Document dQ6peOGOXO4KYe6xb591J3LJQ
M M 6 - 0175
BIODEGRADATION (BOD/COD)
TEST SUBSTANCE________________________________________________
Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-783. (1Octanesulfonic acid) (CAS # 2795-39-3).
Rem arks: The 3M production lot number was not noted. The test sample is FC-783 (cc784-1). Current information indicates it is a mixture of 1.0% PFOS, 2.0% Sultone foamer, 2.3% sodium octyl sulfate, 1.6% polyoxyethylene monooctylphenol ether, 0.1% sodium lauryl sulfate, 25.0% diethylene glycol monobutyl ether, 0.05% tolytriazole, and 67.95% water.
The following summary applies to a mixture with incompletely characterized concentrations o f impurities. Data may not accurately reflect the biodegradability o f die fluorochemicai component o f the test sample.
M E T H O D :________________________________________________________
Method: Not given. Type: Aerobic GLP: No Year completed: 1979 Contact time: 20 days Innoculum: Secondary influent collected from the Metro Wastewater Treatment Plant, St. Paul, MN
RESULTS____________________________________________________
Biochemical Oxygen Demand (BOD): 5-Day:
13-Day: 20-Day:
190.000 mg/kg 470.000 mg/kg 560.000 mg/kg
C O N C L U S IO N S
No conclusions given.
Subm itter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133
DATA QUALITY___________________________________________________
Reliability: Klimisch ranking 3. Study lacks description and records of the method followed. The inoculum is not properly characterized. Sample purity
002585
was not properly characterized and the study lacks analytical confirmation of the amount of fluorochemical proportion in the solution. REFERENCES____________________________________________________ This study was conducted by the 3M Company, Environmental Laboratory, St Paul, MN, Lab Request number 4896S, 1979. O T H E R __________________________________________________________ Last changed: 6/26/00
002586
U L T lM A T T t fcbOD
e J J flR M M C fJ T A L L /V o 'R A ro Y p A T A S t f G e r
C c w P o a /J i): F C ' 1 $ 3 A ajA l Y S t : j c q . DAt : 6 -< 5 > -^
BEST COPY AVAILABLE
S A iH P t c o W C e iJ T A ^T io ^
S *O *r ^ /
l( * * 0
3 Z .0
2 -0 0
M
i' i
C A tfe R A ftG = ________________ _ ; i ' i
B oD s" 09UT / f c - 4
1 4 0 ,0 0 0 % 1 0 /D O O
, qo, oo
o
> 3 7 ^0 0 ^
4 0 ,0 0 0
1& o D | 5
b o ;d 2 lo
V 7 0 ,0 0 0
>W
O /0 0 0 * 9
> Z Z 0 ,6 O
t
1i :
1`
;
d OOO
W O /O o o
>6 , 0 0 0
G ie tJ e -fiu F t y o T f i o T E ?
' i; 0 'V M t d J ^ T ^ /c U ^ C ^ 7 V
Z 2"
@ ^ '%Mu*44*# x M A ^ tJ L & t J f^ 4X k.JP ku^
H o W t U J A ; 2 - > y / - i i&O <^y> / i ^ V yv1 lu A - '-fo
:< !
'
' ' : " - " L a Z- ~X ^^ O
(
t
'b ljtA * - ' bJpU y**-? j / # u ^
Z>
VA. c^yJP r^rbt*. s**^e**4+*t& *^ ^UaUa-# ,
:
jiuc% u~
<<>u V ^ ^1/
Z)0 i 1^ /' a
;VA
v /#) C JJu~J
( u iv O
'/ / i u r d U u J u rtU J V* V^A ju ^ u P
J t * * * A U fs y*K i^' C A 4. .^ V < *6 4' 4 ^"*R < W
.. " ............................. .......... '"
:0 0 2 5 8 7 ,
- O R J M 10440:4 R W O
Bottle No.
Sample Size
s *s 51 . .S i
t>Mo o,$o
/*
ENVIRONMENTAL LABORATORY
B ^ 'C S f'fiS J A IL A B L E
Blanks: ________ , ________ , ________ , ____
1<U. V t 7 i > i
Date: P i ft. V) 1.
Dilution Water:
ty i Bk. A v / *
^aeJ*L.
Description
^ Depletion
/H a y
F C - 7 S3
! * &
- + 1 S 0 s J t*
O .Q O iO *
}
Sf/>0 6 ^ 0 M o SCoo
%<*<> 2 -r ^ O
i f <<s-
5 " - Dev BOD
Ava.
/^ O .o o o S
2 i 0 tooq ? JlO,oOO ./
^ 3 7 .o o o
- - ,* * . e. -- .
Jr / / i
/c c & n Z / ^
_
D ./.
-\A ' -.:r . v . i - r ,>
mu
k C**jQ c**-&*.
!>, d .
t ,::i"
tfy r
'
< 'V
V
/j A A
\X ,
V 'u
w < -V s
-
--
--
002S 88
ORM, lOt'lQ- PWO
Bottle No.
Sample Size
s -s _51
OMo O,%0
t'b ft
Blanks:
ENVIRONMENTAL LABORATORY BOO WORK SHEET
BEST COPY AVAILABLE
<i- V T J <*>
Dilution Water:
t y i '2 - m frJ,'
Bk. A v / __ 1 ___________ __
Description
F C - "7 *3 f'S j - ^ 2
0. OOb0
<7
^ Depletion
( 3 Dsy b o d
Aq.
Mo & 90
*
<0V"
--
*** --
(nO.OMsmAt
> 1 2 o 'o o o
; V * *-'K
-V.
A ti.0
: >
. 'I,'
*' '. i ' l'- '
' & :
t*:
(
'
.1 .
/ ><\
T T t t T ^ i <? ;
'
002S 8
O R * IOUQ-4 W0
Bottle No.
Sample Size
0,^ 0 S 'S O,%0
lt(ff
f0
ENVIRONMENTAL LABORATORY
B E ^ ff^ M lL A B L E
Blanks: __________ , __________ , __________ , ____
^faNo. V Y V to Oat: 1& 7`/ 4. V XdLn,
Oilution Water:
Seed:/L^. L a -2 -j^4y6r*
Bk. A w / '
Oaacription
F C - 7 *3
i# y o j - i s o I'vJ t'* - C.OOt*m
4
/ "S a v
Depletion P O Day BOO
i/* o 2 i> r a t f --
/ V* j"
f.\-L IS a fS i
M SI
_ . , ' li . , ;<' k:d>
- -v ;-. -..' *. .
(
r (
\
- I P 1'
A
U . P TT l/7
,o b (" ji
r tT
- 7 -
G 0 2 S '5 l
4A I
*W O
)ttle No.
23
^2 22
IJ V 2
Sample Size
-- --
--
-- --
ENVIRONMENTAL LABORATORY
BOD WOpK SHEET
BEST COPY AVAILABLE
Blanks: ___________ , ___________ , ___________ . _______
Date: /-?-"7*)' id.0.
Dilution Water: /% P_______
Sd;
<?y*- -
Bk. Avg. ^
' _________ .
Description
Depletion ' 5 ^ - Day BOD
flsjZtfjrv %,`i ' r z . i o
0,7JS~
0SSJO 2'ieO OxbO
t
? *& r S . y r
/30
*.70 2 Y r
Ai!c>. t>e.f>c\
0 ,3 2 * "
^ fvo S -Y s " S //0 ^ '3 *
*'
C
Avg.
7 *9 3/
jr
y , 9 d /rn & L d a J 3 * 7 o " 7 * ^ 0
( -y^Z akaJL / U A . 3oOy*P 5?,S o l . o o
J3 J2^4JL*Ac-cl oUtutlfY!
` to
/7 H-2.0}
3 *7 0 <r,3o
Em/* ^ r. -
<rv- e***J&* CjYyAjtsCA&ti1 V"
--7 )7* kpAiZZ'o i s 3 . J T - 6 1 nr**i Jt D O
7V# 7
73 78
J2-
Y
5"
9
p o t s n > . / o /SV~m a &JUuc4<Jl.
^ / 5 "D-v\<9
/plA. fM % ** V
3 / 7 o ?#o o 3 . 7 0 S-/S2T
` /JO s .*TM ^ - 8 r
z%02 / 0 ^ / j e *
22-0 23o
.._1 _ ...
/ /
4- fix ft ,, /vils rf
/S 'S 'Y 5 Y2 72 5
ys"n s
Y $r<T3 s
-.
7. (T
./T* ^r.V/4r!t f^
002591
I 0C2CJ-4 P W O
ENVIRONMENTAL LABORATORY
BOD WOflK SHEET
BEST COPY AVAILABLE
Blanks: ___________ , ___________ , ___________ , _
Date: 9 " /% -" ? * / (a)m . 5<-x . Dilution Water: / P
S^d: Pj.si&c.Z uz, -
Bk. Avg. *
'
eNo.
Sample Size
Description
1#.<'|,d. 0 ^ ! Depletion J)A -Day BOD
Avg.
13 / /-I'D S" -- ) z --
IZ -- --
2- --
/u s " .7 7,t<s V-frl'SO
M o 7<2 fv&Sforh --
5s.*iO W5** *3.90 fr5T &$ ^rr
'7
A3 /.rj< A/
'1
11
>1 .. S . l U /3
-
.../7
16y& \^ C aJ 3.90 5 ^ 5 "
muJL fus\. 3oc?W *<S<> 3.7P - J
%&> 2,00
H-z.0}
3/70 --
UA**d? "1
/tytx*P
,27 ?-/ V
73 5"
75? 6
./5PZ> St 7 > . / o
./S V m a &JUoc^<Le
_ilrr~& ^/S1)-YV*q
ia^S W ce
/fiiA- f
V
X,7o </.><''
Ur
S**i0 li,6>
. *sC /K it s
`t 'S r f V s S n z S ysfy s m 3s Vsrr3 S
<
f, ' p /*i S^y (,J . w ^ "1 o
/ / v^l n
002592
4 10 ^w '4 **wO
ENVIRONMENTAL LABORATORY
Blanks:
bO T & T O a iu b l e
Date:
Lt).Q,
Dilution Water: /% P_________
Sed: P iS j'x jz . -
Bk. Avg. ^
' ____________ ;
tieNo. 3
'ol ir
22. 13V 2
SampleSize
-- --
.--
-- --
Description
^ ^ ,J r x 'A ,s z A J S ld * & 4 J
/ o - o ^ Depletion'
ff.sra M 8-1st
0,< s -
^ 2 r 0 UffyttUXt^/Ar\1r-
KAO H 'l0 % el 0 $,/*>
-
/3 DayBOD
,
1fl-
Avg.
* { * ^ZcjlJP
tn o n r tr
*/ * '1
a lu L a^ x. 3OO-y^fi <X,%0 <cUO
?/ / 3
oUZu&Ai %Tt>
f' n
3/70 /.(.o
y/vx J -IJ*
0
1
i
*7 */ 73
-7 Jf
24
5"
/SDnm a GM oc&eu &ST-& ^/SV-y^-a
8/*0 ff/io 3,A>
<vi l s
Y Z irz
/SfVS
ZTL s ysf</ s
ym s 3s
,.
a ro ^ M 2.^0
25~0 15*o
.
__
k. 7O 7'
A *XQ
002193