Document bB9JGNZQn0pMp94oB74qK7Kqo

ABD00295676 A SCOPING DOCUMENT: Subject: General Approach for Preparing the Toxic Chemical Release Inventory Forms Required Under Section 313 of SARA Title III October 1987 ENVIROPLAN ABD00295677 ENVIROPLAN SCOPING DOCUMENTS Prepared By: Enviroplan, Inc. 59 Main Street West Orange, NJ 07052 SUBJECT: GENERAL APPROACH FOR PREPARING THE TOXIC CHEMICAL RELEASE INVENTORY FORMS REQUIRED UNDER SECTION 313 OF SARA TITLE III October 1987 59 MAIN STREET WEST ORANGE, N.J. 07052 201-325-1544 TWX: 510-100-5164 ABD00295678 i ENVMOPLAN TABLE OF CONTENTS 1. Introduction 2. Recommended General Approach for Completing the Toxic Chemical Release Inventory Forms 3. Estimating Releases to the Environment 3.1 Emissions to the Air 3.1.1 Stack or Point Source Emission 3.1.2 Fugitive Emissions 3.2 Discharges to Water .3.3 Releases to Land (On-Site) 3.4 Releases to Land (Off-Site) 4. Alternative Ways Enviroplan Can Work With Companies Page 1-1 2-1 3-1 3-3 3-3 3-5 3-7 3-9 3-11 4-1 A ABD00295679 ii ENVIROPLAN LIST OF TABLES Table 1-1: Threshold Quantities Above Which a TCRI Form for a Listed Chemical Must be Prepared Table 1-2: Summary of Information Required for Each Chemical at a Facility Subject to Reporting on the Toxic Chemical Release Inventory Form Table 1-3: Summary of Reporting Requirements Under Federal Right-To-Know Legislation Table 2-1: Overview of Enviroplan*s Recommended Approach for Completing the TCRI Forms Under Section 313 of SARA Title III Table 2-2: Conditions That Must be Satisfied and Reported to Claim Use of a Chemical as a Trade Secret Table 3-1: Common Air Release Source Categories Table 3-2: Methods to Estimate Fugitive Emissions to the Air Table 3-3: Solid, Slurry, and Nonaqueous Waste Stream Sources Table 4-1: Alternative Ways Enviroplan Can Work With Companies to Prepare the Toxic Chemical Release Inventory Forms Page 1-3 1-4 1-6 2-7 2-9 3-12 3-13 3-15 4-2 ABD00295680 ill ENVIROPLAN LIST OF FIGURES Figure 2-1: Block Diagram Illustrating Hypothetical Sources and Releases to Environment of Zinc from Blast Furnace Operations Page 2-10 ABD00295681 nil ENVIROPLAN LIST OF APPENDICES Appendix A: The Chemicals and Chemical Categories Subject to Reporting Under Section 313 of SARA Title III Appendix B: Toxic Chemical Release Inventory Form (6/4/87 Proposed) Page A-l B-l ABD00295682 1-1 ENVIROPLAN A 1. INTRODUCTION Under Section 313 of Title III of the Superfund Amendments and Reauthorization Act (SARA Title III), companies in SIC Codes 20-39 may be required to report the annual emissions into the environment of up to 329 chemicals from each facility in operation in 1987. Such reporting is required for those chemicals that were manufactured, processed or otherwise used at these facilities in 1987 in amounts exceeding the threshold quantities reported in Table 1-1. "Manufacture" means to produce, prepare, import or compound a toxic chemical. Manufacture also refers to substances that are produced coincidentally during the manufacture, processing, use or disposal of another substance or mixture. "Process" means the preparation of a chemical, after its manufacture, for distribution in commerce: 1) in the same or different physical form it was received in, or 2) as part of an article containing the chemical. "Otherwise use" means any use of a toxic chemical that is not covered by the terms manufacture or process (e.g., solvents, lubricants) and includes use of a toxic chemical contained in a mixture or tradename product. Appendix A lists the 329 chemicals and chemical categories subject to reporting under SARA Title III as of 9/1/87. From time to time, U.S. EPA may revise this list of chemicals. Table 1-2 presents a summmary of the information that must be reported on the Toxic Chemical Release Inventory (TCRI) Form, a copy of which is included as Appendix B. These reports are due on 7/1/88 and annually thereafter with penalties of up to $25,000 per day for late reporting. This memorandum outlines Enviroplan's recommended general approach for preparing the TCRI Forms. The actual ABD00295683 1-2 ENVIROPLAN A approach undertaken at each facility is dependent on facility-specific factors. However, this recommended general approach offers an effective starting point for each company to develop its own best approach for each facility. This approach is based on U.S. EPA's 6/4/87 proposed regulation implementing this statutory requirement. When this regulation is issued in final form in January 1988, there may be changes to some of these requirements. However, estimating the 1987 releases to the environment of each chemical is a statutory requirement that cannot change. Enviroplan's recommended approach is also based on the principal guidance U.S. EPA has issued for completing the TCRI Forms, our ongoing work for clients to prepare TCRI Forms, and our 15 years experience in estimating and measuring pollutant releases to the environment for more than 250 industrial and utility clients. Preparation of TCRI Forms under Section 313 represents one of four major reporting requirements under SARA Title III. The other major reporting requirements under this law are specified in Section 302, Section 304 and Sections 311 and 312. Table 1-3 summarizes each of these reporting requirements. This scoping document is divided into four additional parts. Section 2 presents our recommended general approach for completing the TCRI Forms. Section 3 discusses in some detail how to estimate the releases of each chemical to the air, water, and land. Section 4 discusses alternative ways Enviroplan is working with companies to complete the TCRI forms. ABD00295684 1-3 ENVmOPLAN A TABLE 1-1: THRESHOLD QUANTITIES ABOVE WHICH A TCRI FORM FOR A LISTED CHEMICAL MUST BE PREPARED I. For any of the 329 chemicals manufactured or processed at a facility: 1987 75 ,000 lbs/yr 1988 50 ,000 lbs/yr 1989 and thereafter 25 ,000 lbs/yr II. For any of the 329 chemicals otherwise used at a facility: 10,000 lbs/yr ABD00295685 1-4 ENVIROPLAN A TABLE 1-2: SUMMARY OF INFORMATION REQUIRED FOR EACH CHEMICAL AT A FACILITY SUBJECT TO REPORTING ON THE TOXIC CHEMICAL RELEASE INVENTORY FORM 1. Facility identification. 2. Offsite locations to which toxic chemical is transferred and type of treatment/disposal. 3. Chemical identity. 4. Activities and uses of chemical at facility. 5. Maximum amount of chemical on-site at any time during the reporting period. 6. Annual lbs/yr of emissions to the air of this chemical separately for fugitive (non-point) sources and stack (point) sources. 7. Annual lbs/yr of direct discharges to surface water from pipes and other process outfalls, from on-site wastewater treatment systems, and from stormwater runoff (if permits include stormwater sources). 8. Annual lbs/yr of releases to land within facility and the type of disposal, e.g., landfill, underground injection, transfer to waste broker, etc. 9. Annual lbs/yr transferred to each off-site location specified in Item 2. ABD00295686 1-5 ENVIMPLAN TABLE 1-2: (Continued) 10. For releases to air, water, land and off-site locations; the basis for the estimate (e.g., monitoring data, mass balance, published emission factors for designated chemical, or engineering calculation), whether it includes accidental releases reported under Section 304, and whether a permit(s) applies to each release. 11. Specification of the phase of the waste stream for this chemical (e.g., gas, wastewater, non-aqueous liquid, solid), treatment method, range of influent concentrations, treatment efficiency estimate, and whether the treatment efficiency is based on actual operating data. 12. Optional information on waste minimization practices. 13. Information supporting any trade secrecy claims. 14. Information demonstrating that an effort was made to obtain the chemical name of all chemicals included in mixtures or tradename products obtained from suppliers. TABLE 1 - 3 1 SUMMARY OP RBPORTINGI I I REQUIREMENTS UNDER SARA T IT L E 44 st: o& gS U uas co *e4 Mg SI * n o W-H M lh os os fa H <44 <W O I O QO-HC r B O BCD 44 >i '-- v X ** 9 r* *4-H u C U~h M 4i X'--. a&s BobUX 9na-6nixn>. 9TJ CM H 0 ti-g as si uO-j *M 4 yA *4 i-4 8.2 *4 O kX Bo 0 o > o- oooh o o 44 H o B0 6 <H U< Os i--. CD u B< 4k4 a-mH a a -o m ousnu <O44 ot C PS M-O k 44 -H fa C 44 HU a nxx a <409900. iJ Oi < ABD00295687 1-6 flH B 0C0 C0h y U-h &4J fa fa *> a c Sue wzccu UU 44 ea o u a UwUjrtO<-wH a cn 00 s go js I 0r 9i<m SB H-H 0 *> oa -*h4 xo a .4. >i*h H,T*4j fitSU>iCmQM->Pib-HtJ*-0>-B' <h x o aoeoi p|v*h m a c OS-HBB44 pM z-h >-40ub &e x a CO M afc o -*4J 44 N-i <H B 0 k "0 '-*.>, S^COM u c B C43<*>fh4 C *H x ^ . 0 M 9 0 -HX 44 -H . 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O fn m c C CM o O <H H H fO 44 8 CO Ut> S iAns ** ABD00295688 2-1 ENVIROPLAN A 2. RECOMMENDED GENERAL APPROACH FOR COMPLETING THE TOXIC CHEMICAL RELEASE INVENTORY FORMS Our recommended general approach for completing the Toxic Chemical Release Inventory (TCRI) Forms is divided into 18 steps. Step 11, estimating the releases to the environment of each chemical, is described in detail in Section 3 of this memorandum. Our approach is summarized in Table 2-1. It consist of the following steps: 1. We will visit each facility under study and meet with the environmental coordinator and other plant management to discuss the availability of the required information, the division of responsibility between Enviroplan and the plant for providing this information, and the schedule for completing this work. 2. We will assemble from plant records the following required information concerning the facility identification: a. Dun & Bradstreet Number b. EPA Identification Number assigned to facilities covered by RCRA or Superfund regulations c NPDES permit number and receiving surface water body d. Underground Injection Control Identification Number e. SIC Code This information will be used to complete Section II (Facility Identification) of all TCRI Forms. ABD00295689 2-2 ENVIROPLAN A 3. Of the 329 chemicals subject to reporting, we will identify which may be manufactured, processed, or otherwise used at the facility in 1987 in quantities exceeding the applicable threshold quantity shown in Table 1-1. As a starting point in identifying the chemicals potentially subject to reporting, we will review the Material Safety Data Sheets (MSDS) which must be submitted to state emergency response commissions and local emergency planning commissions by 10/17/87 and information used to prepare the Tier One Emergency and Hazardous Chemical Inventory Forms due 3/1/88. 4. We will review plant records and hold discussions with plant personnel to determine which chemicals from Step 3 exceed the applicable threshold quantities. These are the chemicals for which the TCRI Forms must be prepared. 5. For each chemical subject to reporting, we will discuss with the company which, if any, of these chemicals constitute trade secrets. For each chemical a company wishes to claim as a trade secret, we will ask the company to prepare a memorandum justifying this. Table 2-2 lists the statements that must be affirmatively answered to claim use of a chemical as a trade secret. 6. We will complete Section IV (Chemical Identity) of the TCRI Form. For those chemicals whose use are not trade secrets, we will supply one copy of the form with the CAS number and name of each chemical. For those chemicals whose use is a trade secret, we will supply a second "sanitized" copy of this form specifying its generic classification and code with the trade secret justification memorandum described in Step 5. ABD00295690 2-3 ENVIROPLAM A 7. We will identify all off-site locations to which wastes from the facility are sent including information on the type of disposal or treatment applied to waste at that location and whether the off-site location is owned or controlled by the facility owner. This will involve a review of solid waste permits and other RCRA permits for all transport, storage, and disposal facilities for hazardous wastes. We will use this information to complete Section III of the TCRI Form (Off-site Locations to Which Any Toxic Chemical is Transferred). 8. From review of plant records and discussions with plant management, we will prepare Section V of the TCRI Form (Activities and Uses of the Toxic Chemicals at the Facility). 9. For each chemical subject to reporting, we will review with plant management its records and estimates concerning the maximum quantity of the chemical on-site at any time during the year 1987. This data will be entered in Section VI of the TCRI Form (Maximum Amount of the Chemical On-Site Anytime During the Reporting Period). 10. For each chemical subject to reporting, we will prepare a block diagram showing each potential source of release to the environment and the flow of this chemical through the facility in relationship to other sources including delivery points, storage locations, process units, waste treatment units, and waste disposal units, among others. Figure 2-1 illustrates the type of block diagram that will be prepared for each chemical subject to reporting at each facility. 11. We will use the procedures described in Section 3 of this memorandum to estimate the total facility-wide releases to air, water, land, and off-site locations of each chemical subjectr*" ABD00295691 2-4 A ENVIROPLAN to reporting. This information will be estimated by source and then totalled to determine the facility-wide releases. The estimated releases will be entered in Section VII of the TCRI Form (Releases to the Environment) We will also prepare a supporting memorandum for each chemical showing the basis for the determination of the quantity released to the environment in 1987. 12. We will identify each waste stream containing chemicals subject to reporting. We will use the block diagrams prepared in Step 10 to make these determinations. 13. For each waste stream containing the chemicals subject to reporting, we will determine: A. The predominant phase of the waste stream (gaseous, wastewater, nonaqueous liquid waste, solid waste) B. Treatment method C. Range of influent concentrations D. Estimated waste treatment efficiency E. Whether the estimated waste treatment efficiency is based on operating data The data on influent concentration and estimated treatment efficiencies will be obtained from a review of measurements carried out by the facilities under other regulatory programs, permits specifying required treatment efficiencies, published data available to Enviroplan on treatment efficiencies for various treatment methods, mass balance calculations, and/or engineering calculations. For air emissions, if detailed information on treatment efficiency for individual organic chemical emissions is not available, overall information on total VOC emission reductions may be used to estimate the treatment ABD00295692 2-5 ENVIROPLAN A efficiency for the particular chemical. The basis for each treatment efficiency calculation used in the TCRI Form will be documented in a separate memorandum. The above information will be used to complete Section VIII of the TCRI Form (Waste Treatment Methods and Efficiency). 14. We will discuss with company management whether it wishes to provide optional information on waste minimization procedures for each chemical subject to reporting. If so, we will complete Section IX of the TCRI Form (Optional Information on Waste Minimization) including the reduction in the quantity of the chemical released to the environment from the preceding year and the reasons for the reduction. 15. Following review of the above work, we will discuss with company management whether there are some sources for which the estimated releases to the environment are subject to such a large degree of uncertainty or are so toxic that the company may wish to consider selected and limited measurements of these releases to provide more accurate information, e.g. chemicals which are known human carcinogens. For those sources and releases, we will prepare cost estimates for conducting such measurement programs. If such measurements are carried out, this information will be incorporated in Section VII of the TCRI Form (Releases to the Environment). 16. The above information for all TCRI Forms at each facility will be entered into a computer compatible database management system such as DBASE, which will automatically print TCRI Forms for each chemical at each facility on an IBM PC compatible computer. This database will be provided to the ABD00295693 2-6 ENVIROPLAN facility so that future editing and revisions to the TCRI Forms can be carried out at the facility level. 17. The final work products for each chemical subject to reporting will consist of: 1) the completed TCRI Form, 2) the TCRI Form data in a computer-compatible format, 3) a memorandum for each chemical documenting the basis for the release estimates (Step 11) and 4) a memorandum for each chemical documenting the waste treatment efficiencies (Step 13). 18. We will meet with the company personnel responsible for satisfying the Section 313 reporting requirements of SARA Title III to review the TCRI Forms and other work products prepared for each chemical at each facility, and the basis of the procedures for developing the release estimates and other information on this form. This will be done, in part, to permit company personnel to complete Section I of the TCRI Form by certifying that they believe the information on the forms to be true, accurate, and complete. ABD00295694 2-7 ENVIROPLAN A TABLE 2-1s OVERVIEW OF ENVIROPLAN'S RECOMMENDED APPROACH FOR COMPLETING THE TCRI FORMS UNDER SECTION 313 OF SARA TITLE III A. Assemble information to complete the Facility Identification section of all TCRI Forms: Steps 1 and 2 B. Determine for which chemicals TCRI Forms must be prepared for each facility: Steps 3 to 6 C. Assemble information to complete the Off-Site Locations to Which Any Toxic Chemical is Transferred section of the TCRI Form for each chemical: Step 7 D. Review facility records and hold discussions with facility personnel to prepare the Activities and Uses of the Toxic Chemicals section and Maximum Amount of the Chemical On-Site Anytime During the Reporting Period sections of the TCRI Forms: Steps 8 and 9 E. Estimate the total facility-wide releases to the air, water, and land of each chemical subject to reporting and complete the Releases to the Environment section of the TCRI Form for each chemical: Steps 10 and 11 ABD00295695 2-8 TABLE 2-1: (Continued) ENVIROPLAM F. Identify each waste stream including chemicals subject to reporting and assemble the information to complete the Waste Treatment Methods and Efficiency section of the TCRI Form: Steps 12 and 13 G. Discuss with company personnel whether to complete the Optional Information on Waste Minimization section of the TCRI Form and, if so, complete this section: Step 14 H. Decide with company personnel whether to conduct selective measurements to improve the accuracy of the estimated releases to the environment for selected chemicals (especially human carcinogens) and, if so, conduct such measurements to increase the accuracy of these estimates: Step 15 I. Meet with company personnel to finalize the TCRI Forms and work products supporting the information provided in these forms: Steps 16 to 18 ABD00295696 2-9 ENVIROPLAN A TABLE 2-2: CONDITIONS THAT MUST BE SATISFIED AND REPORTED TO CLAIM USE OF A CHEMICAL AS A TRADE SECRET 1. That the facility has not disclosed the fact that the chemical is manufactured, processed or otherwise used at the facility to any other person, other than a member of a local emergency planning committee, an officer or employee of the United States or a State or local government, an employee of such person, or a person who is bound by a confidentiality agreement. 2. That the facility has taken reasonable measures to protect the confidentiality of such information and will continue to take such measures. 3. That the information is not required to be disclosed or otherwise made available to the public under any other Federal or State law. 4. That disclosure of the information is likely to cause substantial harm to the competitive position of the facility. 5. That the chemical identity is not readily discoverable through reverse engineering. ABD00295697 w O.t o<in LU tr D U. W >< Z _J lu m ABD00295698 3-1 ENVIROPLAN A 3. ESTIMATING RELEASES TO THE ENVIRONMENT This section discusses our approach to estimating the total 1987 releases to the environment of each chemical for which a TCRI Form must be prepared. To prepare the Releases to the Environment section of this form, four questions must be answered for releases to each environmental medium: (1) How much of the chemical was released in 1987 (in pounds per year)? (2) Was any portion of that release (except releases to off-site locations) reported under the emergency notification provisions of Section 304 of SARA Title III? (3) What is the basis of the estimate (e.g., what was the primary estimation method used to determine the quantity released)? (4) Is the release specifically covered by a relevant environmental permit held by the facility? For each release estimate, the principal method by which the release estimate was derived must be reported, i.e., the method used to estimate the largest portion of the total release quantity estimated. The alternative methods of estimation are: 1) based on monitoring data or measurement for the chemical in the waste stream as released; 2) based on a mass balance such as the amount of the chemical in streams entering and leaving process equipment; ABD00295699 3-2 ENV/ROPLAN A 3) based on published emission factors such as those relating release to throughput or equipment type; and 4) based on other approaches such as engineering calculations (for example, estimating volatilization using published mathematical formulas) or best engineering judgment. The first three methods may only be used if they are specific for the chemical release being estimated. Otherwise, engineering calculations and judgment should be used. Use of monitoring data or emission measurements are the preferred method if such data are available from other regulatory requirements or process measurements. However, the law requiring preparation of the TCRI Forms specifically states that such monitoring or measurement is not required to complete the Releases to the Environment section of this form; parts: The remainder of this section is divided into four 1. Emissions to the Air 2 . Discharges to Water 3. Releases to Land 4. Transfers to Off-site Locations ABD00295700 3-3 ENVIROPLAN 4 3.1 EMISSIONS TO THE AIR We will review the block diagram prepared in Step 10 of Section 2. All sources of chemical releases to the air will be divided into two categories: 1) stack or point air emissions, and 2) fugitive or non-point air emissions. The following two subsections describe the procedures we will use in developing the estimates of emissions to the air for each of these source categories. Table 3-1 shows typical source categories for releases to the air from manufacturing facilities. 3.1.1 Stack or Point Source Emissions The procedure we will follow to estimate the emissions to the air from stack or other point sources at each facility is as follows: 1. We will prepare a table listing each point source of emissions for each chemical subject to reporting. 2. For each source, we will review any measured flow rates, concentrations, and total emission rate measurements made from the source for each chemical. Such measurements typically will have been taken to satisfy process requirements or other regulatory needs. If air emissions are in the form of particulate matter, we will discuss with company personnel whether to collect selected particulate samples and subject them to laboratory analysis to determine the metal and other chemical fractions of these particulate emissions. ABD00295701 3-4 ENVIROPLAN A 3. We will review all air pollution permits, consent orders and other government directives concerning emission limits ' for each of these sources. 4. We will review 1987 facility production records applicable to each source to determine the total annual production in 1987 by product group. 5. Based on the above information, we will determine if measured concentrations and emission rates can be used to estimate 1987 annual emissions to the air from each of these sources. If so, we will proceed to Step 8. 6. If existing measurements cannot be used, we will discuss with plant engineering personnel the feasibility of completing mass balance calculations to estimate the emissions from each source. Such calculations will be most feasible if the chemical mass in the inlet and outlet streams from the source can be accurately quantified. Because small errors in chemical input or output estimates can produce large errors in emissions to the air, particular care must be taken to assure that accurate values of the input and output streams are available before proceeding with mass balance calculation. 7. We will review the available published literature on air pollution emission factors from each source to determine to what extent appropriate published emission factors for the chemical in question are available. For chemicals emitted in particulate form, published emission factors for total particulates will be considered together with the chemical composition of the particulate matter based on selective measurements as discussed in Step 2. ABD00295702 3-5 ENVIROPLAN 8. Based on the above review, we will determine whether mass balance methods or published emission factors for the chemical in question can be used to estimate the air emissions. If so, these procedures will be used. 9. If not, engineering calculations and judgment will be used. Flow rates will be estimated from equipment design characteristics and annual production records. The physical properties of the chemical in question will be used to estimate gaseous concentrations. The chemical composition of particulate matter will be estimated based on engineering judgement supplemented by available published data. The concentrations will be applied to the estimated flow rates to determine total emission rates. 3.1.2 Fugitive Emissions Fugitive emissions occur from many sources. They include emissions from equipment leaks and maintenance; loading, unloading and other movements of materials in solid, liquid and gaseous form for manufacturing or processing; vehicular activity and wind erosion from storage piles causing reentrainment of dust into ambient air; certain vent emissions not controlled; and secondary emissions from evaporation of liquids stored without total containment in open trenches, ponds, open vats, etc. Table 3-1 details many of the common sources of fugitive emissions. Such emissions are complex and usually extremely difficult to measure. Usually engineering judgment, and published emission factors sometimes supplemented by selective measurements may be used to estimate these emissions. For chemicals characterized as known or suspected human carcinogens, greater emphasis should be-** ABD00295703 3-6 ENVIROPLAN placed on measurements for estimating these emissions since published emission factors can frequently exceed actual emission rates by several orders of magnitude. Table 3-2 summarizes alternative approaches to estimating the fugitive emissions to the air from various sources. Such measurements should employ U.S. BPA Reference Method procedures, the protocol developed by the Chemical Manufacturers' Association for fugitive emission measurements and other established industry procedures for such measurements. ABD00295704 3-7 CNVIROPLAN 3.2 DISCHARGES TO WATER Direct discharges of each chemical to surface waters will be estimated in the following steps. 1. We will review all NPDES permits for the facility to identify all discharge points to rivers, lakes, streams, and other surface water bodies from pipes, open trenches, other process outfalls and wastewater treatment units. Storm water sources will only be considered if they are included in applicable NPDES permits. 2. From process information, NPDES permits and any available measurement flow data; we will estimate the total annual flow volume rate into these water bodies from each waste stream. The annual production rate corresponding to this flow volume will be determined. We will develop with plant personnel the functional relationship between annual flow volume and available measures of production or other reported activities determining flow rates. From the above information, the 1987 annual flow volume in each waste stream will be determined. 3. We will review with the plant environmental coordinator to what extent the chemical concentrations in the wastewater have been measured based on process measurements or measurements required by government agencies. This information will be assembled for subsequent use. 4. If concentration measurements for specific chemicals have been made, they will be applied to the 1987 flow volume information to calculate the total releases to surface water bodies in 1987. We will proceed to Step 8. ABD00295705 3-8 ENVIROPLAN A 5. If the concentration measurements are not available, we will evaluate the feasibility of using mass balance methods to calculate the releases. In evaluating this approach, we will take into account the fact that large errors in estimated releases can result from small uncertainties in process input and output data. 6. We will also review published effluent guidelines for the respective industry. We will evaluate the feasibility of using such published effluent guidelines to estimate chemical releases from each waste stream. 7. Based on the above, we will determine whether the mass balance method or published emission factor method can be used to estimate surface water discharges. If not, engineering calculations will be used based on estimates of chemical concentrations from a variety of sources including detailed plant process engineering calculations. 8. The calculation of 1987 chemical releases from each waste stream will be summarized in a technical memo and submitted for each facility to support the 1987 release estimates entered on the TCRI Form. ABD00295706 3-9 ENVIROPLAN 3.3 RELEASES TO LAND (ON-SITE) Releases to the environment which are neither gaseous nor aqueous are classified as solid, slurry, or nonaqueous liquid wastes. Table 3-3 shows typical industrial operations which may be sources of releases in these categories. These waste products may be disposed of on-site or transferred to an off-site location. This section describes the procedures for estimating on-site releases to the land. Section 3.4 describes procedures for quantifying transfers to off-site locations. Releases to land occur as a result of landfilling, land treatment, underground injection and surface impoundments. Releases to the on-site environment at each facility will be calculated in the following steps. 1. We will identify any landfilling, land treatment, underground injection and surface impoundments. 2. We will review RCRA and solid waste permits and RCRA waste manifests for each activity to identify the expected constituents of the waste and the quantities of material released. 3. We will review production records, records of discharge, and any available information on direct waste measurements to estimate the releases for each reportable chemical. 4. If available data is insufficient, we will review with plant personnel the feasibility of using mass balance or engineering calculations to quantify these releases. The technical approach will be a function of the type of waste and ABD00295707 3-10 ENVIROPLAN A method of generation. The accuracy of this approach will be assessed. 5. Waste treatment systems may be used for solid, slurry, and nonaqueous waste either to recover usable materials, to destroy (incinerate) the waste, to dewater, or to solidify the waste. Therefore, the treatment system may be a source of emissions to the atmosphere or surface water, in addition to residual wastes which may be released to the land. Information on treatment system operation including operation records, permits and testing information will be used to quantify emissions and to calculate the treatment efficiency of the system. 6. On-site land disposal frequently also produces emissions to the air. These land disposal sites will be reviewed to determine whether any additional fugitive emissions to the air should be calculated. ABD00295708 3-11 ENVIROPLAN A 3.4 RELEASES TO LAND (OFF-SITE) Solid, slurry, and nonaqueous liquid wastes may also be transferred to off-site locations. In reporting releases to the environment, it will be necessary to distinguish between these and on-site releases. The methods of quantifying these releases will be essentially the same as discussed in Section 3.3. In addition it will probably be necessary to review shipping invoices and waste manifests to quantify these releases. Under RCRA, companies may already report biennial shipments on EPA Form 8700-13A. ABD00295709 3-12 ENVIROPLAN A TABLE 3-1: COMMON AIR RELEASE SOURCE CATEGORIES Point Source Fugitive Sources Secondary Sources Handling Equipment Leaks Storage, and Maintenance______and Loading Combustion units Reactors Distillation system Vacuum systems Baghouses or pre cipitators Combustion stacks Blow molding Spray drying Lagoons, open trenches, pond evaporation Cooling tower evapor ation Wastewater treatment facilities Curing/drying Scrubbers/absorbers Centrifuges Extrusion operations Pressure safety valves Manual ventings Storage tank breathing and filling losses Other process vents Flanges/connectors Valves Pump seals Compressor seals Sample connections Open-ended lines Pressure relief devices (e.g., rupture disks) Lap hoods Process sampling Equipment inspect ion Equipment cleaning Equipment mainten ance Blowing out pipe lines Storage piles Loading/ unloading Line venting Packaging/ container loading Material storage piles Vehicle activity in vicinity of storage piles Notes: (a) Loading and unloading releases could be categorized as either point or fugitive sources, depending on whether the releases are ducted. (b) The above common air release source categories are most applicable to the chemical industry but are also applicable to a broad range of manufacturing facilities. ABD00295710 3-13 ENVIROPLAN A TABLE 3-2: METHODS TO ESTIMATE FUGITIVE EMISSIONS TO THE AIR Source Category Alternate Methods to Estimate Emissions I. Equipment Leaks and Maintenance 1. Use EPA average emission factors for equipment leaks for the synthetic organic chemical industry (SOCMI factors) applied to component counts (valves, flanges, pumps, seals, compressors, agitators, relief valves, sampling devices) 2. Use EPA Method 21 to measure number of components of each type that are leakers (>10,000 ppm) versus nonleakers (< 10,000 ppm); apply EPA average SOCMI emission factors for leakers versus nonleakers 3. Same as 2 but stratify components into three groups: <10,000 ppm, 1,000 10,000 ppm, >10,000 ppm. 4. Use EPA Method 21 for all components and Chemical Manufacturer's Association protocol for mass emission rate measurements by component type. ABD00295711 3-14 ENVIROPLAN TABLE 3-2: (Continued) II. Solid Materials Storage, Handling and Vehicular Activity 1. Use EPA published emission factors for total fugitive particulate emissions by source category with engineering judgment to estimate the fraction of total particulate emissions of each Section 313 chemical. 2. Same as 1 except selective measure ments are used to determine the fraction of total particulate emissions that are of each Section 313 chemical. III. Secondary Emissions Engineering calculations based on chemical properties of liquid or solid subject to vaporization. ABD00295712 3-15 ENVIROPLAN TABLE 3-3: SOLID, SLURRY, AND NONAQUEOUS WASTE STREAM SOURCES Spent solvents Spent solvents Heavy ends - distillation residues Heavy ends - miscellaneous Light ends - condensable Steam stripping wastes Acid leaching solutions Spent plating, stripping, or cleaning baths Off-spec, discarded products or feedstock Distillation side cuts Residue in containers, liners, drums, cans, cleaning rags, gloves Spills, leaks, vessel overflows Precipitates or filtration residues Spent activated carbon or other adsorber Spent ion-exchange resins Spent catalyst Scrap metal Solid scrap from finishing or trimming operations Untreated solid waste Equipment cleaning sludge (tank bottoms, heat exchangers) Oven residue Wastewater treatment sludges - biological Wastewater treatment sludges - other Treated organics Treated solids Oily waste from treated wastewater ABD00295713 4-1 ENVIROPLAN 4. ALTERNATIVE WAYS ENVIROPLAN CAN WORK WITH COMPANIES There are many ways Enviroplan can work with companies to satisfy the Section 313 reporting requirements. Table 4-1 lists several of these ways. Which way is best depends on: 1) the availability of resources and special expertise to complete all reporting requirements; 2) the desirability of having an independent third party prepare these forms and, in particular, the Releases to the Environment section; and 3) the value of using the expertise and resources of a consulting organization that has specialized in estimating and measuring pollutant releases to the environment from complex sources over the past 15 years. ABD00295714 4-2 ENVIROPLAN TABLE 4-1: ALTERNATIVE WAYS ENVIROPLAN CAN WORK WITH COMPANIES TO PREPARE THE TOXIC CHEMICAL RELEASE INVENTORY FORMS 1. Enviroplan assumes total responsibility for preparing the TCRI Forms. 2. Enviroplan is responsible for preparing the Releases to the Environment section of the TCRI Forms and Company prepares all other parts of Form. 3. Enviroplan is responsible for preparing only the Releases to the Air (point and fugitive or just fugitive) section of the TCRI Forms and Company prepares all other parts of the forms. 4. Enviroplan is responsible for conducting certain chemical analyses of gaseous, liquid, and solid releases to the environment in support of Company preparation of the entire TCRI Form. 5. Enviroplan is responsible for identifying the chemicals subject to reporting on TCRI Forms and Company prepares the Forms. 6. Enviroplan is reponsible for developing written Companyspecific guidance to be given to facility personnel for use in their preparation of the TCRI Forms. ABD00295715 A-l ENVIROPLAN 4 APPENDIX A: THE CHEMICALS AND CHEMICAL CATEGORIES SUBJECT TO REPORTING UNDER SECTION 313 OF SARA TITLE III Ftedera! Regbtor / Vol 81 No. 107 / Hwrtdiy, fane 4, 1187 / Propped Rolf 21169'. Chentfcal name 2-AceMamnofUxxene____________________ _________________ _______ ___________ _____ CAS No. Generic cieesificaiion code Effective date 79-07-0 60*954 87-44-1 79-08-8 93-98-3 C07 01/01787 COO 01/01/87 C07 01/01/87 C11 01/01/87 CIO 01/01/97 ABD00295716 Federal ftegbtw / Vol SI No. 107 f Thareday, fane 4. 1987 / Propoeed Rolet________ filtt*. Chemical name CAS No. Generic dasstteabon code Effective date 4m4am Aevytanwto ......... . .............. AerytanMIe AUrki (M:S.6-OimeVianonaphthalerie,1,2.4.10,10-hexacNor'M.4a, S,6,6frhcuhy*0` (i-atphe.4aiphA.4*eta-.5aipha,6eiphe16aeta.)-J. A*y< (**&&*....... Aluminum (fume or duet)... .. . __ 2-Ammoanthrequinowe -- 4-Ammoazobenrene. Ammonia -........ . ..... ... ..... Ammonium nitrate (eofutoon)_______ _ __ AnAne <vAr<arfcftf p-Arwidwe........... -- ------------------- ----- _ __ _ .............. _ .. Anhmnny ... . ...... ................................ Amnrar. ........ Asbestos (friable)......................... ....... ...... ............. Aummine IBenzeneamine, 4,4'<art>cxwnidoytbis[N,N-<limethy4-l__ ___ ... ______ Rmral rhLyirto ...................... Benzoyf cNoride.... --------------- ...__ ________ Benzoyt peroxide_________ ______ _______ ~ Benzyl rhlnhriA ...................... .................................... ................ Biphenyl--........... ....... ............. ........ ............................._ .. , Bis(2-chtofoethyf) ether....................._. ....____ .......... .. Bis(cWofomethyl) ether...... .............. ............... .... . __ B<s(2-chtoro-l*methytethyt) ether...... . _.... ...... .... .,, __________________ ..... .. . Bromomethane (Methyl bromide)___ ___________ _____ _... 1,34tirtAdi*nfc .. . ........... ..... ............... n-Butyl alcohol..... ......... .... ......................... .......... ......... ,,..... ....... .... _.................. ... ...... ...... sac-Butyl alcohol_________________ _________________ ____ ______ ... terr-Butyf alcohol.... --......................... ........ ..... ................................. ......... .......... .... . Butyl benzyl phthaiate............ .......... ................ ......... ....... ............................ t.2-Butylene oxide........ ..................... ................... . .................... ............ ....... ....... .......... C.l. Ac*d Biue 9, diammonium salt................... ..... ................ ........... ............ .......... ........... . C.t Acid Bkie 9. disodium salt........... ...... ............. ..... ................ ........... ............. ....... .... . Ct Arid S_ ..... ...... C.l. 8as Green 4......... ..................... ............. ........ ........ ........... ........_____ ________ ___ ___ C.l. Rasie Red 1. .................... ...... .................. .... ........ ........... ..... ........... ........ ........ C.t. Disperse Yellow 3................................ -.... ........... ................. ............. ............................. C.l. Food Red 5........................................................... ........ ....... ......... .......... -..... ............ C.l. Food Red 15........... ......................... ........................................................... ................. C.l. Solvent Orange 7................................ ............... ................... ..... .............................. C.t. Solvent Yellow 3............ ............. ......... ................ .... ..._____ ....____________________ C.l. Solvent Yellow 14.............................. ......................................... ................. ...... ................. C.l. Vat Yelow 4............. ............... .............. ....... ...... ........ .................. ..._____ .... Cadmium .... . ............. . .... .... .............................. ........ ......... ..... ........... ..... .... Calcium cyanamide....... ........................................... ........ .......... ....... ................. .......... ...... . Captan [1H-l$oindole-1,3(2H)-dione13a.4,7,7a-tetrahydro-2- ((tricMoromethyQthio)*)-- Carbaryt Il-Naphthalenol.methylcarbamatel........ -- .---- .....____ ____--...... Carbon rfkiiHidfl .................... .......... ............ _........ .. .... .......... _...... .............................. .. Chloramben (Benzoic acid, 5-amino-2.5'dtehforo*)___________ ................. ........ 407-02-6 70-00-1 7B>lO-7 407*10-1 000-00-2 407-05-1 7429-00-5 1344-20-1 117-79-3 00-09-3 02-07-1 02-20-0 7664-41-7 6464-52-2 7763-20-2 62-53-3 00-04-0 404-04-9 134-29-2 120-12-7 7440-36-0 7440-36-2 1332-21-4 492-63-6 7440-39-3 96-67-3 55-21-0 71-43-2 62-67-5 66-07-7 96-65-4 94-36-0 100-44-7 7440-41-7 92-52-4 111-44-4 542-66-1 106-60-1 103-23-1 75-25-2 74-63-9 106-99-0 141-32-2 71-36-3 76-92-2 75-65-0 65-66-7 105-60-7 123-72-6 2650-16-2 3644-45-9 4680-76-6 569-64-2 999-36-6 2632-40-6 3761-53-3 61-66-9 3116-97-6 97-50-3 042-07-9 126-60-5 7440-43-9 156-62-7 133-06-2 63-25-2 75-15-0 56-23-5 463-50-1 120-60-9 133-90-4 CO? 009 006 Oil 003 003 CIS 15 CIO * CIO CIO CIO CIS CIS CIS CIO CIO CIO CIO 001 C15 Cl 5 CIS CIO C15 002 009 cot CIO C02 009 C09 C02 CIS C01 C06 C06 COS 006 C02 C02 C01 coe cos COS C05 coo coe C07 C13 C13 03 CIO CIO C14 C14 CIO C14 C14 C14 C07 Cl 5 C11 Cl 3 009 CIS C02 CIS cos C11 01/01/67 01/01/87 01/01/67 01/01/67 01/01/67 01/01/67 01/01/67 01/01/67 01/01/6? 01/01/87 01/01/6? 01/01/87 . 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/67 01/01/67 01/01/87 01/01/67 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/B7 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 ABD00295717 21170 Federal Register / Vol 52, No. 107 / Thursday, June 4, 1087 / Proposed Rules A Chemical name Chlordane [4,7-Methanoindan, 1,2,4,5,6,7>6,8-octachlor-2,3.3a,4,7,7a- hexahydro-J_______ Chlorinated fluorocarbon (Freon 113)(thane, 1,1,2-&ichloro-1,2, 2>tnfluoro-l~ Chlorine.......... ....... ......... .. ,,,, Chtarine dioxide ............... ........ ......... ChloroecetJC add____ .... ,, 2-CMoroecetophenone....................... _ .. .......... .. . Chlorobenzene_____ ___________________________________ _________ _______ Chtorobenziiate [Benzeneacetic add, 4<hloro-.alpha-(4-chloropheny1)-.alpha-hydroxy-. Chloromethyl methyl ether____ _ _____ CNorothatonil (1,3-Benzenedicarbonttri)e>2,4,5.6-t6trachloroO____________ Cnh*l ._ Cresol (mixed isomers)----------- _____ .. _. - ............... o-Cresol------------- .. . ____ - _ --------- p-Cresd------------------- . __ ___ ......... Cumene..... ....... .. ........ ....... . _______ ____ Cumene hydroperoxide....___ _________ _________ ___ _____ ___ Cupferron [Benzeneamine. N-hydroxy-N-nitroso, ammonium salt}_______________________ Cyanide compounds____ ___ _______ __ _ Cydoheuna ... ....... 2,4-D [Acetic add, (2,4-dkhkxo-phenoxy)-]_______ Diaitate (Carbamo'thioie add. bisO-methytethyfK S-(2.3- dichloro-2*propenyQ ester]_______ 4,4`-0iaminodiphenyl ether........... .......... ........ ..........................._............... ....... ........................ Diaminotoluene (mixed isomers)______ - _____ . 2.4-Oiaminololuene_____________________ __ niarnmethane ........... ____ ________________ _____________ Dihenxnfumn. ......... Dibutyl phthalate............................. ......... Dirhlnrnhn7Anfi (mhrfld nnntor*) ...... ............ , ............... 1,2-DichlOfobenzene______________ 1.3-OcMoroben2ene....-................ . _ __ ____-__ ...... ..... . ___ _ 1.4-0Woobenzene..J_____ _____ __ _____ _ ________ _ _____ ______ 3.3'-Dhlorobenzidine_______ __ _________ ____ ___________ ___ 1,2-Oichloroethane (Ethylene <*cNoride)._ . ___ 1,2-Oichloroethyfene........... .... .................................... ........ Dichioromethane (Methylene chloride).... . ........ . .... ....______ _ ___ ___ ____ 1,3-DtcWoropropylene............................... ....... -.......... .......... ........ .. ........ Oichlorvos [Phosphoric add. 2,2-dichkyoethenyl dimethyl ester]............... ......... ..... ..... Oicofol (Benzenemethanol. 4<hkxo-.alpha-(4-dikxopheriy().alpha.-(tricWoromethyf)*J_____ Di-(2-thylhexyl) phthalate (DEHP).. Diothyt _____ .... . ,, 4-Dimethytaminoa2obenzene________ ..... 3.3'-OimethytbenzkSne(p-Toidine)_______ .... ... . ,,. ___ .... _____ 4.6-Oinrtro-p-creeol........... ...... -- 2,4-OnrtroioJuene. __ -- _____ CAS No. Generic classification code Effective dale 57-74- 76-13-1 7782-50-6 10049-04-4 70-11-6 .532-27-4 106-90-7 610-15-6 75-00-3 67-66-3 74-67-3 107-30-2 126-99-6 1897-45-6 7440-47-3 7440-46-4 7440-50-6 120-71-6 1310-77-3 106-39-4 95-46-7 106-44-5 96-62-6 60-15-9 135-20-6 57-12-5 110-82-7 4-75-7 1163-19-5 2303-16-4 615-05-4 39150-41-7 101-60-4 25370-45-6 95-60-7 334-86-3 132-64-9 96-12-6 100-93-4 64-74-2 25321-22-6 95-50-1 541-73-1 106-46-7 91-94-1 75-27-4 107-00-2 540-59-0 75-09-2 120-63-2 76-67-5 542-75-6 62-73-7 115-52-2 1464-53-5 111-42-2 117-61-7 64-60-2 64-67-5 119-90-4 60-11-7 119-93-7 79-44-7 57-14-7 105-67-9 131-11-3 77-70-1 534-52-1 51-26-6 121-14-2 COS C02 C16 C16 006 C07 C04 coe C02 C02 002 006 C03 009 05 CIS . CIS C06 C05 COS COS C05 COI C05 02 06 COI coe C04 03 CIO CIO CIO CIO CIO C11 coe C02 C02 coe C04 C04 C04 C04 CIO C02 C02 C03 C02 C04 C02 C03 03 C04 C06 CIO coo coe 03 oo CIO oo C09 C11 cos coo 03 02 02 02 01/01/67 01/01/87 01/01/87 01/01/67 01/01/67 01/01/67 . 01/01/67 01/01/87 01/01/87 01/01/67 01/01/87 01/01/67 01/01/87 .01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/67 01/01/67 . 01/01/57 01/01/87 01/01/67 01/01/87 01/01/67 01/01/87 01/01/67 01/01/67 01/01/67 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/67 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/67 01/01/67 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/67 01/01/67 01/01/87 01/01/67 01/01/67 01/01/67 01/01/67 01/01/67 ABD00295718 federal R<^ier / Vol SI No. W / Hmrsday, June 11867 / Proposed Rule* 21171 Qimtal nmi 2.6-Oinltrotoluene.. n-Pioctyl phthalate. 1.4-Otoxane______ 1.20ipheny<hydridne(Hydraiofeorgcna). Oirecl Bleck 38_____________________ Direct Blue 6__ ______ ___r Direct Brown 95__ EpcNorohydrin__ _ 2-Ethoxyetftand Ethyl acrylate-------- Ethytoenzene.... ...... Ethyl chkxoiormate. Ethylene. Ethylene glycol.... -__ ___ ____ Ethylene*mine (AzmdxNQ__________ _----. Ethylene oxide................... ...........................; .......................... Ethylene thiourea___________________ _____ ______________ _ ,,,, Fiuometuron [Urea. N.N-djmethyt-N'-fS-ttrffluoromethyfJphenyl]-]. Formaldehyde___ _________________ Heptachlor [i,4,5,6,7.8.8-Heptachloro-3a,4.7,7a-tetrahy(to-4.7- methano-IH-Indent]. Hexaehtorobenzene__ *___________________________ _____________________ ,, Mexachioro 1,3-butadiene___________ __ --_________________________ ......... HexacNorocyctopentadtene____________ ____ _______________________________, Hexachtoroethane__ __________ ____ --........ .......... _.................................... Hexachtoronaphthalene______ _____- Hexamethytphosphoraffede___ ......................... Hydrazine...... ...... .......... _____..................... Hydrazine sulfate____________________________ Hydrochloric add------------------------------------------- Hydrogen cyanide--.............................. _....... -- Hy*frogen fluoride_____________________ ______ Hydroquinone________________ ___________ ___ IsobutyraJdehyde Isopropyl alcohol (mfg.--strong add processes). 4.4Msopropylidenedtphenol__ Lindane [Cydohexane. l,2.3>4,S,6-hexachtoro-,(1.a1ph&..2.a$ha., 4.afpha,Salpha.,6.beta.)0_____________________________________________ Maleic anhydride____________________________________ Maneb [Carbamodtthioic add. 1,2-ethanediylbis*. manganese complexl. Manganese___________________ Melamine_______________ -_____________ ___________ . ___ _ ,, Mercury_______________ ____________________ .,, Methanol._______ __________________________,,__________________ _____ MethoxycMor [Benzene, 1,1*42,2 2-trichloroethylidene)bist4-methoxy*i .... 2-Methojryethanol_________________ ______ __ _____ __ ,....... ,, ____ Methyl acrylate__ ________________ ____________ _____________________ Methyl ferf-butyl ether.................................. ......................... 4,4'-Meth leneb*s{2-chloro aniline) (MBOCA)______ .......... 4,4'-Methyfenebis(Af/V-<fimethy!) benzenamine________ Methytenebis(pheny1isocyanate) (MBI)________ _____ _______ Methylene bromide..... -........ ............ ........ r......... 4.4`-Methytenedianaine _____________ ______ ____,, Methyl ethyl ketone.... .... .... .............. ...... ........................_..... Methyl hydrazine............ ..... ....,,......... ................... .............. . Methyl iodide........ -................ ..... ...... .................................... Methyl isobutyl ketone.--....... .. ......................................... ...... Methyl isocyanate --.... _............... .... ..................... ...... ..... ..... Methyl methacrylate,,_________________________ ____ ___ Michler*s ketone______________ ____ ____ ... ... .............__...... Molybdenum trioxide.... -..................... ................. ............. ............ Mustard gas [Ethane. 1.1'-thiobistZ-chloro-)......... .......... ............. Naphthalene________ _____________________________ .......... a/pha-Naphthytamine............ ................... ........ , ..................,,,, beta-Naphthytamine._-,_,_,,........... ............. ........ ........ ............ Nickel_______________________ ____ Nitric add...... ....... ......... ........ ....... NitrHotriacetic add............................ 5-Nitro-o-anisidine________________ Nitroberuene................. ........ ,,...... 4-Nitrobiphenyl......... _........ .... ...... S.beta. CAS No. Generic classification coda Effective date 606-20-2 117-64-0 123-91-1 122-96-7 1937-37-7 2602-46-2 16071-66-6 106-69-6 110-60-5 140-66-5 100-41-4 641-41-3 74-65-1 107-21-1 151-56-4 75-21-6 6-45-7 2194-17-2 50-00-0 76-44-6 116-74-1 67-68-3 77-47-4 67-72-1 1335-67-1 680-31-9 302-01-2 10034-93-2 764-01-07 74-90-8 7664-39-3 123-31-9 79-64-2 67-604 60-05-7 7439-92-1 56-69-9 108-31-6 12427-36-2 7439-96-5 108-78-1 7439-97-6 67-56-1 72-43-5 109-66-4 96-33-3 1634-04-4 101-14-4 101-61-1 101-68-6 74-95-3 101-77-9 78-93-3 60-34-4 74-88-4 108-10-1 624-85-9 80-62-6 90-94-6 1313-27-5 505-60-2 91-20-3 134-32-7 91-59-6 7440-02-0 7697-37-2 139-13-9 99-59-2 98-95-3 92-93-3 C12 C06 C06 C11 C14 C14 Cl 4 C06 006 COS C01 COS C01 C05 C11 C06 C13 009 C07 C03 C04 C03 COS C02 C04 CIS C11 C11 Cl 6 C16 Cl 6 C07 C07 C05 COS CIS C02 C08 C16 Cl 5 CIO CIS C05 C03 coe coe 006 CIO CIO C11 COS CIO C07 C11 C02 C07 C11 coe C07 Cl 5 Cl 3 C01 CIO CIO C15 C16 COS C12 Cl2 C12 01/01/67 01/01/87 01/01/67 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/67 01/01/67 01/01/87 01/01/67 01/01/87 01/01/67 01/01/67 01/01/67 01/01/67 01/01/87 01/01/87 01/01/67 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 ABD00295719 21172 Federal Register / Vol 52, No. 107 / Thursday, June 4, 1987 / Proposed Rules Chemical name Nrtrofen {Benzene, 2,4-diehloro*1-<4-nitrophenoxy>-] .........___--^-r-- Nitrogen mustard [2-Chloro-N^-chloroethyQ-N-rnetty1ethanamine].~~ Nitroglycerin____ _r................................ ,,........... ..................... ..... 2-Nrtrophenol...................................--------r----- 4-Nitrophenol_____ ,____________ ______ ,--.... ......... . ,ir-- 8-Nitropropane.......... .......... -..............., ------------- ----- -------------------- p Stitrft*ndtphenytamina---------------- ------------------- A</V-DimethylaniJine.......................... _........... ...... ................... --.......... Af-Nitrosodi-n-butylamine.......................... ....... ........, ,, --------- AfrNitrosodiethyiamine------------ --- ---- ------rr-............ ............... : MNitrosodimethylamine................. --.........--........-- , ..... MNitrosodiphenylamine_____________ __ ____ __________ __ ,,___ ___ N-Nitrosod^n-propytamine.....--...............----------- --------MNitrosomethytvinylamine----------------- --...........................--...... A/-Nitrosomorpholine.............. ........... --........, ..... .......... AZ-Nitroso-Methyturea ........ ............... ..... AMlitroso-AMnetbylurea------------------------- .............................................. AMJitrosonomicotine.... ........ .......... ----------------------- ---------- -------- AZ-Nitrosopiperidine....... .............. ..... ......... ............. ..... ............................ .. Octachioronaphthalene .............. -...................................... .................. Osmium tetromOe............ ........... ......... ............... ....... ........ ......... ,,........... Parathion [Phosphorothioc acid, O.Odtoth 1-0-<4-nitrophenyf)estarJ___ Pentachlorophenol (PCP)................., ,,,--__________ ______________ Peracetic add____________________________________________________ p-Phenylenediamine.................................. ..............................--........... 2-Phenyiphenol---- ------- ----------------------- --------..------- ------- ......... Phosphoric add___:______________________________ _____________ Phosphorus (yeftow or white)..._________ _______________ .. Phthalic anhydride.....______ ____ __ !__ ___________ ______ __________ Picric add.............................................. ................................................ Polychlorinated biphenyls (PCBs)__________ ---------- ------ ----------- ..---- Propane suttone ___ ______ ______ ------------------ -------,--............ beta-Propiolacione____ _____ -........ ... ..... --_______ ,,___,,_____ __ _ Propionaklehyde__ Propoxur [Phenol, 2-(1-methyletho*y)-,methytea^amats]._________ ... Propylene (Propene)____ __ ___ ...______ ___ ___________ .^.____ .... Propyleneimine_________________ __ ,,,................,.... ,,r,,......... Propylene oxide_____________________________ _____________ ____ ____ Pyridine--.... ......... --.--------------rrrrT,--- ------------------ ......___ Oumofine.....-...................... -........... ....... ,___ ______ ____ Quinone_______ ________ ___ _____________________ ____ ,,,, ,, Ouintozene [Benzene. pentachk>ronitro*J....________ _________ -- Saccharin (manufacturing) [1,2-8enzrsothiazol-3{2H)-ooe,1,1*<ficxide]._. Safrole__ ________________________ ___________ ____ __ ____ --........... Selenium........................ .............. ......................... ............ ...................... Silver and compounds_______________ ______-............ .......... Sodium hydroxide (solution)_________________ ______ ______ ___ ..____ Sodium sulfate (solution)____---__________________ ______ , Styrene......... ................ --___.__ --_______ _____________ __________ Styrene oxide________ ..__ ________________ ___________ ___________ Sulfuric acid........................... ... ______________________ ----riTTT, Terephihalic add__________ _________ ____________________ - 1.1,2.2-Tetrachioroethane............................ ............................................ Teirachloroethytene (Perchloroeihylene)__ _________ ___________ _________ .___________ TetracNorvinphos (Phosphoric add, 2-cMoro-l-<2.4,S-tricWorophenyf)etheny1 dbnethyl Thallium..------- -------------------------------__________________________ --_____ , , -.......... Thioacetamide.......--.... ...... ...... ....... .......... ........ ......... f--.............. .............. ..... :............. 4.4'-Thiodianiline Thiourea............. ............... Thorium dioxide....---- Titanium dioxide............ . Titanium tetrachloride ....... Toluene..................... ....... Toluene 2.4 disocyanate..... ToHjene-2.6-diisocyanate ..... O-ToKudine------------------ -- o-Tofuidine hydrochloride__ Toxaphene----------------------- CAS No. Generic classification code Effective date 1836-75-5 61-75-2 65-63-0 66-75-5 100-02-7 70-46-0 156-10-5 121-69-7 024-16-3 55-10-5 62-75-9 06-30-6 621-64-7 4540-40-6 50-69-2 750-73-9 664-03-5 16543-55-5 100-75-4 2234-13-1 20816-12-0 56-36-2 87-66-5 70-21-0 106-95-2 106-50-3 90-43-7 75-44-5 7664-36-2 7723-14-0 65-44-9 88-69-1 1336-36-3 1120-71-4 57-57-6 123-38-6 114-26-1 115-67-1 75-55-6 75-56-0 110-66-1 91-22-5 106-51-4 62-68-6 51-67-2 94-59-7 7782-40-2 7440-22-4 1310-73-2 7757-62-6 100-42-6 96-09-3 7664-93-9 100-21-0 79-34-5 127-18-4 961-11-5 7440-29-0 62-55-5 139-65-1 62-56-6 1314-20-1 13463-67-7 7550-45-0 105-88-3 684-84-9 91-09-7 95-63-4 636-21-6 6001-36-2 Cl 5 CIO C12 C12 C12 02 02 CIO C12 02 02 02 02 02 02 02 02 02 02 C04 05 03 C04 COS cos CIO C05 C09 06 06 COS C08 C04 03 COS C07 C09 C01 C11 C06 C11 C11 C07 02 COO C06 C16 05 06 06 C01 COS 06 COO C02 COS 03 05 03 03 03 05 05 05 C01 C11 C11 CIO CIO C02 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/07 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/87 01/01/87 01/01/87 01/01/87 01/01/67 01/01/67 01/01/67 ABD00295720 Federal Register / Vol 82, No. 107 / Hiursday, Jims 4, 1067 / Proposed Rules_________ >1173 Chemical name Trtokpm* t9 UyWMirarfMM.1 AwftnM,9 1.1 I.TrMtkvrMfharw {Mathyl Vinyl ec*te* 9 ft-Vylirfino CAS No. aBGu- em*ncerriacon code Effective date 08-76-6 62-68-6 120-62-1 71-68-6 79-00-6 7eVOe9-0eFOe1-64a 68-06-2 1962-09-6 95-63-6 128-72-7 91.79-6 7440-62-2 108-05-4 593-60-2 79-01-4 75-39-4 1330-20-7 106-38-3 99-47-6 106-42-3 67-62-7 7440-66-6 12122-67-7 C11 Cl 3 004 C02 C02 C03 004 C04 Cl 2 cot Cl 3 cos C15 COS C03 C03 COS C01 C01 C01 C01 CIO Cl 5 Cl 5 01/01/67 01/01/67 01/01/67 01/01/87 01/01/67 01/01/67 01/01/87 01/01/67 01/01/67 01/01/67 01/01/87 01/01/67 01/01/67 01/01/67 01/01/87 01/01/67 'I/O1/67 01/01/67 01/01/87 01/01/67 01/01/87 01/01/67 01/01/87 01/01/67 21178 ABD00295721 Federal Register / Vo) S2. No. 107 / Thursday. June 4, 1B67 / Proposed Rules (c) Chrmicaf cafexoriet in alphabetical orxfcr. Category name Generic tfasaftcaaon Effector# le Antimony compounds--indudes any unique chemical eubetenee tiat contain* antimony as part of thet ehemiceJ'* ..... ... ........... -- .............- Arsenic compounds-include* any mque chemical eubetenee Vwt oontain* arsenic a* part at thet Chemicei'* infrastructure................ ......... ..... -............... ............... .... --,,.................... _ --. ............... - Benum compounds--includes any irique chemical eubetenee Viet contains barium as part of Viat ehemcar* Infrastructure............................................ , ......... - , ................... Berytoum compounds--indudes any imique Chemical substance Vwl conteine bary*um as part of Ml chemical's rnfrastruetoee-- ................... . .................... -- ................. Cedmtum compounds--Indudes any tmique chemicei substance Viet contains cadmium as part of Vwt chemical'sinfrestruefcre-------------------,, ..... .....---- .......... CMorophenol*.,.... , ......... ........................ ..................... ..... ....... CIS CIS CIS CIS CIS CDS 01/01/87 01/01/87 C1/01/S7 01/01/67 1/01/87 01/01/17 Where s*1 lo 5 Chromium compounds--indudes any unique chemieat eubstenoe Viet contains Chromium as pert Of that Chemcart infrastructure_________________:............................................................ .. .......... -- , Cobalt compounds--indudes any unique chemical substance that oonteins cobalt as pert of that chemictf'a infrastructiee......................................... ...............................--,................... ................ ...... -........................... .. Copper compounds-indudes any unique chemical substance that contains copper as pert of Viet chont cel's infrastructure............................................ ......... ...............-.........................-...... ...................... ....... Cyanide compounds--X* CN* whera X=H* or any other group where a formal dissociation can be made. For eumpfe KCN, or CafCNh___________ _____ --.___________________________________________________ Glycol ethea--includes mono- and di- ethers of ethylene glycol diethyfene glycol, end triethytene g*ycd. . Where n1. 2. or 3 R = alkyl or aryl groups. R-R. H. or groups which, when removed, yield glycol ethers with the structure: R-(OCH2CMJ..w Polymers are eiduded from this category lead compounds--indudes any unique chemical substance that contains lead as pad of that chemical's infrastructure------------------------------------------- ----------------------------------------------------------------------------------------- Manganese compounds --indudes any unique chemical instance that contains manganese as pad of Viat Chemist's infrastructure______ --________ __ ____________ ---------------------- ---- ------------------------------- --- Mercury compounds--indudes any unique chemical substance that contains mercury as pad of Viat chemical's infrastructureI--------------------------------------------------------------------------------------------------- --- Nickd compounds--includes any unique chemical substance that contains ruckd as pad of that chemieaTs infrastructure.... .......................... ......... ......--.................................. --- Potybrominated biphenyl* (PBBs)__ _______________________ ...................--_____________ --........................- C15 01/01/67 CIS 01/01/67 CIS 01/01/67 CIS 01/01/07 006 01/01/67 CIS 01/01/67 CIS 01/01/87 CIS 01/01/87 CIS 01/01/67 COS 01/01/67 Where 1 lo 10 Selenium corr^aunds--indudes any unique chemical substance that contains selenium as pad Of Ml chemical's infrastructure____ --.____ _______________-----------------------------------------------------------------Silver compounds--indudes any unique chemical substance that contains s8ver as pad of that chemical's infrastructure________________--......................................................................... .... Tha'i'jm compounds--indudes any unique chemical substance Vial contains thtltum as pad of Viet chemical's infrastructure --------- -------------- ------------ --------------- ------------- ----- ------------------------------- ---- Zmc composmds todudet vy deque Chemical substance that contains tine as part of Vwl chamiears Mrastrucuae........... -- ..-- ................................. .......................... CIS 01/01/67 CIS 01/01/67 CIS 01/01/67 CIS 01/01/67 ABD00295722 B-l ENVIROPLAN APPENDIX B: TOXIC CHEMICAL RELEASE INVENTORY FORM (6/4/87 PROPOSED) ABD00295723 21180__________ Federal Register / Vol. 52, No. 107 / Thursday, June 4,19B7 / Proposed Rules Page 1 - of -- 5 Page* Form Approved OMB No. Important: Read instructions before completing form U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY Saction 313. Tltio IU of Tho Suporfund Amondmonta and Roauthorization Act of 1966 Approve Expfres: --T...... RJ,, H'k EPA Form A Report Number Calendar Year I. CERTIFICATION (toad end 4ign efltr eomplttbig all tftUonl '.s. ; I certify under penalty etliwMI have personally oamlnad and am familiar with tha *formation aubmtitad to tNa and aH attached Oximanta. ard mat i an my Inquiry of thoaa motvtduala Imrrwdlatoiy rasponalWo lor obtaining the Information, t boiiom that tho awBmlttod Informally la trua. ace*ato. erd wtmt. Slgnatura Name and official tltio of owner/operator or aanlor myagomeni official Oaio Signed II. FACILITY IDENTIFICATION A. Nam# and Location Namo___________________________________ Straot ADOwi City--------------State -- Zip. Canty. i i i-n rnC. FaeBty 1dent(fire _________ 6PA tdannncation Nurrtwr 1 I I I I 1 II I I j 1~| III III I I I I I I I Namo of ReedvtnQ Stream or Body of Water , . LOC ttamlHcalion fAxndar Q.i ~L 1.1 I I I I 1 I I II D. Parent Company Namo. B. Technical Contact Stroot Aooroaa FoeHtty Primary SC Coda | | | | | OBW MamFacturlng 1 I 8JC Code I___ | ~"~srs3QXI Owi S Bradatroot Nwrttor m-rm-rrmof Parent Comoany III. OFF-SITE LOCATIONS TO WHICH ANY TOXIC CHEMICAL 18 TRANSFERRED : < X A. Publicly Owned Treatment Works (POTW) Name ***-- 1 Typa of troatmont/diaooaal (antar oodo)' 1 1 Namo 1 s-*!: v 1 1 1 B. 1. Other off-stte location . _l la location unMr oontrqf of reporting facility or parent oompanyf ym no Typo of troatmant/diepoaal (arrtar oodol 1 1 1 1 1 Namo Typo Of troaimoni/dlepoeaf (antar ooda) 1111 J' |_Jh location trdm oorttrof of ropwttog faoUfty or parant oompany7 ^ Q m n Cheek If supplemental sheet Is atteched la location year control of reporting faculty or parent oompanyT ym no EPA Form 77*0-20 (6/67) ABD00295724 Federal Register / Vol. 52, No. 107 f Thursday, June 4.1987 / Proposed Rules_______ 21181 Pi|e . 2 of * _ pages Form R (continued) v.'Acnvm*<es***ain'vo./ uses OF.'THE TOXIC CHEMICACATYHEPACaJTY <CSdk *U th*t *ppiy) A. MANUFACTURE Produca) 1 C. OTHERWISE USED Aa a dwoieil pmaaa>og M| j - i yi.;;:maximum amount of the chemical:- . fcaj^-ON-SITE at ANY TIME DURtNO THE *>*$?5 ME- VP.., O-.A iRf. TlN''O -WPv.E. ,Rs I*OaTSDi.--' r*rWi'AA>'\W V^o>aaVOA--.,v.. f Check the Reporting Range Thai AppUe Weight Range to Pound* From... To... t"Pon| 1 Per on-alial 1 Mt/pTOCMi^LJ for Mi>iilnMla| | A* a byt'MuetJ^J Aa an Impurity[^"1 a. process Aa a raacianf | Ai tofwyittiqi; | | AaC*m*pno>n*enit*1| | fltptettjinj orv*y| ) Aa a "Wteh/iog aid Q Ancillary or gp ma [ | 0 90 100 1000 999 9.999 10.000 99.999 100.000 999.999 1.000.000 9.999.999 10.000.000 49.999.999 60.000.000 99.999.999 100.000.000 500.000.000 499.999.999 999.999.999 1 boon more then 1 bwon ABD00295725 21182 Federal Register / VoL 52. No. 107 / Thursday, June 4,1987 / Proposed Rules Page of pages Form R (continued) : v -<.:A.~>v:z:'<:.\.z: Tetri Release (fte^r) A. Emission to the Air Stc* or point air omisclona 8. Discharges to Water C. Releases to Land ] [ ,. Enter cods J D. Transfers to Off-Site Locations A OEnthtaerr HofoTc-k*itnoumlocfiaortion X OEnthteerr Hofofc-*kttfekjmlooceartion X Otnor o-ollo location - Entor Hock ntanoor f1-^1 f1""11 p--* 11 Basis of Estimate (Enter Code) n n n Tweni Sec. 304 Release 7 Yes No Permit Appsss to Relesse? Yes No n ... n Yes No Yes No n Yes No n Check If supplomontri sheet is attached. ABD00295726 Federal Register / Vol 82, No. 107 / Thursday, June 4,1987 / Proposed Rules Page of pages Form R (continued) VUf. WASTE TREATMENT METHODS AND EFFICIENCY^, General Wastestroam Check the box corretpondHg to the general waste#trearn. Q Gaseous W Watlewater L Uquld Waste (Non-Aqueous) 8 Solid Waste (Ineluding slurry/sludge) GWl 8 i- a. >. 4. . .. a. .. .. ii. . 14- Treatment Method (Enter Code) cITX1 c1 1 1 1 c1 1 1 c1 I 1 1 c1 1 1 1 c1 1 1 1 c1X1 1 c I11 c1 1 1 1 c1 1 1 1 c1 1 1 1 c1 1 1 1 L1 1 1 1 c_]_XXJ Range of Treatment Influent Efficiency Concentration Estimate (Enter Code) n ______% _% - % -. % % .. % ______ % ______ % % ______% % ______ Eased on Operating Data? yea no n " IX.\:PT10NAL INPORMAT1QNONWASTE Deserve actions taken since the last report to reduce the amount of toxic chemicals being released from the faculty. See the Instruction# for cooed items and explanation of what Information to Inciudo. or provfdo a narrative explanation In the space provided. Type |X*ti& ^Quantity of chemical tn the waslestrsam +:* Smo. d1*fk' --a. lioA nWi-'xi5' >. * prior to traatment/dlsposal^rrv ^tndeJt^vml 'Reason forAction ;(Enter Code) -: >GUirreennt^a4>^v.is*,^`^>J Prior h | OR Prc#Mj reporting" ' ^yav^fivifehang#^,,.,.., ..... <,**;<*'*' pCOS: Narrative Description 21183 Check If supplemental sheet is attached. ABD00295727 (O ENVIROPLAN