Document dQaG78LQ9E28Yjqj4RQvDmy8q
AUTHOR*. o . M ason Hughe**
TITLt: A N A LY S IS OP DELAWARE RIVER WATER SAMPLES
Monsanto
11394 COPY!
MONSANTO RESEARCH CORROTATION / DAYTON LASORATORY / DAYTON. OHIO 45407
ESC - PATTON lOIM /HC1d">
ANALYTICAL tvpi o> ftfPOfli
REPORT NO. MDA-370 JO* PROJECT NO 483.4110
OATI April 22, 1983
FILE COPY
00 NOE REMOVE fROM HIE
RE ROD COVERED
TITLE ANALYSIS OF DELAWARE RIVER WATER SAMPLES
AUTHORS B. Mason Hughes
RECEIVED
APR 221983
AtSTRACT:
O vsanio-DAYTON
LfclNTRAL FILES Samples from the Delaware River Pla.it were analysed for specified organic compounds. The results of these analyses are shown in
this report.
Technical Approval: Research Group Leader
Approved by:
1
R. F. Ivory cJ Environmental Science Center Service Project Manager
Approval date: */.?.'//J
COMPANY CONFIDENTIAL
MPT. NO.: HDA - 370 ^
COPYNO.: %
HONS 022591
COFY NUMBER
1-ft C. Jaaro
1290
7 R. P. Ivory
12S0
Central Files
12 SO
9 Technical Reports Libr. R2C
ABSTRACT ONLY
R. M. Scott
H. L. wllllaae N. B. Hltatr H. A. Holtermenn
1250 02B 1250 1250
COMPANY CONFIDENTIAL When no longer needed, or upon requeet. return thie report to Central Filet, Dayton.
HONS 022592
UCTtWCICTIOW 11394 COPY 1
Twelve tuple* and (oar duplicate eaaplea vers received (roa the Delever# River Pleat (or analyaie o( benzyl coapoaade and ttoclor 1240. lha aaaplaa vara (iltared and the eolld realdee and (lltreta analysed using nethode prevloualy deacrlbed.il)
RESULTS Saaplat, duplicates, aethod blank* and atandarda war* analysed. Tablet 1-4 show the result* of the residue analysis; Tablet 5 - I show the reaulta of the filtrate analysis. No bensal chloride, wits a level of detection of 1.0 ug/aL, was detected in any of the staples.
DO NOT REMOVE FROM FILE
(1) Monsanto CSC Report No. MDA-3S9, Job No. 403.40(0, April IS, 1003.
1 HONS 022593
NNGNBS-S/S-1
nau i. HSH.TS or cviuin oc/hs analyses or scsiMin non dcuwase atvta rum tarn iwtn
403.41110
April 7. 1003
I-23D
1-27D
Ml< Identification 1*390 1-43-1 1-43-2
l-40-l
ImIvU BenMldehrde aowyl chloride aoaoyl alcohol Oroclor 1240
aoactor IMa
Analysis Method CC/NS
GC/NS
GC/HS
OC/IO
oc/oc
L.O.S.* 1.0 1.0 1.0 o.s o.s
Mb NO NO NO* NO
Concantratloo (ua/L) NO NO NO ND NO NO ND m NO NO ND m HA aui NO NS NO ND ND m
m ND'' 2.0 0.14 OJt
111
1
!
fimrn
OMlyoia
Nothod
_________________________ (\)___________________________________
GC/NS
41
120
70 07 97 40 n
I-ClfhOMl-^
0C/NS
43
100
04
09 UG 44 77
I.Kll-tUNM-l)
GC/NS
42
93 SO 49 SO 20 32
Him <io CteyotM-Oii
GC/IB
40
140 130 120
90 39 SO
GC/NS
40
110 110 110
99
M
73
K tatfaction Ihnhir
2100-S 2170-S 2171*9 2172*9 2170-9 217S-G
Sa^le *ol. Extracted (L)
1 1 i1i1
Vo.l. lltit of *iK(la 1> tt/L. Sh mm datactad With a detection Unit given by the l.O.D. nlw for ooch caagnund.
*aa Mt Mifud.
HONS 022594
WWES-S/D-2 TAIL! 2. RESULTS OP CAPILLARY CC/HS ANALYSES OP SEDIMENT PROM DELAWARE river PLANT HATER SAMPLES
4E3.41I1S
April 7. ITS)
Sarnie Idtntificotito
Aatlrtt NmMtlifk
Antlysli Hetfcod
GC/NS
L.O.D.* 1.0
1-48-2 -H_Db
1-llflfik-
1-48-3
48-3
1-53-1
1-S3-2
Concrntrstlon (ua/Ll NO S.4 mb
1-54-2 MB
teeeyl cklerlie
cc/ns
1.0
NO
NO
HD
ND
MB
m
ieoeyl tlcokol
CC/HS
1.0
NO
l.S
1.1 4.1 10*
0.84
MB
Asocltr 1244 Artelor 1244
hrrmtt Solkiao Ceosound Pfctool-d,
CC/HS
GC/SC
AMlytls Ntlhod CC/HS
o.s
o.s Aaount edded (M/l)
41
NAC NO
100
0.44 0.74
N4 NO
0.17 0.38
8.14 4.42
lot 1.1
Atcootnr <\)
TO70 44 70 118
l-Cl-pkeoel-d.
GC/MS
43
120
80
43 118 128
91
1.2-Cl| Iimhi-4)
CC/HS
42
47 38 18 47 42 44
M-4,,
GC/NS
40
41 34 40 V 43 47
CkrytEoi in
OC/NS
40
SO 47 100 84 72 44
K MtrocUeo Maker Mfb M. iRtrected (L)
-
2174-4 1
2177-4 1
2170-4 1
2179-4 1
2144-4 1
2144-4
t
ltait ( Muctloa la p/L. *W mm 4rttct#d vlik s fettctlon Halt given by tke L.O.D. veloe for tick rnopmewl.
*MR ml tMlyaed.
HONS 022595
taau l. Damn or erniun oc/io Naums or snmn non ocumat um run aona iwnrt
411.OHIO
April 7. 1001
AMlvte oaooMtkydt myl cklorl* amyl olcoaol Oroclor 1140 troclor 1240
11
JkMlyiif ItelM GC/NS
GC/NS
ccm
GC/NS
GC/1C
t.O.D.* 1.0 1.0 1.0 o.s
. o.s
S*U Identification
I1-23-0-
duplicete
1-43-2duplicate
1-40-2duplicate
[Mmaopl-l1c-tul
Concentration (M/Ll NOb NO ND ND
ND ND ND m
1.2 O.OS 0.40 O.H
MC NA
M
0.72
ND ND ND
1.2
111
iMlyili tarraaott Solklao Caaawa* NttkaO
______________________ attmry (\)_____________________
rkml-Ot
GC/NS
41
00 SO 04 u
2-Cl-akml-4
GC/NS
43
110 100 100
TO
1.1-C1, Nmim-6
GC/NS
42
02 7S 74 43
lyraHii
OC/NS
40
0$ 40 SO 34
Ckrpm-0,1
GC/NS
40
04 42 40 S4
aac latroetita Makar
2I01-S 21S2-S 21S3*S 2104-S
Oml* *! OatraetiO (1)
-
I111
*1.0.0. Halt of fctoctioa la |*/L. Si am fetactoO 1U> littclla Halt ylvta toy tba L.O.a. nla (or rat a*ow4.
Sa aat mlyio*.
HONS 022596
WOSS-S/t-4
nau . wtui or curiiAMT ac/m WU.TSI] or nram non ocuunw mu turn MlTVS -win
W) 4lll*
Mil i. INI
Mil Idntificatioa
Netted Netted Netted Blank lank Blank
AMlVtl MMtlOrfcr*!
Analysis Netted oc/m
L.O.t.1 1.0 ^0^
NO
M0
tatyl cklorltr
ocm
1.0
m
NO
HD
Mql tictktl
ec/m
1.0
m
m
NO
krtclor IM*
ec/ie
o.j
wc M
M
krttlor 1244 Ntaol-Ot
CC/IC
OS
m
NO
MO
4*0unt AMlyiit addtd Netted tvo/U
lecenrv I%1
ec/m
41
47 41 04
l-Cl-*ll--1~4
OC/HS
41
120 no 100
l,t-Cl|-kton*t-4(
cm
42
M Of 42
lyrtot-Oit
OC/NB
40
74 40 34
Cte|MM`l|t
oc/m
40
73 73 41
we (atrtctli* Mir
3173'$ 210S-S 2107-S
(tgli 9*1. Wtroctt* (t)
111
Vo.*. Halt of Oattctloa U */L. > mm MmM rltt * klKIla Halt girt* kg tkt L.O.*. rtlnt lor tack capoaad.
Si at aatlym*.
"
1
u 1
M
*
S
1
1
HONS 022597
NMU-i/t-S TMIS S. HMH or CATILUST OC/W MU.TK3 Of rlLTSMB flOR DOUWM8 IIVIR KMR tn OORTIM
403.41111
April 7. 1003
1*230
noli Identification 1-270 1-300 1-43-1 1-43-2
1-40-1
Aaalvta OiaailOibyOt
AMlytii Method
OC/RS
L.O.D.* 1.0
NDb
Concentration (n/1)
NO NO NO m
HO
Oaaayl aMarlSt
ec/w
1.0
MO
MO
NO
MO
HO
1.1
Oaaayl alcainl
OC/Ni
1.0
MO
MO
m
m
m
2.1
kraclar IMO
OC/M
o.s
NAC NO
MO
n
m
0.30
Oraclar 1240
OorroatU Oaikiaa Caniuad rhtaal-S.
GC/tC
tMlpil Method GC/IB
05
iMUAl AM (M/l)
41
MO NO MO MO
0.17
________________________ Ottaaanr (V_______________________ 7.0 42 37 40 27 u
2-CI-plnaal-S.
GC/MS
43
32 110 ISO 120 70 ao
l.l-tlt Iwiaa l)
OC/RS
42
10 00 120 2 47 72
OyraafSta Chryaaaa-0||
OC/M5 ec/M
40 40
20 120 110 04 0 as
10 OS K 04 OS ia
HOC latractlaa M^ar lapli M. SatractaO <l)
-
2100-0/M 2170-0/N 2171-0/R 2172-0/11 2174-ora aiTHa
1 1 1111
*1.0.0. Halt of Satactiaa la pg/L. No a Mat Sotactatf vltk Satactiaa lialt giaaa by tin L.0.0. aalaa far tack *00 aat taalyaaS.
HONS 022598
MWU-S/-t
mu t. msoits or cwauunr cc/n mints or nuno nm nuwux um run am anus
403.41110
April 7. 1003
awl. lOmtlfteatiaa
1-sUfik1-40-2 1-40-3 40-3 1-53-1 1-33*2 1-54-2
kMlyslt
___________ *or*_________ Hvthod
OoaoolMr*
PC/Rt
L.O.D.* 1.0
mb
Conc.ntratlaa (im/L) m m 200 m
tm
koncyl chlarM. Omfl olcohpl
oc/n
1.0
HO
m <100
m
m#
oc/m
1.0
m
m
m 1.2 a It4 14
m
Oroclor 1140
ocm
o.s
Oi*
0.00 n
<0.5 HO
0.S0
Oroclor 1140
0C/IC
o.s
m
0.30 m
<50
0
0.00
Oaolyala SI?
Mrmoto klUa Cwound IbIM MO
Oacaaanr (%)
'
rk.o.1-0.
oc/m
41
It 20 20 --i-- 20 20
1-C1 nuK
oc/m
43
M 73 00
05 0 *
oc/m
42
43 44 47
so 32 '
linHil
oc/m
40
77 70 05
m 30 '
ckrrooot On
cc/oo
40
72 70 20
7 IS
M lotracUoa Makar
-
2174-0/0 1177-0/0 2170-0/M 2174-0/0 2I0P-0/H 204-a/
Male *al. OotrocM (L)
-
I 1 1 1 1 a.
*1.0.0. Halt ot Ottoctlaa la Hf/L.
No oooo OtuM *Uk o dtuctloa lialt glna by tbt 1.0.0. nla (or ooch emfomd. *00 oot awlfon.
* - kltfi kali rrtsrat. Mpll M U b. OllattO.
M0NS 022599
mm-tn-t mu i. mun or ctmun oc/m mums or mm not ctutiua urn rum on iprw
403.41110
Oprtl 7. 1001
tailt MntnTcitlH'
1-23-D- 1-43-2- 1-40-2- 1-40-3- 1 duplicatt duplicate iduplicata IdupllcaU I
iMlvtl 0noilf>b|i
loaayl (MarMo
Onalyais MtM oc/m
oc/m
L.O.D.* 1.0
1.0
m*
m
Caacaatratiaa laa/LI NO HO NO
NO NO NO
Omari oltobol
oc/m
1.0
44
2.3 2.0 1.4
Oroclor IM0
GC/NS
o.s
me M
NO
0.41
ftroclar IIN
oc/oc
OS
NO
0
HD
0.11
Oarraatta taiklaa CaaaiaaO
taalytis MthaO
iMWl OM
ioo/U
Noun IU
fi
6C/M
41
27 30 20 24
f-Cl-ffcaaal-4'
oc/m
43
S 44 44 SO
1 .Klfloam-l)
oc/m
42
SI 44 30 37
ryroat-Oto
QC/NS
40
S4 4S 33 42
CWyaaat-On
oc/m
40
41 71 14 42
mC btractiaa M^or
-
2101-0/M 2102-0/M 2103-0/M 2104-0/M
fimlo 0ol. OatractaO (L)
1 1*1
*1.0.0. Halt of Ortactlaa 1b H0/t. ^lo atat OtMtrf oltk Oitoctloa Halt glna by Uw L.0.0. volao for oack cayMai.
*00 Bit oaolpotf.
1 '
HONS 02260
tmu . msxts or cwiiun oc/ib nmitsu or riinmo non ncumu uvu nm nia imvus
4*1.4111*
April 7. 1**3
Saaala Idaatlticatia*
Method Method Slenk lank
Method Slenk
AMlytis
____________Saslxi*_________ Method
(mmim*
gc/hs
aMyl cMwl6
cc/m
L.O.D.* 1.0
1.0
m
Cancaatratiaa (ua/L) NO NO
HD NO
Myi ictoi
GC/HS
1.0
HD
0.94 HD
Meter 124*
sc/n
0.4
** ns
fi
InclH IMS Mnau MUm C*mmh*
oc/tc
AMlyala MtlM* GC/M
o.s
Aaaunt ***4 Ml
41
m
13
HD 33
M
m
Racavarv IU 21
MlfkMWl-4,
GC/NS
43
33 S2 43
t il-tlftlMW*)
GC/NS
42
24 $2 30
rpwiii Bl--l *l MC MrMttea Makar
OC/NS
40
21 92 31
GC/NS
40
17 32
S.G
2173-i/N 2i*s-*/a 21*7-*/*
*> tel. Mracta* (L)
*
111
V*.l. IWt if *atactla* la Pf/l. Vl MM *atacta* aitfc *atactia* Halt fim by tha L.O.*. valoa far rack caapaoi*.
*m M4 Ml|H4.
MONS 022601