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Analysis of PFOA and PFOS in Water Samples from OakdaleMunicipality E05-0184
Exygen Report No. L0004708
Testing Laboratory
Exygen Research 3058 Research Drive State College, PA 16801
Requester
Gary A, Hohenstein Manager, Environmental Operations
EHS Operations 3M Company
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1 Introduction
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2 SampleReceipt
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3 Methods -AnalayndtPriepacraatolry
TWuhalteaeErtx"eypmeo(dnPiFfmiOea)di,fhPooedreitnsuoctmreeodrosc.etpa"enMreeattehilooondm,owjfaeAmsinudasei(esPdFlOooSprrAhe)p,eaDrexedtoaPnmediraunnotraoonzocoaafnhPoeearstfasum(rpFolOoeAdsAi.)anAe scounmdimtaironyoforthsosmaemsspelpeeprraeopnarceainobnocofonubned 1fSouencdtoinnS3e2c.tan 3.1 sndthe modified navel 3.1Water Sample Preparation wFSaoorslthdyepmdriwalisitooherxsStormfa.ctohiofown8(4aS0rP%Esm)aewmtahpalsneuowlsa:es6d0tFo%apnwrsaeflpaearrrewedat1sh0he.w8 aCTthyeSscPaarEmtcpraildtegisedwfgoeers.LoTCuIhtMeeSdcIwMaiStahniaSlimyws.gioosesf. u1s0i0n%gsmeectohasnpcrla.yLACpoMrSioMnSo.f he exvoctwas tensteredtoaudosamplrvelsandenalyzad
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32 SampleAnalbyyLCs/MiS/sMS
r1oHuigghhPrseIsqsuuirtepLhiaqsueiCdhCrhormoamtaotgorgarpahpihccyo(lHuPmLnC.),aBnasaeld uonotfheexatfrfiancityiofinijheectaendaalnydpfaosrstheed schtaartaicolneerriyspthiacasmeoiuntnthoefcoilmuem.nFoelilaoiwviengtHPhLeCsuepiadramtoiboln,epmhaassses,petchteraonmaetbryeprsorveitdaienseadfopriad afndracacugramteeemnendatneslefecdoie,da.nalTyzhinegi8ownisdechraarnagcetoefnoarigcaonfictchoemcpoomupndosu.ndMs oerle eobcsaerurevolendiezeasndd, `quaaganns!etxacitedzstaencadrc.
A`SnompHlPeHe100xsysaftoemcqiunstntrittaestcoandtoanApplodBiosystemsAPI4000wasused to ensyzethe
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Thefolowing grdientwasperformed:
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"Thefolowing paramelerswereusedforoperationofte massspecirometar:
TTaornaizmaeitonerModo PToralnasittonsMontorod SGeaspToGmes0
sew `NeEglactriovsepray 4111355537609,(CCPRO49a959m0(PFoOcSo)sk,e) 37.00 UnCmin
4 Analysis 44 Calibration
PFAO7A-p,oiPntFcOalSiabrnadtionCGPiFvOeAw.aTshaencaalylzbeadtnonipodliesnwdertehprroeupgahretdtehtea0n,a2l,yi5c0e,ls1e00q,u2e5n0,ce60f0o.r `saanmde1S0P00Enpigr(pop)fcuorsaeLdfCdoMrSusMamSrpiaesnsel.yTssh."eCionlsbtrruamleonntrsetsapnodanrsdesvoarrseysprtehpeacroendcuesnitrnagttihoen Wasplftoreiachepoidnt. Using nearr&rossion wih 1xwoghtng.thesie, ynlrcopt
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a0n%decso.afiientofdetrmiation (7)weredetained. Acab curveri acaceptaoble n>
FionrtoheerwedsoutasrineApratcedhneron,Cc.albratncrtarawaremat. Thecalbcurrvesaarotnuodend
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42 Surrogates
W5aGsPaFdOdoAd(0CiFhe"oCmIpFlCysIaOmOpHl)ecIonutsaeidnearss baesfuorrootghaeebfoorttiheeswwaetresrssaemnptle0s.theClPidFOfoAr wsiamtphliansg.amipltehefkalsampleandqualtycont orlesware led 18vokmetcline C PFOArecoveriescanbefoundhAtcha . 43 Laboratory Control Spikes
L`oaafbsPosrFeaOstAom,reytchCoonPtdrFsoOlcsAcp,riaoknecsydi.PnETtGhheSeatnaoabloaybrtosirocsarllysoceroy!wrneetraegsepnprtekp.easrLmeudbsaytahdbdoicwnogorneaockolrnvseoprwikoneecssboetnrcteewnuertersnatc1yi0oo.n W1i3b0i%nohrotahcocdeapttaabrlejreacntgaed..ForTuresusrepored he, 3 abet Corlspikeswere
44 Fleld Matrix Spikes
Aswlaeoprwioaandgnd.eMdai1r5gxhhmsepaiekmiepsselpryioskueaswmeopdrlee0pcra8e5rp9ta0ar3ie3ndemfseobtehefovoderroeycwctuehretabcasyItanthmseewmeairrnaxts.eefnTlthle.maCisooimxpesolpudknedossr Wsohroduwdisthiotwhreocaocvceorpiieasbbleereanegne,Te0xc-e1p30a%s.poFloerdh1seSeecsoln6re.p1o4rtSe(dphrost,.the ma spkes
4.5 Sample Related Comments
A0lwsaatomrpsamrpelseustswenrAetacoclhemceiendti.ncuplica.Duplicatesampleresusae aporedsongwin 5 Data Summary
pPiaoarssespooetracnhm(negn/tmL)foorrPadFeOlAlaenddtPRgOSo.f heanslicaresus.The ouaretreposrisd 6 StatoefmAcocunracty
s`Bpaahnsaeyestdc,oaslnuaorcegcsuaurltatocsyosffpolriaPbsoRarOantSdoafrynckodnPtmrFaoOltsAiprisekaesksue,ssfisflhoerdoawMfeasdtarimexpcsolpveieksreise,se2Wn3id0ts%uh.r(Lreaobgsoaertaertsaopnrgkyeecss,o,wtnihvhe nefolowing exceptions:
pacesces
+ The PFOAandPROS recovry In O-We-572608LowSpike,O-PukcWorksLinch RSo0mkiISnnighrackrooLnnotcsweaSnpmtipkrleae,.caonndcaOn-tWa5t-o1n2728F7isLsoawmSppliekweacsouolvdenot3beacaslcruleasteerdbeacnautsee
+ Th13e6%P.OSrecoveryforsampleO-PublcWorksLunchRmSin HehSeikawas `Spachsepiarecoveriesa giveninAtschment3.
7 Data/SampleRetontion `oSfaimoplveasbwoimlabadraoaumehdrod3cMop6y0redpaoyrstsflrrofsaorreoderiticnga. AflodldoorcsmoabidaianteadsbarycEhixvyepdeonn. tHheorddcaapydpotfiohsascsoopdayfdoalrnm. mmoffv yoors.Th clonwlbenoted30days priora
8 Attachments
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`Summary of PFOA and PFOS in Water Samples E05-0184.
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3 Sample Namber__Sampled Date _ Sample Description
BOSOIBA9N (cont) unisCats
A2u2u92i0c0l5MethodO-W3.20`0C4aD5omn4eos
AmaDanepaii
770A ros
PFOA
ro
PES byESMS
rros
ansaoos 52008
msoerss AbPFaOAsCoe
ros
amon o.wsaan
APuFtOtAi Moti CPormopaen
PrOS by ESM
ros
A 31572n00D5asuute saws
SOILS AvPtOnAs Cots pros
An22t8t20i05MategOWSAZ`TCIoDmwers
rroA
PFOA
PFS by ESMS
#5
sAansauc pnute: nos
Aasn onCsoet PFOA pros
Aanntiocs)Made owa`sComments
Poa
PRO
PROS by Ess
pros
A 31572n00D5acapat 3nsnoos
ASvOiLCIoeS PFOA ros
A2m2i0ci03MogOWTAGCMompDawnsnte
Poa
Pron
Pros by Esns
ros
A3157n200D5auepsute snsms
AsEaostoiuCmoetrei:ss Pron ros
Azntiaca Mth Fron
o-wesmCeonmssnare 7ron
7505 by Esms pros
3A13u720s0D8ubite 052008
EOSOMATN0 A#nraoA Cate #ros
2008 Alta Met
OWesTIDu `Commie
Pron
#rOA
#408 by Esws Pros
A SisrnuoDsucnus 31305
BOSOIAI96s APurlounsCats #ros
A2u0d05aMatedPubli WoCrkosmBipdeany
Fron
#roA
POS by EMS pros
A3157u200Dt5ocDout snsnoos
EOSOIAIN66 APsroaniCote ros
a2n90i0aSMottPublic WorCksonBdseumDeuos
Pron
Fron
5705 by BSMS
sos
3A11572n00D5aeeDate. 30152005
00.8
Taam
CONTRA3CMT ELNAVBIORROANTMOERNYTWAOLRLKABOORRDAETROBRYYSAMPLE.
Page3of3
Project: EO5-0184 (cont)
ContractLabs): EXYGEN
3M Sample Number Sampled Date _ Sample Description
B0S-018479867 Assisi Code PFOA EOS
22872005 Trio Blank
Amsivical Method Compensay
PFOA
PFOA
PFOS by ESMS.
Pros
A3n5s1i2z0e0D5ueDate 30152005
0070
