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Tucker
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R&D Laboratories
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Second St.
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Louis
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August 20/ 1969
REFERENCE SAMPLE - BUREAU OF . FISHERIES; MONSANTO SAMPLE #2084
cc R. E. Keller - So. M. W. Farrar - So. W, R. Richard.- GO E. P. Wheeler - GO
Second Second
TO : C. R. Campbell - Pensacola Tuck Dean - Pensacola
We have completed the analysis of the exchange water sample .
120 84 and I have included with this memo a. Xeroxed copy of the
complete run calculations and calibration curve.
Three 250 ml aliquots were taken from the 5 pint bottle and analyzed directly after extraction with hexane and concentration to a specific volume. Sample #201-1 was taken prior to shaking the bottle vigorously, samples #201-2 and #201-3 after. The material extracted is as they reported - Aroclor 1254. Their reported concentration of 274 ppb agrees well with our duplicate analysis, #201-2 and #201-3, which were 270 ppb and 269 ppb, respectively. In sample #201-1, we found 17.2 ppb Aroclor 1254 indicating that most of the Aroclor 1254 is adsorbed by the particulate matter present.
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We also have received the fish samples and the other water
samples which we talked about. We analyzed one of the larger
Bluegills.(65.37g) and found 133 +2 ppm Aroclor 1254.
We will report the results of our analysis of the other samples
as soon as they are completed.
. ..
db Enel.
Scott Tucker
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