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J AR226-2-- 822 ! sn bRETETTpLp, ma | ns,i en oi vs | | EE 2z& || E StRn T R T EO R Ld ]S T. EESTcE oIltsR SiRihbwEtetltiSeemiclsn1r SeEsRe 0 RR F :2 | in t, 20BhHAitvEeeB,Eiet,get,SB rsaaeocso8sLetsmaritilesr ttmtA oeee .tigetnSctysL7sogtE rseeeCeorL merteestsedtsamae r L [i IeEe yI 6e GIN, TEE , ow se dmes om nods ose iiP2{: a40m,000 p.n " 1.92 wh frpS t fSreprrdlp eT, t: i Hraptd, dEeeo ep,e in e p SE ma seaet tt eoh n, SaTdeer : Eri SEE -- Nominal Concentration 20,000 ppm (ca. 200 mg/L) Exposure Time (hrs.) 4 10,000 ppm 4 (ca,, 100 mg/L) 23.4 rag/L 13,9 mg/L Air Plow (liters An in,) 1.96 1.98 2.00 2.28 Mortality Ratio 2/4 Clinical Signs of Toxic <ty_ Duri.np Sxpoavre: 40,000 ppm same as at After Exposure: 2/4 died 1 day after exposure; Labored respi ration and weight loss for 2 days 0/4 During Exposure: labored respi ration; lacrlmation with pig-i merited discharge around eyes and nose After Exposure: recovery withiin 1 day "Bottom Fraction' 2/4 During Exposure; discomfort;^ labored respiration; gasping After Exposure: labored respiration up to 9 days; weight loss In one survivor until sacrificed; death of 2/4 at 1 and 9 days 0/4 During Exposure: same as at 23.4 mg/L; irritation of nose,i mouth and eyes, pigmented dis charge from eyes, in addition; After Exposure: marked weight loss first day followed by ! irregular losses and gains; "noisy" respiration for 8 days, Gross P Nonleth;.! attributab 1<4 days po Lethal Con lung damag lung weigh 14 days po of liver, testes dep 14 days po Nor. lethal tion of lu pose expo abscesses -^ SKIM IRRITATION AND SENSITIZATION TESTS Procedure: In the tost for primary irritancy, each material was applied undiluted, and as a sol-^i intact anrl abraded skin of 10 male palnea pigs. In the test Co produce skin sehsitization, each m undiluted Co the abraded skiii cf 10 male albino guinea pigs, nine times over a thiee-week period. weeks later, the animals were given challenge cests to intact and abraded skin to see whether they Results: Concentration 100% 107,* 24-Hour Observation of Irritation HHHBBH----------------^^2906^ Mild to severe irritation on intact and abraded sRin Mild irritation on IntacC and abraded skin 100% 107,* No Irritation on intact or abraded skin No irritation on intact or abraded sktn 100% 10%* No irritation on intact or abraded skin No Irritation on ii.cact or abraded skin 1007. 107o* Bo Irritation on intact or abraded skin No irritation on intact or abraded gktn * 1:1 Acetone-dioxanc containing 13% guinea pig fat ** Higher-boiling liquid fraction only Summary: Both fractions of the crude i-elomer mixcure have relatively low acute innalation toxic to c'.ie mucous membranes (such as eyes ind nose); at high concentrations, they produce a marked ir the lungs of rats. The "bott ;' fraction".consisting of liquid higher-boiling components, appeare ' ' TM ' p* is more toKic thanT----------~'------------------------ u - - The liquid fraction of the crude telomer mixture was irritating to the skin of guinea p produce an allergic contact dermatitis. The other three mixtures were. non-irritating t" ^uinra pig skin; neither of them produc dermatitis, HS/mfs Date: November 3, 1964 Report by: / ^ ^ 7Henry Chief, Oral T Approved ,'''' ,./. h by: .^'^',-i'<?^/y . ' ,-/',' J. V^ley / ' i^asistan