Document b5vGBqXJEQ4o42x2jo6kqNx5D
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1
CERTIFICATE OF ANALYSIS
A
Date:
September 29, 1992
Customer:
United Technologies P. O. Box 807
Mt. Airy, NC 27030
VBIA
Product 5415 PLWX 44258
Attention: Quality Control Manager
Order No* 0016404-000
Ship Date: September 28, 1992
Customer PO. No. 050-03088
Property
Test Method Specification Analysis
Moisture, %
ABR-1A
0.3 Max
0.14
Hard Particles 8 7 Mins.
ABR-12
25 Max.
2
Contamination, BLK/BRN
ABR-5A
35/100 Max.
4/7
Bulk Density, gm/cc
ABR-2B
0.460 Min.
0.504
Brabender Dry Time, Mins.
ABR-7
4.0 - 5.5
4.7
Particle Size Distribution
ABR-3
% On 40 Mesh
0.1 Max.
0.00
% On 200 Mesh
*NDS
5.2
% On Pan
2.0 Max*
1.8
Specification is 15.0% Max. for the 200 Mesh plus Pan
Residual VCM, ppm
ABGC-26
0.2 Max.
0.017
Inherent Viscosity
ABR-10
1.00 - 1.04
1.02
METS IR, % of Control
ABR-13
95% Min.
134%
h
Q>JUJ
Amy E. Bagwel Laboratory Supervisor
(601) 369-3624
VAB.0001202432
Vista Polymer's
Highway 25
Aberdeen, MS 3973q
A
RAXLOAR ANALY3 XS
Tb-ioy.
Load Date:
Product:
Car Ho.:
Time Logged In : ,lP JOC>
Logged In By: 7^/4 _____ Sllo(s): i //ZQ/
Ship Date:
Order No: Dol(,ik>U~ooo OS-0 oaoss'
Customer: Uju-fruf M4-. Aifi
(7TK)
Compartment Sample From Moisture %
A Bottom Top
CA
Bottom Top
CB Bottom Top
B Bottom Top
BL Contamination
BR
3 7
Bulk Density
/ 'J-fb
5 Hard Particle
7
2
Viscosity
\.0V2^
RVCM
y
l,
2 6
i
3 3 L 3
7J
7
SO?
Screen Analysis
_
<
_ m.
Mesh Weight
40
>>
% o.o
60
t.53
3.\
80
)% le(o 37-3
100
/<&2?
27?
120
78$
if' 8
140
3.^b ~7 /
200
a.
8- 2-
Pan 7
f.X
Drytime:
Static Flow: fP/
Avg . Microns: J
Color L:
O' VO b _bXL
METS:
Technician:
i*li T
//
VAB.0001202433
Vista Polymen A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
CERTIFICATE OF ANALYSIS
A
September 21, 1992
Customer:
United Technologies P. O. Box 807 Mt. Airy, NC 27030
VISIA
Product: 5415 Railcar No.: UTCX 46483
Attention: Quality Control Manager
Order No.: 0015945-000
Ship Date: September 11, 1992
Customer P.O. No.: 050-03033
Property
Test Method Specification Analvs
Moisture, %
ABR-1A
0.3 Max.
0.12
Hard Particles 8 7 Mins
ABR-12
25 Max.
1
Contamination, BLK/BRN
ABR-5A
35/100 Max. 23 / 8
Bulk Density, gm/cc
ABR-2B
0.460 Min.
0.494
Brabender Dry Time, Mins.
ABR-7
4.0 - 5.5
4.7
Particle Size Distribution
ABR-3
% On 40 Mesh
0.1 Max.
0.00
% On 200 Mesh
*NDS
5.1
% On Pan
2.0 Max.
1.6
is 15.0% Max. for the 200 Mesh plus Pan.
Residual VCM, ppm
ABGC-2 6
0.2 Max.
0.021
Inherent Viscosity
ABR-10
1.00 1.04
1.03
METS IR, % of Control
ABR-13
95% Min.
114%
///
Amy E .(JJagwel Laboratory Supervisor (601) 369-3624
m
pew
mmmm*
VAB.0001202434
Vista Polymers
Highway 25
Aberdeen, MS 3973q
RA.XRCAR ARALY3X3 UTOf.
Load Date:
Time Logged In: Di 07)
Product: Logged In By:
Car No.: Silo(s):
Ship Date:
Pi 2- Order No
D303S
Customer U.'TZLs, AAH-AlrTM
Compartment
*
Sample From
/ A
Bottom Top
Moisture %
BL Contamination
BR
Bulk Density
./
1x
7
io
CA Bottom Top
(!
u
CB Bottom Top
i
u9
to
B Bottom Top
/.
=3/ 4
&
5 Hard Particle
7
3
l
Viscosity RVCM
l.OZtff
.02A
Screen Analysis
Mesh
40
Weight % r7
0*2
60
i.SS
80
/%/*
32- 3
100 mi
<7$. 2
120
140
111 J.7/
iSJf 7.y
200
_St
Pan
8.7?
/
Drytime:
2
Static Flow
^
j
^ Avg Microns:
Color L: /&/*/_
0 03 b ///
METS: %21 /
%
Technician:
VAB.0001202435
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
CERTIRIGAY E OR ANALYSIS
Date:
September 4, 1992
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
Product: 5415 Railcar No.: PLWX 44723
Attention: Quality Control Manager
Order No.: 0015461-000
Ship Date: August 31, 1992
Customer P.0. No.: 050-02955
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh 515 On Pan Residual VCM, PPM Inherent Viscosity Hard Particle 0 7 Mins. Contamination, BLK/BRN METS IR, 515 of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analvsis 0.13 0.496 4.8
0.00 4.8 1 .6 0.011 1 .01 2 8/8 129
Amy E: Bagwe Laboratory Supervisor
(601) 369-3624
VAB.0001202436
Vista Polymar's
Highway 25
Aberdee n Ms 39730
A
Load Date :
T
Time Logged In: *
Ship Date: i^L
RAXLOAR ANALYSI3
Product: Logged In By: Order
Car No.: +*?Z3
Silo(s) : Customer:
UldjA
Screen Analysis
Me6h
40
Weight XP
&G
60 t'io /6
80
.37.0
100 120 140 /jT-37 X.fK sk3
4^1 7-3
200
2 Mt
y-ff
Pan
l?o
/<^
Drytime:
4-9
Static Flow: O
Avg. Microns:
Color L:
.
b / Y7
9%*4 ,i7X.u>
M ETS :
ISl
Technician:
/ .AtL
VAB.0001202437
Vista Polymers A Division of Vista Chemicol Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1
&
Date: 24 Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
visiaProduct: 541
Trailer No.: T- 32o
Attention: Quality Control Manager Ship Date: Z4
Order No.:
Customer P.0. No.: o SO -
9
Property
Test Method Specification Analysis
Moisture, %
ABR-1A
0.3 Max.
.n
Contamination, BLK/BRN
ABR-5A
35/100 Max.
2/7
Hard Particles @ 7 mins.
ABR-12
25 Max.
/
Bulk Density, gm/cc
ABR-2B
0.460 Min.
Brabender Drytime, mins.
ABR-7
4.0 - 5.5
s:o
Resin Flow Time, seconds
ABR-8
12 Max.
SJ
Particle Size Distribution
ABR-3
% On 40 Mesh
0.1 Max.
c.o
% On 200 Mesh
*NDS
6J
% On Pan
2.0 Max.
/.t
Specification is 15.0% Max. for the 200 Mesh plus Pan.
Residual VCM, ppm Inherent Viscosity
ABGC-26 ABR-10
/.02,
METS IR, % of Control
ABR-13
//7
** The value for this property is determined by our SQC Program and is not tested on truck shipments.
oratory Supervasor/Lead
(601) 369-8111
VAB.0001202438
PVC BULK TRAILER ANALYSIS
A
Date. t-zv-f z_
Product
Customer
, Silo ll
Technician
Al-A_______
Trailer Number Time
Order No.
FRONT
MOIST
Top Bottom
I w/
2.
CONT.
Ty I Bottom I
7
GEL
BULK OENSITY
I
166 2.
DRY TIME
l
sr.o
COLOR
L =/a#, ft
A=
B - A <v
II
I. I
L=
vise
RVCM
MIDDLE
I.
END
1
A=
B=
I I L*
A=
B=
Particle Size Distribution:
Screen Analysis_______ Z&_______Min
On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb
Mesh Size
40 60 80 100 120 140 200
Glassy Pan Part.
Gross Wt.
Tare
Net Wt.
% on Mesh
--A# ..
i Screen Analysis t
Mesh Size Gross Wt.
40
-
Min. 60
/t.J*
Us 3 2f* /
7.o4 Ji.S~
3.7~ 3. >V 7. 4, J
. *1 __J7ZA
A.t
On Rotap shaker 49 gms. Resin plus t .0 gms. Carb
Pan 80 100 120 140 200
Glassy Part.
Tare
Net Wt.
% on Mesh
Remarks
VAB.0001202439
Iw
Vista P6lymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111
CERTIRICATIE OR ANALYSIS
Date:
August 20, 1992
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
Product: 5415 Railcar No.: GACX 73408
Attention: Quality Control Manager
Order No.: 0014890-000
Ship Date: August 17, 1992
Customer P.O. No.: 050-02900
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh % On Pan Residual VCM, PPM Inherent Viscosity Hard Particle 9 1 Mins. Contarnination, BLK/BRN METS IR, % of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysis 0.12 0.496 4.7
0.00 4.6 1.5 0.014 1.02 1 4/4 130
Bagwe Laboratory Supervisor
(601) 369-3624
VAB.0001202440
*
Vista Polymers
Highway 25
Aberdeen, MS 3973q
:pvc railcar analysis
Load Date: P'/ffZ
Product
Car No.: 3of
Time Logged In : $000
Ship Date: dn
Logged In By:
Order No
-obO
Sllo(s): Customer
V 2. Cff~dL f
Compartment
A
Sample From
Bottom Top
Moisture %
BL Contamination
BR
, (2-
Bulk Density
.W
5 Hard Particle
7
3 J's
/
Viscosity
/<>W
RVCM
.0/4
2 Y
CA Bottom Top
Y
*s&o
4
-
Screen Analysis
Mesh Weight
%-P
40
o<o
o.O
60
/SI 3.0
80
if. 33 36?
100 /if 2^
JO<?
CB Bottom Top
B Bottom Top
.//
J' z
3
.// jr
,</9?
120 fccfg
J (*> la
140
7- 1
200 Pan </. 4 /<r
Drytime: < ?
Static F low :
o / s.fe Avg. Microns:
Color L: {00 -Z1 a <> b />^Q
METS:
z/35-6 %
Technician
/ZL' f
rr
VAB.0001202441
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
CERTIFICATE OE
Aberdeen, Mississippi 39730-0091 Phone {601)369*8111
ANALYSIS
k
Date:
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
visiaProduct: 541
Trailer No. : 7-^0/
Attention: Quality Control Manager Ship Date: >l/>/92~-
Order No.: 00!l{ci'7&-600 Customer P.0. No.: O50-0SLqt&
Property Moisture, %
Test Method ABR-1A
Specification 0.3 Max.
Analysis
,/7
Contamination, BLK/BRN
ABR-5A
35/100 Max.
*3 /
Hard Particles @ 7 mins.
ABR-12
25 Max.
i
Bulk Density, gm/cc
ABR-2B
0.460 Min.
5^1to
Brabender Drytime, mins. Resin Flow Time, seconds
ABR-7 ABR-8
4.0 - 5.5 12 Max.
q.n
Particle Size Distribution % On 40 Mesh % On 200 Mesh
ABR-3
0.1 Max. *NDS
o. o 4.Z
% On Pan
2.0 Max.
___/ b
Specification is 15.0% Max. for the 200 Mesh plus Pan.
Residual VCM, ppm
ABGC-26
.603
Inherent Viscosity
ABR-10
LOZ **
METS IR, % of Control
ABR-13
m
** The value for this property is determined by our SQC Program and is not tested on truck shipments.
Laboratory S
(601) 369-8111
al
sor/Lead
M vmm
mrnmmmmmmmmm
VAB.0001202442
mm
*
PVC BULK TRAILER ANALYSIS
Date Customer Technician
FRONT
Product Silo___
MOIST
Top Bottom
17.l
mmm
2.
CON'T.
Bottom
i
GEL
I
Trailer Number
_ Time (3t
Order No. >01+411:-pod
BULK DENSITY
DRY TIME
I
0
COLOR
Lp&s
A
vise CL
RVCM
* t,n
I L=
MIDDLE 2.
I
END
II
A=
B=
L= A= B=
Particle Size Distribution:
Screen Analysis
Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis
40
9.0
Mesh Size Gross Wt Tare Net Wt. % on Mesh
40
Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb 60 80 100 120 140 200
Glassy
Pan
Part.
_L93
ff&
3fP
P./P
lU
Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
Pan
60 80 100 120 140 200
Glassy Part.
Vista Polymers A Division of Vista Chemical Compony
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1
CERTX FICATE OF ANALYST
Date:
July 29, 1992
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
VISIA
Product: 5415 Railcar No.: UTCX 46555
Attention: Quality Control Manager
Order No.: 0014039-000
Ship Date: July 28, 1992
Customer P.0. No.: 050-02816
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh % On Pan Residual VCM, PPM Inherent Viscosity Hard Particle @ 7 Mins. Contamination, BLK/BRN METS IR, % of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysis 0.08 0.491 4.8
0.00 4.5
1.5
0.001 1.03 2 8/7 121
H. D. Lucas Laboratory Supervisor (601) 369-3624
mmm
m wrnmmmmmmmrnimmmmmKmmmm
p
VAB.0001202444
1
Vista Polymers
Highway 25
ifnt Aberdeen, MS 39730
7Load Date: //? /?
Time Logged Ship Date:
HAILCAH ANALYSTS
Cc'Tcr
Product
Car No.:
Logged In By: m
Silo(s) : L 9o
Order No
Customer ML
Compartment
A
Sample From
Bottom Top
Moisture %
BL Contamination
BR
,e?f
Bulk Density
5 Hard Particle
7
<ffZ -
f
(?
Viscosity RVCM
hOStf .oo\
CA Bottom Top
,<?7
7
&
.V7/
CB Bottom Top
o? f
7
/
..0f 5' _UIJ-
B Bottom Top
. 02
_L
7
. '/n''
=> 7
Screen Analysis
Mesh
40
Weight
% >.>
60
Drytime:
M
80 JD.8C
100
120
/?.r
Static Flow
&/
140 J?-91
Sjl
200
Avg. Microns:
Pan 22 /.
l(r s
Color L: /00*?? a 0-0/ b A r*'
METS:
/ /ZV. I %
Technician:
/?? * r ^ 4-t
VAB.0001202445
t
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
i F
Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1
V'S I S
A
.*
Date:
Customer:
United Technologies
P. 0. Box 807
Mt. Airy, NC
27030
Product: 5415
Trailer No.: 5~--37T
Attention: Quality Control Manager
Order No. : 00/3 "7
OQQ
Ship Date: z7--
Customer P.0. No.: &
" C) 2 7 Q</
Property
Moisture, V.
Contamination, BLK/BRN Hard Particles < 7 mins. Bulk Density, gm/cc
Test Method ABR-iA ABR-5A ABR-12 ABR-2B
Analysis
/3 3 /f
35 ,S03
Brabender Drytime, mins. Resin Flow Time, tap/sec.
ABR-7 ABR-8
>/ 8. V.
Particle Size, % on 40 Mesh
ABR-3
0,0
200 Mesh
Pan Residual VCM, ppm
ABGC-26
.DU
Inherent Viscosity
METS IR, V. of Control
ABR-10 ABR-13
/ '3
** **
Values for this property has been determined by our SQC Program and is not tested on truck shipments.
Laboratory Supervisor/Lead (601) 369-8111
mm
m mmi
wm
VAB.0001202446
1
PVC BULK TRAILER ANALYSIS
A
Date Customer
aac Aj*ry>
FRONT
Product *y/r Silo___ U ?o
Trailer Number 7^777
Time 0 O
Order Nn.
~o o o
MOIST
Top Bunoni
I 17..
CON'T.
I"E Bottom l
GEL
BULK DENSITY
I
2. 2.
DRY TIME
yj
COLOR
vise
= [0<U^|
= .*7
I
I
II
l
L-
RVCM
07^2.
MIDDLE 2.
I.
END
A=
B=
i L=
A=
B=
Particle Size Distribution:
Screen Analysis
/a
Mesh Size
40
Gross Wt.
Tare Net Wt. H on Mesh
-o^> 0,0
c. Screen Analysis
Mesh Size Gross Wt. Tare
Net Wt.
% on Mesh
40
Min On Rotap shaker. 49 gms. Resin plus l.Ogms. Carb 60 80 100 120 140 200
Glassy Pan Part.
a.3 OoSI P, 3? (Co MZ, 3.
ns xil.O v
i
J7l2 C-.6 m
Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
60 80 100
/SC8 <$'`Z7V'
120 140 200
/A'. 6? 8'Z r.9V
/ If ?.3
Glassy
/71 <Pan Part. ro^-7 *&S {76.??
Remarks
mm mm
*
X VAtf.uuuizuz4T7
Vista Polymers
A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1
Date:
July 15, 1992
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
...yisiA
Product Railcar No. VIPX 45897
Attention: Quality Control Manager
Order No. 0013462-000
Ship Date: July 10, 1992
Customer P.0. No. 050-02758
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh % On Pan Residual VCM, PPM Inherent Viscosity Hard Particle @ 7 Mins. Contamination, BLK/BRN METS IR, % of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysis 0.14 0.491 4.8
0.00
5.7
1.6 0.071 1.01 2 17 / 5 119
Laboratory Supervisor (601) 369-3624
VAB.0001202448
4
Vista Polymers
Highway 25
RAILCAR
Aberdeen, MS 39730
HI
SIS
Load Date
7
Time Logged
Ship Date
Product: 5415
Car No.:
Logged In By: l?> 4(,'Z't6 o
Order No oS~0-az7sry
s) : ^~&7(
U&ctiui
V5^ is] ..........
_________n
Compartment
Sample From
Bottom Top
Moisture %
BL Contamination
BR
`f
7
Bulk Density
WO
5 Hard Particle
7
'S ^t4fr
Viscosity
1.00*1
RVCM
.Oil
7
Y
Bottom Top
IT*
jL.
(&
j
7
jASa)
Bottom Top
.13
(p 2^ 2-
&
Bottom Top
,/J
17
J'
3L.
S~
i
Screen Analysis
Mesh
40
Weight %?
&*o &p
60
^vTS-
60
<5*)&& (*
100
_Y . _
Jt-7
3S.S-
120
Ms
140
3.S#
7/2^
200
-?-*Y ~ r"
sn
Pan
,g2_
Drytime:
Static Flow:
0 /ft.3 Avg. Microns:
/??>
Color L:
ab
METS: tf&'Z'O / I 1*1-0 %
Technician:
yf, 77 ft A_____
VAB.0001202449
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730 Phone (601} 369-8111
A
Date: Customer:
June 23, 1992
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
-VEIAProduct:
Railcar No.: VIPX 45900
Attention: Quality Control Manager
Order No.: 0012622-000
Ship Date: June 19, 1992
Customer P.O. No.: 050-02696
Property
Volatiles, %
Bulk Density, GM/CC
Brabender Dry Time, Mins.
Particle Size Distribution
% On 40 Mesh
% On 200 Mesh
X On Pan
Residual VCM, PPM
Inherent Viscosity
Hard Particle @ 7 Mins.
Contamination, BLK/BRN METS IR, % of Control
*
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR--5A ABR-13
Analysis 0.13 0.499 4.7
0.00 4.8 1.6 0.009 1.00 2 5/6 115
Amy Laboratory Supervisor
(601) 369-3624
VAB.0001202450
Vista Polymers
Highway 25
Aberdeen, MS 39730
Load Date: ~/<P- 9Z,
Product:
Car No. : */?&&
Time Logged In: 3>6>0O
Logged In By:
Silo(s):
Ship Date
Order No: 1
^ ^ "ODD Customer 02i> f/
Compartment Sample From
A Bottom Top
CA Bottom Top
CB Bottom Top
Moisture %
BL Contamination
BR
03
2A_
f
Bulk Density
5 Hard Particle
7
>?<?
\y>
V
/2--
2 1 jr
^fbO
Y 7
3
/
Viscosity RVCM
i.604 >004
B Bottom Top
n YJ
Jc
i
Screen Analysis
Mesh
40
Weight
X
60 J2JL
7
80
37-3
100
v
120
/>? 3/.3
140 _3L2
200
Pan
<2^^ ;0
/_
Drytime:
Static Flow:
/ ' b? Avg. Microns:
Color L: /O/ o? a & o2> b /'*/
METS: 21M /
%
Technician
W ST 4^ /, H
VAB.0001202451
>V
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111
A
Date:
June 8, 1992
VKIA
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
Product: 5415 Railcar No.: ACFX 53666
Attention: Quality Control Manager
Order No.: 0011990-000
Ship Date: June 3, 1992
Customer P.O. No.: 050-02610
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh % On Pan Residual VCM, PPM Inherent Viscosity Hard Particle @ 7 Mins. Contamination , BLK/BRN METS IR, % of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
CO
Analysis 0.19 0.511
0.00 6.4 1.8 0.024 1.01 1 7/8 113
Amy E. Bagwe Laboratory Supervisor
(601) 369-3624
VAB.0001202452
b
Vista Polvmers
Highway 25
Aberdeen, MS 3973ft
PVC R A I LO AR ANALYSIS
Load Date
-zh 9Z
Time Logged In:
Ship Date:
Product:
Car No.
Logged In By: Order No: m/to -60 0
02Mf b
Silo(6):
Customer JkR&d.Je-cK
Compartment
A
Sample From
Bottom Top
Moisture %
BL Contamination
BB
Bulk Density
n j_
$
5 Hard Particle
7
Viscosity
2/ ss
RVCM
D2&
CA Bottom Top
7 s -SO?
3 g
CB Bottom Top
B Bottom Top
, o2
7S
? 8e
.JS7
Screen Analysis
Mesh Weight
%
40
? <d > O
60
9?-
80 100 120 140 200 Pan
$ OZ toS ct./F >-9i-
^4.-4- (
2-1
6>,f IzX
Drytime: S&.
Static Flow: > L
Avg. Microns:
Color L: ff)/-
O'O ? b /.
METS: 4i4l L H3-I %
Technician:
VAB.0001202453
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111
CERTIFX CATE OF ANALYSX S
A
Date:
May 22, 1992
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
Attention: Quality Control Manager Ship Date: May 18, 1992
Product: Railcar No.: PLCX 43865
Order No.: 0011157-000 Customer P.0. No.: 050-02442
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh % On Pan Residual VCM, PPM Inherent Viscosity Hard Particle 7 Mins. Contamination, BLK/BRN METS IR, % of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysis 0.23 0.517 4.8
0.00 4.7 1.7 0.020 1.01 2 8/ 7 119
w lift Laboratory Supervisor (601) 369-3624
mmnmpN
VAB.0001202454
p
Vista Polymers
Highway 25
Aberdeen, MS 39730
RAILCAR ANALYSIS
Load Date : Time Logged In: Ship Date
*? Product:
Car No.:
o > Logged In By:
Silo(e) : <.93
Order No:
i %n~oco Customer:
Ob 6
Ujr /ki-
Compartment
A
Sample From
Bottom Top
Moisture %
.93
BL Contamination
BR
4~
Bulk Density
5
Hard Particle
7
44C-
Viscosity
hot*5
RVCM
.Dio
CA Bottom Top
21
g
.5f_
CB Bottom Top
T
B Bottom Top
>/(&
Screen Analysis
Mesh Weight
X
40
P-o*
0.0
60
j-30
80 100
D83M JOM,
MI
120
140
200
3
Pan
Drytime:
Static Flow: o L
Avg. Microns: IX ^
Color L:
cl<>3 b LSI
METS:
2*2/
L
ttf-4
ft*
Technician:
VAB.0001202455
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
IFIC
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
ANALYSIS
b
Date
Customer:
United Technologies
P. O. Box 807
Mt. Airy, NC
27030
Attention: Quality Control Manager
Ship Date:
VIS1AProduct: 5415
Trailer No.
5^7*7
Order No.: QO /
= 05d-024b<f
Customer P.0. No
Property
Moisture, V.
Contamination, BLK/BRN Hard Particles < 7 mins
Test Method ABR-1A ABR-5A ABR-12
Ana 1vsis
J23. 3 / S'
I
Bulk Density, gm/cc
ABR-2B
Brabender Drytime, mins Resin Flow Time, tap/sec.
ABR-7 ABR-8
0 / /0-O
Particle Size, 7. on
ABR-3
40 Mesh 200 Mesh Pan Residual VCM, ppm
ABGC-26
0.0 5-3 1.1
030
Inherent Viscosity METS IR, 7 of Control
ABR-10 ABR-13
LOob **
12-3 * #
* Values for this property has been determined by our SQC Program and is not tested on truck shipments.
ory Sup
(601) 369-8111
isor/Lead
VAB.0001202456
%
V
PVC BULK TRAILER ANALYSIS
4.
&
Date Customer Technician
Product .Jejd 7Silo
V- tf
>*7 > -<>*?__
Trailer Number / -3"?? Time /*?*>o
Order
FRONT
MOIST
CONT.
Bottom ) Top
Bottom
, o5 ' 3
fir
GEL
i
BULK DENSITY
1
/* *
Il
DRY TIME
COLOR
L=
=
=
L=
vise
RVCM
.<>3^
MIDDLE
A=
ii
END
A=
Particle Size Distribution:
Screen Analysis
Mesh Size
Gross Wt.
Tare
S?
Net Wt.
% on Mesh
Screen Analysis
Mesh Size
*
Gross Wt.
Tare
Net Wt.
% on Mesh
40
{P. &
D-- -O
40
Min On Rotap sibaker. 49 gms. Resin |>lus 1.0 gins. Carb 60 80 100 120 140 200
Glassy Pan Part.
(\
1
-SV
//
Min.
8-37 37. U 2? 7i A-7* 7-7
On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
60 80 100 120 140 200
.g3
A7
vI'GsoaJ /*7C
Glassy Pan Part.
Remarks
+ T
--"mumu mmmmm
1
%
Vista Polymers
Highway 25
Aderdeen, Mississippi 39730-0091
A
A Division of
Post Office Box 91
Phone (601) 369-8111
Vista Chemical Company
Date:
5/7/92
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
Attention: Quality Control Manager
Ship Date: 5/5/92
VISIA
Product 5415
Railcar No. UTCX 46550
Order No. 0010666-000
Customer P.0. No. 050-02485
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh % On Pan Residual VCM, PPM Inherent Viscosity Hard Particle @ 7 Mins. Contamination, BLK/BRN METS IR, % of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
o
o*
Analysis
0.499 4.8
0.00 4.3 1.3 0.026 1.03 2 6/8 120
H.D. Lucas Laboratory Supervisor
(601) 369-3624
m
VAB.0001202458
Vista Polymers
Highway 25
Aberdeen, MS 39730
/r
Load Date Time Logged In: Ship Date :
RAILCAR ANALYSIS
Cl TCX
Product:
Car No.
^^3 O
2-3 00
Logged In By: s* r
Silo(s): >?o -6 ?/-
---- Order No:
(ofoCp'^iDOl?, ustomer
//Tomr
Screen Analysis
Mesh
40
Weight
%P
O
60 .<?$
2.V
80 JlaSt
4PX
100 3s?C
120
/S-<f
140 3-1^
&?- 2_
200
3
Pan ' (p (z>
Aj
Drytime:
Static Flow: >
Avg. Microns: / *7J5T
Color L: /^- 91 a 0-1? b /V?
Q3ooMETS:
/ //?< %
Technician: stfa'T'
VAB.0001202459
Vista Polymers
A Division of
Vista Chemical Company
I
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1
ANALYSIS
Date:
/ 0 - "2__
Customer:
United Technologies
P- O. Box 807
Mt. Airy, NC
27030
Product: 5415
Trailer No.:
88
Attention: Quality Control Manager
Ship Date:
2___
Order No.: #0/0 23 /" 00
Customer P.0. No.:
Propertv
7.Moisture,
Contamination, BLK/BRN
@Hard Particles
7 mins.
Bulk Density, gm/cc
Test Method ABR-1A ABR-5A ABR-12 ABR-2B
Analvsis
.0? 3
/ SO'-I
Brabender Drytime, mins.
Resin Flow Time, tap/sec.
7.Particle Size,
on
ABR-7 ABR-8 ABR-3
,,.0 / 9-/
40 Mesh 200 Mesh Pan
d>-o /S'
Residual VCM, ppm
Inherent Viscosity
7.METS IR,
of Control
ABGC-26 ABR-10 ABR-13
,0/U / 0 *2- * * /JlS **
** Values for this property has been determined by our SQC Program and is not tested on truck shipments.
Laboratory Supervisor/Lead (601) 369-8111
VAB.0001202460
t
PVC BULK TRAILER ANALYSIS
Date Customer LKT2L
Technician Zx&HPL-
Product Silo___
#o
Trailer Number. Time 3*^ ~finS"
Order No.
k
Panicle Size Distribution:
Screen Analysis
Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis
Mesh Size Gross Wt. Tare Net Wt. % on Mesh
40
Remarks
Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb
80 100 120 140 200
Glassy Pan Part.
&S?
II.ZL fa. S.4
fi.Vf-
If
On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
Glassy Pan Part.
60 100 120 140 200
Stsr 207A
Revised 1/12/87
nppv
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
CERT
OF ANALYSIS
Date:
Customer:
United Technologies 2500 Highway 6E Iowa City, IA 52240
Product: 5415
Trailer No. : /
Attention: Quality Control Manager
Order No.: >008& g <f--o o o
Ship Date: 3-2'*?'*?^'
Customer P.0. No.:
3
Propertv
Test Method
Analysis
Moisture, V.
ABR-1A
Contamination, BLK/BRN
ABR-5A
7 / /D
Hard Particles & 7 mins.
ABR-12
G?
Bulk Density, gm/cc
ABR-2B
Brabender Drytime, mins.
ABR-7
7
Resin Flow Time, tap/sec.
ABR-8
/
Particle Size, V. on
ABR-3
40 Mesh
>. O
200 Mesh
Pan
/ 2.
Residual VCM, ppm
ABGC-26
.ML,
Inherent Viscosity
ABR-10
I . o'X' **
METS IR,
of Control
ABR-13
lit
He*
#* Values for this property has been determined by our SQC Program and is not tested on truck s ipments.
Laboratory Supervisor/Lead (601) 369-8111
VAB.0001202462
- * *
*
PVC BULK TRAILER ANALYSIS
*
Date T- 27- y
Customer
Technician
<7
Product
l-KUN I
MOIST
CONT.
Top | Bottom Top
Bottom
0&I
1
2.
'?
1 /*>
lI
GEL
I
Trailer Number
Time / 7^ *
Order No. >&& 8%&
BULK DENSITY
I
.4-9
DRY TIME
I
Y-7
COLOR
L =/>
= ~0.O7
B = /<z / I L*
> Q&
vise RVCM
MIDDLE 2.
I
END
A-
B=
i.
ii
i
L-
A=
B=
Particle Size Distribution:
m
Screen Analysis/S.______________ Min
On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb
Mesh Size
60 80 100 120 140 200
Glassy Pan Part.
Gross Wt.
Tare Net Wt. % on Mesh
0.0 0*0
/.i:2-
aa.S' /3-'
3/2- a-22-
2 .
J. Screen Analysis
____ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
Mesh Size Gross Wt.
40 60 80 __________ _________ _________
100 _________
120 _________
140 200 _________ _________
Pan
Glassy Part.
Tare
_________ _________ ________ _ _________ _________ ________
Net Wt.
..................
............................ ..................... ................. ................. ................. .................. ........
% on Mesh
__________ _________
Remarks
%
Star 207A Revised 1/12/87
4
Vista Polymers
A Division of
Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1
A
IFIC
VS I S
Da te: sjsd/qa.
Customer:
United Technologies
P. 0. Box 807
Mt. Airy, NC
27030
Attention: Quality Control Manager
VIS1AProduct: 5415
Trailer No.:
Order No.: 0DOQC^f^C)O2^
Ship Date:
Customer P.0. No.: CK50-02-32 /
Property
Moisture, V,
Contamination, BLK/BRN Hard Particles @ 7 mins.
Test Method ABR-1A ABR-5A ABR-12
Ana1ysis
. lo
f/6
0-
Bulk Density, gm/cc
ABR-2B
Brabender Drytime, mins. Resin Flow Time, tap/sec.
ABR-7 ABR-8
O / //. u
Particle Size, /i on 40 Mesh
ABR-3
0.0
200 Mesh Pan
J. (jp
Residual VCM, ppm Inherent Viscosity
METS IR, 7. of Control
ABGC--26 ABR-10 ABR-13
-<932-
/ *
/!&
*
** Values for this property has been determined by our SQC Program and is not tested on truck shipments.
Laboratory Supet-visor/Lead (601) 369-8111
m mrnmmmmmmm m
VAB.0001202464
*
PVC BULK TRAILER ANALYSIS
Date Customer Technician
UT<Z~~
m^L
Product S^/JT Silo___ &?o
Trailer Number
Time fi * Order No f)0 O ZLfiST-002^
FRONT
MOIST
Top Bottom
1 r/O
2.
CON'T.
Top 1 Bottom
'..A....
/\
2
GEL
l
BULK DENSITY
l
2-Ar , SO?
2.
DRY TIME
.1
'
I
I
I I.
I
COLOR
vise RVCM
A = -v/J
B = JJC
L=
MIDDLE 2.
A=
B=
i
ii
I
L=
END
2.
A= B-
Particle Size Distribution:
Screen Analyst*______ LQlMin
On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carto
Mesh Size
40 60 80 100 120 140 200
Glassy Pan Part.
Gross Wt.
Tare Net Wt. H on Mesh
4*60
.s-f
11.17 7.l4 J.3? 2*7,7 # $ o
0.0 /iO 43.7 17.1
C.f 4*f~ At.
i Screen Analysis t
$
Mesh Size Gross Wt.
40
Min.
3.1f
60
On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
f3.XZ 4kT^7 /f.r4> y.rz. 4.0 f
80 100 120 140 200
* 3,7, Glassy Pan Part.
/7
Tare
Net Wt.
% on Mesh
Remarks
Star 207A Revised 1/12/87
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1
CERT I
I CATE O F~ ANALYS I S
k
Date:
Customer:
United Technologies
P. 0. Box 807
Mt. Airy, NC
27030
Produc t: Trai1er No.:
Attention Quality Control Manager
Order No . : OOO
Ship Date
Customer P.0. No.: OSO w
3<5 /
Propertv
Test Method
Ana 1ysis
Moisture, V.
ABR-1A
Contamination, BLK/BRN Hard Particles @ 7 mins. Bulk Density, gm/cc Brabender Drytime, mins. Resin Flow Time, tap/sec
ABR-5A ABR-12 ABR-2B ABR-7 ABR-8
/ . 56*)
S~ o o ,9.&
Particle Size, 7. on 40 Mesh 200 Mesh Pan
Residual VCM, ppm Inherent Viscosity METS IR, 7. of Control
ABR-3
ABGC-26 ABR-10 ABR-13
o. o
44
Lb___
,0Z 7
/ 02- * *
//&
**
Values for this property has been determined by our SQC Program and is not tested on truck shipments.
Laboratory (601) 369--Bi11
VAB.0001202466
PVC BULK TRAILER ANALYSIS
Date Customer u.T~C.
Technician UlA: >
Product Silo___
5<//i
MOIST
Top | Bottom
13
CONT.
Top Bottom
i
GEL
l
FRONT 2.
2.
Trailer Number
377
Time 111
Order No. O &C>S^OOQ-
BULK DENSITY
I
>3
DRY TIME
I
fie
COLOR
L =f0f,0
RVCM
1. I. I
MIDDLE 2.
i. i
END
Particle Size Distribution:
Screen Analysis
Mesh Size
40
Gross Wt.
Tare
Net Wt.
0.0 0
H on Mesh Screen Analysis
oh. .o
Mesh Size Gross Wt. Tare Net Wt. % on Mesh
40
Min On Rotap shlaker. 49<jms. Resin |plus 1.0 gims. Carb 60 80 100 120 140 200
Glassy Pan Pari.
.33 3 0.72. IS. io 7SO 3.33 3.n "or i?3.l 3o.3 IS.*: Ul MH i.s
Min. On Rotap shaker 49 gma. Resin plus 1.0 gms. Carb
Pan 60 80 100 120 140 200
Glassy Part.
Remarks
Star 207A Revised 1/12/87
4 v
Aberdeen Chemical Plant
LOADING ORDER
DATE PREPARED: ORDER NO.: SHIP DATE CUSTOMER
OOo
a/2- ?
(AV/ttf TEjCU-
PRODUCT TYPE: PRODUCT FROM CUSTOMER LOCATION:
SPECIAL INSTRUCTIONS:
3WWE&T ny4rt
VISTA A 1
, Me
YARD LOADING
LAB APPROVAL
LOADED/SAMPLED BY:
APPROVED BY
zTIME/DATE:
(VI I Z?SCOMMENTS
2
TIME/DATE:
YARD OPERATOR SHIPPING INSPECTION
CAR/TRAILER INSPECTED BY:
TIME/DATE:
PRODUCT LAST CONTAINED
APPROVAL FOR LOADING:
RAILCAR INSPECTION
COMPARTMENT
A
oJc. x = Problem
CA CB
B
CAR/TRAILER APPROVED
NO
d(f^?
GENERAL APPEARANCE - GOO
POOR
TRAILER INSPECTION
TIRES
PRODUCT IN CAR DOMELIDS WALKWAYS HANDWHEELS CAPS LOCKING ARMS CAP HOLDERS/LOCKS PUNCTURES
TRAILER BODY CONDITION
DOME LIDS (INCLUDING GASKETS)
HOSES (IF USED)
UNLOADING/SAMPLE VALVES
LANDING GEAR (DOLLEY LEGS)
DUST CAPS (U/L LIN E CAP)
MUD FLAPS WINTERIZATION NEED TO WASH
YES NO
COMMENTS: -Vo Da,, 7tfW\
2468
f-
DELIVER 8 8 A.H
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111
CERTI RICAT E O R ANALYSTS
Date:
April 3, 1992
Customer:
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
Attention: Quality Control Manager
Ship Date: March 31, 1992
Product: 5415 Railcar No.: UTCX 46550
Order No.: 0009075-000 Customer P.0. No.: 050-02347
Property
Volatiles, %
Bulk Density, GM/CC
Brabender Dry Time, Mins.
Particle Size Distribution
% On 40 Mesh
% On 200 Mesh
% On Pan
Residual VCM, PPM Inherent Viscosity
h
Hard Particle Q 1 Mins.
Contamination, BLK/BRN
METS IR, SIS of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysi 0.14 0.513 4.7
0.00 5.0 0.6 0.288 1 .02 18 7/8
0
i<
UJ
Amy E. Bagwell Laboratory Supervisor
(601) 369-3624
VAB.0001202470
Vista Polymers
Highway 25
Aberdeen, MS 39730
RAILCAR ANALYSIS
; J3 -/2 '92.
Load Date:
Product:
Car No.:
Time Logged
: ALogged In By
Silo(6): ^ 96 +69/
Ship Date:
: UXCL' Mrh XLOrder No:. tfD'?cT''C,oo Customer
ioa j
Screen Analysis
Mesh Weight
%f
40
9.*
a. _
60
(f> /-^
80
/?.f^
37.2
100
a?.?
120
g.s-1
/7.y
140
3-SS IS
200
Pan
22_
*&
Drytime:
Static Flow:
/ iz./ Avg. Microns: .
Color L: J&L 12L a
b /' ^
METS: %tc L I'M- s~
Technician
JL
VAB.0001202471
Vista Polymers
A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111
CERTIRICATE OR ANALYSIS
Date:
March 16, 1992
Customer:
United Technologies P. O. Box 807 Mt. Airy, NC 27030
Attention: Quality Control Manager
Ship Date: March 12, 1992
VKAProduct: 5415
Railcar No. VIPX Order No.: 0008338-000
Customer P.0. No.: 050-02294
Property Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
% On 40 Mesh % On 200 Mesh % On Pan Residual VCM, PPM Inherent Viscosity Hard Particle e 1 Mins. Contamination, BLK/BRN METS IR, % of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysis 0.17 0.503 5.0
0.00
5.5
1 .8
0.017 1 .01
1
6/9 122
my E. Bagwell Laboratory Supervisor
(601 ) 369-3624
%
VAB.0001202472
*
t
Vista Polymers
Highway 25
Aberdeen, MS 39730
&
rvc railcar analysis
Load Date: Time Logged In: Ship Date:
Product:
Car No.:
Logged In By: Order No: f)0O&
Silo(s)
Customer:
A/---~
Compartment
A
Sample From
_
Bottom Top
Moisture %
BL Contamination
BR
Bulk Density
5 Hard Particle
7
. /r
*? , r2/
tPc-
l)
Viscosity RVCM
IM 't>m
CA Bottom Top
v/
f (=>
i^
H T
.
CB Bottom Top
,/J
& . r*/
7
B Bottom Top
,/7
9
,SoJ
f=
Screen Analysis
Mesh
40
Weight
i*Q0
60 /
6
80
ZJ.I* 42.3
100
11,7/ Z<L4
120 7.2 S'
Jt.k
140
0
7.7
200 *.?7
.S
Pan
. 70 /. P
Dry time:
Static Flow: * /17 Avg. Microns: 17S-.2,
Color L: /**+*<> a
*6 b
METS: %zjb,m~x
Technician:
St4 ^TB
1
VAB.0001202473
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1
CERTIPICATE OF ANALYSIS
Date:
March 2, 1992
Customer
United Technologies P. 0. Box 807 Mt. Airy, NC 27030
Attention: Quality Control Manager
Ship Date: February 25, 1992
VISIAProduct: 5415
Railcar No.: ACFX 54589 Order No.: 0007457-001
Customer P.Q. No.: 050-02214
Property
* HUM!
Volatiles, %
Bulk Density, GM/CC
Brabender Dry Time, Mins.
Particle Size Distribution
% On 40 Mesh
% On 200 Mesh
% On Pan
Residual VCM, PPM
Inherent Viscosity
Hard Particle @ 7 Mins.
Contamination, BLK/BRN
METS IR, % of Control
Test Method
****n^Mii
in+ii
ABR-1A
ABR-2B
ABR-7
ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysis
0.18 0.516 5.0
0.00
4.9 1.5
0.010 1.01
1
3/ 4 119
Laboratory Supervisor
(601) 369-3624
VAB.0001202474
Viata Polymers
Highway 25
Aberdeen, MS 39730
fa \
RAILCAR ANALYSIS
Load Date: z
-72-
Product :
Time Logged In: /L oo
Ship Date:
'ihC
/Vo M77
Compartment
Logged In By: Order No
050
A CA
Sample From
Bottom Top Bottom Top
Moisture %
BL Contamination
BR
VZ
z
J5
JLZ
l 5
j
Bulk Density
- .5/6
7 Hard Particle
5
2, Ijti,
Viscosity RVCM
hccf>
M
Car Ho.: Silo(s);
Customer -*
CB
Bottom Top
JS
3 c
510
Z
11
B
Bottom Top
/
/d
Screen Analysis
Mesh Weight
40
Q.oo
% Q.CO
60
0.3Z
&.h
80
/f.So
37.0
100
Zf.O
120
jtA.
140
3. SO
7-6
200
4l
Pan
/ 5"
Drytime:
N.ZStatic Flow: o /
Avg. Microns
Color L: //, o/
b/
METS
%
Technician:
mmm mm wmmmm
4- 1 *n
VAB.0001202475
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
IF I C
El O
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
A N A vs i s
ft
Date: ftJo. 17.
Customer:
United Technologies
P. 0. Box 807
Mt. Airy. NC
27030
VIS1AProduct: 5415
Trailer No.
Attention: Quality Control Manager
Order No.: 000*71*4*}'OO /
Ship Date:
)/7(
Customer P.0. No
2/74
Propertv Moisture, 7. Contamination, BLK/BRN Hard Particles @ 7 mins
Test Method ABR-1A ABR-5A ABR-I2
Analysis
J2l
6
/
/
Bulk Density, gm/cc Brabender Drytime, mins. Resin Flow Time, tap/sec
ABR-2B ABR-7 ABR-8
<64
0 / Ho
Particle Size, V. on
ABR-3
40 Mesh 200 Mesh Pan
QJL
3.4
L
Residual VCM, ppm Inherent Viscosity METS IR, 7. of Control
ABGC-26 ABR-10
ABR-13
lDol
J. o3 * *
//4 *#
Values for this property has been determined by our SQC Program and is not tested on truck shipments.
Laboratory Sup (601) 369-8111
sor/Lead
VAB.0001202476
1
4
77-52=
Customer Technician
PVC BULK TRAILER ANALYSIS
Particle Size Distribution:
Screen Analyst*
Min On Rotap shaker* 49 gins. Resin |)lus 1.0 gims. Cart)
Mesh Size
40 60 80 100 120 140 200
Gross Wt.
Tare /P V
Net Wt.
% on Mesh
o. tx? 0.0
0.3&
f#$3 /Ce ls' #7
A&
37
/*/
7.0
t Screen Analysis
Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
Mesh Size Gross Wt.
40 60 80 100 120 140 200
Tare
Net Wt.
% on Mesh
Glassy Psn Part.
aC4t l*f-
Glassy Pan Part.
Remarks
*
VAB.0001202477
IHIP
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 9 1
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
CERTIFICATE OF ANALYSIS
Date: ft\o. 13, tWZ-
Customer:
United Technologies
P. O. Box B07
Mt. Airy, NC
27030
Product: 5415
Trailer No.: (fSQ
Attention: Quality Control Manager
Order No. : OOQ*")'/"0&&
Ship Date:
Customer P.0. No.: 0~~&LI*1
Property
Moisture, V.
Contamination, BLK/BRN
Hard Particles @ 7 mins.
Bulk Density, gm/cc
Test Method ABR-1A ABR-5A ABR-12 ABR-2B
Analysis
. o6~ 6/3
/
.447
Brabender Drytime, mins. Resin Flow Time, tap/sec.
Particle Size, V. on
ABR-7 ABR-B ABR-3
0 / /0.8
40 Mesh 200 Mesh Pan
0.0
4.5 /.4
Residual VCM, ppm Inherent Viscosity
ABGC-26 ABR-10
.on /*03 *#
METS IR, 7. of Control
ABR-13
*
Values for this property has been determined by our SQC Program and is not tested on truck shipments.
Laborat (601) 369-8111
isor/Lead
M mm
mm m
VAB.0001202478
Hflt
"2. - / 3 Z--
PVC BULK TRAILER ANALYSIS
Product
______________ Trailer Number /
Particle Size Distribution:
Screen Analysts
Mesh Size Gross W1 Tare Net Wt % on Mesh Screen Analysis
40
oQ &,<=>
Mesh Size
40
Gross Wt.
Tsre rtj.e'**
Net Wt
H on Mesh
Min On Rotsp shaker. 49 ams. Resin plus 1.0 gms. Csrh 60 80 100 120 140 200
Glassy Pan Part.
Lf
Min.
/?. ro
77
3,7 7 ?
29.S ns 7^
-
On Rotsp shaker 49 gms. Resin plus 1.0 gms. Carfo
60 100 120 140 200
2n Hi Yf- /
H
JZ2,
id
Glassy Pan Part.
. 2> mi
Remarks
VAB.0001202479
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
CERTIFICATE OF
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
XS
Date:
February 12, 1992
Customer:
United Technologies
P. 0. Box 807
Mt. Airy, NC
27030
Attention: Quality Control Manager
Ship Date: February 5, 1992
Product: Railcar No.: ACFX 41140
Order No.: 0006764-000 Customer P.0. No. 050-02148
Property Volatiles, 7. Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
V. On 40 Mesh V. On 200 Mesh
7. On Pan Residual VCM, PPM Inherent Viscosity Hard Particle @ 7 Mins. Contamination, BLK/BRN METS IR, 7. of Contro1
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analvsis
0.20
0.504 4.9
0.00
4.4 1.3 0.009
1.01
1
18 / 29
122
agw Laboratory
dl
'visor
(601) 369-3624
VAB.0001202480
Viata Polymers r
Load Date: 2-5
Time Logged Ship Date
z-
Highway 25
Aberdeen, MS 39730
h
RAILCAR ANALYSTS
Product:
Logged In By:
0OC>L%<-f
QSb-oaifi
Car No. : iZZ/V0
Silo(s) :
-6?Z
LLitizi
1M
pi*-folds
Compartment
A
Sample From
Bottom Top
Moisture %
BL Contamination
BR
. 2o
/f
24
Bulk Density
,5&?
7
Hard Particle
/
5 LM
Viscosity RVCM
Loll
jM
CA Bottom Top
CB Bottom Top
dl.
+
Ill
jS
to 2,
2
B Bottom Top
+
23
Screen Analysis
0.C
Mesh
40
Weight 0*00
% *0
-2.2 60
/,/
: 49 Drytime
St>.s 80
22-Sir
'9.6 100
ts.gy
felt
P7.r7.
A?./ 120
7.cS 1.2.
140 3. //
(>.2-
A *7 200
VI
Static Flow:
0 /X3.P Avg. Microns:
'z Pan c.is
/3
A 7Color L: /^<
a b7_ b /*
, to / m. 7
METS
Technician:
VAB.0001202481
9
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
CERTIFICATE OF
Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111
IS
4
Date:
January 20, 1992
Customer:
United Technologies
P. 0. Box 807
Mt. Airy, NC
27030
Attention: Quality Control Manager
Ship Date: January 17, 1992
VEIAProduct: 5415
Railcar No. PLWX 44680
Order No. 0005888-000
Customer P.0. No
050-02072
Property Vo 1 a t i 1 es, 7. Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution
7. On 40 Mesh
Vm On 200 Mesh
7. On Pan Residual VCM, PPM Inherent Viscosity Hard Particle @ 7 Mins. Contamination, BLK/BRN METS IR, 7. of Control
Test Method ABR-1A ABR-2B ABR-7 ABR-3
ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13
Analysis
0.11
0.510 4.8
0.00
5.1 1.4
0.010 1.02
2
3/ 5 119
t
Amy E. Bagvtell '-- Laboratory Supervisor
(601) 369-3624
VAB.0001202482
Viata Polymers
Highway 25
Aberdeen, MS 39730
*
Load Date:
Product:
Time Logged In: / ~?3
Ship Date: / / ("7 /*7^"
Logged In By: Order No:
4?o
Silo(s) U,C9/ 00& Customer:
Compartment
A
Sample From
Bottom Top
Moisture %
BL Contamination
BR
3
7
t.
Bulk Density
7 Hard Particle
5 pa.lP
Viscosity RVCM
foul'
*0(0
CA Bottom Top
* 0 C?
*L
3
*//
CB Bottom Top
I
H
.Si7
S
1
B
Bottom Top
ol
z&
z
Screen Awnalysis
Mesh
40
Weight 0.00
%
60 0.1!
0.4
80
IS. so 3t?,b
100 IS.<e
31.1
120
S7o J7S
140 S.ftf
7.9
200 JS.I
Pan 0.72-
A4
Drytime: 4.p
Static Flow:
o //// Avg. Microns:
Color L:
&O a
b
METS:
/ llrf-4*.
/
CoTechnician:
V"
VAB.0001202483
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111
A
CD V S I s
Date: / -- 7"7ff-
Customer:
United Technologies
P. Q. Box 807
Mt. Airy, NC
27030
Attention: Ship Date:
Quality Control
Manager
4 a*
- VISIAProduc t
Trailer No.
Order No.: t>oe> *?6>3l~e>o&
Customer P.0. No. : Q 0 ~~ 0
Property
Moisture, 7.
Contamination, BLK/BRN Hard Particles @ 7 mins.
Test Method ABR-1A ABR-5A ABR-12
Analysis
-Pb
7 / *b
/
Bulk Density, gm/cc
ABR-2B
Brabender Drytime, mins. Resin Flow Time, tap/sec.
ABR-7 ABR-8
o / //.?
Particle Size, 7. on
40 Mesh
ABR-3
e.6c>
200 Mesh
Pan Residual VCM, ppm
ABGC-26
.00)
Inherent Viscosity METS IR, % of Control
ABR-10 ABR-13
117 **
** Values for this property has been determi ned by our SQC Program and is not tested on truck shipments.
Laboratory Supervisor/Lead (601) 369-8111
VAB.0001202484
PVC BULK TRAILER ANALYSIS
\
A
Date
Product
Trailer Number
Customer L&L
Silo
Time
Technician.
m
FRONT
Order No.
MOIST
Too Bottom
. 'if
2.
CON'T.
Top Bottom
/T
GEL
iytUP
BULK DENSITY
l
DRY TIME
I
MsS
COLOR
vise
/odM-
0.6U
1. i I
B /-= S(
L=
RVCM
%.i
MIDDLE
I
ENDMl MM
i
i
A=
B= L= A= B=
Particle Size Distribution:
Screen Analysis
Mesh Size
40
Gross Wt
Tare Net Wt % on Mesh
> --
e> O
"
1. Screen Analysis
Mesh Size Gross Wt. Tare Net Wt % on Mesh
40
Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200
Glassy Pan Part.
9M-
Min.
l`745' (SVV3V7 Zl.l t&X
^
c,.i-
IS
On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb
Pan 60 80 100 120 140 200
Glassy Part.
f7A7
Remarks
wt- ihtpit
Hi*
nNMPMmniWVIIMHI
*#
VAB.0001202485
mum
Vista Polymers A Division of Vista Chemical Company
Highway 25 Post Office Box 91
XI
T
Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1
^ l\l L__ V' S I S
A
Da te
Customer:
United Technologies
P. . Box 807
Mt. Airy, NC
27030
Attention: Quality Control Manager
Ship Date:
VISIAProduc t 5415
Trailer No. ULKkViO OJA
Order No.: DC)&>O~&OO
Customer P.0. No . : 0.PV kl|A6
Property
Moisture, V.
Contamination, BLK/BRN Hard Particles < 7 mins. Bulk Density, gm/cc Brabender Drytime, mins.
Test Method ABR-iA ABR-5A ABR-12 ABR-2B ABR-7
Analysis
/3
4/5 I
- '445'
42>
Resin Flow Time, tap/sec.
Particle Size, V. on
40 Mesh 200 Mesh
ABR-8 ABR-3
D/
n.o
4.5
Pan Residual VCM, ppm Inherent Viscosity
METS IR, V. of Control
ABGC-26 ABR-10 ABR-13
.Dot
/. DsL* * /\5~ * *
Values for this property has been determined by our SQC Program and is not tested on truck shipments.
Laboratory Su
visor/Lead
(601) 369-8111
VAB.0001202486