Document byYLnjd1bYmeE6axnD31nZroZ
s/v.
C.V.mii9i
D.V. 902,904
DATE PRINTED: 6/02782
CO 32
CODE RT-428-D PKG
fpJUN 1982 ___,,_E2K2a.
("d a t e ;)""
(LOT NUMBER)
!3J
sr.' WT. Is*## LBS .
PROCESSES
( )RT-428-D (A)
() ()
'( )
()
TYPED BY: JLC
STANDARD HRS. _________
APPROVED BY EWK 12/11/81
TIME
PREPARATION NOTES :_____________
N-CQDE
ACCT LBS
NOTE: DO NOT START IE PRESS WILL NOT BE AVAILABLE WITHIN 3 HRS AFTER MAKING. MAKING SUPV TO REVIEW WITH P.R. .SUPV & RECORD:
PRESS WILL BE READY _____M_____ /.______ PR SUP START MAKINGM:/_____MAKG SUPV NOTE: RUN 15' WATER INTO V-904. PUMP WATER FROM V-904 THRU DISTRIBUTOR. IF WATER DOES NOT COME OUT OF ALL D.ISTRiBUTOR HOLES WITH I I FULL FORCE, NOTIFY SUPERVISOR 1i
PREP 1
RECORD: ____BATCHES SINCE SPARKLER LAST
f7f i
!1
CLEANED. AFTER 4 BATCHES, CLEAN, DRESS | ] SPARKLER & PRE-COAT WITH 154= DICALITE
Jl\1 777-A
1 (^FILTER AID `
\JHf \ OBTAIN FOR S11 2-CHL0R0-4-AMIN0T0LUENE-5-
I L SULFONIC ACID
>-0 j 11
7740- -C { /k-\
I^^TOBTAIN FOR S40 3-HYDROXY-2-NAPHTH01C ACID \ JSCINSTALL DV % CV RECORDER & CONTROLLER CHART
r I NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF
1 82-C 11i
;
I L^fREA UNDER V 922 -
i
iCLOSE OVERFLOW OUTLET VALVE FOR DISTRIBUTOR
i
r I LINE AT REAR OF VAT.
i
921/ 931
>
\JST\ RUN 11 * (110G) WATER INTO | L.80-100 DEG F*
HEAT TO
I jrL*ADD IN 2-3 MIN DRESINATE X R 5.MIN 6 RECORD: PH_/*_(9.5-10.5)
\JgT\ STIR 20 MIN OR LONGER TO .DISSOLVE FOR S53
i i 110 1 11 i1
i I 530-A 1 '110 1. .1.
IjJPTJLTrrf UN 31* (639G) WATER. INTO V-922
ON 161982.
ixn WEIGH SODIUM HYDROXIDE IN Vr-926 & RUN IN \ M__________
Ml-
7-D 1 T82 k
\Jff \ TURN ON AGITATOR & STEAM U DUMP IN FROM S2
740-C 1 ,927 *
| 2-CHL0R0
LOT
| 4-AMINOTOLUENE ,,Jk23.
f&zJ ikl
1 1
5-SULFONIC
1.
ACID
MM
4^*3 DUMP IN ACTIVATED CARBON
JWT DUMP IN DICALITE FILTER AID
.U<LNEAT TO 212-214 DEG F WATCH FOAM
----
i 25 113-B i 25 1 0 777-A 1 10
1
RECORD: BY__4r_< + ) IF NECESSARY ADJ TO +BY
| | SODIUM HYDROXIDE
.
ASSUME 50%
7-D
II
DUP050047283
EQUIP 1 MENT |
922 3
CONT
I PACE 2 OF 3 CG 32 CODE RT-428-D (A)
Ls? STIR 30 MIN AT 212-214 DEC F THEN SHUT OFF
I STEAM WATCH FOAM*
* *
RECORD; SPARKLER PRESSURE __K.____ PS I
F NOT ZERO NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER THRU SPARKLER I UNTIL SOL'N IS CLEAR*. MAINIAN*AT Am~i95 F
I FOR S22- RECORD :. START ^Jf***
I TOTAL MIN_^J!*L<L, CLARITY^_Z4fe^_, I HT___ EC F., AND REC,,_|^_*gi DEG F*
USE | N-COD LBS I ________|_
MEASURE WXL_|.IUNITS IN V-928 FOR S33
/AtA. 28-D
ROCHLORIC ACID
M_____7____________________ %
447
DISSOLVE STRONTIUM NITRATE IN 30 GAL WATER | 1|
55 GAL DRUM AT 90-110 DEG F FOR S52
52 |246-B,E
52
WEIGH SODIUM NITRITE IN PT FOR S36^ ^ 3 .
(
725-A i 321
2^ RUN 1" <_J._G> WATER INTO V-,,Jf_f
NOTE: USE CV IF MTY. IF CV IS NOT AVAILABLE
USE V-904
WHEN SI7 COMPLETE, PUMP IN V-922 THRU
I SPARKLER, MAINTAIN .V-922 AT. 1.90-195 DEG F
I RECORD; START^^^wtf, fOTAL MIN_JJ<2_.,,;_
;* \ *
A:
902 6
56* <14550 WATER INTO V-902 IXT DUMP IN CALCIUM HYDROXIDE & STIR tO SMOOTH
I I SLURRY FOR S42
922 I WHEN S22 COMPLETE, STOP PUMP & INSERT V-922
7 OOT PLUG
5A I RUN IN 10* <2070 WATER 6HEAT TO 180-190 F
CIRCULATE 15 MIN THRU SPARKLER.
904/CV 8
PUMP V922. THRU SPARKLER INTO V904/CV
RUN IN 4* <1030 WATER INTO V922 6 HEAT TO I 19^,195 F CIRCULATE 15 MIN THRU SPARKLER
P V-922 THRU SPARKLER INTO V 904/CV , WHEN MTY BLOW OUT SPARKLER INTO V 904/CV
FOUR IN IGEPAL CO-630 I HEAT TO 165-170 DEG. F
j I I 21 I
I 33;l
i I I 6I |
NOTE; IF N-740-C SOL'N (S21&22) WAS PUMPED DIRECTLY FROM SPARKLER TO CV OMIT S'S 31,32 RUN IN 1' <950 WATER INTO V-__2L/ PUMP V-904 AT 165-170 F THRU UNDERSURFACE DISTRIBUTOR INTO CV AFAP <12-15 MIN).
MAINTAIN 165-170 DEG F IN CV* RUN IN N-28-D HYDROCHLORIC ACID FROM S18 IN 12-15 MIN STIR 15 MIN AT 165-170 DEG F ADJ TO 43" <40800 AT32-38 DEG F RUN IN N-725-A SODIUM NITRITE FROM S20 AFAP <5-10 MIN) 6 RINSE IN PT
I 50X3301
57-A
440 62.
DUP050047284
EQUIP I ME NT |-
CV ~\f$7
11, CONT
I I
I
I
MAKING INSTRUCTIONS:BATCH UNIT
PAGE 3 OF 4 CG 32 CODE RT-428-D (A)
STIR 30 MIN AT 32-38 DEG F MAINTAINING +CR, +KI RECORD; TIME START_&i/fc*__,
CR in <+>, KI_ tz. < + ) NOTE:
1) IF CR-, KI-, ADD 20$ "AS IS* INCREMENTS
HYDROCHLORIC ACID RCRD; CR______< + >,
KI< + )
ASSUME 32%
2) IF CR+, KI-, ADD 20* *AS IS" INCREMENTS
SODIUM NITRITE RCRD; CR_;___ _< + ),
KI, _l_<+>
ASSUME 33%
DUMP IN STRONTIUM NITRATE
DUMP IN BARIUM SULFATE
DUMP IN FROM S3 6 STIR 10 MIN ' LOT
3-HYDRQXY-2-NAPHTH0IC ACID
USE
N-CQDE | ACCT
LBS 1
LBS
28-D
1 725-A
""?53~1 246-B,E
A9sS"i 65--A
All. j 82-C
rTss"
\A#S 1 848 I
902 12
m vf?2
I
ADD FOR MAINTAINING 32-38 DEG F THRU S 48
-DUMP AMMONIUM CHLORIDE INTO V-902 4, STIR 2-3 MIN
30X330 20?
57-A 165-A
209
CV |^3 13 I
WITH V-902 AGITATOR ON, IMMEDIATELY AFTER
S42 COMPLETE, RUN V-902 THRU UNDERSURFACE DISTRIBUTOR INTO CV IN 18-22 MIN. MAINTAIN 32-38 DEG F IN CV. RECORD: START, TOTAL MIN,,_^|(._____
___U i I
57-A
PT 4 DURING S43, WEIGH SODIUM H^DRQXI^JNPT ^ 14 45 DILUTE TO MAXIMUM VOLUmI^T+Z-To Og T ' FOR^S
SL_ I 7-D
165'
' CV 15
WHEN S43 COMPLETE, STIR 30 MIN
RCRD PHjSuSL-< 5 .0-6*0> TEMP_.3IL._F (32-38 F)
V
RUN IN N-7-D FROM S45 THRU UNDRSURFACE LINE
4. RINSE IN PT
' '-
STIR 15 MIN & RECORD: PH_&L.<9.-9.8)
yjrso IF PH IS BELOW 9.0 ADJ TO PH 9.0-9.8
; tUi
SODIUM HYDROXIDE V
ASSUME 50%
RECORD: PSi.,DIAZO_r^_<->,BASE_;fc_._ < + >
POUR IN N-246~B,E SOLUTION FROM SI9
STEAM EJECT IN V-921/931 SQL'N FROM S8
I HEAT TO 180-182 DEG F IN 65-75 MIN AND
1 L-RECORD: HT_Z^__DEG F & REC_Zg3' IDEG F
STIR 30 MIN AT 180-182 DEG F.
T ^RECORD: START_^i5i&#_ '
J^J>FLO0D TO 180-190" (+/-18,000G) ,
)#7JrsTIR 5 MIN &-RECORD:
C2.__<8.8?-9.3>
J4r8 I IF PH BELOW 8.8, ADJ TO PH 8.8-9.3
I RECORD PH
____SODIUM HYDROXIDE
| ASSUME 50%
STOP AGITATOR
JaJ\
7-D 7-D
Jl
OPEN WATER VALVE AT OVERFLOW FOR DISTRBUTR AND BACK FLUSH THRU CHECK VALVE AND DISTRIBUTOR FOR 2 MINUTES. SHUT OFF WATER.
OPEN OVERFLOW OUTLET VALVE FOR DISTRIBUTOR
REAR OF VAT.
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!7
CG 32 CODE RT-428-D
DATE PRINTED: <5/02/32
"7~usi~'T"N-coDi ACCT
(A) I LBS I
LBS
I WHEN INSTRUCTED BY PROCESSING "AREA HALFWAY |
|
I | THRU PRESSING
`
I I (1) DUMP IN I OCTANOL
'll | 101 588-A
I , J (2) STIR '5 MIN
V II
10
j
t. :
.. fc *
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