Document ba2jj7RKYXYVYME7zE7ORzY2g

5 * eSh&Ei 6BBNBE3RUN s CHANGE RUN 1 STOP OPTN #33 INJ/BTLSTROKE: 1 1 3 ^4 / ^/'*W 3~/?/&</ c 15.89 HP RUN # ID:1-10 ESTD 1 MAY/09^84 BOTTLE 1 RT EXP RT BREA 2.68 2.68 342 DIL FACTOR 1.0000 E+ 0 TIME 09:11:43 CAL # fR1 1 AMT 4.4457 E+ 6 TTMF A9:11:7R no 104975 confidential 2.98 3.39 3.46 3.75 7.38 ^10.29 U\ 13.82 w 14.60 15.89 18.21 19.84 4715 827 2110 19130 7674 6440 4642 255 79 5549 132 7.939 1.558 3.974 36.032 14.454 12.130 8.743 0.480 0. 149 10.452 0.249 DIL FACTOR : 1 . 0000 1E+ 0 NO METHOD ESTD TEMPI 150 125 TIME1 20. 00 INJ TEMP 400 250 FID TEMP 400 300 AUX TEMP 175 100 ESCAPE TIME 09:11 : 96 DELETE ESCAPE TIME1 4 0 3 125 250 300 100 TEMPI 150 125 125 TIME1. 40. 00 INJ TEMP 400 250 250 FID TEMP 400 300 300 ESCAPE DELETE CHANGE RUN 3 HRNGE RUN 0 3 SHANGE RUN 1 STOP OPTN #33 IN J/'BTL* STROKE: 1 t 3 STOP ESCRPE START "L, 29 -a. as . 3------6 - 76 iL8.99 14.56 15.99 19.87 21.54 3.39 t3.84 '18. 74 7.39 10.31 <5% 31.41 31 .R7 33.59 35.75 HP RUN # ID:1-10 ESTD MAY^09/84 BOTTLE 1 RT EXP RT AREA 2.29 2.29 33 DIL FACTOR: 1.0000 E+ 0 o HP RUN # ID:1-10 BRER 7; MRVV09X84 BOTTLE 1 RT RRFR AREA * 2.29 2.69 2.85 2.98 3.39 3.46 3.75 7.39 10.31 13.84 14.56 15.99 18.24 19.87 21.54 22. 43 23.93 27.53 28.89 ,31.41 31.87 33.59 35.75 33 347 1721 4274 824 1906 19160 7296 6460 4703 265 108 6048 472 31 35 6554 32 123 219 35 129 5869 0.050 0.521 2.582 6.413 1.236 2.860 28.750 10.948 9.693 7.057 0.398 0. 162 9.075 0.708 0.047 0.053 9.834 0.048 0. 185 0.329 0.053 0.194 8.806 DIL FACTOR: 1.0000 E+ 0 CRLIB ESTD TIME 09:11:95 CRL # RMT fRl t 204.240 TIME 09:11:30 00 104977 CONFIDENTIAL REF <"1 RT. 3 a 46 7 w 39 10w31 1 3w 84 18m 24 23 B 93 35 a 75 DIL FACTORS READY DELETE CHANGE RUN 3 CHANGE RUN 0 3 CHANGE RUN 1 STOP OPTN #33 INJ/BTL*STROKES 1 1 STRRTj- r Or 95 :U AMT 99 w 9 1 2 fi 3 . 1 2 1 1 47. 84 1 1 A5. 25 1 021 . 48 1 205 . 4 1 1 1 3 . 95 2.70 3.40 3-89 -- 1R. 29 23. 99 iZJ 7.41 10.34 29.28 O 35.88 coPr'5Jj9^s T0^Tlt,, HP RUN # ID:1-10 ESTD 1 MAY/09/84 BOTTLE 1 RT ^ 3.47 7.41 10.34 13.89 18.29 23.99 35.88 EXP RT 3.46 7.41 10.33 13.88 18.29 23. 99 35. 85 AREA 2059 7276 6484 4695 5869 6572 5748 BIL FACTOR: 1.0000 E+ 0 T T ME 09:11:49 CAL # AMT f R1 1 107.919 2 1259.66 3 1151.30 4 1163.27 5 991.251 6 1208.71 7 1090.98 CALIB 2 3 READY CALIB 3 READY ESTD RTI.I: 7.00 CALIB RUNS 3 CAL # RT AMT AMT^APEA (Ri 0 1 5 j 4 5 6 7 3.46 7. 39 10.32 13.86 18.26 23.96 35.82 9.9900 E+ 1 1.2631 E+ 3 1.1470 E+ 3 1.1653 E+ 3 1.0215 E+ 3 1.2054 E+ 3 1.1140 E+ 3 5.0250 E- 2 1.7339 F- 1 1.7720 F- 1 2.4800 E- 1 1.7176 F- 1 1.8364 E- 1 1.9?0? E- 1 I DIL FACTOR: 1.0000 E+ 0 DELETE CHANGE RUN STOP ESCAPE DELETE CHANGE RUN CHANGE RUN 0 3 CHANGE RUN 1 3 CHANGE RUN 1 STOP 3 3 OPTN #33 INJ/BTL*STROKE: 1 1 3 START; 1 -------*=-------------- -------------------------3.40-------------------- f 1 7.4? 10-36 D0 104979 confidential $ -L -- fl9.92 - 18.31 ! 22.23 r =" 24.04 30.92 . 32.52 - > 35.91 ... 39.60 HP RUH # ID:1-10 USTD RT 2 EXP RT MRY^09284 BOTTLE 1 RRER *$ 3.47 7.42 10.36 13.92 18.31 24.04 35. 91 3.46 7.41 10.34 13. 90 18.31 24.02 35.92 1899 7148 6332 4640 58^ 1 6432 5773 DIL FACTOR: 1.0000 E + 0 STRRT | STOP HP RUN # RRERS9 3 MRY^09/84 TTME 09: 11:42 ORL # RMT 1R) 1 95.424 2 1239.39 3 1122.00 4 1150.73 5 1001.52 6 1 1 R1 . 1 f. 7 1108.54 TIME 09:11:00 ( c: ' i- k DO 104980 CONFIDENTIAL ST7T" rjffsft ?o TEMPI TIME1 INJ TEMP FID TEMP RUX TEMP 150 125 40. 00 400 250 400 300 175 100 125 250 300 100 CHT SPD 0. 50 ZERO 10.0 RTTN 2t 1 FID SGML +B SLP SENS 0.01 RRER REJ 25 I FLOW R 35.0 35. 0 FLOW B 20.0 19.7 $ l f | i ^f 0 aJ i t= 3: a ? 7.09 9 _ 99 21.46 25.94 r/Q*fc 22.94 t ^ o HP RUN # ID:1-10 AREA 2 MRY/09^84 BOTTLE 34 RT RREA AREA * 2.20 2.58 2. 73 2.86 3.25 3.32 3.61 7.09 9.88 13.28 13.97 15.29 17.48 21.46 22.94 25.94 29.36 34.29 WlTL FACTOR: 42 341 1688 4251 839 2148 15930 6416 6746 5061 282 185 6428 31 7594 258 62 5403 1.0000 E+ 0 0.066 0.535 2.650 6.677 1.317 3.372 25.006 10.071 10.589 7.944 0.443 0.290 10.090 0. 049 11.921 0.405 0.097 8. 481 CAL T B ESTD y. RTU! 5 t 0 3 5 4 0 READY ESTD * RTLi: 5. 00 CAL # AMT (R) 1 .0000 E+ lT&e^L^+ 1.1470 ' E+ 1.0715 E+ 1.7054 E+ 1.1140 E+ 3 4 DIL FACTOR! 1.0000 E+ 0 CAL TB RUNS 1 AMT/APFA 6. 7775 FF+ 0 _1_. 7007 F + 0 ?T3 1.5891 E+ 1.5A73 E+ 0 2.0618 F+ 0 c c OO 10498? confidential * RTW: 5 RT REF: 3.61 : 7 . ESCAPE ESTD (1^ RTW: 5 AMT 10 0 0 REF DIL RT 3 61 7 09 .9 8 8 13 2 17.4 .2 2 . 9 34 2 0 FACTOR: ft 8 4 9 AMT 10 0 0 26 14 16 02 205 114 2 3 4 #-2 READY ESTD * RTW: 5. 00 CAL IB RIJNS 1 CAL # RT AMT AMT/AREA (R1 1 2 3 4 5 6 7 3.61 7.09 9.88 13.28 17. 48 22. 94 34.29 1.0000 E+ 3 1.2631 E+ 3 1.1470 E + 3 1.1653 E+ 3 1.0215 E+ 3 1.2054 E+ 3 1.1140 E+ 3 .0,L FACTOR : 1.0000 E+ 0 6.2775 F -- 2 1.9687 E- 1 1.7003 E- 1 2.3025 F- 1 1.5891 F- 1 1.5R73 F- 1 2.061ft E- 1 14 START -L2. 2.58 3. 25 f? 7.09 9, Rft Q 20.26 22.97 104983 , CHFmrNTTA, 34.30 HP RUN # ID:1-10 ESTB 3 MAY/09/84 BOTTLE 23 RT EXP RT RREfi 3.61 7.09 9.88 13.29 17.50 22.97 34.30 3.61 7. 09 9.88 13.28 17.48 22.94 34.29 15690 6360 6752 5066 6556 8054 5743 DIL FACTOR: 1.0000 E+ 0 h I (^HLIE: 8 READY CAL # AMT (R) 1 984.933 2 1252.07 3 1148.02 4 1166.45 5 1041.84 6 1278.42 7 1184.10 c D  25.96 * 27.16 ft 34.33 HP RUH # ID:1-10 ESCAPE STOP 3 MAYX09X84 BOTTLE 22 HP RUH # ID:1-10 AREA X 4 RT AREA 2.20 9 2.58 2.74 2.86 3.25 3.32 3.61 7. 10 9.89 13.29 13.98 15.37 17.51 20.79 22.96 27. 16 34.33 39.22 37 338 1713 4258 836 1932 15940 6212 6478 451 1 261 73 6704 29 7530 57 5186 26 DIL FACTOR : 1.0000 Ki + UJ MAY^09/84 BOTTLE 23 AREA * 0.060 0.544 2.758 6.854 t . 346 3.110 25.660 10.000 10.428 7. 262 0.420 0.118 10.792 0.047 12.122 0.092 8.348 0.042 CALIB 8 READY ESTD ^ RTW: \\ *CAL # (R) 1V"!.i; 1 2 3 4 5 ft 5.00 RT 3.61 7.09 9.88 13.28 17.49 ??..9.w5i AMT 1.0000 E+ 1.2631 E + 1.1470 E+ 1.1653 E+ 1.0215 E+ 1.2054. F+ 3 3 3 3 3 3 CALIB RUNS 3 flMT/RP 6.3082 1.9960 1.7232 2.3953 1.5570 1.5616 EEE- EEE- 4f-3 DO 104985 CONFTOENTTAl DIL FACTORS 1.0000 E+ 0 U o ,m 7 - 06 A. ftfi HP RUN # IB:1-10 ESTD RT 3.59 ...a--oc. 5 EXP RT 3.61 -----7--0S J rj , MflY/09/84 BOTTLE 22 # AMT 1 1016.BB 2 1231.33 DO 104986 1 CONFTDFNTTAI TEMPI 150 125 TIME1 40.00 INJ TEMP 400 250 FIB TEMP 400 300 HUX TEMP 175 100 1.25 250 300 100 CHT SPB ZERO ATTN 2T FID SGNL SLP SENS AREA REJ FLOW A FLOW B .0.50 10 0 1 +B 0.01 35.0 20.0 25 35.4 19.9 ESTD * RTW: 5.00 CAL # RT AMT f R1 1 2 3 4 5 8 7 3.81 7.09 9. 88 13.28 17. 49 22. 95 34.30 1.0000 E + 3 1.2831 F+ 3 1.1470 F + 1.1853 E + 3 1.0215 E+ 3 1.2054 E+ 3 1.1140 E+ 3 DIL FACTOR: 1.0000 E+ S dtfs { <? fi S//^~/8'</ OflLIB RUNS 3 AMT/RRFA 8.3082 F" 2 1.9980 E- 1 1.7232 F- 1 2.3953 F- 1 1.5570 F- 1 1.5818 E- 1 2.0499 F- 1 /&T*& 26.56 30.39 lf:5f 33.98 G*. ff jit^ra+) G/* c /( C r HP RUN # ID:1-10 ESTB 7 MAY/09784 BOTTLE 36 RT EXP RT AREA 3.57 7.03 9.79 13. 16 17.33 22.73 0 33.98 3. 61 7.01 9.77 13. 13 17. 29 22.69 33.91 DIL FACTOR: 1.0000 E+ 0 16270 7512 6918 6546 6810 7320 5827 STOP t^gHTRRT -2*12. CAl f R1 * AMT t 1026.34 2 1489.40 3 1192.12 4 1567.9ft 5 1060.31 6 1143.08 7 1194.47 / I/-Y7 US'S IO A ft. /* */y /*.? 3. * S'- X, 3. ? J". / ? / 3.24 7.05 9 . 81 13.18 20.92 00 104968 C0NFTDFHT1W c c 33. 99 HP RUN # ID:1-10 ESTD 8 MAY r09>'84 BOTTLE 36 RT EXP RT AREA 3.58 7.05 9.81 13. 18 ^17.35 1^22.76 33.99 3.61 7.03 9.79 13. 16 17.34 22.75 34.01 16560 7490 7066 6209 7072 7578 571 1 DIL FACTOR: 1.0000 E+ 0 CAL # AMT (R) 1 1044.63 fmmm 2 1495.00 IAtS 3 1217.63 IIM 1 4 1487.26 u r 5 1101.10 6 1183.37 7 1170.69 i4 r I Il4f % C**mr /jtc 9.C /#.# *2.7 ' Jr-o STOP ESCAPE CHANGE RUN STOP DELETE CHANGE RUN 3 CHANGE RUN STOP CHANGE RUN 1 0 3 DELETE CHANGE RUN 3 CHANGE RUN 103 DELETE CHANGE PUN 3 CHANGE RUN 1 ESCAPE CHANGE RUN 5 STOP OPTN #33 INJ/BTL*STROKE: 1 1 START. i ^18 3 B+ / j jO Tf. tf# /'Ip*. /f S a} /*/ e /t'0 <0 4A P /s*oo /9 0 C y x- */;jx 0* Am V />ia - t f** /0t 2.56 3.23 S: Q DO 104989 CONFTDFNTT AL 16.41 ) 17.17 19.37 20.07 20.72 22.62 24.79 <*0 ^JO 0 A* #*V< r I A*# /<5 4 /jo /*#l t, W-c : 11:?S " 30.35 I*#*//*m ./*/ */// /* jtmiib /A * / i/*i / * fy //irfy , ^V// fA A A 33.65 /*/* *+L i irm^ //*> % ^<cA/ 36.73 t t ac Qi<t P RUN # 11 i ID:1-10 i ESTB RT EXP RT 4 X cS MftY/fPV84 BOTTLE 1 fW/ AtUk*. -- MltM* U, 7 97 63 SaT / *0 A*V SL / vr -/r * 1/ +J - Jv -- /r AREA CAL # AMT 3.57 7. 01 9.78 13.10 17. 17 22.62 33.65 3.61 7.01 9.77 13. 13 17.29 22.69 33.91 DIL FACTOR: 1.0000 E+ 0 16690 201 121 267 9S 135 220 fR) 1 1052.83 2 40.120 3 20.851 50 T 4 63.955 ** 5 6 7 15.259 21.082 45.098 /S~ X Ml * vr * 16. 10 18.24 O' SB: 5? 22.61 25. 13 . 28. 74 29.82 30.43 32.46 *; 33.25 - 34.44 35.37 V s. 6t--l*-t-- ff^r V 337<ra 4: sc --* ifso lev m/a> 39.42 <3p RUN # ID: 1-10 ESTD 12 MRY/09^84 BOTTLE 2 RT EXP RT 2 j 3 . 57 3.61 7 .02 7.01 9 .78 9.77 22 .61 22. 69 34 .44 33.91 AREA 16900 385 271 168 106 DIL FACTOR: 1.0000 E+ 0 STAR CAL # AMT 1R1 1 1R66.08 P 76.846 i".r ti.g 3 46.699 6 76.235 */ 7 71.7P9 /A 6 .V . 0/ S $ % j 13.16 ggEBgsqaB DO 104491 CONFTDFNTTAI 17.32 18: IS # 21.26 22.50 25.30 29.33 30. 30 32.34 34.36 JJL zr 4 -*> -ft;so 600 h i rS* 7*" ysae*/z *S'/S" 38. 12 HP RUH # 13 5 {)D: 1-10 i ^'STD MRY^09^84 BOTTLE 3 RT EXP RT AREA 3.57 7.01 9.78 13. 16 17.32 22.50 34.36 3.61 7.01 9.77 13.13 17.29 22.69 33.91 17190 280 300 73 111 60 40 \i DIL FACTOR : 1.0000 E+ 0 CAL # AMT (R l 1 1084.37 2 55, 888 <*.y 3 51.697 4 17,486 5 17.283 6 9.370 7 8.200 MdV #*. 4.#| 4 .# I *< * J 4, .| 17.30 18.80 25. 10 28.50 ' 30.84 ' 31.57 * 32.80 ' 33.99 35.86 yO#^S or ti&a.*?. 4-- C 73lo HP RUN # g-Ds 1-10 STD 14 MRY/09^84 BOTTLE 4 PT 3.57 7.03 9.78 17.30 33.99 EXP RT 3.61 7.01 9.77 17.29 33.91 ARFA 16900 342 464 76 73 DIL FACTORS 1.0000 E+ 0 START l&. -2- 56 CAL # AMT fR i 1 1066.0A 3 6R.263 S*% 4, afit .*3 3 79.957 5 t1.833 r?.cr * r 7 14.964 z, */ -3.23 f==7. /l' 01 9.77 = 15:1! 14.61 p 16.16 !..> ;Mr 00 104993 00NFTDFNTT6 AOr 1 / . 84 18.67 19.43 21.93 22.69 ' 24.15 26.50 26.87 ' 28.62 30.67 31.16 32.52 ' 34.42 35. 40 " 36.68 j 18:81 (3 ml /So !'OtO </310 if 3 6-* 4;j/o OS <46 HP RUN # ID:1-10 ESTD J RT 15 EXP RT MRY/09/84 BOTTLE 5 RRER 3.57 i 7. 01 9.77 22.69 34.42 3.61 7.01 9.77 22.69 33. 91 16870 206 169 117 49 DIL FACTOR : 1.0000 E+ 0 STOP ESCRPE 5 STOP TEMPI ESCRPE 150 125 125 5 STOP CHRNGE RUN DELETE DELETE CHRNGE RUN CHRNGE RUN 0 3 CHRNGE RUN 5 STOP ESCRPE 3 5 STOP OPTN #13 lD: 1-13 e1PTN #23 y(M-D-Y)DRTE: 5-16-84 (H.M.S) TIMES 1.00.03 CHRNGE RUN 6 3 DELETE STOP CHANGE RUN 8 STOP CHRNGE RUN 6 3 CAL # RMT 1R1 1 1064.19 2 41.118 3 29.122 6 18.271 7 10.045 *>/ <0$ 0 <01 <! DO 104994 CONFTDFNTTAl _ DELETE CHANGE RUN 3 CHANGE RUN 63 CHANGE RUN 8 STOP 8 STOP OPTN #33 INJ/BTL? STROKE: 1 1 A C O HP RUN # ID:1-1 ESTD RT 7 EXP RT MAY/16^84 BOTTLE 6 AREA TIME 81:04:01 CAL # AMT jfr,.rvi> DO 104995 OONFTDFNTTAl r vj 9.83 16.95 23.18 34.37 9.82 17.39 22.82 34. 10 BIL FRCTOR: 1,0000 F+ 0 190 50 105 39 3 32.741 9 5 7.7R5 6 16.397 7 7.995 < < + I ID:1-1 ESTD RT 3.60 EXP RT 3.61 BOTTLE 7 BRER 16790 -.336 CRL RMT tR) 1 1059.14 DO 104996 CONFTDFNTTAl 13. ltf 13. 24 BIL FACTOR: 1.0000 E+ 0 BELETE CHANGE RUN 8 3 r\)HANGE RUN 9 3 ^CHANGE RUN 1 0 STOP OPTN #33 INJ/BTL,STROKE: 1 t 3 35 4 ft. 384 ESTD RT EXP RT AREA 1 >, -; CAL # 1 1 AMT 1O4997 OONFrDFNTrA!