____ ( + ), KI______ ( + )
(2) IF CR+,KI-, ADD 20# "AS IS* INCREMENTS
SODIUM NITRITE
ASSUME 33%
RECORD: CR,,___ ___ ( + ), KT_, ; < + >
57-A 725-A
28-D 725-A
405
DUP050061294
MAKING INSTRUCTIONS:BATCH UNIT
ESjUIP I MENT }
I USE I N-CODE i ACCT
PAGE. 2 OF 3 CG 46 CODE YC-ii-A
<C) I LBS ,1
1 LBS
I---------------
SLURRY IN 40 GAL WATER IN DRUM & PRECOAT
1I
CLARIF PRESS WITH DICALITE FILTER AID
5 I 777-A. |
VI
1 V WHEN S10 STIR COMPLETE,
J
DUjj&~IN DICALITE FILTER AID
I I 10
777-A I
fflR 30 MIN At 28-32 DEG F MAINTAINING
I
+ CR, + KI FOR S 20 ' &
,
RECORD: TIME START^JI___ CR_JTr_< + >,
i_____
57-A I____ *
KI_Jr__(+)
\
NOTE: (1) IF CR--, KI-, ADD 20* "AS IS* INCREMENTS HYDROCHLORIC ACID
Ir
ASSUME 32%
2S-D j______
RECORD: CR_____ < + >', KI___( + > . , (2) IF CR+,KI-, ADD 20*'"AS IS" INCREMENTS
l
I I
' SODIUM NITRITE
; ASSUME 33%
725-A |___
RECORD: CR____,,.*( + >, KI_,___._( + >
~~~
I
I
I
I 150 RUJM-0" (970 G) WATER INTO V_.
>05STALL TEMP CHART
,v
16O30UR IN SODIUM HYDROXIDE
TO 40" (3904 G) AT 66-70 DEG F
LSO^SLOSE STACK'DAMPER
19>t STIR FOR S 22
II
I
7.__i
3X3301
I
J/ 7-D 4 57-A
WHEN S 14 STIR COMPLETE, TEST DV & RECORD
CR__#T (O, KI_dr__( + ) TEMP:_3rA-*.(28-32 F)
NOTE: (1) IF CR-, KI-, ADD 20* "AS ISV
INCREMENTS HYDROCHLORIC ACID
. .
ASSUME 32%
RECORD: CR______!(+), KI______C+>
IF CR+,KI-, ADD 20* "AS IS" INCREMENTS!
SODIUM NITRITE
ASSUME 33%
RECORD: UR______( + ), KI_____( + >
URN ON V-JU& AGITATOR, CHOP & ADD ICE,
EN SHUT ,OFF AGITATOR,
.
PUMA DV THRU CLARIF" PRESS INTO DV
MAINTAINING TEMP AT 28-32 DEG F
RECORD: . TIME STARtJLlSlgXr TOTAL MINSferSS-.
I 28-D |___ _
I J 725-A |_____
I 330 57-A |
I
DUMP INTO CV FROM a n is Id id e , NOTE:
BREAK UP UMPS '; c
MIN TO DISSOLVE
'STACK DAMPER
RUN IN UNDERSURFACE IN 20
'ACID. .
I STIR 5 MIN & RECORD: PH^OJ^__(5.8-6.3)
27 j IF NECESSARY, ADJ TO PH 5.8-6.3
f?I %* > J
SODIUM HYDROXIDE ACETIC/ACID
ASSUME 50% ... ASSUME 70%
! RECORD: PM..... Z... (5.8-6.3) *
DUP050061295
MAKING INSTRUCTIONS:BATCH UNIT
EQUIP I WENT I }
OF 3 CG 46 CODE YC-11-A
<C)
b'V >, S
IS WHEN S 21 CLARIF COMPLETE, WASH DV (S 4)
LINES, PUMP & PRESS FOR 20 MIN OR TO A -CR
ON A SAMPLE TO TOTAL PRESS EFFLUENT, I WHICHEVER COMES FIRST* ;; COLLECT- WASHINGS
< S21B). iCORD:.; ?TIME STARtdffSlCRiirr< - OR +) r| STIR 5. MIN & RECORD: TEMP_$C_<28-32 DEG I F) & IF NECESSARY, ADJ TO 28-32 DEG F RECORD: ' #a*._DG F
ruiri/cT 1: 11 ft Till Tltin IT '
USE { N-CODE | . ACCT
LBS |
| LBS
^ M
I '~
' - i
r i
57-A
dfcrRECORD: K I^_,,L~. < j ADJ TO "fat 6 RECORD: k i; /l/, 7Vt Arc
l WEIGH SODIUM fHYDROXIDE IN DRU_MS_ aFr_OF_ _S_4_i _ %
I DISSOLVE IGEPAL C0630-IN 20 GAL WATER IN I . '<52:. |
M5XF0R S43
I1
'I 7-D | 296
979-D
62
CV !36r t WHEN^S 33 COMPLETE, ADJ CV TO 48* (4685 G)
19 f J^f?T 89-84 DEG F
.
I3T CH&etr ACCURACY:
sf!_.l__Dj;
REC0RDER_^2!1_,, DEG F
IMMEDIATELY RUN IN DV THRU UNDERSURFACE
DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV
$M*9-84 DEG F
,,/^L
RECORDTIME STARTfc^LX, TOTAL MIN
WHEN S 3B COMPLETE, STIR 10 MIN NOIEWmMEDIATELY AFTER COUPLING DISCONNECT
TRANSFER LINE AT CV
RECORD: DIAZD^_ir_i-(">, BASE__ r PH <4*3-4*7) .
NOTE:
.<+),
<1) IF DIAZO +, BASE -,/ AND PH BELOW 4*3:
! < A) ADJ TO PH 4*3-4.7 SODIUM HYDROXIDE
RECORD: PH
ASSUME 50%
*____ -- i 7-D
IF DIAZO +, BASE
6 PH 4.3 OR ABOVE
ADD 8# 100% N-7-D SODIUM HYDROXIDE TO
A 55G DRUM
7-D
ADJ WITH WATER TO 25G
ADD 20# 190% N-46-C ACETQ ACET ORTHO ANISIDIDE
!I 46-C
STIR TO DISSOLVE POUR INTO CV
1
SXI.R 19 MIN
* u-
REPEAT (1)6 (2) ABOVE AS NECESSARY
I TO - DIAZO, + BASE J POUR IN N-7-D SODIUM HYDROXIDE FR0M.S34 6
1
143^J1^SRTEICROR5D: MPINH*jji3L<8.0-8.5) & IF NECESSARY ADJ I
I
l i TO PH 8.0-38.5. SODIUM HYDROXIDE. ASSUME 50%I_Z I 7-D | | RECORD PHi6Ji<-HYDR0CHL0RIC ACID.ASSUME 32%|_______ | 28-D
nl
DUP050061296
'i
MAKING INSTRUCTIONS:BATCH UNIT /
EQUIP | KENT 1
1. 1 .PAGE 04 OF 04 CG 46 CODE YC-11-A
1 USE | N-CODE { ACCT
(C) f LBS I
| LBS
CVi |4<
N-979-D IGEPAL COr-630 FROM S3S
to \p
jfl^-200-204 DEG F IN 58-62 MIN
CON1D 142rj 'Spfr6 MIN AT 200-204 DEG^F < '
3,.; i i^ECORD: TIHE START^HiE?/:'
/
' I*5^ FLOOD TO 94" <9174 G) & STOP AGITATOR
* . ` I I -
; 1 `: I 1 i
" .. STA^X
: v.v FINISH
OPTji
1 . , 1. i
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DUP050061297
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DUP050061298
DUP050061299
DUP050061300