Document dQ6peOGOXO4KYe6xb591J3LJQ

M M 6 - 0175 BIODEGRADATION (BOD/COD) TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-783. (1Octanesulfonic acid) (CAS # 2795-39-3). Rem arks: The 3M production lot number was not noted. The test sample is FC-783 (cc784-1). Current information indicates it is a mixture of 1.0% PFOS, 2.0% Sultone foamer, 2.3% sodium octyl sulfate, 1.6% polyoxyethylene monooctylphenol ether, 0.1% sodium lauryl sulfate, 25.0% diethylene glycol monobutyl ether, 0.05% tolytriazole, and 67.95% water. The following summary applies to a mixture with incompletely characterized concentrations o f impurities. Data may not accurately reflect the biodegradability o f die fluorochemicai component o f the test sample. M E T H O D :________________________________________________________ Method: Not given. Type: Aerobic GLP: No Year completed: 1979 Contact time: 20 days Innoculum: Secondary influent collected from the Metro Wastewater Treatment Plant, St. Paul, MN RESULTS____________________________________________________ Biochemical Oxygen Demand (BOD): 5-Day: 13-Day: 20-Day: 190.000 mg/kg 470.000 mg/kg 560.000 mg/kg C O N C L U S IO N S No conclusions given. Subm itter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY___________________________________________________ Reliability: Klimisch ranking 3. Study lacks description and records of the method followed. The inoculum is not properly characterized. Sample purity 002585 was not properly characterized and the study lacks analytical confirmation of the amount of fluorochemical proportion in the solution. REFERENCES____________________________________________________ This study was conducted by the 3M Company, Environmental Laboratory, St Paul, MN, Lab Request number 4896S, 1979. O T H E R __________________________________________________________ Last changed: 6/26/00 002586 U L T lM A T T t fcbOD e J J flR M M C fJ T A L L /V o 'R A ro Y p A T A S t f G e r C c w P o a /J i): F C ' 1 $ 3 A ajA l Y S t : j c q . DAt : 6 -< 5 > -^ BEST COPY AVAILABLE S A iH P t c o W C e iJ T A ^T io ^ S *O *r ^ / l( * * 0 3 Z .0 2 -0 0 M i' i C A tfe R A ftG = ________________ _ ; i ' i B oD s" 09UT / f c - 4 1 4 0 ,0 0 0 % 1 0 /D O O , qo, oo o > 3 7 ^0 0 ^ 4 0 ,0 0 0 1& o D | 5 b o ;d 2 lo V 7 0 ,0 0 0 >W O /0 0 0 * 9 > Z Z 0 ,6 O t 1i : 1` ; d OOO W O /O o o >6 , 0 0 0 G ie tJ e -fiu F t y o T f i o T E ? ' i; 0 'V M t d J ^ T ^ /c U ^ C ^ 7 V Z 2" @ ^ '%Mu*44*# x M A ^ tJ L & t J f^ 4X k.JP ku^ H o W t U J A ; 2 - > y / - i i&O <^y> / i ^ V yv1 lu A - '-fo :< ! 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Jr / / i /c c & n Z / ^ _ D ./. -\A ' -.:r . v . i - r ,> mu k C**jQ c**-&*. !>, d . t ,::i" tfy r ' < 'V V /j A A \X , V 'u w < -V s - -- -- 002S 88 ORM, lOt'lQ- PWO Bottle No. Sample Size s -s _51 OMo O,%0 t'b ft Blanks: ENVIRONMENTAL LABORATORY BOO WORK SHEET BEST COPY AVAILABLE <i- V T J <*> Dilution Water: t y i '2 - m frJ,' Bk. A v / __ 1 ___________ __ Description F C - "7 *3 f'S j - ^ 2 0. OOb0 <7 ^ Depletion ( 3 Dsy b o d Aq. Mo & 90 * <0V" -- *** -- (nO.OMsmAt > 1 2 o 'o o o ; V * *-'K -V. A ti.0 : > . 'I,' *' '. i ' l'- ' ' & : t*: ( ' .1 . / ><\ T T t t T ^ i <? ; ' 002S 8 O R * IOUQ-4 W0 Bottle No. Sample Size 0,^ 0 S 'S O,%0 lt(ff f0 ENVIRONMENTAL LABORATORY B E ^ ff^ M lL A B L E Blanks: __________ , __________ , __________ , ____ ^faNo. V Y V to Oat: 1& 7`/ 4. V XdLn, Oilution Water: Seed:/L^. L a -2 -j^4y6r* Bk. A w / ' Oaacription F C - 7 *3 i# y o j - i s o I'vJ t'* - C.OOt*m 4 / "S a v Depletion P O Day BOO i/* o 2 i> r a t f -- / V* j" f.\-L IS a fS i M SI _ . , ' li . , ;<' k:d> - -v ;-. -..' *. . ( r ( \ - I P 1' A U . P TT l/7 ,o b (" ji r tT - 7 - G 0 2 S '5 l 4A I *W O )ttle No. 23 ^2 22 IJ V 2 Sample Size -- -- -- -- -- ENVIRONMENTAL LABORATORY BOD WOpK SHEET BEST COPY AVAILABLE Blanks: ___________ , ___________ , ___________ . _______ Date: /-?-"7*)' id.0. Dilution Water: /% P_______ Sd; <?y*- - Bk. Avg. ^ ' _________ . Description Depletion ' 5 ^ - Day BOD flsjZtfjrv %,`i ' r z . i o 0,7JS~ 0SSJO 2'ieO OxbO t ? *& r S . y r /30 *.70 2 Y r Ai!c>. t>e.f>c\ 0 ,3 2 * " ^ fvo S -Y s " S //0 ^ '3 * *' C Avg. 7 *9 3/ jr y , 9 d /rn & L d a J 3 * 7 o " 7 * ^ 0 ( -y^Z akaJL / U A . 3oOy*P 5?,S o l . o o J3 J2^4JL*Ac-cl oUtutlfY! ` to /7 H-2.0} 3 *7 0 <r,3o Em/* ^ r. - <rv- e***J&* CjYyAjtsCA&ti1 V" --7 )7* kpAiZZ'o i s 3 . J T - 6 1 nr**i Jt D O 7V# 7 73 78 J2- Y 5" 9 p o t s n > . / o /SV~m a &JUuc4<Jl. ^ / 5 "D-v\<9 /plA. fM % ** V 3 / 7 o ?#o o 3 . 7 0 S-/S2T ` /JO s .*TM ^ - 8 r z%02 / 0 ^ / j e * 22-0 23o .._1 _ ... / / 4- fix ft ,, /vils rf /S 'S 'Y 5 Y2 72 5 ys"n s Y $r<T3 s -. 7. (T ./T* ^r.V/4r!t f^ 002591 I 0C2CJ-4 P W O ENVIRONMENTAL LABORATORY BOD WOflK SHEET BEST COPY AVAILABLE Blanks: ___________ , ___________ , ___________ , _ Date: 9 " /% -" ? * / (a)m . 5<-x . Dilution Water: / P S^d: Pj.si&c.Z uz, - Bk. Avg. * ' eNo. Sample Size Description 1#.<'|,d. 0 ^ ! Depletion J)A -Day BOD Avg. 13 / /-I'D S" -- ) z -- IZ -- -- 2- -- /u s " .7 7,t<s V-frl'SO M o 7<2 fv&Sforh -- 5s.*iO W5** *3.90 fr5T &$ ^rr '7 A3 /.rj< A/ '1 11 >1 .. S . l U /3 - .../7 16y& \^ C aJ 3.90 5 ^ 5 " muJL fus\. 3oc?W *<S<> 3.7P - J %&> 2,00 H-z.0} 3/70 -- UA**d? "1 /tytx*P ,27 ?-/ V 73 5" 75? 6 ./5PZ> St 7 > . / o ./S V m a &JUoc^<Le _ilrr~& ^/S1)-YV*q ia^S W ce /fiiA- f V X,7o </.><'' Ur S**i0 li,6> . *sC /K it s `t 'S r f V s S n z S ysfy s m 3s Vsrr3 S < f, ' p /*i S^y (,J . w ^ "1 o / / v^l n 002592 4 10 ^w '4 **wO ENVIRONMENTAL LABORATORY Blanks: bO T & T O a iu b l e Date: Lt).Q, Dilution Water: /% P_________ Sed: P iS j'x jz . - Bk. Avg. ^ ' ____________ ; tieNo. 3 'ol ir 22. 13V 2 SampleSize -- -- .-- -- -- Description ^ ^ ,J r x 'A ,s z A J S ld * & 4 J / o - o ^ Depletion' ff.sra M 8-1st 0,< s - ^ 2 r 0 UffyttUXt^/Ar\1r- KAO H 'l0 % el 0 $,/*> - /3 DayBOD , 1fl- Avg. * { * ^ZcjlJP tn o n r tr */ * '1 a lu L a^ x. 3OO-y^fi <X,%0 <cUO ?/ / 3 oUZu&Ai %Tt> f' n 3/70 /.(.o y/vx J -IJ* 0 1 i *7 */ 73 -7 Jf 24 5" /SDnm a GM oc&eu &ST-& ^/SV-y^-a 8/*0 ff/io 3,A> <vi l s Y Z irz /SfVS ZTL s ysf</ s ym s 3s ,. a ro ^ M 2.^0 25~0 15*o . __ k. 7O 7' A *XQ 002193