Document dQybpZqYokynea3r9nV8RG5dB
Analytical Data of S-309, S-306 and S-307 Organic Phases
(Kanegafuchi's No. 2 Plant)
Sampling date: Jan. 12, 1982 HC1 feed rate: 6,300 STP m^/hr.
Component ~~ '
____ S-309
S-306
S-307 Combined
(wt.%)
(wt.%)
(wt.%)
(wt. %)
Ethylene Vinyl chloride Ethyl chloride Dichloroethylene (tr.) Dichloroethylene (cis) 1,1-dichloroethane Chloroform Carbon tetrachloride 1,1,2-trichloroethane 1,1,2,2-tetrachloroethane Trichloroethylene Perchloroethylene Chloral Ethylene chlorohydrin 2,2-dichloroether 1,1,1-trichloroethane 1,2-dichloroethane
0.015 0.0028 0.223 0.0037 0.0027 0.0069 0.015 0.028 0.284 0.0075 0.0060 0.0016 0.236 0.065 0.0013 0.0086 99.09
0.0008 0.0019 0.245 0.0039 0.0058 0.0065 0.014 0.018 0.195 0.0029 0.0006 0.0016 0.383 0.578 0.116 0.0098 98.40
0.0008 0.0069 1.39 0.015 0.0026 0.019 0.030 0.028 0.086 0.0005 0.012 0.0011 0.177 0.194 0.016 trace 97.93
0.014 0.0031 0.359 0.0052 0.0051 0.0080 0.016 0.032 0.286 0.0070 0.0039 0.0017 0.210 0.100 0.011 0.0089 98.92
Notes: (1) CO and C02 in vent gas from S-307: 0.25 and 0.39 mol %
(2) HC1 content in S-309 aqueous phase: 67 q/l
(3) Catalysts:
KOC-101 for R-301, "KOC-R2 for R-302,
KOC-R3 for R-303 and KOC-102 etc. for R-304
(4) Acetylene in feed HC1: hydrogenated
1 0000180^3 ccft
Analytical Data of S-309, S-306 and S-306 Organic Phases
(Kanegafuchi's No. 2 Plant)
Sampling date: May 7, 1982 HC1 feed rate: 6,000 STP m-Vhr.
Component
S-309 (wt.%)
S-306 (wt.%)
S-307 (wt.%)
Combined (wt.%)
Ethylene
0.028
Vinyl chloride
0.0050
Ethyl chloride
0.315
Dichloroethylene (tr.)
0.0092
Dichloroethylene (cis)
0.0085
1,1-dichloroethane
0.0093
Chloroform
' 0.016
Carbon tetrachloride
0.021
1,1,2-trichloroethane
0.308
1,1,2,2-tetrachloroethane 0.011
Trichloroethylene
0.012
Perchloroethylene
0.0023
Chloral
0.267
Ethylene chlorohydrin
0.064
2,2-dichloroether
0.0009
1,1,1-trichloroethane
0.0044
1,2-dichloroethane
98.89
0.0005 0.0024 0.275 0.0073 0.0059 0.0072 0.012 trace 0.249 0.0043 0.0011 0.0030 0.549 0.408 0.074 0.017 98.38
0.0004 0.016 1.00 0.026 0.013 0.017 0.026 0.034 0.089 0.0011 0.0083 0.0020 0.208 0.144 0.012 0.016 98.38
0.020 0.0051 0.388 0.0094 0.0077 0.0090 0.016 0.018 0.306 0.0092 0.011 0.0023 0.258 0.091 0.011 0.0075 98.81
Notes: (1) CO and CO2 in vent gas from S-307: 0.23 and 0.32 mol %
(2) HC1 content in S-309 aqueous phase: 57 g/l
(3) Catalysts:
KOC-101 for R-301, -KOC-R2 for R-302, KOC-R3 for R-303 and KOC-102 etc. for R-304
(4) Acetylene in feed HC1: hydrogenated
-2
CCR 0000180A4
AP
t t -tft *(!?
t M n + r PW-U
** NO.2-PLANT **
Op
CK-'O
OXY REACTOR ?7"J <301,302,303>.
GJ I
* <* ARP
52-11-13 1l:16
HCL FEED
7022 M3/H
REACTOR
R-301 R--302 R-303
n7"i CHCL
AP
0.20 KG
0. 24 0.31
7000 M3^H *tO
0.00 KG^DAY 0. 00 0. 01
CCR 0 0 0 0 1 8 0 4 5
dp OXY *7J KU^h"' 2-PLANT
I--711.
2-MONTH
I
11