Document b5joOVm4Xke6kQVddpajpOYG1
Data Package
Contract Lab Program Data Package for
DuPont Env. Remediation Svc.
TYPE IV INORGANICS DATA PACKAGE
DuPont Fort Madison GW Monitoring - 1996 Annual Water Samples
Collected on 09/17/96 - 09/18/96 Sample No. 2583205-2583210, 2583823-2583827
*mp*m*:a-a
PA Cert. # 36-037 NY Cert. # 10670 NJ Cert. # 77011
Prepared by_ $(Lu>^L (4hJLJiJUAlJLU au /rf Af 4/1A. ^
Quality Assurance Review,
-djL&Ajl&LL/ oJi r^A-*'--'
Date_________if}- Jt-fIz
Delivery Date_
idnhi*
Lancaster Laboratories
A Thermo Analytical Laboratory
N36820
Lancaster Laboratories 2425 Mew Holland Pike, P0 Box 12425, Lancaster, PA 17605-2425 * 717-656-2300 Fax: 717-656-2681
DUP050307520
Lancaster LaboratoriesA division of Thermo Analytical Inc.___ _ r; <i soeoa.-
Sample Reference List for SDG # FMDOl with a Package Type of IV-I
Lab Sample Number
2583205 2583206 2583207 2583208 2583200 2583210 2583823 2583824 2583825 2583826 2583827
sample Code
BRA5S BRA4D BR4DD BRS4S BRS3D DRA3S BR&2D BR&2S BR&1D BRA1S BRAF1
Client Sample Description
FMN-BRA-5S Water Sample FMN-BRA-4D Water Sample FHN-BRA-4D-DUP Water Sample FMN-BRA-4S Water Sample FMN-BR&-3D Dnspiked Water Sample FMN-BRA-3S Water Sample FMN-BRA-2D Water sample FMN-BRA-2S water Sample FMN-BRA-1D water Sample FMN-BRA-1S water Sample FMN-BRA-FBLK-1 Water Sample
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Shipping Address: LcDOViKM if:-.
247!-. i'iew Holland
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Environmental "Foods `Pharmaceuticals 'KaSSlIi A wbvui.vy of Thermo Twra'fech Inc., a Tneono Electron rompn'.'
DUP050307521
TABLE OF CONTENTS A. Case Narrative-Conformance/Nonconformance Summary............................ .1 B. Sample Data....................................................... ...............................................................................4 C. Quality Control Data...............................................................................................................16 D. Verification of instrument Parameters................................................................35 E. Preparation and Run Logs....................................................................................................46 F. Raw Data..........................-.................................................................................................................69
1. ICP Data..........................................................................................................................70 2. Furnace Data.............................. ........................................................................153 3. Mercury Data.............................. ........................................................................217 4. Extraction/Distillation/Digestion Logs....................................225 G. Chain-of-Custody Record..................................................................................................229
DU P050307522
Case Narrative Conformance/Nonconformance Summary
i DUP05 0307523
Lancaster Laboratories A Thermo Analytical Laboratory Where quality is a science..
CASE NARRATIVE FOR INORGANICS
Laboratory Name: Lancaster Laboratories SDG Number: FMD01 Date Received: 09/19/96
calibration Standards.:
, ^ ^,
Instrument calibration standards are prepared monthly from stock
solutions purchased from Spex Industries Inc., JT Baker, Aldrich
Chemical, VWR Scientific, EM Science, or VHG Laboratories.
Case Narrative reviewed and approved by: _______Date A pill Ik
Diane L. Lbckard-, SpeciaXi^t l Coordinator
Inorganic Data Packages
--
Lancaster Laboratories 2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 A subsidiary of Thermo Process Systems Inc., a Thermo Electron company
9
DUP050307524
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSIS DATA PACKAGE
^ Lab Name: LANCASTER__LABORATORIES____
Lab Code:
Case No.:
SOW No.: ILM04.0
EPA SAMPLE No. BR4DD
_BRA1D_____ _BRA1S______ _BRA2D______
BRA2S _BRA4D______
_BRA5S______ BRAP1 BRS3D
_BRS4S______ DRA3S______
Contract:
SAS NO.: _________ SDG No.: FMD01
Lab Sample ID. _2583207 _2583825___ _2583826___ 2583823 _2583824 _2583206___ _2583205___ _2583827 _2583209___ _2583208 2583210
Were ICP interelement corrections applied ?
Were ICP background corrections applied ? If yes - were raw data generated before application of background corrections ?
Comments:
Yes/No Yes/No Yes/No
YES YES NO_
I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer-readable data submitted on diskette has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature.
S ignature:
^ ^ Name: _Diane L. Lockard
Date:
\ b \ ~~\ \ 9l?________________
Title:
COVER PAGE - IN
_Specialist I Coordinator Inorganic Data Packages ILM04.0
n o
DUP050307525
Sample Data
4
DU PO50307526
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIES_
Lab Code: _________
Case No.: _
Matrix (soil/water): WATER
Level (low/med);
LOW
Contract:
BR4DD
SAS No.:
SDG No.: FMD01
Lab Sample ID: 2583207
Date Received: 09/18/96
% Solids:
0.0 Concentration Units {ug/L or mg/kg dry weight): UG/L____
CAS NO.
Analyte Concentration C Q
7429-90-5 Aluminum7440-36-0 Antimony 7440-38-2 Arsenic 7440-39-3 Barium 7440-41-7 Beryllium
7440-43-9" Cadmium 7440-70-2 Calcium 7440-47-3 Chromium 7440-48-4 Cobalt 7440-50-8 Conner 7439-89-6 Iron 7439-92-1 Lead 7439-95-4 Magnesium 7439-96-5 Manganese
7439-97-6 Mercury 7440-02-0 Nickel 7440-09-7 Potassium 7782-49-2 Selenium 7440-22-4 Silver 7440-23-5 Sodium ' 7440-28-0 Thallium
7440-62-2 Vanadium 7440-66-6 Zinc
846
1.9 u 1.3 u
65.6 B
0.56 U 0.38 U 202000
1.4 B 5.6 B 3.0 B 1850 1.5 B 80800 689 0.011 B 6.1 B 4080 B 0.70 U
0.72 u
63600
1.1 U
2.6 B 13.3 B
WN W
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS. Color After: COLORLESS. Comments:
Clarity Before: CLOUDY Clarity After: CLEAR_______
Texture: Artifacts:
FORM I - IN
ILM04.0
5
DUP050307527
U.S. EPA - CLP
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTERJLABORATORIES
Contract
BRAID
Lab Code: _________
Case No.: .
SAS No.: _________ SDG No.: FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583825
Level (low/med):
LOW
Date Received: 09/19/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6
Analyte Concentration C
AluminumAntimony Arsenic Barium Beryllium Cadmium Calcium
Chromium Cobalt
Copper Iron
Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium
Thallium Vanadium Zinc
41.2 U 1.9 U 1.6 B 121 B
0.56 U 0.55 B 96600 0.58 U
1.0 B
0.48 U 365
0.85 B 29400
726 0.0090 U
2.9 B 2950 B 0.70 U 0.72 U
48900 1.1 U
0.50 U 22.2
Q
WN w
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS. Comments:
Clarity Before: CLEAR Clarity After: CLEAR
Texture: Artifacts:
A
FORM I - IN
ILM04.0
6
DUP050307528
U.S. EPA - CLP
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTERJLABORATORIES.
Contract: ___
BRA1S
Lab Code: _________
Case No.: .
____ SAS No _________ SDG NO.: FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583826
Level (low/med): .
LOW
Date Received: 09/19/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 "7440-36-0
7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2
7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 "7440-28-0
7440-62-2 7440-66-6
Aluminum Antimony Arsenic Barium Beryllium cadmium Calcium Chromium Cobalt
Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver
Sodium
Thallium
Vanadium Zinc
224 1.9 U 1.3 U 76.6 B 0.56 U 0.38 U
156000 0.96 B 0.76 U
0.48 u
408
0.86 B 55800
23.5
0.0090 U 1.8 B
1610 B 124
0.72 U
40800
1.1 U
1.3 B
12.7 B
WN
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS, Comments:
Clarity Before: CLEAR Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILM04.0
f*' (
DUP050307529
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER.LABORATORIES.
Contract:
BRA2D
Lab Code: _________
Case No.: _
SAS No.:
SDG No.: FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583823
Level (low/med):
LOW
Date Received: 09/19/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 7440-36-0
7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6
Aluminum Antimony Arsenic
Barium Beryllium Cadmium Calcium chromium Cobalt Conner Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
41.2 U 1.9 U 1.3 U 119 B
0.56 U 0.38 U 72700 0.58 U 0.76 U 0.48 U
358
1.0 B 30200
250
0.0090 B 1.6 B
5550 0.70 U 0.72 U 48300
1.1 U 0.58 B
9.7 B
WN
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS Comments:
Clarity Before: CLEAR_ Clarity After: CLEAR
Texture: Artifacts:
FORM I - IN
ILM04.0 8
DUP050307530
U.S. EPA - CLP
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER._LABORATORIES____ Contract: ___
BRA2S
Lab Code: ________
Case No.: _____________ SAS No ________ SDG No.: FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583824
Level (low/med):
LOW
Date Received: 09/19/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 7440-36-0
7440-38-2 7440-39-3
7440-41-7 7440-43-9 7440-70-2
7440-47-3 7440-48-4 7440-50-8 7439-89-6
7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0
7440-62-2 7440-66-6
AluminumAntimony
Arsenic Barium
Beryllium Cadmium Calcium
Chromium Cobalt Copper Iron
Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver
Sodium Thallium
Vanadium Zinc
276 1.9 U
1.9 B 78.0 B 0.56 U 0.49 B 197000
0.96 B 1.3 B
0.48 U 463
0.96 B
80300
670 0.0090 U
7.7 B 4540 B
4.7 B
0.72 U
60100
1.1 u
1.7 B 9.2 B
WN
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS, color After: COLORLESS Comments:
Clarity Before: CLEAR Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILM04.0
9
DUP050307531
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER__LABORATORIES_
Contract:
BRA4D
Lab Code: ________
Case No. : _
SAS No.:
SDG No.: FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583206
Level (low/med):
LOW
Date Received: 09/18/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS NO.
Analyte Concentration C Q
7429--90--3 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2
7440-47-3 7440-48-4
7440-50-8 7439-89-6
7439-92-1
7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4
7440-23-5 7440-28-0
7440-62-2 7440-66-6
Aluminum
Antimony Arsenic Barium Beryllium Cadmium Calcium
Chromium Cobalt
Copper Iron
Lead Magnesium Manganese
Mercurv Nickel Potassium Selenium Silver Sodium Thallium
Vanadium Zinc
344 1.9 U 1.3 U 55.7 B 0.56 U 0.38 U 206000 0.60 B 5.1 B
1.7 B 1030
0.92 B 82100
663 0.0090 U
5.5 B 3980 B 0.70 U 0.72 U
61800 1.1 U
1.2 B 9.6 B
WN W
M
P P F P P P P P P P P F P P CV P P F P P F P P
color Before: COLORLESS Color After: COLORLESS Comments:
Clarity Before: CLOUDY Clarity After: CLEAR__
Texture: Artifacts:
FORM I - IN
ILM04.0
A
1C
DUP050307532
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTER__LABORATORIES_
Contract:
BRA5S
Lab Code: ________
Case No.:
Matrix (soil/water): WATER
SAS No.:
SDG No.: FMD01
Lab Sample ID: 2583205
Level (low/med):
LOW
Date Received: 09/18/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 -7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 -7439-97-6 "7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6
Analyte Concentration C
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium
Silver Sodium Thallium Vanadium
Zinc
49.5 B 1.9 U 1.3 U
29.2 B 0.56 U 0.38 U 280000 0.58 U
1.1 B 0.48 U
125 1.0 B 94900 330 0.0090 U 8.8 B 3450 B 17.0 0.72 U 45400 1.1 U 0.50 U 14.8 B
Q WN
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS. Comments:
Clarity Before: CLEAR. Clarity After: CLEAR
Texture: Artifacts:
FORM I - IN
ILM04.0
11
DUP050307533
U.S. EPA - CUP
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER LABORATORIES____ Contract: ____________
BRAF1
Lab Code: ________
Case No
SAS No.: ________ SDG No.: FMD01
Matrix (soil/water) : WATER
Lab Sample ID: 25S3827
Level (low/med):
LOW
Date Received: 09/19/96
% Solids:
o.o
Concentration Units (ug/L or mg/kg dry weight): UG/L.
CAS No.
Analyte Concentration C Q
7429-90-5 Aluminum 7440-36-0" Antimony 7440-38-2 Arsenic " "7440-39-3 Barium 7440-41-7 Beryllium 7440-43-9 Cadmium 7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
"7440-50-8 Cooper
7439-89-6 Iron
7439-92-1 Lead 7439-95-4 Magnesium "7439-96-5 Manganese 7439-97-6 Mercury 7440-02-0 Nickel 7440-09-7 Potassium 7782-49-2 Selenium 7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium 7440-66-6 Zinc
41.2 U 1.9 U 2.1 B 1.4 B
0.56 U 0.38 U
143 B
0.58 U 0.76 U
0.48 U
45.2 B
0.84 U 38.2 B 0.60 B 0.0090 U
1.3 U 56.0 B 0.70 U 0.72 U
287 B 1.1 U
0.53 B
8.3 B
N W
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS. Comments:
Clarity Before: CLEAR. Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILMQ4.0 .2
DUP050307534
U.Sv EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIES_
Contract:
BRS3D
Lab Code: ________
Case No.:
SAS No.
SDG No. FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583209
Level (low/med):
LOW
Date Received: 09/18/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 7440-36-0 7440-38-2 7440-39-3
7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0
7440-09-7 7782-49-2
7440-22-4 7440-23-5 7440-28-0
7440-62-2 7440-66-6
AluminumAntimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt
Copper Iron Lead Magnesium Manganese Mercury Nickel
Potassium
Selenium Silver Sodium Thallium
Vanadium Zinc
41.2 u 1.9 U 1.5 B 153 B
0.56 U 0.38 U 67400
0.58 u
2.6 B
5.48 U 198
0.86 B 27900
772
0.0090 U 5.6 B
2750 B
0.70 U
0.72 U 51400
1.1 U
1.0 B 12.8 B
WN
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS Comments:
Clarity Before: CLEAR. Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILM04.0
A
13
D UP050307535
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: LANCASTERLABORATORIES
Contract
BRS4S
Lab code: ________
Case No.:
SAS No.: ________ SDG No.: FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583208
Level (low/med):
LOW
Date Received: 09/18/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 7440-36-0
7440-38-2 7440-39-3
7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6
7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4
7440-23-5 7440-28-0
7440-62-2 7440-66-6
Aluminum
Antimony Arsenic Barium
Beryllium Cadmium
Calcium Chromium Cobalt Conner
Iron Lead Magnesium Manganese
Mercurv Nickel Potassium
Selenium Silver
Sodium Thallium Vanadium Zinc
49.0 B
1.9 U 1.3 U 101 B 0.56 U 0.38 U 138000 0.58 U 4.3 B 0.48 U 116
1.1 B 55900
946 0.0090 U
9.3 B 2240 B 0.70 U 0.72 U 35900
1.1 U 1.1 B 11.6 B
WN
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS. Color Afters c o l o r l e s s Comments:
Clarity Before: CLEAR. Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILK04.0
DUP050307536
U.S. EPA - CLP
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTERLABORATORIES____ Contract: _________
DRA3S
Lab Code: ________
Case No..: _____________ SAS No.: ______ _
SDG No.: FMD01
Matrix (soil/water): WATER
Lab Sample ID: 2583210
Level (low/med):
LOW
Date Received: 09/18/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5
7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 ""7440-47-3 7440-48-4 7440-50-8 "7439-89-6 "7439-92-1 7439-95-4 "7439-96-5 7439-97-6 7440-02-0
7440-09-7 7782-49-2 7440-22-4
7440-23-5 7440-28-0 7440-62-2 7440-66-6
Aluminum Antimony Arsenic Barium
Beryllium Cadmium Calcium Chromium Cobalt copper Iron Lead Magnesium Manganese Mercury Nickel
Potassium Selenium Silver
Sodium Thallium Vanadium Zinc
2640 1.9 U 4.9 B
80.0 B
0.56 U 0.38 U 245000
1.8 B 3.6 B 1.4 B 2010 2.0 B 98500 410 0.017 B 8.8 B 2890 B 13.9 0.72 U 47800 1.1 U 4.0 B .15.0 B
WN
M
P P_ F_ P_ P_ P_ P_ P_ P_ P P_ F_ P P_ CV P_ P_ F P_ P_ F_ P_ P
color Before: COLORLESS. Color After: COLORLESS Comments:
Clarity Before: CLOUDY Clarity After: CLOUDY
Texture: Artifacts:
A
FORM I - IN
ILM04.0
? o
DUP050307537
Quality Control Data
b
DUP050307538
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_.LABORATORIES____
Lab Code: ________
Case No.: _____________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: SAS No.: _________
SDG No.: FMD01
Concentration Units: ug/L
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead. Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Calibration
True
Found %R(1)
30000.0 29385.00 98.0
600.0 573.47 95.6
50.0
53.47 106.9
600.0 595.58 99.3
600.0 609.29 101.5
600.0 592.54 98.8
30000.0 29358.74 97.9
600.0 595.17 99.2
600.0 592.88 98.3
600.0 605.09 100.8
30000.0 29266.08 97.6
20.0
19.93 99.6
30000.0 29298.72 97.7
600.0 598.07 99.7
2.0
2.04 102.0
600.0 597.77 99.6
30000.0 28979.17 96.6
20.0
19.85 99.2
600.0 60482 100.8
30000.0 30124.32 100.4
50.0
49.34 98.7
600.0 593.05 98.8
600.0 597.61 99.6
True
Continuing Calibration Found %R(l) Found %R(1)
25000.0 25071.47 100.3 25732.08 102.9
500.0 455.31 91.1 470.96 94.2
40.0
42.39 106.0
41.90 104.8
500.0 487.36 97.5 506.44 101.3
500.0 497.15 99.4 512.20 102.4
500.0 492.86 98.6 508.63 101.7
25000.0 25320.26 101.3 25994.52 104.0
500.0 489.35 97.9 504.82 101.0
500.0 485.69 97.1 492.43 98.5
500.0 498.81 99.8 516.15 103.2
25000.0 24604.21 98.4 25117.93 100.5
25.0
23.92 95.7
24.99 100.0
25000.0 24924.19 99.7 25557.46 102.2
500.0 494.68 98.9 509.50 101.9
1.0
1.04 104.0
1.05 105.0
500.0 495.08 99.0 510.55 102.1
25000.0 25252.24 101.0 26220.91 104.9
25.0
24.55 98.2
23.78 95.1
500.0 495.99 99.2 512.95 102.6
25000.0 25781.98 103.1 26418.66 105.7
40.0
41.00 102.5
44.00 110.0
500.0 494.09 98.8 510.50 102.1
500.0 497.07 99.4 513.77 102.8
M
P P F P
P P P P P P P F P P CV P P F P P F P P
fl) Control Limits: Mercury 80-120? Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
17
DUP050307539
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_LABORATORIES____
Lab Code: ______ __
Case No.: _____________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: SAS No.: ________
SDG No.: FMD01
Concentration units: ug/L
Analyte
Aluminum_ Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium_ Cobalt____ Copper Iron Lead Magnesium Manganese Mercury Nickel_i___ Potassium Selenium Silver Sodium Thallium_ Vanadium Zinc
Initial Calibration
True
Found %R(1)
True
Continuing Calibration Found %R(1) Found %R(1)
25000.0 25042.35 100.2
500.0 458.89 91.8
40.0
41.77 104.4
42.63 106.6
500.0 493.83 98.8
500.0 497.49 99.5
500.0 497.16 99.4
25000.0 25247.21 101.0
500.0 491.58 98.3
500.0 472.70 94.5
500.0 499.87 100.0
25000.0 24055.58 96.2
25.0
26.02 104.1 ____ 26.16 104.6
25000.0 24781.73 99.1
500.0 494.77 99.0
1.0
0.97 97.0
500.0 500.57 100.1
25000.0 25671.76 102.7
25.0
23.23 92.9 ____ 23.04 _92.2
500.0 498.44 99.7
25000.0 25721.61 102.9
40.0
42.30 105.8
43.55 108.9
500.0 496.21 99.2
500.0 500.93 100.2
A ft
M
P P' F" P" P F*
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
A
FORM II (PART 1) - IN
ILM04.0
DUP0503 07540
U. S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_LABORATORIES____
Lab Code: ________
Case No.: _____________
Initial calibration Source:
LLI
Continuing calibration Source: LLI
Contract: SAS No.: ________
Concentration Units: ug/L
SDG No.: FMD01
Analyte
Initial Calibration
True
Found %R(1)
True
Continuing Calibration Found %R(1) Found %R(1)
M
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium
Chromium Cobalt
Copper Iron
Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver
Sodium Thallium
Vanadium Zinc
20.0
19.58 97.9
30000.0 30599.42 102.0
50.0
46.71 93.4
25.0
26.01 104.0
2>. 0
24.85 99.4
24.76 99.0
25000.0 26363.00 105.5 26100.69 104.4
40.0
42.15 105.4
40.61 101.5
NR NR
NR NR NR NR NR
NR NR NR NR
F NR NR NR NR NR F NR
P F
NR NR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
X1 9
DU P050307541
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTERJLABORATORIES____
Lab Code: ________
Case No.: ___________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: SAS No.: ________
SDG No.: FMD01
Concentration Units: ug/L
Analyte
initial calibration
True
Found %R(1)
Continuing Calibration
True
Found %R(1) Found %R(1)
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
A
Thallium Vanadium
Zinc
25000.0 25967.51 103.9
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
IIM04.0
A
20
A
DUP050307542
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: IANCASTER_LABORATORIES____
Lab Code: _______
Case No.: ___________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: SAS No.: ________
SDG No.: FMD01
Concentration Units: ug/L
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Calibration
True
Found %R(1)
30000.0 28878.07 96.3
Continuing Calibration
True
Found %R(l) Found %R(1)
25000.0 24193.14 96.8 24625.98 98.5
M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR P NR NR NR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
21
DUP050307543
U.S. EPA - Clip
2B CRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTERJ^BORATORIES____
Lab Code: _______
Case No.: ___________
AA CRDL Standard Source: LLI
ICP CRDL Standard Source: LLI
Contract: SAS No.: ________
SDG No.: FMD01
Concentration Units: ug/L
Analyte
Aluminum Antimony Arsenic__ Barium Beryllium Cadmium Calcium Chromium_ Cobalt____ Copper___ Iron Lead Magnesium Manganese Mercury Nickel^___ Potassium Selenium_ Silver Sodium Thallium Vanadium_ Zinc
CRDL Standard for AA
True
Found
%R
True
CRDL Standard for ICP
Initial
Final
Found %R Found
%R
10.0
3.0 0.2 5.0 10.0
____120.0 ____117.55 _98.0 ____116.23 _96.9 12.41 124.1
10.0 10.0
10.19 101.9 10.20 102.0
10.21 102.1 10.41 104.1
20.0 100.0
50.0
20.28 101.4 101.18 101.2
51.48 103.0
20.79 104.0 99.57 99.6 50.44 100.9
4.29 143.0
0.19 _95.0
30.0 80.0
30.67 102.2 81.00 101.2
31.02 103.4 83.67 104.6
4.07 _81.4
20.0
20.68 103.4
20.82 104.1
12.38 123.8
100.0 40.0
103.33 103.3 40.88 102.2
105.42 105.4 41.80 104.5
FORM II (PART 2) - IN
ILMQ4.0
a 0^
DUPO 50307544
I*'!-S.''^ ^SilRSrH >rvT-"'
l
U.S. EPA - CLP
2B CRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTER_LABORATORIES___
Lab Code: .
Case No.: ___________
AA CRDL Standard Source: LLI
ICP CRDL Standard Source: LLI
Contract: SAS No.: ________
SDG No.: FMD01
Concentration Units: ug/L
Analyte
AluminumAntimony Arsenic Barium Beryllium cadmium. Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury NicJcel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
CRDL Standard for AA
True
Found
%R
5.0 10.0
4.05 81.0 9.64 96.4
True
CRDL Standard for ICP
Initial
Final
Found %R Found
%R
A
FORM II (PART 2) - IN
ILM04.G
2S
DUP050307545
tr.S. EPA - CLP 3
BLANKS
Lab Name: LANCASTER LABORATORIES____
Contract:
T.ah Code: _______
Case No.: ___________ SAS No.: ________
Preparation Blank Matrix (soil/water): WATER_
Preparation Blank Concentration Units (ug/L or mg/kg): UG/L_
SDG No.: FMD01
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Calib. Blank
(ug/L)
C
41.2 U
1.9 u
1.6 B 0.16 U 0.56 U 0.38 B 80.0 B 0.58 U 0.76 U
0.48 u
42.1 B
0.84 u 34.8 u 0.18 u
-0.017 B
1.3 U 52.6 B
-0.91 B
0.72 U 189 B
1.1 U 0.50 U
1.1 U
Continuing Calibration Blank (ug/L)
1C2 C3
C
56.3 B
3.0 B
1.3 U
0.16 U 0.56 U 0.38 B
125 B 0.58 U 0.76 U
0.48 u
52.5 B
0.84 u
66.5 B 0.18 U -0.020 B
1.3 U 52.8 B -1.1 B
0.72 U
175 B
1.1 U 0.50 U
1.1 U
41.2 U 1.9 U
1.3 U 0.16 U 0.56 U 0.38 U
114 B 0.58 U
0.76 u
-0.99 B 29.0 B 0.89 B 35.4 B 0.18 U
-0.028 B 1.3 U
49.1 B -1.2 B 0.72 U
164 B 1.1 U 0.50 U 1.1 U
75.2 B
1.9 U
1.7 B 0.16 U 0.56 U 0.38 U
135 B 0.58 U 0.76 U -1.1 B
55.7 B
1.0 B 74.5 B 0.18 U -0.031 B
1.3 U
55.0 B -1.3 B
0.72 U
173 B
1.1 U 0.50 U
1.1 U
Prepa ration
Blank C
M
48.160 B
1.900 U
1.300 B 0.160 U
0.560 u 0.380 u
106.010 B
0.580 u 0.760 u 0.480 u
46.400 B 0.840 U
44.640 B 0.240 B 0.010 B
1.300 U 50.170 B
-1.1600 B
0.720 U
160.980 B
1.100 U 0.500 U 6.930 B
P
P F P P P P P P P P F P P CV
P P F
P P
F P P
FORM III - IN
ILM04.0
QA
DUPO 50307 546
U.S. EPA - CLP
3 BLANKS
Lab Name: LANCASTER .LABORATORIES____
Contract:
'
Lab Code: _______
Case No.: ___________ SAS No.: ______ _
SDG No.: FMD01
Preparation Blank Matrix (soil/water): ______ ______
Preparation Blank Concentration Units (ug/L or mg/kg): _____________
Analyte
Initial Calib. Blank (ug/L)
C
Aluminum Antimony_ Arsenic
Barium Beryllium Cadmium
Calcium Chromium
Cobalt Copper Iron Lead Magnesium Manganese Mercury
Nickel
Potassium Selenium
Silver Sodium Thallium Vanadium Zinc
296 B
Continuing Calibration Blank (ug/L)
1C2 C 3
2.0 B
C
0.84 U
1.0 6
-2.2 B
299 B 1.1 U
230 1
196 B
Prepa ration
Blank C
M
NR NR F
NR NR
NR
NR NR NR NR NR F NR NR NR
NR NR F
NR P F NR NR
FORM III - IN
ILM04.0
OSW -l J
DUP050307547
U.S. EPA - CLP
3 BLANKS
Lab Name: LANCASTER,LABORATORIES____
Contract:
Lab Code: ________
Case No.: ___________ SAS No.: ________
SDG No.: FMD01
Preparation Blank Matrix (soil/water): _____________
Preparation Blank Concentration Units (ug/L or mg/kg): _____________
Analyte
Initial Calib. Blank
(ug/L)
C
Continuing Calibration Blank (ug/L)
1C2C3
Prepa
ration C Blank C M
Aluminum
Antimony"
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
A
Nickel Potassium
Selenium
Silver
Sodium
Thallium
Vanadium A Zinc
io
CO
174 B 1.1 U
-1.2 B
214 B 1.1 U
-1.5 B
186 B 1.1 U
NR
NR
NR
NR NR NR NR NR NR NR
NR NR NR NR NR NR NR F NR P
F NR
NR
FORM III - IN
ILM04.0
A
DUP050307548
U.S. EPA - CLP
4 ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTER_LABQRATORIES___
Contract:
Tab Code: ________
Case No.: ___________ SAS No.: ________
ICP ID Number: 05478________
ICS Source: LLI
SDG No.: FMD01
Concentration Units: ug/L
Analyte
True
Sol. Sol. A AB
Aluminum_ 500000 500000
Antimony_ 0 600
Arsenic__
Barium
0 500
Beryllium 0 500
Cadmium
0 1000
Calcium 500000 500000
Chromium_ 0 500
Cobalt____ 0 500
Copper____ 0 500
Iron
200000 __ 200000
Lead
Magnesium 500000 500000
Manganese 0 500
Mercury
Nickel^___
0 1000
Potassium
0
0
Selenium_
Silver___
0 200
Sodium
00
Thallium_
Vanadium
0 500
Zinc
0 1000
Initial Found
Sol. Sol.
A AB
%R
Final Found
Sol. Sol.
A AB
%R
532256 539960.4 108.0 -3 619.2 103.2
530676 525618.3 105.1 -3 ____603.2 100.5
8 530.8 106.2
8 526.7 105.3
2 490.5 98.1
2 483.0 96.6
1 957.9 95.8
1 952.4 95.2
512734 522813.8 104.6 520787 510843.9 102.2
7 499.6 99.9
7 493.8 98.8
-1 485.8 97.2
-1 464.0 92.8
-1 551.5 110.3
-2 541.3 108.3
__ 208401 211889.5 105.9 __ 206646 202329.9 101.2
554176 562507.4 112.5 4 502.6 100.5
55?004 >47774.6 109.6 4 494.2 98.8
6 962.2 96.2 37 56.9
6 957.2 95.7 46 45.0
0 218.2 109.1 176 210.0
0 214.9 107.4 266 232.4
-2 509.4 101.9 2 __ 1016.9 101.7
-3 501.7 100.3 5 __ 1010.6 101.1
FORM IV - IN
ILM04.0
9*V
DUP050307549
U.S.. EPA - CUP
ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _____ .
Case No.: ___________ SAS No.: _______
ICP ID Number: 05478
ICS Source: LLI
SDG No.: FMD01
Concentration Units: ug/L
Analyte
Time
Sol. Sol. A AB
Aluminum_ 500000 __ 500000
Antimony_
Arsenic
Barium
Beryllium
Cadmium
Calcium 500000 __ 500000
Chromium_
Cobalt____
Conner
Iron
200000 __200000
Lead
Magnesium 500000 __500000
Manganese
Mercury
Nickel_>___
Potassium
Selenium_
Silver
Sodium
00
Thallium_
Vanadium
Zinc
Initial Found
Sol.
Sol.
Final Found
Sol.
Sol.
FORM IV - IN
ILM04.0
28
DUPO 50307550
U.S. EPA - CLP
4 ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTER_LABORATORIES___
Contract:
Lab Code: ________
Case No. : ___________ SAS No. :
ICP ID Number: 05478_________
ICS Source: LLI
SDG No.: FMD01
Concentration Units: ug/L
Analyte
True;
Sol.
Sol.
A AB
Aluminum_ 500000 __ 500000
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium 500000 __ 500000
Chromium
Cobalt
Copper
Iron
200000 200000
Lead
Magnesium 500000 __ 500000
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
00
Thallium
Vanadium
Zinc
Initial Found
Sol. Sol.
A AB
%R
Final Found
Sol. Sol.
A AB
%R
__ 473163 474555.3 _94.9 __ 478946 466421.5 _93.3
__ 463351 467353.6 _93.5 __ 463737 451998.0 _90.4
188283 188695.3 94.3 187801 182711.3 91.4 __ 486725 488253.2 _97.7 __ 489272 477281.9 _95.5
214 226.2
203 174.7
FORM IV - IN
ILM04.0 Oi
DUP050307551
O.S. EPA - Clip
5A SPIKE SAMPLE RECOVERY
EPA SAMPLE NO.
Lab Name: LANCASTER.LABORATORIES____ Contract: ____
BRS3DS
T.ab code: ________
Case No.: ___________ SAS No.:
SDG No.: FMD01
Matrix (soil/water) : WATER_______
Level (low/med):
LOW
% Solids for Sample: 0.0
Concentration units (ug/L or mg/kg dry weight): UG/L
Control Analyte Limit
%R
Aluminum 75-125
Antimony 75-125
Arsenic 75-125
Barium
75-125
Beryllium 75-125
Cadmium 75-125
Calcium
Chromium 75-125
Cobalt
75-125
Copper
75-125
Iron
75-125
Lead
75-125
Magnesium
Manganese 75-125
Mercury 75-125
Nickel
75-125
Potassium
Selenium 75-125
Silver
75-125
Sodium
Thallium 75-125
Vanadium 75-125
zinc
75-125
Spiked Sample Result (SSR) C
2126.6300 498.3200 40.9100
2132.9300 49.8800 50.0500
198.8700 490.8000 254.0600 1220.4700
15.6500
1257.8000 1.0900
502.8700
7.6000 52.1500
44.0300 499.9700 509.7900
_
Sample
Spike
Result (SR) C Added (SA)
41.2000 u 1.9000 u
1.5300 B 153.0600 B
0.5600 U
0.3800 u
2000.00 500.00
40.00 2000.00
50.00 50.00
0.5800 u
2.5500 B
0.4800 u
197.7500 0.8600 B
200.00
500.00 250.00 1000.00
20.00
771.5600 0.0090 U 5.6300 B
500.00
1.00 500.00
0.7000 U 0.7200 U
10.00 50.00
1.1000 U
1.0000 B 12.8500 B
50.00
500.00 500.00
%R Q M
106.3 P 99.7 P 98.4 F 99.0 P 99.8 P
100.1 P NR
99.4 P 97.6 P 101.6 P 102.3 P 74.0 N F
NR 97.2 P 109.0 CV 99.4 P
NR 76.0 F 104.3 P
NR 88.1 F 99.8 P 99.4 P
Comments:
FORM V (PART 1) - IN
ILM04.0
DUP050307552
U.S. EPA - CLP
6 DUPLICATES
EPA SAMPLE NO.
Lab Name: LANCASTERLABORATORIES
Contract:
BRS3DD
Lab Code: ________
Case No.:
SAS No.:
SDG No.: FMD01
Matrix (soil/water): WATER
Level (low/med):
LOW
% Solids for Sample: 0.0
% Solids for Duplicate: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L____
Control Analyte Limit
Aluminum
Antimony_
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
100.0
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
50000.0
Thallium
Vanadium
Zinc
Sample (S)
C
41.2000 U
1.9000 U 1.5300 B 153.0600 B 0.5600 U 0.3800 U 67439.1700 0.5800 U 2.5500 B 0.4800 U 197.7500 0.8600 B 27941.6800 771.5600 0.0090 U
5.6300 B 2746.4400 B
0.7000 U 0.7200 U 51385.7000 1.1000 U 1.0000 B 12.8500 B
Duplicate (D) C
41.2000 U 1.9000 U 1.3000 U
152.0400 B 0.5600 U 0.3800 U
67306.7100 1.2700 B 2.9500 B 1.0300 B
189.8500 0.8400 U
27885.5600 782.6300 0.0090 u 12.7400 B
2776.1900 B 0.7000 U 0.7200 U
50853.6000 1.1000 U 1.0400 B
13.8400 B
RPD
200.0 0.7
0.2 200.0
14.5 200.0
4.1 200.0
0.2 1.4
7774 l.l
1.0
3.9 7.4
QM
P P F P P P P P P P P' F P P CV P P F P P F P P
FORM VI - IN
ILM04.0
31
DUP050307553
tr.S. EPA - CLP
7 LABORATORY CONTROL SAMPLE
Lab Name: LANCASTER_LABORATORIES____
Code: ________
Case No.: _____________
Solid LCS Source: _________________
Aqueous LCS Source: LLI
Contract: SAS No.: _________
SDG No.: FMD01
Analyte
Aqueous (ug/L)
True
Found %R
Aluminum_ 2000.0 2118.78 105.9
Antimony_ 500.0 522.61 104.5
Arsenic__
40.0 " 42.12 105.3
Barium
2000.0 2050.71 102.5
Beryllium
50.0
50.94 101.9
Cadmium
50.0
51.90 103.8
Calcium
4000.0 4246.28 106.2
Chromium_ 200.0 205.18 102.6
Cobalt____ 500.0 502.33 100.5
Cooper
250.0 259.12 103.6
Iron
1000.0 1078.97 107.9
Lead
20.0
20.83 104.2
Magnesium 2000.0 2042.05 102.1
Manganese 500.0 " 515.74 103.1
Mercury
1.0
0.80 80.0
Nickel___ 500.0 519.45 103.9
Potassium 4000.0 3740.78 93.5
Selenium_ " 10.0
8.78 87.8
Silver____
50.0
52.47 104.9
Sodium
4000.0 4034.82 100.9
Thallium_
50.0
47.28 94.6
Vanadium_ 500.0 517.00 103.4
Zinc
500.0 538.98 107.8
True
Solid (mg/kg)
Found C
Limits
--
%R
FORM VII - IN
ILM04.0
A
ar O ,-j
DUP050307554
iff'WianiSKWyi^
$5-sr "Brow
.-.. .' -.';.4*.v.(.. <:*>- .. r&i^iiB^r^'i-'- *:&,
U.S. EPA - CLP
8 STANDARD ADDITION RESULTS
Lab Name: LANCASTER_LABORATORIES____
Lab Code: ________
Case No.:
_______
Contract: SAS No.: _________
Concentration Units: ug/L
SDG No.: FMD01
EPA
Sample
0 ADD
No. An ABS
1 ADD CON ABS
2 ADD CON ABS
3 ADD CON ABS
Final Cone.
r
FORM VIII IN
ILM04.0 o r*
DUP050307555
U.S. EPA - CLP
9 ICP SERIAL DILUTIONS
Lab Name: LANCASTERJBABORATORIES____ Contract: ____
Lab Code: ________
Case No.: ________
SAS No
Matrix (soil/water): WATER
Concentration Units: ug/L
Analyte
initial Sample Result (1) C
Serial
Dilution Result (S)
Aluminum Antimony Arsenic Barium
Beryllium Cadmium
Calcium Chromium Cobalt
Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium
Zinc
41.20 x3 1.90 U
153.06 B 0.56 U 0.38 U
67439.17 0.58 U 2.55 B 0.48 U
197.75
27941.68 771.56
5.6 B 2746.44 B
0.72 U 5138.57
1.00 B 12.85 B
206.00 9.50
152.65 2.80 1.90
65112.65 2.90 3.80 2.40
368.45
26637.20 759.15
6.50 2598.70
3.60 5397.15
2.55 27.00
EPA SAMPLE NO.
BRS3D L
____
SDG No.: FMD01
Level (low/med): LQW_
5------Differ
ence
0.3
3.4 ___100.0 ____ 86.3
4.7 1.6 100.0 5.4
5.0 155.0 ___110.1
M
p^ p
FORM IX - IN
ILM04.0
DUP050307556
Verification of instrument Parameters
a
DUP050307557
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER.LABORATORIES____
Contract:
Lab Code: ________
Case No.: _____________ SAS No.: ________ SDG No.: FMD01
ICP ID Number:
__________ _
Date:
07/15/96
Flame AA ID Number: _________________
Furnace AA ID Number: ____ 02803___ __
Analyte
Wave length Back CRDL
(nm) ground (ug/L)
IDL (ug/L) M
Aluminum.
NR
Antimony_
NR
Arsenic___
NR
Barium
NR
Beryllium
NR
Cadmium
NR
Calcium
NR
Chromium_
NR
Cobalt____
NR
Copper____
NR
Iron
NR
Lead
NR
Magnesium
NR
Manganese
NR
Mercury
NR
Nickel
NR
Potassium
NR
Selenium_
NR
Silver
NR
A Sodium
NR
Thallium. 276.80___ BD
10 1.1 F_
Vanadium"
NR
Zinc
NR
Comments:
A
FORM X ~ IN
ILM04.0 O
DUP050307558
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER .LABORATORIES____
Contract:
Lab Code: ________
Case No.: _____________ SAS No.: _________ SDG No.: FMD01
ICP ID Number:
_________________
Date:
07/15/96
Flame AA ID Number: _________________
Furnace AA ID Number: ____ 03812_____
Analyte
Wave length Back CRDL
(nm) ground (ug/L)
IDL (ug/L) M
Aluminum_
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium_
Cobalt____
Copper
Iron
Lead
283.30___ BZ
Magnesium
Manganese
Mercury
Nickel^___
Potassium
Selenium_
Silver____
Sodium
Thallium
Vanadium
Zinc
NR
NR NR
NR NR NR NR NR NR NR NR 3 ____ 0.84 F NR NR NR
NR
NR NR
NR
NR
NR NR NR
Comments s
FORM X - IN
ILM04.0 3ni
DUP050307559
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: ________
Case No.: SAS No.: ______________________ SDG No.: FMD01
ICP ID Number:
_________________
Date:
07/15/96
Flame AA ID Number: _________________
Furnace AA ID Number: ____ 04724
Analyte
Wave length Back CRDL
(nm) ground (ug/L)
Aluminum
Antimony_ Arsenic 193.70
Barium Beryllium Cadmium Calcium Chromium Cobalt Conner Iron Lead Magnesium Manganese Mercurv Nickel Potassium Selenium
Silver
Sodium Thallium
Vanadium
Zinc
BZ
10
IDL (ug/L) M
NR NR 1.3 F NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
Comments:
FORM X - IN
ILM04.0 %> KJ
DUP050307560
U.S. EPA - CUP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER.LABORATORIES____
contract:
Lab Code: ________
Case No.: _____________ SAS No.: _________ SDG No.: FMD01
ICP ID Number:
_________________
Date:
07/15/96
Flame AA ID Number: _________________
Furnace AA ID Number: ____ 04725_____
Analyte
Wave length Back CRDL
(nm) ground (ug/L)
Aluminum
Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper
Iron Lead Magnesium Manganese Mercury
Nickel Potassium Selenium 196.00
Silver. Sodium Thallium Vanadium
Zinc
BZ
5
IDL (ug/L) M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 0.70 F NR NR NR NR NR
Comments:
FORM X - IN
ILM04.0 - 39
DUP050307561
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTERLABORATORIES____
Contract:
Lab Code: ________
Case No.: _____________ SAS No.: ________ SDG No.: FMD01
ICP ID Number:
_________________
Date:
07/15/96
Flame AA ID Number: ____ 05220
^ Furnace AA ID Number:
Analyte
Wave length
(nm)
Aluminum-
Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium
Cobalt Copper
Iron Lead Magnesium Manganese Mercury 254.00 Nickel Potassium
Selenium Silver Sodium
Thallium Vanadium
Zinc
Back ground
CRDL (ug/L)
0.2
IDL (ug/L) M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR 0.0090 CV NR NR NR NR NR NR NR NR
Comments:
FORM X - IN
ILM04.0
A
%
?
*
DU P050307562
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: ________ SDG No.: FMD01
ICP ID Number:
____ 05478_____
Date:
07/15/96
Flame AA ID Number: _________________
Furnace AA ID Number: ______________ __
Analyte
Wave length Back
<nm) ground
Aluminum 308.21
Antimony 206.83
Arsenic
Barium
493.40
Beryllium 313.04
Cadmium 226.50
Calcium 317.93
Chromium 267.71
Cobalt
228.61
Cooper
324.75
Iron
271.44
Lead
Magnesium 279.07
Manganese 257.61___
Mercury
Nickel
231.60
Potassium 766.49
Selenium
Silver
328.06
Sodium
330.23
Thallium"
Vanadium 292.40
Zinc
213.85
CRDL (ug/L)
200 60
200 5 5
5000 10 50 25
100
feooo 15
40 5000
10 5000
50 20
IDL (ug/L) M
41.2 P 1.9 P NR
0.16 P 0.56 P 0.38 P 39.3 P 0.58 P 0.76 P 0.48 P 15.6 P
NR 34.8 P 0.18 P
NR 1.3 P 45.3 P
NR 0.72 P 94.3 P
NR 0.50 P
1.1 P
A
Comments:
FORM X - IN
ILM04.0
41
DUP050307563
U.S. EPA - CLP
11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER__LABORATORIES____
Contract:
Lab Code: ________
Case No.: SAS No.:
ICP ID Number: ____ 05478 ____
Date:
. SDG No.: FMD01 09/12/96
Analyte
wave length
(nm)
Interelement Correction Factors for: A1 Ca Fe Mg
CO
Alumirium_ 308.21 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Antimonyl 206.83 0.0000000 0.0000000 0.0000470 0.0000000 0.0000000
Antimony2 ___206.83 _0.0000040 _0.0000000 _0.0000550 _o.ooooooo _o.ooooooo
Arsenic
Barium Beryllium
493.40 0.0000000 0.0000000 0.0000030 0.0000000 0.0000000 313.04 -0.0000040 0.0000000 0.0000000 0.0000000 0.0000000
Cadmium
226.50 -0.0000010 0.0000000 0.0000560 0.0000000 -0.0001810
Calcium
317.93 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Chromium_ 267.71 0.0000000 0.0000000 0.0000140 0.0000000 0.0000000
Cobalt____ 228.61 0.0000000 0.0000000 0.0000040 0.0000000 0.0000000
Copper____ 324.75 0.0000000 0.0000000 0.0000140 0.0000000 0.0000000
Iron
___271.44 _0.0000000 _0.0000000 ~o-ooooooo _o.ooooooo _0.0106600
Leadl
Lead2
Magnesium 279.07 0.0000000 O.oooOooo o.dOooooo 0.0000000 -0.0006820
Manganese ___257.61 -0.0000020 _0.0000000 _o.ooooooo _o.ooooooo _o.ooooooo
Mercury
Nickel^___ 231.60 0.0000000 0.0000000 0.0000220 0.0000000 -0.0006690
Potassium ___766.49 _0.0000000 _0.0000000 _o.ooooooo _o.ooooooo _o.ooooooo
Seleniuml
Selenium2
Silver
328.06 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Sodium
___330.23 _0.0000000 _0.0000000 _o.ooooooo _o.ooooooo _o.ooooooo
Thallium
Vanadium_ 292.40 0.0000000 0.0000000 -0.0002070 0.0000000 0.0000000
Zinc
___213.85 _0.0000190 _0.0000000 _0.0000730 _0.0000180 _o.ooooooo
Comments:
FORM XI (PART 1) - IN
ILM04.0
DUP050307564
""W /
I*.*'* '
*.r;^1e^HW!lrij)..^e:*ililillHli4!,,'r:wtife
U.S. EPA - CLP
11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER_LABORATORIES.
T.ah Code: ________
Case No.:
ICP ID Number: ____ 05478 ____
contract: _ SAS No
Date:
________ SDG No 09/12/96
FMD01
Analyte
wave
length (nm)
Interelement Correction Factors for: CR CU MN MO
NI
Aluminum
308.21 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Antimonyl 206.83 0.0093720 0.0000000 0.0000000 -0.0026820 -0.0018610
Antimony2 ~206.83 _0.0034430 _0.0000000 "0.0000000 -0.0044830 _0.0000000
Arsenic
Barium
493.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Cadmium
226.50 0.0000000 0.0000000 0.0000000 -0.0000580 0.0000000
Calcium
317.93 0.0000000 0.0000000 0.0000000 0.0000000 0*. 0000000
Chromium_ 267.71 0.0000000 0.0000000 0.0001250 0.0000000 0.0000000
Cobalt____ 228.61 -0.0007770 0.0000000 0.0000000 -0.0003680 0.0001680
Copper
324.75 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Iron
___271.44 _0.0009810 _0.0000000 _0.0000000 _0.0038230 _0.0000000
Leadl
Lead2
Magnesium 279.07 0.0000000 0.0000000 -0.0015070 0.0000000 0.0000000
Manganese ___257.61 -0.0000180 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Mercury
Nickel
231.60 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Potassium ___766.49 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Seleniuml
Selenium2
Silver
328.06 0.0000120 0.0000000 -0.0001030 -0.0005270 0.0000000
Sodium
___330.23 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Thallium_
Vanadiura_ 292.40 -0.0017640 0.0000000 0.0000000 0.0000000 0.0000000
Zinc
___213.85 _0.0000000 _0.0002170 _0.0000000 _0.0000000 _0.0052470
Comments:
FORM XI (PART 2) - IN
ILM04.0
DUP050307565
U.S. EPA - CLP
118 ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTERJLABORATORIES____
Contract:
Lab Code: ________
Case No.: _____________ SAS No.: _________ SDG No.: FMD01
ICP ID Number: ____ 05478 ____
Date:
09/12/96
Analyte
Wave
length (nm)
Interelement Correction Factors for:
TI V
___ ___
.___
Alumlnum_ 308.21 0.0000000 0.0166850 0.0000000 0.0000000 0.0000000
Antimonyl 206.83 "0.0003700 -0.0043130 0.0000000 0.0000000 0.0000000 Antimony2 ___206.83 _0.0000570 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Arsenic___
Barium
493.40
Beryllium 313.04
Cadmium
226.50
Calcium --317.93
Chromium_ 267.71
0.0000000 0.0000000
0.0000000 0.0000000 0.0000000
0.0000000 0.0003900 0.0000000 0.0000000 0.0000000
0.6000000 0.0000000
0.0000000 0.0000000 0.0000000
0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
0.0000000 0.0000000
0.0000000 0.0000000 0.0000000
Cobalt Copper
Iron
228.61 0.0041510 0.0000250 0.0000000 0.0000000 0.0000000 324.75 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 ___271.44 _0.0000000 _0.0233670 _0.0000000 _0.0000000 __0.0000000
Leadl
Lead2
Magnesium 279.07 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Manganese ___257.61 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000 Mercury
Nickel^___ 231.60 0.0000006 0.0000000 0.0000000 0.0000000 0.0000000 Potassium ___766.49 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Seleniuml
Seleniura2
Silver Sodium
328.06 0.0000000 0.0000480 0.0000000 0.0000000 0.0000000 ___330.23 -0.4112480 _0.0000000 _0.0000000 _0.0000000 "0*0000000
Thallium
Vanadium
292.40 0.0006940 0.0000000 0.0000000 0.0000000 0.0000000
Zinc
___213.85 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Comments:
FORM XI (PART 2) - IN
ILM04.0
DUP050307566
U.S. EPA - CUP
12 ICP LINEAR RANGES (QUARTERLY)
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: ________
Case No.: SAS No.: ______________________ SDG No.: FMD01
ICP ID Number:
05478_____
Date:
07/15/96
Analyte
Aluminum Antimony_ Arsenic -- Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Integ. Time (Sec.)
10.00 10.00
10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00
10.00 10.00
10.00 10.00
10.00 10.00
10.00 10.00
Concentration (ug/L)
M
600000.0 P 50000.0 P NR
5000.0 P
5000.0 P 20000.0 P 600000.0 P 100000.0 P 50000.0 P 50000.0 P 300000.0 P
NR 600000.0 P
50000.0 P NR
50000.0 P 50000.0 P
NR 5000.0 P 50000.0 P
NR 50000.0 P
5000.0 P
Comments:
FORM XII ~ IN
ILM04.0
4h
DUP050307567
Preparation and Run Logs
46
DUP050307568
U.S. EPA - CLP
13 PREPARATION LOG
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: ________
Case No.: ______ SAS No.: ________
Method: P
SDG No.: FMD01
EPA Sample
No.
BR4DD BRAID BRA1S BRA2D BRA2S BRA4D BRA5S BRAF1 BRS3D BRS3DD BRS3DS BRS4S DRA3S LCSW PBW
Preparation Date
09/24/96 09/24/96 09/24/96 09/24/96 ""09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96
Weight (gram)
Volume (ml)
100 100 100 100 100 100 100 100 100 100 100 100 100 100 100
FORM XIII - IN
ILM04.0
47
DUP050307569
U.S. EPA - CLP
13 PREPARATION LOG
Lab Name: LfiNCASTER_LABORATORIES
Lab Code: ________
Case No.:
Method: F
Contract: SAS No.: ________
SDG No.: FMD01
EPA Sample
No.
BR4DD BRAID BRA1S BRA2D BRA2S BRA4D BRA5S BRAF1 BRS3D BRS3DD BRS3DS BRS4S DRA3S LCSW PBW
Preparation Date
09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96
Weight (gram)
Volume (ml)
100 100 100 100 100 100 100 100 100 100 100 100 100 100 100
FORM XIII - IN
ILM04.0
48
DUP050307570
U.S. EPA - CLP
13 PREPARATION LOG
Lab Name: LANCASTER_LABORATORIES____
Contract: _______________
Lab Code: _________ Method: CV
Case No.: _____________ SAS No.: ________
s d g No.: f md o i
EPA Sample
No.
BR4DD BRAID BRA1S BRA2D BRA2S BRA4D BRA5S BRAF1 BRS3D BRS3DD BRS3DS BRS4S DRA3S LCSW PBW
Preparation Date
09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96
Weight (gram)
Volume (ml)
8 8 8 8 8 8 8 8 8 8 8 8 8 8 8
FORM XIII ~ IN
ILM04.0
49
DUP050307571
U.S. EPA - CLP 14
ANALYSIS RON LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: _________
Case No.:
SAS No.: ________ SDG No. EMD01
Instrument: ID Number: 05478_
Method: P_
Start Date: 09/24/96
End Date: 09/24/96
EPA Sample
No.
D/F
Time
%R
Analytes
A s A B B C c c c <!: F p M M H N K s A N T V z LBs AE DARouE BGNG I E GA L N
SO
S
S S ICV
ICB CRI ICSA ICSAB CCV
CCB PBW LCSW
BRS3D BRS3DA BRS3DD BRS3DS
BRS3DL BRA5S BRA4D BR4DD CCV
CCB
BRS4S
DRA3S BRA2D BRA2S BRAID BRA1S BRAF1 CRI ICSA
1.00 2059
1.00 2104
1.00 2108
1.00 2112 1.00 2115 1.00 2120 1.00 2125 1.00 2130 1.00 2135 1.00 2140
1.00 2145 1.00 2150
1.00 2155
1.00 2200
1.00 2205 1.00 2210 1.00 2215
5.00 2220 1.00 2225 1.00 2230
1.00 2235
1.00 2240
1.00 2245
1.00 2249
1.00 2254 1.00 2259 1.00 2304 1.00 2309 1.00 2314 1.00 2319 1.00 2324 1.00 2329
XX X
X XX XX
X XX XX XX XX XX XX XX
XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX
X XX
XXXXXXXX
XX
XXX
XX
X
X X 5c X X 3E 3c 3c
XXXXXXXX
XX XXX
3C X X X X X X X
XXXXXXXX
XXXX XX X X
XXXXXXXX
XXX X XX X X
XXXXXXX X
XXXX XX X X
XXXXXXXX XXX XXXX XX XX XX X X XXXXXXXX XXXXXXXX
XXXX XXX X
XXXXXXXX
XXXXXXXX
XXXX XXXX
XXXXXXXX XXXX XXXX XX XX XXXX XX XX XX XX XXXXXXXX XXXXXXXX
XX XXX XXXXXXXX
XX X
X
XX XX
X XX XX XX XX XX XX XX
XX X
X
X 3c
XX X
X 5c
XX XX XX XX XX XX
X 3c
X X
3c X
XX X
X 3c
XX XX XX XX XX X
XX
X X
X 3c
XX XX XX XX XX XX XX X X-- XX
XX X
XX X
X X
X X_ XX
X X X X X 3c X X
XX XX
X X--X X XX X
XX XX
XX XX X
XX
XX XX
XX XX
XX XX
XX-- XX
XX XX
XX XX
XX XX
XX X X"
XX XX X
XX
XX XX
X X
X X
--
X X
"" X
X X "" X X X X
X X--X X-- X X
XX
X X MM
X X
X X
""
X
3c X
X
X 3c
X MM X X XX XX
FORM XIV - IN
ILMQ4.0
50
DUP050307572
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Lab Code: ________
Case No.:
Instrument ID Number: 05478
Start Date: 09/24/96
Contract: _ SAS No.: ________ SDG No. Method: P End Date: 09/24/96
FMD01
A
FORM XIV - IN
ILM04.0
A
51
DUP050307573
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Contract; ____________
Lab code: ________
Case No.:
"1 Instrument ID Number: 05478_
SAS NO.: _____ __ Method: P
SDG No. FMD01
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS ABBCc cCcF PMMHN KS ANTV z LBSAEDAROUE BGNG I E GAL N
SO S S
S ICV
ICB CRI
ICSA ICSAB CCV CCB BRS3D BRS3DA BRS3DD BRS3DS BRS3DL
BRA4D BR4DD BRA2D BRA2S
CCV CCB
CRI ICSA
ICSAB CCV
CCB
1.00 0047 1.00 0052 1.00 0055 1.00 0059 1.00 0103
1.00 0107 1.00 0112 1.00 0116 1.00 0120 1.00 0125 1.00 0129 10.00 0134 10.00 0138 10.00 0143 10.00 0147
50.00 0151 10.00 0156 10.00 0200 10.00 0205 10.00 0209
1.00 0214 1.00 0218
1.00 0222 1.00 0227
1.00 0231 1.00 0236 1.00 0240
X X
X X
X X X X X
X
X X X
X X X
X X X X
FORM XIV - IN
IEM04,0 53
DUP050307574
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: l a n c a s t e r _l a b o r a t o r ie s .
Lab Code: ________
Case No.:
Instrument ID Number: 05478_
Start Date: 09/30/96
Contract: ________________ SAS No. : ________ SDG No. : FMD01 Method: P_ End Date: 09/30/96
FORM XIV - IN
ILM04.0 53
DU P05 0307575
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTEBJLABORATORIES____
Contract:
Lab Code: ________
Case No.: SAS No.: _____________________ SDG No.: FMD01
Instrument ID Number: 04724_
Method: F_
Start Date: 09/24/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
A SABB C CCCCFPMMHNKS ANTV Z LBSAE DAR0UE BGN6 I EGAL N
SO S10
S20 S40 S60 S80 ICV ICB CRA CCV
CCB PBW
PBWA LCSW LCSWA
BRASS BRA5SA BRA4D BRA4DA BR4DD BR4DDA
CCV
CCB BRS4S
BRS4SA BRS3D BRS3DA BRS3DD BRS3DDA BRS3DS
ZZZZZZ DRA3S
1.00 2109
1.00 2113 1.00 2117 1.00 2121 1.00 2125 1.00 2129 1.00 2134 1.00 2138 1.00 2142 1.00 2146
1.00 2150 1.00 2154 1.00 2159 1.00 2203 1.00 2207
1.00 2212 1.00 2216 1.00 2220 1.00 2225 1.00 2229 1.00 2233
1.00 2238 1.00 2242 1.00 2246
1.00 2250 1.00 2254 1.00 2258 1.00 2303 1.00 2307
1.00 2311
1.00 2315
1.00 2319
100.7 93.2 95.6 94.8 95.9
102.4 92.8 97.5
X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X
X
FORM XIV - IN
ILM04.0
5
DUP050307576
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: ________
Case No.: ___
SAS No.: ________ SDG No. FMD01
Instrument ID Number: 04724_
Method: F_
Start Date: 09/24/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABB C C C C CF PMMHN KS AN TV Z L BSA E DAROuE BG N G I E GA L N
DRA3SA CCV CCB BRA2D BRA2DA BRA2S BRA2SA
BRAID BRA1DA
BRA1S
BRA1SA BRAF1 BRAF1A CCV CCB
1.00 2324 1.00 2328 1.00 2332 1.00 2336 1.00 2340
1.00 2344 1.00 2348
1.00 2352
1.00 2356 1.00 0000
1.00 0004 1.00 0008 1.00 0013 1.00 0017 1.00 0021
87.0
101.5 89.3 96.3
107.2 104.0
X X X X X
X X
X X X X X X X X
FORM XIV - IN
ILMQ4.0
55
DUP050307577
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: ________
Case No.:
SAS No.: ________ SDG No. FMD01
Instrument ID Number: 03812_
Method: F_
Start Date: 09/24/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABBCC CC CFPMMHNKS ANTVz
LBSAE DAR0 UE BGNG I E GAL N
SO 1.00 2048
S3 1.00 2053
S9 1.00 2058
S15
1.00 2103
S30
1.00 2108
S60
1.00 2113
ICV
1.00 2117
ICB
1.00 2122
CRA
1.00 2126
ZZZZZZ
1.00 2131
CCV
1. 00 2136
CCB
1.00 2141
ZZZZZZ
1. 00 2145
ZZZZZZ
1.00 2150
ZZZZZZ
1.00 2154
ZZZZZZ
1.00 2159
ZZZZZZ
1.00 2204
ZZZZZZ
1.00 2209
ZZZZZZ
2.00 2213
ZZZZZZ
2.00 2218
ZZZZZZ
1.00 2223
A
ZZZZZZ CCV
1.00 2227 I.00 2232
CCB
1.00 2237
PBW
1.00 2241
PBWA
1.00 2246 __ 107.0
LCSW
1.00 2250
LCSWA
1.00 2255 __ 109.1
BRA5S
1.00 2300
BRA5SA
1.00 2304
61.7
BRA4D
1.00 2309
BRA4DA
1.00 2314
68.2
X X X X X X X X X
X X--
X
X X
-- ~ ~ ***"
X
X
X
X
X
X
X
FORM XIV - IN
ILM04.0
DUP050307578
U.S. ERA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES____
Contract:
Code: ________
Case No.: SAS No.: _____________________ SDG No.: FMD01
Instrument ID Number: 03812_
Method: F_
Start Date: 09/24/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes A S AB BCCCC c F PMMHN K S AN TV Z
LBS AE DAROuE BGN G I E GA L N
BR4DD BR4DDA CCV CCB
BRS4S BRS4SA BRS3D BRS3DA
BRS3DD BRS3DDA BRS3DS ZZZZZZ DRA3S DRA3SA CCV
CCB BRA2D
BRA2DA BRA2S BRA2SA BRAID BRA1DA BRA1S BRA1SA BRAF1 BRAF1A CCV
CCB
1.00 2318 1.00 2323 1.00 2327 1.00 2332 1.00 2336 1.00 2341
1.00 2346 1.00 2350
1.00 2355 1.00 0000 1.00 0004 1.00 0009 1.00 0013 1.00 0018 1.00 0023 1.00 0027 1.00 0032 1.00 0037
1.00 0041 1.00 0046 1.00 0051 1.00 0056 1.00 0100 1.00 0105 1.00 0110 1.00 0114 1.00 0119 1.00 0124
61.3
70.6 72.0 94.6
65.7
63.7 62.4 63.6 59.0 114.4
X X X X X X X X X X X
X X X X X X X X X X X X X X X X
POEM XIV - IN
ILM04.0 57
DUP050307579
- T* " "* *
V""U-:J --'' ' ***#.... :-
.. .
:
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES_
Contract:
Lab Code: ________
Case No.:
SAS No.:
' SDG No. FMD01
Instrument ID Number: 04725_
Method: F_
Start Date: 09/24/96
End Date: 09/24/96
EPA Sample
No.
D/F
Time
%R
Analytes
A S A B B C C C C1 C F P M M H N K S A N T V z
LB SAEDARouE BGNG I E GA L N
SO S3
S9
S15 S30 S60 ICV ICB CRA
CCV CCB ZZZZZZ
zzzzzz
ZZZZZZ
zzzzzz zzzzzz zzzzzz
BRA2D
BRA2DA
BRA2S
BRA2SA CCV
CCB BRAID BRA1DA BRA1S BRA1SA BRA1SD BRA1SDA
BRA1SS
zzzzzz
BRAF1
1.00 0123 1.00 0127 1.00 0131 1.00 0135
1.00 0139 1.00 0143 1.00 0147
1.00 0151
1.00 0155 1.00 0159 1.00 0203
1.00 0207 1.00 0211 1.00 0216 1.00 0220 1.00 0224 1.00 0228 1.00 0232
1.00 0237
1.00 0241
1.00 0245 1.00 0249 1.00 0253 1.00 0257
1.00 0301 1.00 0305
1.00 0309 1.00 0313 1.00 0317
1.00 0321 1.00 0325 1.00 0329
93.9 73.7
101.5 97.6 98.8
--
_~ --
FORM XIV - IN
ILM04.0
5S
DUPO 50307580
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: IANCASTER__LABORATORIES
Contract:
Lab Code: ________
Case No-:
SAS No.: ________ SDG No. FMD01
Instrument ID Number: 04725_
Method: F_
Start Date: 09/24/96
End Date: 09/24/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABBC C CC CFPMMHNKS AN TVZ LBSAEDAR0UEBGNG I E GAL N
BRAF1A CCV
CCB
ZZZZZZ ZZZZZZ zzzzzz ZZZZZZ zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz CCV CCB PBW PBWA
LSCW
LCSWA
BRA5S
BRA5SA
BRA4D
BRA4DA BRA4DD
BRA4DDA CCV CCB BRS4S BRS4SA BRS3D
BRS4DA
BRS4DD
BRS4DDA
1.00 0333
1.00 0337 1.00 0341 1.00 0345 1.00 0349 1.00 0353 1.00 0357
1.00 0401 1.00 0405 1. 00 0409
1.00 0413 1.00 0417 1. 00 0421 1.00 0426 1.00 0429 1.00 0433 1.00 0437 1.00 0442 1.00 0446
1.00 0450
1.00 0454
1.00 0458 1.00 0502 1.00 0507 1.00 0511 1.00 0515 1.00 0519 1.00 0523 1.00 0527 1.00 0531 1.00 0535 1.00 0540
1.00 0544
88.0
0.0 120.5
86.4 69.0 64.5 91.6 119.2 125.2
_
--
FORM XIV - IN
ILM04.0
5*
DUP05 0307581
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES.
.Contract:
Lab Code: ________
Case No.;
SAS NO.: ________ SDG No.: FMD01
Instrument ID Number: 04725_
Method: F_
Start Date; 09/24/96
End Date: 09/24/96
EPA Sample
No.
D/P
Time
%R
Analytes
ASABBC C CC CFPMMHN KS AN TVZ LBSAE DAROuE BGN G I E GA L N
BRS3DS ZZZZZZ DRA3S
DRA3SA
CCV
CCB BRA2D BRA2DA BRA2S BRA2SA
BRAID BRA1DA BRA1S BRA1SA
BRAP1 BRAF1A CCV CCB
1.00 0548
1.00 0552
1.00 0556
1.00 0600 118.3
1.00 0604
1.00 0608
1.00 0612
1.00 0616
90.7
1.00 0620
1. 00 0624
90.1
1. 00 0628
1.00 0632
86.8
1.00 0636
1.00 0640 -9999.9
1.00 0644
1.00 0648 102.7
1.00 0652
1.00 0656
FORM XIV - IN
ILM04.0
6y
DUP050307582
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTEE_LABORATORIES
Contract:
Lab Code: ________
Case No.:
SAS NO.: ________ SDG No.: FMD01
Instrument ID Number: 04725
Method: F
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASA BBC CCC CF PMMHNKSANTVz
L B S A E D A R 0 O' E B G N G I E G A L N
SO S5 S15
S25 S40 S50 ICV ICB CRA CCV CCB PBW
PBWA LCSW
LCSWA BRA5S BRA5SA BRA4D BRA4DA BR4DD BR4DDA CCV
CCB BRS4S BRS4SA
BRS3D BRS3DA BRS3DD BRS3DDA BRS3DS ZZZZZZ DRA3S
1.00 0837
1.00 0841
1.00 0845
1.00 0849
1.00 0853
1.00 0857
1.00 0901
1.00 0905
1.00 0909
1.00 0913
1.00 0917
1.00 0921
1.00 0925 __ 101.2
1.00 0930
1.00 0934 108.8
1.00 0938
1.00 0942
86.2
1.00 0946
1.00 0950
72.3
1.00 0955
1.00 0959
84.7
1.00 1003
1.00 1007
1.00 1010
1.00 1015
99.3
1.00 1019
1.00 1023
88.7
1.00 1027
1.00 1031
91.1
1.00 1035
1.00 1039
1.00 1043
X
X
X
X X -- ""
X
X X"
--*
X
X X
""-- -- --
X
X
-- ~ _--
X
X --
X X X
X X
X X
X --
X
X X X X ~X
X ~ mmm --
M. _ _ _ _
X
FORM XIV - IN
ILM04.0
81
DUP050307583
U.S. ERA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES.
Contract:
Lab Code:
Case No.: ____________ SAS No.: ______ SDG No.: FMD01
Instrument ID Number 04725_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
A S ABBC CCCC FPMMHNKS ANTV Z LBSAE DAROUE B GN G I E GA L N
DRA3SA CCV CCB BRA2D
BRA2DA BRA2S BRA2SA BRAID BRA1DA BRA1S
BRA1SA BRAF1
BRAF1A CCV CCB
1.00 1047 1.00 1051
1.00 1055 1.00 1059 1.00 1103 1.00 1107 1.00 1111 1.00 1115
1.00 1119 5.00 1123 5.00 1127 1.00 1131
1.00 1135 1.00 1139 1.00 1143
94.0
99.5 94.6 22.9 103.6 175.6
X X X X X X X
X X
X X
FORM XIV - IN
ILM04.0
A
6
DUP05 0307584
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: ________
Case No.:
SAS No.: ________ SDG No. FMD01
Instrument ID Number: 04725_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
A S A B B C C C C C F PMMHN K S AN TV z LB S AE DAROu E B GN G I E G A L N
SO S5 S15 S25 S40 S50 ICV ICB
CRA CCV
CCB BRAID BRA1DA BRAF1 BRAF1A ZZZZZZ ZZZZZZ
ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV
CCB
1.00 1546 1.00 1550 1.00 1554
1.00 1558 1.00 1602 1.00 1606 1.00 1610 1.00 1614
1.00 1618 1.00 1622
1.00 1626 1.00 1630
1.00 1635 1.00 1639 1.00 1643
5.00 1647 5.00 1651
5.00 1656 5.00 1700 5.00 .1704
5.00 1708 1.00 1712
1.00 1716
123.1 131.8
X
X
X
X
X
X
X
X
X
X
X
X
--
--
""
X X
""
X
X X
FORM XIV - IN
ILM04.0
DUP050307585
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: ________ Instrument ID Number:
Case No.: ___ G2803_
SAS No.: _____ __
*
Method: F_
SDG No.: FMD01
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No,
D/F
Time
%R
Analytes
ASABBC C C CCFPMMHN KS ANTV z LBSAE DAROUE BGN G I E GAL N
SO S10 S20
S40 S60 S80 ICV ICB CRA ZZZZZZ CCV CCB
PBW PBWA LCSW LCSWA BRASS BRA5SA BRA4D BRA4DA BR4DD BR4DDA
CCV CCB BRS4S
BRS4SA BRS3D
BRS3DA BRS3DD BRS3DDA BRS3DS ZZZZZZ
1.00 0523 1.00 0527 1.00 0530 1.00 0534 1.00 0538 1.00 0541 1.00 0545 1.00 0548 1.00 0551 1.00 0555 1.00 0558 1.00 0602
1.00 0605 1.00 0609
1.00 0612 1.00 0615 1.00 0619 1.00 0622 1.00 0626 1.00 0629 1.00 0633 1.00 0636
1.00 0640 1.00 0643 1.00 0646
1.00 0650 1.00 0653 1.00 0657 1.00 0700
1.00 0703 1.00 0706 1.00 0710
110.3 106.2
96.2 96.8 98.0
93.0 100.0
93.5
X X X X X X X X X
X X X X X X X X X X X X X X X X
X X X
FORM XIV - IN
ILM04.0
f*
to'
DU P 050307586
U.S. EPA - CLP 14
ANALYSIS RON LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: ________
Case No.:
SAS No.: ________ SDG No.: FMD01
Instrument ID Number: 02803_
Method: F_
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABBCC CCC FPMMHNKS ANTV z
LBS AE DAROU E BGN G I E GA L N
DRA3S DRA3SA
CCV CCB BRA2D
BRA2DA BRA2S BRA2SA BRAID BRA1DA
BRA1S BRA1SA BRAF1 BRAF1A CCV
CCB
1.00 0713 1.00 0717 1.00 0720 1.00 0723
1.00 0727
1.00 0730 1.00 0733 1.00 0737 1.00 0740 1.00 0744 1.00 0747 1.00 0751 1.00 0754 1.00 0757 1.00 0801
1.00 0804
t
aCO
87.0
101.1 104.8 105.2
104.0
X X X X X
X X X X X X X X X X
X
FORM XIV - IN
ILM04.0
\ *3
DUP050 307587
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: ________
case No.:
SAS No.: ________ SDG No.: FMDQ1
Instrument ID Number: 02803
Method: F
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
A S A B B CC C C C F PMMHN KSANTV z
L BS AE DAR0 U E B GNG I E G A L N
SO
S10
S20
S40
S60
S80
ICV
ICB
CRA
zzzzzz ccv
CCB
BRS3D
BRS3DA
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
zzzzzz zzzzzz
zzzzzz zzzzzz
A
CCV CCB
A
1.00 1225
1.00 1228
1.00 1232 1.00 1236 1.00 1239 1.00 1243 1.00 1246 1.00 1250 1.00 1253 1.00 1256
1.00 1300 1.00 1303
1.00 1306 1.00 1310 __ 100.0 1.00 1313 1.00 1317 1.00 1320
1.00 1324 1.00 1327
1.00 1331
1.00 1334 1.00 1338
1.00 1341 1.00 1344
. . _____
X X X X X X X X X
X X X X
~ *** " M--
X X
A
FORM XIV - IN
ILM04.0
66
DUP050307588
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTERJLABORATORIES
Contract:
Lab Code: ________
Case No.:
SAS NO.: ________ SDG No.: FMD01
Instrument ID Number: 05220_
Method: CV
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABBC C C CC F PMMHNKSANTV z
LBS AE DAR0U E BGNG I E GA L N
SO SO.2 SO.5 S1.0 S2.5 S5.0 ICV
ICB CRA CCV
CCB PBW LCSW
BRA5S BRA4D
BR4DD
BRS4S
BRS3D BRS3DD BRS3DS DRA3S CCV CCB BRA2D BRA2S BRAID
BRA1S
BRAF1
zzzzzz zzzzzz zzzzzz zzzzzz
1.00 1714 1.00 1716 1.00 1718 1.00 1721 1.00 1723
1.00 1726 1.00 1728 1.00 1731 1.00 1733 1.00 1735 1.00 1738 1.00 1740 1.00 1742 1.00 1745 1.00 1747
1.00 1749
1.00 1751
1.00 1754 1.00 1756 1.00 1758 1.00 1800 1.00 1803 1.00 1805 1.00 1807 1.00 1809 1.00 1812
1.00 1814
1.00 1816 1.00 1818 1.00 1821 1.00 1823 1.00 1825
X X X X X
X X X
X X X X X X X
X
X
X X X X X
X X X X
X
X
A
FORM XIV - IN
ILM04.0
6> ' K
DUP050307589
Sra.|iw
D.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTEK_LABORATORIES____
Contract:
Lab Code: ________
Case No.: SAS No.: _____________________ SDG No.: FMD01
Instrument ID Number: 05220_
Method: CV
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS AB B C C C C CF PMMHN KSAN TV Z LBS AE DAR0UE B GNG I E GAL N
ZZZZZZ CCV CCB
1.00 1827
1.00 1830 1.00 1832
X X
FORM XIV - IN
ILM04.0 /% * 00
DUP050307590
Raw Data
6
DUP050 307591
ICP Data
70
DUP050307592
Pace:
Lancaster Laboratories
Data Reviewed By: (0^245 q-zs-<iU
Data Verified Bvv: =q.
Analyst:
811
Data rile Name: 26806T61.DA7 Run Narrie: 9626S06T61
Instrument Parameters:
Rinse Time: Individual Integration Time: Total Integration Time:
60 sec 10 sec 30 sec
Element Ag'
Al^' As Eta Re Ca Cd Co Cr C'u Pe K
Symbol
Hn Mo Na Ni
Pb Ph
Rb V' O R ( Sn 11 11 V "t
n
Element Name Silver
Aluminum Arsenic Ba r I urn Beryllium Calcium Cadmium Cobalt Chromium Conner I ron Potassium Magnesium Manganese Molybdenum Sodium Nickel Lead L ead Antimony Antimony Selenium ' Selenium Ti n Titan!um Thallium Vanadium Yttrium Zinc
Wavelength(nm) 328,06 * 30S.21 189.04 493.40 313.04 317.93 226.50 228.61 267.71 324.75 271.44 766.A 9 279.07 257.61 202.03 330.23 231.60 220.55/1 420.55/2 206.83/1 206.S3/2 196.02/1 1.96.02/2 '189.98 C4>4.94 190.86 292.40 371.03 213.85
71
DUP050307593
The 6 IE TRh CE 3CR uses a Crawf orci-Kunselmari Hcise < eouc i u.i Techniaue for lead, antimony, ana selenium. This require--, r he ut.i i iz*tion of tne first and second order wavelengths in the calculation of each of these meta.l determinations. The 61E TRACE TCP also utilizes - Yttrium as an internal standard to compensate for fluctuations in nebulization and plasma conditions All Yttrium readings are expressed in counts.
Page:- 2.
LANCASTER LABORATORIES
Run Name: 9626806T61
INSTRUMENT ID: 054
Tube: 1
SO
ELEM
. CONC (ppm )
AVG INTENSITY
RATIO
09/24/96
%RSD
' #1
20:59
INTEGRATIONS 2
' it3 '
___Ag ___A1 ___AS ___Ba ___Be ___Ca ___Cd ___Co ___Cr ___Cu ___Fe
K ___Mg
. tin ___Mo ___Na ___Ni ___Pb ___Sb ___Se ___Sn ___Ti ___Tl ___V ___Y __Z n
0.000
o .poo o.ooo
0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 '
0.000 0.000
0.000 0.000
0.000 0.000 0.000 0.000 0.000 0.000 0.000 0. OOO 0.000
N/A 0.000
-0.00046 0.00655 0.000060.00006
-0.04990 -0.00072
0.00017 -0.00018
0.00003 -0.00131 -0.00001
0.00316 0.00021 0.00038 -0.00051 `
-0.00020 0.00018 0.00130 0.00090
--0.00163 -O'. 00003
-0.00039 -0.00109
0.00003 1639 1.1.00000
-0.00005
12.32 1.509 583.5 14.54 0.913 3.101 8.626 51.85 96.64 2.795 161.9 19.43 25.73 5.452' 29.78 17.77 56.49 3S. 75 30.39 33.93 291.6 8.906 23.76 65.88 0.226
11.24
-0.00040 0.00657 0.00048 0.00007
-0.05015 -0.00071
0.00018 -0.00025
0.00002 -0.00131
0.00001 0.00387 0.00025 0.00040 -0.0.0035 -0.00019 0.00006 0.00169 0.00089 -0.00199 -0.00012 --0.00036 -0.00090 O.00001 169324.00000 -0.00004
-0.00052 0.00663
-0.00013 0.00005
-0.05019 -0.00071
0.00016 -0.00007
0.00007 -0.00134 -0.00002
0.00278 . 0.00024
0.00039 -0.00065 -0.00017
0.00023 0.00116 0.00119 -0.00191 0.00005 -0.00037 -0.00139 0.00002 163563.Q0000 -0.00005
-0.00047 0.00644
-0.00016 0.00005
-0.04938 -0.00075
0.00018 -0.00020
0.00000 -0.00127 -0.00002
0.00283 0.00015 0.00036 -0.00052 -0.00024 0.00025 0.00254 0.00063 -0.00099 -0.00002 -0.00043 -0.00099 0.00005 168841.00000 -0.00005
DUPO 50307594
I'age: 3
LANCASTER LABORATORIES
Run Name: . 9626806T61
1 ube : 2
C-.' SI
09/24/96
21:04
INSTRUMENT ID: 054
1 LEM
_A1 __Ca '"f _K l_Mg _Na ~_Y
CQNC (ppm)
50.000 50.000 50.000 50.000 ' 50.000 50.000
N/A
AVG INTENSITY
RATIO .
*
%RSD
#1
0.68269 0.74698 0.22032 1.16425 " 0.70452 0.-10852 169820.32812
0.121' 0.307 0.329 '0.150 0. 194 0.110 0 -177
0.68196 0.74561 0.21973 1.16456 0.70331 0.10866 169753.00000
INTEGRATIONS ft 2
3.
0.68359 0.74570 0.22011 1.16583 0.70424 0.10847 170150.00000
0.68253 4 0.74964
0.22115 1.16237 0.70601 0.10844 169558.00000
O
DUP050307595
Page: 4
LANCASTER' LABORATORIES
Run 1'lame:' 9626806T61
INSTRUMENT ID: 0547
T ube : 3
S2 5 .
09/24/96
21:08
ELEM.
CONC ( ppm )
AVG INTENSITY
RATIO
. %RSD
41
INTEGRATIONS . ' 42
43
___Aa ___As ___8 a ___Be ___Cd
___Co ___Cu
___Mn ___Ni ___Pb ___Se
__T1 __Y __Zn
. 1.000 1.000 t .000 1.000 1.000
1. OOO
1.000
T.000 1.000 1.000 1.000
1.000 N/A
1.000
0.20739 0.23178 0.23137 4.26776 1 .18286 0.23704 0.18232 0.97159 0.16178 0.29078 0.11607 0.09725 171027.67187 0.09568
0.583 0.58S 0.640 0.4 64 0.497 0.341 0.690 0.505. 0.550 0.461 0.522 T. 544 0.516 0 .. 503
0.20639 0.23041 0.23030 4.25455 1.17977 0.23647 0.18125 0.96815 0.16103 0.28997 0.11558 0.09571 171713.00000 0.09531
0.20703
0.20873
0.23180 "
0.23313
0.23076
0.23306
4.25815
4.29058
1.17917 .
1.18964
0.23668
0.23796
0.18201
0.1B371
0.96942
0.97721
0.16155 .
0.16277
0.29005
0.29233
0.11589
0.11675
0.09735
0.09871
171339.00000 170031.00000
0.09551
0.09622
7-J
DUP050307596
i`age:. 5
LANCASTER LABORATORIES
Kun Name: '(u be: 4
9626806T61 3
S3 '
09/24/96. .
21:12
INSTRUMENT ID: 0547S
F..LEM.
CO.NC (ppm.)
AVG INTENSITY
RATIO
%RSD
#1'
INTEGRATIONS #2
#3
___Cr ___MO ___Sb
__Sn .___Ti ___V '__Y'
1.000 1.000 1 .000 1 .OOO 1 .OOO 1.000
N/A
0.13241 0.4003S 0.33137 0.09330 0.46603 0.13638 170769.67187
0.408 0.770 1.983 0.313 0.372 0.395 0.485
0.13237 0.39719 0.32^445 0.09373 0.46580 . 0.13654 170807.00000
0.13296 0.40335 0.33742 0.09412 0.46787 0.13713 169923.00000
0.13188 0.40059 0.33283 0.09354 0.46443 0.13605 171579.00000
n> <3 %J DU P050307597
Page: 6
LANCASTER LABORATORIES
Run Name : 9626806T61
Tube: 5
ICV
' 09/24/96
21:15
INSTRUMENT
ELEM
___Ag A1
___As ,___Ba ___Be' ___Ca ___Cd ___Co ___Cr ___Cu
- Fe ___K ___Mg ___Mn
' Mo ___Na .___Ni ___P-fo. ___Sb ___Se ___3 n ___Ti . ___Tl ___V ___Y ___Zn
AVG
INTEGRATIONS
(ppm)
%RSD
#1
#2
#3 R
0.60482 29;38S00
0.60890 0.59558 0.609.29 29.35874 0.59254 0.59288 0.59517 0:60509 29.26608 - 28.97917 . 29.29872 0.59807 0.60114 30-12432 0.59777 O.59272 0.57347 0.60060 0.59411 0.60741 0.59313 0.59305 170740.00000 0.59761
0.210 0.226 0.676 0.106 0.505 0.576 0.322 0.692 0.326 0.21-3 0.720 0.573 0.343 0.316 0.436 O . 496 0.420 0 .-747 0:540 1.119 0.677 0.244 3.575. 0.251 0.394 0.301
0.60335
. . 0.60555'
0.60556
29.36579
29.45919
29.33003
0.60595
0.60713
0.61361
0.59614
0.59570
0.. 59489
0,,60631
0.60911
0.61246
29.18472
29.36904 '
29.52247
0.59114
0.59176 .
0.59472
0.5S837
0.59388
0.59639
0.59359
0.59459
0.59734
0.60444
0.60658
0.60426
29.02645
29.34920
29.42260
29.12981
29.0.0704
23.80066
29.-18828
29.32270
29.38517
0.59618
0.59805
0.59997
0.59964
0.59961
0.60417
30.19440
30.22581
' 29.95274
0.59500
0.59840
0.59991
0.58851
0.59231
0.59735
0.56991
0.57496
0.57555
0.59358
0.60123
0.60698
0.59027 .
0.59375
0.59830
0.60583
0.60764
0.60S77
0.56933
0.60003
0.61003
0.59154
0.59309
0.59452
170509.00000 171498.00000 170213.00000
0.59627
0.59689
0.59965
0547E REDIG
>7
DUP050307598
I i.i.if-sr t
LANCASTER LABORATORIES
nin Name: iiif.e: 6
9626806T61 ICB ,
09/24/96
21:20
INSTRUMENT ID: 054 7S
AVG
IM
(ppm)
% RSD '
#1
INTEGRATIONS #2
tt3 REREAD REDIG
AO
0.00020 162-8 .
0.00042
0.00033
-0.00018
fU
0.00188 216.5
0.00656
--6.00102
0.00012
tis
-0.00054 411.6
0.00028
0.00117
-0.00310
lia '
0.00007 50.02
0.00010
0.00008
o:oooos
he
0.00031 14.14
0.00030
0.00036
0.00027
i. a ,
0.07995 1.832
0.08163
0.07924-
0.07893
id
0.00038 6.123
0.00037
- ' 0.00040
0.00036
t :n
0.00033 80.24
0.00005
0.00059
0.00035
i.' r
0.00025 76.39
0;00006
0.00045
0.00024
Tu
0.00001 1784.
0.0002.1
- 0.00003
-0.00021
Fe
0.04209 1.746
0.04253
0.04250
0.04124
l\
0.05260 4.111
0.05027
0.05299
0.05454
no
0.02379 9.791
0.02639 '
0.02307-
0.02191
rin
0.00009 17.44
0.00009
0.00007
0.00010
no
O.. 00104 24.36
0.00100
0.00131
0.00081
i ! *
0.18881 15.62
0.15776
0.21648
0.19220
Hi t*h
-0.00057 221.3 0.00059 14 9.7
-0.00204 0.00012
0.00034 0.00003
-0.00004 0.00161
hh
0.00045 448.7
0.00161
0.00168 .
-0.00191
* ,r?
-0.00014 317.6
-0.00064
0.00022
0.00000
; ,n
0.00119 74.28
0.00193
0.00143
0.00021
1
0.00020 23.62
0.00024
0.00015
0.00021
11
0.00014 982.6
-0.00098
0.00176
"0.00033
V
0.00023 69.59
0.00016
0.00011
0.00041
Y 173548.67187 0.301 173230.00000 174.1 53.00000 173263.00000
/n
0.00013 79.69
0.00020
0.00019
0.00001
,
t
DUP050307599
Page: 8
LANCASTER LABORATORIES
Run Name: 9626806T61
Tube: 7
CRI
09/24/96
21:25
INSTRUMENT ID': 0o47
ELEM
___Ag ___A1 ___As ___Ba ___Be ___Ca ___Cd . Co ___Cr ___Cu ___Fe ___K ___Mg __^Mn ___Mo ___.Na ___Ni ___Pb ___Sb ___5e ___Sn Ti ___Tl ___V ___Y ___Z n
AVG
INTEGRATIONS
(ppm.)
%RSD
#1
#2
#3 REREAD REDI:
0.02068 0.00302 . 0.01893 0.00021 0.01019 0.07907 .0.01020 0.10118 0.02028 0.051-48 0.04162 0.04804 0.02568 0.03067 0.00065 0.14738 0.08100 0.00612 0.11755 0.01018 -0.00006 0.00032 0.01810 0.10333 171837.67187 0.04088
2.024 55.33 9.615 23.68 1.548 0.443 1.453 0.805 0.997 0.546 32.25 17.75 19.07 0.282 109.2 31.98 1.712 8.072 i - 206 18.98' 2539. 68.56 5.907 0.556 0.326 0.4 83
0.02069 0.00405 0.01909 0.00021 0.01017 0.07913 0.01035 0.10190 0.02036' 0.05175 0.03517 0.04690 0.02422 0.03076 0.00143 0.13085 0.08226 0.00557 0.11898 0.00300 -0..00184 0.00030 0*019w>3 0.10368 171208.00000 0.04110
0.02110 0.00393 0.01703 ' 0.00026 0.01004 0.07938 0.01019 0.10133 0.02044
0.05148 0.057060.05708 0.03114 0.03065 0.00004 0.20056 0.08122 0.00652 0.11753 0.01170 0.00113 0.00056 0.01757 0.10337 172023.00000 0.04073
0.02026 0.00109 0.02067 0.00016 0.01036 0.07869 0.01005 0.10030 0.02006 0.05119 0.03264 0.04013 0.02167 ' 0.03059 0.00047 0.11073 0.07952 0.00628 0.11614 0.01084 0.00051 .0.00011 0.01739 0.10295 172282.00000 0.04080
78
DUP050307600
, i6> r
LANCASTER LABORATORIES
h i Name : 9626806T61
il'iis: 8
ICSA
09/24/96
21:30
IHSTRUMEN ID: 05^
t-.Pl
.01 ns lia . lie ia jd .CO 0r C Ll ,l:e
k
jig jin . Ho ,ua Ni pb !: ; b \:e Si n
U :i
,v
Y /n
AVG . (ppm)
%RSD
#1
INTEGRATIONS #2
#3 1REREAD REDIG
0.00005 532.25592
-0.00220 6.00770
0.00162 512.73449
0.00119 -0.00077
0.00660 -0.00104 208.40.107
0.03714 554.17578
0.00421 -0.00072
0.17570 0.00608 0.00055 -0.00303 -O-j 00267 0.00022 -0.00129 0.00093 -0.00201 159367.00000 0.00217
1103. 0.526 37.40 0.444 3.768 0.598 23.11 77.20 11.68 14.86 0.329 29.53 0.081 1.077 64.55 38.25 7.743 136.9 40.20 116.4 890.8 8.638 229. 5 18.32 0.202 7.474
-0.00048 535.47369
-0.00144 0.00773
. 0.00168 509.29757
0.00149 -O'. 00147
0.00576 -0.00122 207.62466
0.02484 553.70031
0.00425 -0.00033
0.12493 0.00622 -0.00026 -0.00435 -0.00043 0.00180 -0.00141 0.00048 -0.00228 159441.00000 0.00214
-0.00009 530.93133
-0.00207 0.00766
. 0.00156 513.714`3S
0.00096 -0.00044 . 0.00675 -0.00096 208.65461
0..04069 554.60400
0.00416 -0.00059
0.15026 0 .-00555 0.00122 -0.00280 -0.00136 -0.00203 -0.00128 -0.00095-0.00159. 159647.00000 0.00235
0.00074 530.36279
-0.00307 0.00769 0.00160
515.19165 0.00111
-0.00041 0.00728
-0.00095 208.92393
0.04590 .554.22308
0.00423 -0.00125
0.25193 0.00646 0.00069 -0.00194 -0.00623 0.00091 -0.00119 0.00326 -0.00217 159013.00000 0.00203
'i
DUPO 50307601
Page: 10
LANCASTER LABORATORIES
Run Name:. 9626806T61
Tube: 9
ICSA8
09/24/96
21:
INSTRUMENT ID: 0547E
ELEM
AVG (ppm)
%R5D
INTEGRATIONS
#1 :
82
#3 REREAD REDIG
___Ag
0.21825 0.090
0.21840
0.21803
0.21833
___A1
539.96038 0.092
'540.17498
539.39208
540.31402
'___As
0.10306 1.395
0.10156 "
0.10320
O.10442
___Ba
0.53083 0.133
0.53138
0.53003
0.53107
______________
___Be
0.49049 0.334
0.49158
0.48860
0.49127
___Ca
522.81378 0.390
.524.41772
520.51483
523.50878
___Cd
.0.95787 0.298
0.96008
0.95464
0.95889 _________ ;
___Co
0.48575 0.258
' 0.48716
0.48475
0.48533 ________
___Cr
0.49960 0.272
0.50096
0.49824
0.49960 _________
___Cu
0.55148 0.051
0.55179
0.55123
0.55140
___Fe
211.88954 0.306-
' 212.42016
211.16601
212.08245 __
___K
0.05692 1.674
0.05585
0.05767
0.05724 __________________
___Mg '
562.50744 0.233
563.58367-
561.04626
562.89233
___Mn
.0.50265 0.301
0.50392
0.50098
0.50307 :
___Mo
0.00033 293.9
0.00109
-0.00078
0.00069
___Na
0.20998 30.41
0.22987
0.13855
' 0.26154 .
___Ni
0.96220 0.348
0.96551
0.95880
0.96229
___Pb
0.05061 3.117
0.04879
0.05155
0.05149
A
___5b
0.61917 O. 181
0.61787
0.61982
0.619S1
___Se
0.04893 4.716
0.05126
0.04664
0.04889
___Sn Ti
-0.00228 4 5.13 -0.00143 14.50
-0.00198 -0.00160
-0.00343 -0.00120
-0.00144 ________ _______ -0.00149 '
___Tl
0.09945 4.431
0.09456
0.10065
0.10312
___V
0.50938 0.377
0.51047
0.50716
0.51051
___Y
158866.00000 0.255 .58494.00000 159298.00000
158806.00000
___Zn -
1.01690 0.204
1.01853
1.01455
1.01761 ________
80
A DUP050307602
11
LANCASTER LABORATORIES
Name: 9626806T61
1 11*:: 10
CCV
09/24/96
21:40
INSTRUMENT ID: 05478
AVG
INTEGRATIONS
1 1 1 f`
( ppm)
%RSD
#1
... #2
#3 ` REREAD REDIG
rKi
0.49599 0.577
0.49897
0.4.9572
0.49326
Al
25.07147 0.445
25.17289
25.08963
24.95189
AS
0.49815 0.606
0.50152
0.49715
0.49572
1 la
0.48736 0.529
0.49023
0.48664
0.48522
|fa
0.49715 0.530
0.50009
0.49657
0.49499
\a
25.52026 0.577
25.47739
25.29534
25.18804
i <$
0.49286 0.510
0.49556
0.49245
0.4905S
1O
0.48569 0.584 .
,0.48838
0.48597
0.48272
rr
0.48935 .0.547
0.49205
0.48929
0.48669
rn
0.49881 0.485
0.50121
0.49885
0.49636
IB
24.60421 0.396
24r70601
24.59486
24;51176
l<
25.25224 0.408
25.35941
25.24394
25.15337
MO
24/92419 0.567
25.06753
24.92033
24.7347.1
fin
0.49468 0.549
0.49766
0.49405
0.49233
l-io
0.49421 0.421
0.49525
0.49558
0.49181
na
25.78198 0.321
25.84791
25.80929
25.68875
Hi
0.49508 0.613
0.49853
0.49391
0.49280
tJt>
0.48995 0.4 70
0.49245
0.48951 .
. 0.48790
Mo
0.45531 0.498.
0.45339
0.45473
0.45782
we
0.48910 0.384
0.49126
0.48821
0.48782
t:i n
0.49058 0.704
0.49439
0.48968
0.48766
1i
0.49939 0.507
0.50220
0.49871
0.49727
11
0.49092 1.181
0.48424
0.49377
0.49474
V
0.49409 0.695
0.49762
0.49390
0.49076
Y 169601.67187 0.872 168156.00000 169537.00000 171112.00000
A In
0.49707 0.574
0;50010
0.49670
0.49442
ai
DU P05 0307603
rr
Page: 12
LANCASTER LABORATORIES
Run iName: 9626806T61 Tube 11 CCB
09/24/96
21:45
INSTRUMENT ID: 05478
ELEM
___Ag ___AI ___As ___Ba ___Be ___Ca ___Cd ___Co ____Cr ___Cu ___Fe ___K ___Mg ___Mn ___Mo ___Na __Ni ___.Pb ___Sb
. Se ___Sn ___Ti ___Tl ___V . ___Y ___Zn
AVG (ppm)
%RS0
' #1
INTEGRATIONS 82
#3 REREAD REDIG
0.00020 194.8 0.05628 6.375 -0.00154 34.96 0.00008 47.72 0.00013 45.35 0.12475 2.939 0.00038 33.61 0.00000 8103. -0.00001- 3151.' -0.00022 91.48 0.05253 22.43 0.05280 6.363 0.06649 1.010 0.00006 93.53 0.00116 33.08' O.17536 26.04 0.00067 16.69 0.00000 17003 0.00299 10.44 0.00069 115.3 0.00149 50.32 0.00012 1.64.5 -0.00056 643.7 0.00032 94.24 170718.32812 0.191 0.00020 34.89
0.00065 0.05844 -O'. 00114 0.00011
0.00008 0.12461 . 0.00041 0.00059 0.00051 0.00000 0.06595 0.05662 0,,06646 0.00009 0.00142 0.22658 0.00059 0.00054 0.00290 -0.00022 0.00064 0.00031 0.00257 0.00060 170388.00000 0.00023
-0.00010 0.05826
-0.00216 0.00003 0.00020 0.12849 0.00024
-0.00061 -0.00014 -O.00029
0.04388 0.05032 0.06718 * 0.00009 0.00134 0.138S5 .0.00062 "0;00022 0.00274 0.00119 0.00176 -0.00008 -0.00455 0.00038 170725.00000 0.00011
0.00006 0.05214
-0.00133 0.00008 0.00011 0.12116 0.00049 0.00004
-0.00041 . -0.00037
0.04776 0.05145 0.06584
0.00000 0.00072 0.16064 0.00080 -0.00030 0.00334 0.00110 0.00207 0.00014 0.00028 0.00000 171042.00000 0.00024
'
D UP0503 07604
LANCASTER LABORATORIES
|,un Name: 9626806T61
11 if>e: 12
P8W
l , 100-100,DF1,962685720001, B,,
09/24/96
.21:50 .'
INSTRUMENT ID: 0547S
1 1 I'M
/ fig / Al
As
/. Ba
/ Ca ifed /So '/..C r
S~Cu / Fe
]/ Mg /.fin
..MO / Na ..Hi
'pb
,Sb Se Sn
' ri
,T 1 /y
y / 7n
AVG
(ppm)
%RSD
4*1
INTEGRATIONS #2
#3 REREAD REDIG
0.00001 3300. 0.04816 8.346 -0.00196 48.47 0.00002 132.1 0.00014 69.75 0.10601..4.071 0.00009 108.9 0.00013 203.2 0.00033 82.16 -0.00021 150.5 0.04640 14.60 0.05017 4.846 0.04464 16.94 0.00024 12.75 -0.00006 792.7 0.16098 23.72 0.00000 5525. 0.00039 104.9 0.00019 4 73.7 0.00067 170.3 0.00074 96.31 0.00007 155.3 -0.00081 24 6.3 -0.00011 211.2 172299.00000 0.439 0.00693 1.421
0.00058 0.04989 -0.00141 0.00003 0.00010 0.10745 '-0.00001
' 0.00044 ' 0.00055
0.00015 0.05409 ' ' 0.05205 0.05022 0.00027 0.00052 0.20278 -0.00064 -0.00002 0.00075 -0.00044 0.00027 0.00017 0.00114 0.000.1.6 17 2481.OOOOO 0.00697
-0.00007
-0.00046
0.05103 ,
0.04357
-0.00141
-0.00306
0.00006
-0.00001
0.00025
. 0.00006
0.10942
0.10116
0.00018
0.00010
-0.00008
0.00005
0.00041
0.00002
-0.00035
-0:00045
0.04383
0.04129
0.05103
0.04742
0.04766
0.03603
0.00024
0.00021
-0.00022
-0.00049
0.12792
0.15223
0.00035
0.00025
0.00080
0.00041
0.00069
-0.00086
0.00061
0.00186
0.00039
0.00157
0.00003
-0.00004
-0.00071
-0.00288
-O.00030
-0.00021
172949.00000 171467.OOOOO
0.00701
0.00682
DUP050307605
Page: 14
LANCASTER LABORATORIES
Run Name: 9626806T61
_
Tube:" 13 LCSW **** ,.1-1 ,, DEI , 962685720001 ,S , ,
09/24/96
21:55
INSTRUMENT ID: 0547
ELEM
^Aq
___As Ba
Be Ca Cd
Co Cr Cu
Fa K
j_Mg
___Mo S Na Ni ___Pb Sb ___Se
___Sn ___Ti ___Tl
*^V ___Y y Zn
. AVQ
INTEGRATIONS
(ppm)
%RSD
41
42
#3 REREAD REDI
0.05247 0.585 2.11878 0.432 2.08573 0.292 2.05071 0.259 0.05094 0.272 ' 4.24628 0.273 0.05190 0.457. 0.50233. 0.235 0.20518 0.3050.25912 0.223 1.07897 0.982
3.74078 0.202
2.04205 0.360 0.51574 0.278 2.07577 0.465 4.03482 0.827 . 0.. 51945 0.188 0.51712 0.353 0.52261 0.309 2.05270 0.342 4.11773 0.283 1.01707 0.290 2.04229 2.831' 0.51700 0.342 168687.67187 0.441
0.53898 0.256
0.05277 2.10860 2.08415 2.04813 0.05085 4.24497 0.05217 0.50275 0.20521. 0.25894 1.08219 3.73509 2;04244 0.51576 2.06639 4.04727 0.51837 0.51797 0.52371 2.05555 4.12275 1.01593 1.97630 0.51698 168387.00000 0.53920
0.05215 2.12139 . 2.08057
1 2.04717
0.05088 4.23539 0.05176 0.50100 0.20453 0.25865 .1.06713 3.73788 2.03451 0.51429 2.07522 4.06021 0.51970 0.51502 0.52075 2.04470 4.10437 1.01487 2.06645 0.51524 169536.OOOOO 0.53750
0.05248 2.12635 2.09248 2.05684 0.05110 4.25849 0.05175 0.50325 0.20578. 0.25976 1.08759 5.74937 2.04921 0.51717 2.08570 3.9969S 0.52027 0.51836 0.52336 . ' 2.05785 4.12608 1.02043 2.08412 0.51879 168140.OOOOO O'. 54024
s`
DUP050307606
15
LANCASTER LABORATORIES
j;iin Name: 9626806T61
llihe: 14 2583209 11+ t *,100-100,DF1,962685720001,8,
09/24/96
22:00
INSTRUMENT ID: 05478
,| 1 M
X.ol AS
X Ra X He y r.-a yea
X.c X..fi r x.Cu .J/Lfe >,K j/.r'g' /Mn
MO Na /.Hi fJb
SB . 3n
1i
n.
&v
Y / ln
AVG ( ppm )
%RSD
#1
0.00000 2958 .
0.03265 1 . 196 -0.00098 155.8
0.15306 0.374 -0.00008 22.56 67,43917 0.552
0.00025 57.0.9 0.00255 3.458 0.00004 752.0 0.00017 153.1 0;19775 2.231 . 2.74644 0.295 27.94168 0.508 0.77156 0.486 0.01252 2.540 52.11627 0.369 0- 00563 3.391 0.00043""79.04 -0.00048 219.6 -0.00033 278.8. 0.00117 140.2 0.00037 13.51 0.00587 79.29
0.00100 16.14
169208.67137 0.164 0.01285 0.840
0.00001
0.03303 -0.00256 0.15240 -0.00010 67.00941
0.00013 0.00266 -0.00010 -0.00011 0.19975 2.73739 27.77883 0.76724 0.01230 51.89437 0.00567 0.00068 -0.00149 0.00162 0.002S5 0.00042 0.01057 0.00082 168937.00000 0.01281
INTEGRATIONS
#2 3
RREREAD REDIG
-0.00015 0.03267
-0.00090 0.15345
-0.00007 67.63230
0.00021
0.00250 -0.00019
0.00038 0.19269 2.74839 28.03952 0.77345 0.01238 52.21729 0.00542 0.00004 0.00063 -0.00298 O.OOIOS 0.00037 0.00577 0.00107 169492.00000 0.01276
0.00015 ' 0.03225
0.00050 0.15331 -0.00006 67.67579 0:00041 0.00251 0.00043 0.00024 0.20080 2.75304 28.00669 0.77399 0.01289
52.23714 0.00580 0.00057
-0.00060 -0.00113 -0.00042
0.00032 0.00126
0.00112
169197.00000 0.01297
a
DUP0503 07607
Page: 16
LANCASTER.LABORATORIES
Run Name: 9626806T61
Tube: 15
-2583209 WS3 t>ft
UP**, 100-100,.DF.i; 962685720001 ,8,,
09/24/96.
22:05
INSTRUMENT ID: 0547E
ELEM
___AS __AI ___As ___Ba ___Be
Ca Cd Co ___c r ___Cu Fe ___K ___Mg. ___Mn J__MO ___Na ___Ni ___Pb ___Sb Se Sn ___Ti ___Tl ___V ___Y ___Zn
AVG (ppm)
%RSD
#1
INTEGRATIONS 42'
43 1REREAD REDIC
0.02071 1.699 0.45415 0.515 0.02030 2.765
, 0.56287; 0.378 0.01016 0.402
67.32511 0.355 0.01031 1.760 0.10360 0.343 0.0.2057 0.973 0.05221 0.522 0.38684 2.175 4.80761 0.662
28.52578 0 ..394 ' 0.79004 0.343
0.20781 0.364 53.46469 0.450
0.08648 0.146 0.01122 9.938 0.11054 1.518 0.01123 9.006 0.55796 0485 0.10412 0.284 . 0.01552 23.44 0.10301. 0.237 167878.32812 0.102 0.05574 0.460
0.02042 0.45621 . 0.02013 0.56533' 0.01020 67;56819 0.01046 0.10323 0.02034 0.05250. 0.38130 4.84349 28.65058 0.79294 0.20798 53.70262 0-OS662 0.01247 0.11145 0.01022 0.56107 0.10438 0.01161 0.10329 167794.00000 0.05593
0.02110 0.45160 0.01984
0.56173, 0.01012 67.31762. 0.01036 0.10393 0.02066 0.05219 0.39653 4.78260 28.49469 0.78960 .0.20848 53.22115 0.08644 0.01031 0.10860 0.01122 0.55664 0.10418 0.01881 O'. 10286 168076.00000 0.05584
0.02062 0.45463 0.02093 0.56156 0.01015 67.08953 0.01011 0.10365 0.02070 .0.05195 0.38269 4.79675
28.43208 0.78756 0.20699
'53.47031 0.08638 0.01090 0.11157 0.01225 0.55615
. 0.10379 0.Q1615 0.10288
167765.00000 0.05545
36
DUP050307608
'-'. vie: 1 7
LANCASTER LABORATORIES
Pun Name: 9626806T61
i ube
16 2583209
O * 100 1 OO , DF 1 , 9fo2685720001
09/24/96
22 : 10
INSTRUMENT IP: 054
I. I' M
A VO (ppm)
%R3D
INTEGRATIONS
2
43 REREAD RED
'''A cl S A1
y"B's
.o.ooooj.Be
03 r;cl if Co y Or y Ou ip ^K V Ma Mn
Mo
y Hi P'o
/ Sb . se
f-/n ri 'ri ~y\ i
A v/ ? n
0.00008 294.3
0.03304 7.311
-0.00077 58.31
0.15204 0.707
-0.00001 651.3
67 .. 3067 .1 0.767
0.00021 48.66
0.00295 .10.39
0.00127 6.924
0.00103 9.959
0.18985 1.021
2.77619 0.396
27.88556 0.708
0.78263 0.704.
.0.01.094 9.725
52.00482 0.358
*'3Sr*''
0.01274 0.921
0.00013 599.2
-0.00185 58.92
0.00009 555.6
0.00124 147.4 0.00054 13.27
-0.00040 577.8
0.00104 16.54
.1.69 7 56.32812 0.4 39
0.01384 ,1.332
0.00013 . 0.03101 . -0.00045 - 0.15279
67.55967 0.00029 0.00292 0.00136
0.00102
0.19009 2.78763 27.95882 0.78568 0.01216 52.09741 0.01262 --O.00026 "0.00311
. 0.00011
-0.00073 . 0;00060
0.00.193
0.00120
169466". 00000 0.01378
0.00032 0.03571 -0.00128 0.15252 , -0.00016 67.64842 0.00025 O.00328 0.00118 0.00114 0.19165
2.77529 28.03617
0.78595 0.01028 52.12677 0.01275 -0.00039 -0.00132 0.00058 0.00158 0.00057 "0.00042 0.00086 .169199.00000 0.01404
"0.00019 0.. 03239 _____
-0.00056 _____ 0.15081 _____ 0.00008 _____
66.71205 _____ 0.00009 _____
` 0.00266 _____ 0.00126 _____ 0.00094 ____ 0.18780 _____ 2.76566 ____
27.66169 ____ 0.77627 ____ 0.01037 _
51.79028 G"
' 0.01285 ____ 0.00105 ____
-0.00112 ___ -0.00042 ____
0.00289 ____ 0.00046 ____ -0.00271 __ 0.00106 ___ 170604.00000 ___ O.01369 ___
8<
DUP050307609
Page: 18
LANCASTER- LABORATORIES
Run Name: 9626806T61
^ps?>t>s T ube: 17 . 2583209
100-100,DF1,962685720001,8 9 9
09/24/96.
22:15
INSTRUMENT ID: 0547;-
ELEM
*^Aa
___As *-"Ba Be Ca * Cd v" Co /Cr
Zcu i/ Fe Zk
Mg slMn ___Mo
Na Ni ___Pb j2L.Sb ___Se ___Sn ___Ti ___Tl \/y ___Y iZ^Zn
AVG
INTEGRATIONS
(ppm)
%RSD
#1
#2
#3 REREAD REDI.'
0.05215 2.12663 0.04404 . 2.13293 0.04988 ' 70.40019 0.05005 0.49080 0.19887 ' 0.25406 1.22047 6.85321 29.51737 1.25780 2.01472 55.60460 0.50287 0.02051 0.49832 0.01041 4.10938 1.023S0 0.04606 0.49997 168349.00000 0.50979
0.448 0.613 4.902 0.282 0.396 0.408 0.815 0,487 0.286 0.354 1.157 0.379' 0.380 0.2920.754
0.562 0.441 4.974 0.456 ' 12 - 38 0.271 0.307 8.618 0.336 0.156 0.303
0.05238 2.13189 0.04459 2.13099 0.04973 70.46321 Q.05001 0.49276 0.19898 . 0.25433 1.23432 6'. 85401 29.55412 1.25741 1.99942 55.62997 0.50210 0.02123 0.49603 0.00906 4.10890 1.02337 0.04151 0.49993 168197.00000 0.50909
0.05191 .2.11178 . 0.04587
2.12811 0.04982 70.08609 0.04966 0.48813 0.19826 0.25305 1.20608 6.82680 29.39134 1.25433 2.01494 55.27972 0.50114 0.01935 0.49835 0.01053 4.09846 1.02088 0.04883 0.49831 168654.00000 0.50871
0.05217 2.13624 0.04166 2.13969 0.05011 ' 70.65127 0.05047. 0.49150 . 0.19938 0.25479 1.22101 6.87883 29.60665 1.26165 ' 2.02981 55.90410 <2_____ 0.50538 0.02097 0.50058 0 - 0116 3 4.12077 1.02714 0.04784 0.50167 168196.00000 0.51156
88
DUP05030761 0
Page: 19
LANCASTER LABORATORIES
Hun Name: lube: 18
9626806T61 2583209 13R5 3D^-
t ft. ** . 100-100 , OF5,962685720001,8 ,
09/24/96
INSTRUMENT ID: 0522:20 '
INTEGRATION'
A LFM
AVG (ppm)
%RSD
#1
#2'
#3 REREAD RE!
AA
_ _.Ag
,_A1
.__As
__ Ba
____He
__ Ca __Cd
_Je o
.... C r Cu
___f e
_"k __ Mg __ Mn
__Mo
___Na
.... Ni __ Pb __H; l __So
,~'_Sn
___T-'j
,.r i. __ v ___v __I n
-0.00010 181.4 0.03867 4.160
-0.00033 314.5 0:03053 0..546
-0.00058 9.378 .13.02253 0.552
0.00035 41.53 -0.00049 24.49
0.00032 20.61 -O.00061 14.87
0.07369 6.408 0.51974 0.412 5.32744 0.632 0.15183 0.575 0.00389 56.80 10.21795 1.589 0.00.106. 81.34 0.00284 13.53 0.00140 58.16 0.00096 196.1 O . 0022.1. 11 99 -0.00003 524.9 -0.00732 37.10 0.0005.1 30.03 164289.00000 0.429
0.00540 4.189
-0.000.10 0.03686
-0.00140 0.03035
~0.00064 12.93959'
0.00051 ' -0/00054
0.00025 -O.00052
0.06846 0.51837 5.28887 0.15082 0.00635 10.03613 0.00199 0.00248 0.00133 0.00229 0.00241 O.O0O14 -O.00489
0.00037 163483.00000
0.00536
0.00008 '0.03923 -O.00027
0.03054 -0.00055. 13.0591?
O.00026 -O.00036
0.00034 -0.00070
O.07498 0,52221 5.35099 0.15239 O.00324 10.34867 0.00092 0.00325 0.00224 -O. OOO'SO 0.00247 -0.00018 -O;00683
0.00067 164587.00000
0.00565
-0.00029 0.03992 O.00068 0.0306S
-0.00054 13.06884
0.00026 -0.. 00059
O.00038 -0.00059
0.07763 0.51865 5 ...34247 0.15228 0.00207 10.26904 0.00027 .0:00279 0.00061 0.00139 , 0.00175 -0.00005 -0.01026
0.00050 164797.00000
0.00520
39
DUP050307611
Page: 20
LANCASTER LABORATORIES
Run N&me: 9626806T61
****, -Tube: T9
2583205
100 100,DPI,962685720001,8 ,
09/24/96'
22:25
INSTRUMENT ID: 0547S
ELEH
X Aq
Xjil,
As
X Ba
^ Be
X Ca
jLfid
_XCo X Cr X Cu' X Fa
XK
JLMg JX-Nn
___Mo
XNa JLNi
Pb
Xsb
Se ___Sn
__ Ti __ Tl jLy __ Y
%-Zn
AVG (ppm)
%RSD
0.00015 73.87 0.04947 3.672 -0:00154 129.4 0.02923 0,622 -0.00008 103.9 280.44287 0.401 0.00029 38.61 0.00108 26.05. -0.00007 513.1 ' 0.00028 82.60 0.12530 3.457 3.44840 0.574 94.94965 0.499
0.33000 0.468 0.00083 76.18 45.39560 0.4.52 0.00381 0.148 0.00027 182.9 -0.00143 103.2 0.02402 2.775 0.00240 33.15 0.00092 15.25 -0.00239 23.70 0.00047 50.71 167785.00000 0.131
0.01484 0.963
INTEGRATIONS
#1 #2 .
0.00005
0.00028
0.04864
0.05155
-0.00204
0.00065
0.02933.
0.02935
-0.00002
-0.00017
281.39221
280.73797
0.00028
0.00018 .
0.00091
0.00093
0.00031
-0.00049
0.00001
0.00045
0.12851
0.12702
3.46929
3.44602
95.36868
95.04567
0.33121.
0.33053
0.00124
i 0.00115
45.59362
45.39136 `
0.00382
0.00880
0.00070
-0.00028
-0.00070
-0.00315
0.02478
0.02370
0.00230
0.00166
0.00085
0.00108
-0.00175
-0.00231
0.00045
0.00023
167535.00000 167866.00000
0.01500 ,
0.01478
#3'
REREAD REDIf
o.oooir
0.04821 ________ .______
-0.00325
0.02902
-0.00003 _________________
279.19842 __________________
0.00041
0.00141
-0.00004
0.00039
0.12037 ________ _______
3.42988
94.43459
0.32825
0.00010
45.20131
_____________L
' 0.00880 _
0.00042
-0.00046
0.02357 _
0.00325
0.00082
-0.00263
0.00071
167954.00000 ________ _____
0.01473
9<j
DUP05 0307612
l-MOR " 21
LANCASTER LABORATORIES
Run Name: ru.be.: 20
9626806T61 2583206 S r=S &4 ^
****,, :l 00-100 .`DPI ,9626857-20001,8, ,
09/24/96
22:30
INSTRUMENT ID: 054
f-LEM .
X Aq X_>1 ___As
XT'a
X_Ca
Xjld
jt.Co
X_C r X Cu X F e.
Xj-
X Nn ,i.Mn
___Mo ___N a "Xi'li
_ Pb
7k>t*
__ Sn
..... T i
. Tl
_V
X ;'r'
AVG' (ppm)
%RSD
tu
-0.00038 42.40 0.34437 0.804
-0-0O1B3 34.89 0.05566 0.272
.-0.00006 116.0 205.548'29 0.295 ' 0.00024 39.02
0.00512 5.751 0.00060 68.75' 0.00168 17.37 1.02805 0.128 3.98313 0.41.2 82 .. 11 1.56 0.278 0.66318 0.245 0.00648 4.359
62.07401 0.235 0.00546 1.682 0.00035 162.3
-0.00255 19 .-37 . 0.00000 93968
0.00032 29.1.8 0.01067 5.837 -0.00072 363.5 0.00122 21.47 67530.00000 0.284
0.00961 0.882
-0.00048 0.34744
-0.00133 0.05583
-0.00011 205.62783
0.000130.00525 0.00012 0.00135 1.02816 4.00125 82.19277 0.66394 0.00652 62.22286 0.00543 0.00052 - -0.00305 0.00020 -0.00045 0.01051 -0.00242
0.00092 167140.00000
0.00953
INTEGRATIONS
#2
#3 REREAD RED
-0.00047 0.34207
-0.00255 0.05555 0.00002
204.90425 0.00032 0.00478 0.00088 0.00177 1.02931 3.96915
81.85302 0.-66130 0.00673
61.93017 0.00539
-0.00028 -0.00205
0.00171 0.00138 0.01014 O.00230 0.00140. 1-68062.. 00000 0.00960
-0.OOO L9 0.34359
-0.00161 0.05559
-0.00009 206.11280
0.00026 0.00532 0.00080 0.00191 1.02668 3.97900 82.23889 0.66428 ! 0.0061.7 62.06900 0.00557 0.00081 -0.00256 -0.00190 0.00005 < 0.0.1.136. -0.00204
0.00136 167388.00000
0.00970
91
DUP050307613
page: 22
LANCASTER LABORATORIES
Run Name: 9626806T61
Tube: 21
2583207
****,,100-100,DF1,962685720001,8,,
09/24/96
22:35
INSTRUMENT ID: 05478
ELEM
AVG . (ppm)
%RSD
#1 '
INTEGRATIONS #2
#3 REREAD REDIG
-0.00013 226.5''
0.00018
-0.00016
-0.00043 __________
AJ
A
zSi
___AS
XBa ' XBe
Xca JLCd
JLCo
X_Cr
JLCu .
JC_Ee X*
XM3 XMn '___Mo ___Na XNi ___Pb
XSb
___Se ___Sn ,___Ti/ ___Tl Xv
__ Y
XZn
. 0.84648 0.780 -0;00086 28.37 0.06556 0.218 -0.00018 19.62
202.37734' 0.145 0.00036 50.96 O.00559 6.173 0.00145 29.92 0.00296 5.235 1.85463 0.506 4.08196 0.143
80.82465 0.101-. 0.68881 01113
0.00593 2.846 64.23705 0.149 0.00611 2.235 0.00016 367.7 -0.00053 49.56 0.00077 72.52 0.00068 157.1 0.02759 3.855 -0.00183 145.7 0.00258 13.59
165510.32812 0.242 0.01331 1.391
0.85281 -0.00079
0.06548
-Q.00019 202.66539
0.00056 0.00595 0.00184 0.00296 1.86347 4.08774 80.78174 0.68896 0.00585 64.12642 0.00626 O.00073 -0.00042 0.00099
0.00092 0.02855 -0.00015 0.00292 165679.00000 0.01342
0.84698 -0.00066
O.06548 -0.00014. 202.07684
0.00032 0.00555 O.00152 0.00280 1.84476 '4.08213 80.77294 0.68796 0.00581 64.29570 0.00610 -0.00047 -O.00083 0.00119
0.00163 0.0277S -0.00492 0.00260 165800.00000 0.01341
0.83963 -----------------------------
-0.00114 _______ .-------------
0.06573 ----------------------------
-0.00020 ________ _
202.38983 ..................................
0.00020 ___________________
0.00527 ________
0.00098 _____________:------
0.00311 __-
1.85565 -
4.07600 _---------------------------
80.91927
0.68951 ______ ________
0.00612
________________
64.28902
------------------- -
0.00598 _-
0.00023 ________ ____
-0.00034 _
'0.00013 _
-0.00049 _
0.02645 _-
-0.00043 __-
0.00222 ________________--
165052.00000
;----------------
0.01310 ________ _______
9
DUP050307614
, n:': 23
LANCASTER LABORATORIES
ii i Nam r 9626806.T61
11 >B : 22 CCV
09/24/96 .
22:40
INSTRUMENT ID: 05478
ItM
09 tU (is Ha H
ia .i.-d Co Cr
. i,u
f-'e
K
iig
Hn Mn
Ha
Hi
Pto
:>b t-.a sn Ti
11
v
AVG (opm)
%RSD
0.51295 2.303 25.73203 2.494
0.51611. 2.020 0.50644 2.235 0.51220 2.225 25.99452 2.320 0.50863 2.208 0.49243 2.366 0.50482 2.271 0.5I615 2.400 25.11793 2.362 26.22091 2.261 25.55746 2.385 0.50950 2.275 0.51152 1.595
26.41866 2.319 0.51055 2,456 0.50194 1.311 0.47096 0.837 0.50620 1.095 0.50011 2.470 0.SI563 2.321 0.50935 0.444 0.51050 2.231
SI-
0.52656 26.47300
0.52815 0.51980 0.52535 26.69038 0.52156 O.50588 O.51805 0.53045 25.80303 26.90563 26.26052 0.52288 0.52093
INTEGRATIONS
#2
0.50530 25.37452
0.51003 0.49990 0.50509 25.62315 0.50131 0.48520 0.49775' 0.50908 24.76909' 25.88622 25.17593 0.50252 0.50630
27.12618 0.524970.50952 0.47524 0.51258 0.51437 O.52945 0.51183 0.52364
26.06829 0.50217 0.49770 0.46748 0..50350 0.49286 0.50879 0.50740 0.50341
#3 REREAD REDIG
0.50699 25.34871
0.51015 0.49962 0.50616 25.67003 O.50302 0.48623 0.49867 0.50891 24.78168 25.87087 25.23593 0.50311 0.50734
26.06150 0.50452 0.49859 .0.47017 0.50252 0,49308 O.50864 0.50880 0.50445
Y
in
163520.00000 2.323 0.51377 2.379
159135.00000 0.52786
165804.00000 0.50603
165621.00000 0.50740
DUP050307615
Page: 24
LANCASTER LABORATORIES
Run Name: 9626806T61
T ube: 23
CCB
09/24/96
22:45
INSTRUMENT ID: 0547;
.
ELEM
___Ag ' A1 ___As ___Ba ___Be ___Ca ___Cd . ___Co ;___Cr . Cu ___Fe ___K ___Mg ___Mn * ___Mo ___Na ;___Ni ___Pb ___Sb ___Se
Sn TI ___T1 ___V ___Y ___Zn
AVG (ppm)
% RSD'
#1
INTEGRATIONS .. #2
#3
P
0.00002 0.01948 -0.00006 0.00004 0.00000 0.11384 0.00006 -0.00001 -0.00025 -0.00099 0.02903 0.04907 0.03539 0.00009 0.00075 O.16356 -0.00077 0.00041 0.00094 0.00022 0.00122 0.00026 0.00063 0.OOOOO 168330.OOOOO 0.00012
517.8 28.05 633.7 62.65 2500. 2.672 367.4 2247. 124.2 23.82 25.23 2.356 5h 400 18.32 134.3 12.61 127.8 290.5. 134.5 892.7 54.53 111.6 568.4 1048. 0.694 149.2
0.00004 0.02527 ^0'. 00021 0.0,0007 -0.00008 0.11699 -0.00020 0.00038 -0.00028 -0.00078 0.02146 0.04899 0.03755, 0.00011 0.00154 0.18707 0.00029 -0.00096 0.00227 ' ` 0.00230 0.00129 0.00012 -0.00332 0.00008 167003.00000 0.00011
0.00012 0.014*40
-0.00010 0.01879
0.00039
-0.00037
0.00001
0.00004
0.00007
0.00002
0.11360
0.11092
0.00012
0.00029
-0.00048
0.00004
. -0.00055 -0.00125
0.00007 -0.00094
0.02952 '
0.03609
0.05027 0.03392
0.04796 0.03470
0.00007
0.00010
0.00111.
-0.00039
0.14849
0.15511
-0.00166
-0.00096
.0.00122
0.00097
0.00079
-0.00024
-0.00162 0.00184 0.00061 0.00146
-0.00001 0.00052 0.00006 0.00377
0.00003
-0.00009
168776.00000 169211.00000
-0.00005
0.00031
RED 11
9*
DUP050307616
|Mae: 25
LANCASTER LABORATORIES
pun Name: 9626806T61
lube: 24 2583208-
5
4-+** , 100-100, DF1,962685720001,8 , , -
09/24/96
22:49
INSTRUMENT ID: 05478
. v AVG
INTEGRATIONS
It-EM
(ppm)
%RSD
#1
#2
#3 REREAD REDIG
0.00044 53.45
0.00029
0.00071 .
0.00031.
Sl ai As
X_Be X-Ca X~cd x~co-
0.04901 1.255 -0.00008 1808. 0.10141 0.605 -0.00004 161.8 137.78384 0.206
0.00022 19.32 0.00426 3.847
0:04854 -0.00177
O.10072
0.00000
137.47343 0.00018
s 0.00420
0.04971 0.00111 0.10160 -0.00011 137.84457 0.00026 0.00444
0.04879 0.00041 0.10190 0.00000 138.03350 0.00024 0.00413
*_Cr
.X-Cu.
0.00053 48.35 0.00033 89.75
0.00045 0.00022
-0.00082 0.00067
0:00032 OIOOOIO
A &A
O;11578 8.735 2.23712 0.457
0.10983 '2.22664
0.12746 2.23762
0.11005 2.24711
55.88039 0.-359
55.66714
55.90744
56.06658
X-Mn
0.94599 0.342
0.94246
0 ."94667
0.94883
__Mo
0.00199 24.86
0.00187
0.00157
0.00254
A
>C_Na
35.85942 0.380
35.71160
35.98054
' 35.88611
XNi
__PP
4SP
0.00932 7.943 -0.00009 539.3 -0.00116 95.66
0.00347 -0.00005 -0.00166
0.00986 0.00038 -0.00195
0.00961
-0.00060 0.00011
__Se
0.00465 25.09
0.00598
0.00414
0.00382
__Sn
0.00181 61.64
0.00191
0.00288
0.00065
__T i
0.00060 21.25
0.00061
0.00072
0.00047
_T1
-0.00001 .7681 .
-0.00123
0.00064
0.00055
i.v
0.00106 36.22
0.00088
0.00151
0.00080
_Y 167364.67137 0.281 167847.00000 166904.00000 167343.00000
jCzn
0.01162 0.373
0.01157
0.01163
0.01166
9b
DUP050307617
U* " Vyh ^Jv-^iEStyiw
Page: 26
LANCASTER LABORATORIES
Run Name: 9626806T61
Tube: 25
2583210 T>"P.^55
, ,, '****,100-100,DPI,962685720001 8
09/24/96 .
INSTRUMENT ID
22:54 `
0547;
ELEM
_^_Ag j[>i
As X Ba jLBe _X_Ca JS_Cd "X Co XCr /Cu X Fe
_X_K JC-Mg % Mn ___Mo
X.Na *P Ni
Pb XSb
Se ___Sn ___Ti
T1
XV Y
AVG(ppm)
%RSD
. #1
INTEGRATIONS, #2
43 , REREAD REDH
0.00043 137.8 2.63741 1.949 0.00190 49.93
0.07998 1.488 0.00021 117.3 244.61120 2.011 0.00025 67.90 0.00357 14.97 0.00177. 29.88 0.00136 10.32 2.00778 2.577 2.89321 1.063 98.49494 1.697 0.40961 1.803 0.00467 14.28 47.80621 1.007 0.00875 7.698 0.00183 24.74 0.00040 232. i 0.02173 9.065
0. OOS^vi J/S. 69
0.06660 4.101 -0.00189 154.5
0.00402 7.328 167917.67187 1.570
0.01505 1.949
-0.00020 2.57895
. GY 00191 0.07862 0.00049
239\01487 0.00013 0.00295 0.00120' 0.00124 1.95344 2.85902
96.58389 0.40119 0.00391
47.25038 0.00915 0.00220
-0.00056 0.01946 0.00276 0.06422
-0.00145 0.00369
170859.00000 0.01472
0.00052 2.67559 0.00284 0.08048 0.00013 246.56326 0.. 00018 0.00384 0.00187 0.00133 2.01343 2.90196 99.21250 0.41267 0.00517 48.07551 . 0.00797 0.00132 0.00130 O'. 02273 0.00346 0.06958 -0.00502 0.00409 167130.00000 0.01516
0.00099 2.65769 0.00094 0.08083 0.00000 248.25546 0.00045 0.00391 0.00225 . 0.00152 2.05646 2'. 91864 99.68842 0.41498 0.00494 48.09273 0.00913 0.00197 0.00047 0.02300 0.00258 0.06601 0.00079 0.00427 165764.00000 0.01528
3
DUP05030761 8
27 LANCASTER LABORATORIES
i.'iifi Name; %^680M6I
26 2586823
i.***.. 100-100. OF l ,962685720001,8, ,
09/24/96
22:59
INSTRUMENT ID: 0547
INTEGRATIONS
1 f~M
. AVG (ppm.)
%RSD
#1
#2
#3 REREAD RED]
x ix .
Aa
A1 _ As.
y. Re
0.00020. 107.3 0.03663 8.441 -0.00029 596.1. O.11852 0.740 -0.00009 109.8 72.6621.1. 0.723
.O.00000
0.04011 -0.00231 . 0.11945
-0.00020
73.23554
0.00016 0.03559 0.00061 0.11840
0.00000
72.54710
0.00042 _____ 0.03419 _____ 0.00081. ___ 0.11771 _____ -0.00007 _____ 72.20368 _____
X(-:a
<j n JL. Co X Cr 7.CU
X_/e
*-K .X.Mo .jX-Nn
__Mn
0.00002 546.9 0.00054 57.86 -0.00011 100.3 -0.00126 8.167 0.35827 0,888 5.55003 0.806 30,1671.6 0.713 0.24957 0.714 0.00832 1.437
-0.00013 0.00058
-0.00007 -0.00132
0.35967 5.59495 30.39034 0.25151 0.00831
0.00004
0.00021 ~0.00002
-0.00114 0.36052 5.54965
30.15035 0.24921 0.00820
0.00016 _____ 0.00083 _____ -0.00025 _____ -0.00132 _____ 0.35463 _____ 5.50548 ' 29.96080 ____:
0.24800 _____ 6.00844 50.74400 IS
A __Na X_Ni J_Pb JC.Sb S
n __ Ti
Ti
XV
.... Y i-f b
51.04218 0.678 0.00159 7.312 0.00068 129.3
-0.00109 '27.42
0.00079 108.8 0.00098 87.60 0.00029 34.13 -0.00035 720.6 0.00058 37.00 167 36.1. .52812 0.622 0.00969 0.811
5.1.42179 0.00146 0.00074
-0.00076
0.00000
' 0.00109
0.00019 0.00045 0.00035 166173.00000 0.00978
50.96075 0.00.162
-O'. 00023 -0.00115
0.00171 0.00007 0.00039 0.00170 0.00061 167796.00000 O'. 00963
0.00169 ____ 0.00152 ____ -0.00135 ____ 0.00065 ____ 0.00178 ____ .0.00028 ____ -0.00323 ____ 0.00070 ____ 168115.00000 ____ 0.00967 ____
A
DUP050307619
LANCASTER LABORATORIES
Run Name: 9626806T61
Tube:- 27
2583824
5
****,100-100,DF1,962685720001,8,,
09/24/96
' 23:04
INSTRUMENT ID: 0547:
ELEM
X Aq
Xa i
A.ve
Cbpm)
%RSD
#1
0.00032 108.0
0.00066
0.27574 0.061_0.27586
INTEGRATIONS #2
0.00004 0.27582
fls._____________-0.00049 377.1____________0.00124
-0.00026
Jc_Ba "X Be
.. 0.07801 0.413 -0.00021 38.53
0.07838 -0.00028
0.07787 -0.00012
#3 REREAD REDIi 0.00035 0.27555
-0.00246
0.0777S -0.00024
J
i
DUP050307620
LANCASTER LABORATORIES
Run Name: 9626806161
I' i! he : 28
2583825
ft i t>
V t * * ^ 100-100,DF1.962685720001, 8, .
09/24/96
23:09
INSTRUMENT ID: 05471
1-1. EM
X An
X Ai ___As X.fia XLBb X f;a X CM X. Co _X_Cr X i.'u X 'c e -Y-X x ..MO X Mn __MO _X Ma X..Ni
I'b -X-Rlr>
..
.Sn li 1f
\V Y
1 /n
A VC ( ppm)
V %RSD
. ,ttl
INTEGRATIONS *t2
#3 REREAD REDIC
0.00040 0.03019 -0.00010 0.]2122 O . 00013 96.62507 0.00055 0.00101 0.00027 -0.00024 0.36489 2.94537 29.44571 0.72579 0.00745 48.87559 O.00286 0.00145 -0.00143 -0.00085 0.00093 0.00002 -0.00192 0.00038 170530.32.812 0.02222
32.81
0.00026
3.470'
0.02914
2349.
-0.00086
0.613
0.12045
49.27
0.00021
0.680
95.88851
13.53
0.00053
26.90
0.00101
40.90
. . 0.00025
50.82
-0.00029
1.210
0.35989
0.243
2.94326
0.529
29.27752
O'. 711
0.72005
11.37
0.00806
0.249
48.79664
20.18
0.00228
21.05
0.00135
68.55 ,
-0.00243.
211.1
-0.00204
200.5
-0.00122
352.9
0.00010
176.4
0.00017 '
100.5
0.00000
0.533 171572.00000
0.539
0.02209
0.00052 0.03019 0.00268 0.12128 0.00008 . .96.83293 0.00063 0.00074. 0.0003.9 --0.00033 0.35827 2.93948 29.47409 ` 0.72726 0.00648 48.81419 0.00286 0.00180 -0.00137 -0.00174. 0.00214 -0.00006 -0.000110.00077 169894.00000 0.02224
0.0004 1 0.03124 -0.00213 0.12193 0.00012 . 97.15376 0.00049 0.00128 0.00017 -0.00010 0.36651 2.95337 29.58551 0.73006 0.00781 49.01594 0.00344 0.00121 -0.00047 0.00122 0.00189 0.00003 -0.00583. 0.00038 1 70125.OOOOO 0.02232
't* DUP050307621
page: 30
LANCASTER LABORATORIES
Run Name: 9626806T61
Tube: 29 2583826
^
****,100-100,DF1,962685720001f8f,
09/24/96
23:14
INSTRUMENT ID: 0547S
ELEM
AVG Cppm)
%RSD
* #1 -
INTEGRATIONS #2
#3 REREAD REDIG
_.Ag
0.00043 99.21
0.00000
0.00086
0.00045
0.22354 1.108
0.22626
0.22295
0.22141
___As
-0.00040 36.30
-0.0002-3
-0.00052
-0.00044
XBa
0.07660 0.341
0.07689
0.07640
0.07651
X Be ~^~Ca
0.00003 44 * 43 155.89045 0.090
0.00005 155..8239 7
0.00003 155.79457
. 0.00001 156.05284
X Cd -
0.00023 37.67
0.-00033
0.00020
0.00016
X C'6 % Cr
'
0.00037 81.13 0.00096 25.65
0.00003 0.00067
0.00048 0.00112
. 0.00060 0.00108
X Cu
-0.00065 51.14
. ` -0.00092
-0.00028
-0.00076
V Fe
0.40792 1.817
0.40193
' 0.41621
0.40563
XK
1.60855 0.358
. 1-. 61204
1.60189
1.61170
% Ma.
55.77170 0.095
55.82098
55.71517
55.77894
JLMn
0.023S4- 0.369
0.02362.
0.02345
0.02355
___Mo
0.00061 46.84
0.00094
0.00041
0.00048
>CNa
40.82687 0.176
40.89031
40.84182
40.74847
A * Ni
0.OO183 23.00
0.00222
0.00125
0.00203
Pb
Xsb
-0.00027 44.63 -0.00091 122.8
-0.00039 -0.00213
-0.00026 -0.00067
-0.00015 0.00007
___Se ___Sn ___Ti
0.15390 0.490 0.00083 52.96
0.00711 5.993
0.15303 0.00108 0.00684
0.15424 0.00032 0.00689
0.15443 0.00108 0.00760
__T1
ITv .
Y
X_zn
-0.00056 . 0.00131 167837.00000
0.01268
343.5 11.95 0.221 1 .122'
-0.00100 0.00118
167568.00000 0.01285
-0.00222 0.00127
168262.00000 0.0126i
0.00154 0.00149 167681.00000 0.01259
100
DUP050307622
LANCASTER LABORATORIES
Run Name: 9626806T61
lube: 30
2'..-83827
***** 100-100,DPI,962685720001,8,
09/24/96
23:19
INSTRUMENT ID: 0547
f 1 KM
X AO X aI
A'~. V Ba
ZLCa X on X Co Ter
_>0u XJe XK
MO * Mn
Mn X Na X Ni
Pb Tsb
___ .s n i j. T1
X.V ___V i rn
AVG (. pr>m
%RSD
O . 0< 0031 54.29 0 .'02393 5,600 -0 .' 00036 316.80 . 00144 3.0.19 C.i . 00016 50.95
0 . 14265 1.001 o. 00018 161.3
-0 . 00005- 885.4 0 . 00027 115.4
-0 - 00107 15.63 0 - 04518 17.93 0 . 05603 16.52 o. 03819 2.053 o. 00060 13.68
-o. 00073 23.85 o. 28660 16.16 o, 00003 770.4 o 00092 56.62
-0 ,00146 46.46 0. .00179 38.77 .00072 131.6
' 0 .00035. 32.15 --0 .00.1.47 40.38
0 .00053 38.41 l 708 58 .32812 0.300
oV. 00829 0.6fc>4
81
O.00026 O.02239 0.00080 0.00140 0.00026 0.14429 -0.00005
0.00002
0.00007 -0.00090
0.03869 "0.06081 0.03893
0.00060
-0.00068 0.30848
-0.00028 . ` 0.00032
-0,00217 0.00255 0.00027
.0.00047 -0.00082 0.00046
.171388.00000 0.00823
INTEGRATIONS
' #2
0.00050 0.02450 -0.00039 0.00148 0.00009 0.14205 0.00051 0.00041 0.00064 -0.00123 0.05427 0.04536 ' 0,03827 0.00069 -0.00093
0.31792 0.00016 0.00118 -0.00139 0.00119 0.00,008 0.00033 -0.00161 0.00077 170362.00000 0.00833
83 REREAD REDT
0.00017
0.02488 -0.00151
0.00145 0.00013 0.14163 0.00009 -0.00061
.0.00011
-0.00108 - 0.04259
0.06193 0.03737 0.00052 -0.00059 - 0.23369 0.00022 0.00127 -0.00081 0.00163 0.00383 0.00025 -0.00199 0.00038 170825.00000 0.00831
iOi
DU PO 50307623
s'gfiSSfe
Page: 32
LANCASTER LABORATORIES
Run Name: 9626806T61
Tube: 31
CRI
09/24/96 .
23:24
INSTRUMENT ID: 0547E
ELEM
___Ag A1
___AS ___8a ' ___8e
Ca ___Cd ___Co _Cr
CCl Fe ___K - Mg ___Mn ___Mo Na __N\ . ___Pb ___Sb ___Se ___Sn ___Ti ___Tl V ___Y ___Zn
AVG (ppm)
%RSD
ai
INTEGRATIONS -#2`
* #3 REREA'D
0.02082 0.02252 0.01953 0.00012 0.01021 0.10133 0.01041 0.09957 0.02079 0.05044 0.03517 0.05167 0.02707 0.03102 -0.00047 0.19095 0.08367 0.00643 0.11623 ' 0.00901 0.00132 0.00005 0.01848 0.10542 168668.67187 0.04180
0.814 5.228 3.167. 12.62 0 -. 060 4.221 1.988 0.863 1.339 0.080
11.12' 13.70 6.036 0.472 54.28 12.19 0.733 2.215 1.805 7.077 83.65 124.2 24.07 0.551 0.372 0.264
0.02100 0.02380 0.02025 0.Q0011 0.01021 0.10540 0.01021 0.09981 0.02079 0.05048 0.03516 0.0S236 0.02775 0.03il5
-0.00066 0.16800 0.08436 0.00651 O. 1.1399 O..00835 0.00248 0.00005 0.01337 0.10545
168823.00000 0.04192
0.02079
0.02067
0.02226
0.02149
0.01915
0.01920.
0.00011
0.00014
0.01022 ' ` 0.01020
0.09687 '
0.10174
0.01040
0.01062
,0.09862-
0.10029
0.02051
0.02107
0.05042
0.05041
0.03126
0.03909
0.04427
0.05837
0.02521
0.02826
0.03086
0.03104
-0.00058
-0.00018
0.19029
0.21455
0.08350
0.08316
0.00652
0.00627
0.11654
0.11815
0.00962 .
0.00908
0.00027 -0.00001
0.00122 0.00013
0.02058
0.02149.
O.10483
0.10599
169205.00000 167978.OOOOO
0.04171
0.04176
10
DUP050307624
I i f f `r 33
LANCASTER LABORATORIES
Ni.U "*me: 11 it' 32
9626806T61 ICSA
AVG. (ppm)
%RSD"
0.00029 25.52 530.67584 0.542
-0.00141 82-23 0.00791 0.982 0.00152 ,3.573
520.78656 0.535 0.00116 17.20
-0.00082 35.54 0.00688 1.416
-0.00220 5.759 206.64642 0.494
O.. 04599 6.450 557.00427 0.453
0.00415 1.157 -0.00068 61.80
0.26587 13.35 0.00591 5.563 0.00051 141.4 -0.00277 55.56 -0.00028 584.2 0.00021' 642.8 -0.00137 6.676 -o;00274 83.83 -0.00286 81.947 158261.00000 0.600 0.00469 2.742
09/24/96
'INSTRUMENT ID: 05473 23:29
.#1 .
-INTEGRATIONS tt 2
0.00020 533.10260
-O'. 00228 0.00794 0.00154
523.27294 0.00136
-0.00097 0.00683
-0.00210 207.70159
0.04922 559.48828 . 0.00421
-0.00032 0.28127 O:00629 0.00018
-0.00102 0.00120
-0.00135 -0.00148 -0.00450 -0.00256 7173.00000
0.00459
0.00035 527.49487
-0.00185 .0.00782
0.0015.6 517.77099
0.00117 -0.00101
0.00681 -0.00234 205.66278
0.04338 554.43414
0.00413. -0.00115
0.22527 0.00575 0.00000 -0.00393' -0.00210 O.00086 -0.00131 -0.00359 -0.00302 158924.00000 0.00484
#3 REREAD REDIG
0.00031
531.43011
. -0.00009
0.00796 ________;
0.00146
521.31573'
- 0.00096 _
-0.00048 _
0.00699
-0.00216 __________________
206:57490 __________________
0.04537
557-09039 _________________
0.00412
-0.00057
_
0.29107-
0.00570
-0.00334
0.00134
0.00003
0.00112
-0.00132
-0.00013
-0.00299
1S86S6.00000 __________ _______
0.00464
ID O
DUP050307625
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LANCASTER LABORATORIES '
Run Name: 9626806T61
T ube: 33
ICSAB-
-
09/24/96
23:34
INSTRUMENT ID: 05478
AVG
INTEGRATIONS
ELEM .
( PPm)
%RSD
#1
#2 #3, - REREAD REDIG
___Ag A1
As ;___Ba
..Be : _______Ca
Cd ___Co ___Cr
_i_Cu ___Fe ___K ___Mg ___Mn ___Mo ___Na ___Hi J___Pb . ___Sb ___Se ___Sn ___Ti ___Tl ___V
___Y ___Zn
'
0.21486 525.61828
O.10247 0.52672 0.4S300 510.84393 0.95240 0.46405 0.49380 0.54133 202.32991 0.04505 547.77459 0.49415 -0.00026 0.23238 0.95717 ' 0.05010 0.60317 0.04607 -0.00093 -0.00128 0.09747 0.50166 160215.32812 1.01058
0.380 0.438. 2.886 0.315 0.249 0.370 0.288 0.335 0.367 0.398 0.354 20.65 0.370 0.275 170.2 25,89 0.430 1.062 0.530 4.770 235.9 11.96 2.249 0.222 0.319 0.340
0.21456
0.21424
525:34515
.523.46441
0.09940
0.10531
0.52685
6.52500
0.48216
0.48245
' 509.60488
509.90307
0.95030
0.95138
0.46277
0.46360
0.49221
0.49341
0.54143
0.53912
201.90391
201.92813
0.05488
0.04388
547.10620
546.16296
0.49358 -6.00031
0.49316 -0.00068
0.22549
' 0 * 29571
0.95459
0.95499
0.05018
0.05059
0.60211
0.60064
0.04733
0.04353
0.00159
-0.00201
-0.00145
-0.00118
0.09502
0.09815
0.50185 :
0.50046
159954:00000 1.00909
160805.00000 1.00813
0.21579.
528.04534 0.10270
0.52831 0.48437
513.02380 0.95551
0.46579 0.49577
0.54344
203.15766 '0.03639
550.05456
0.49570
0.00021
0.17594 '
0.96191 0.04953
1
0.60676
0.04735 -0.00236
-0.00120 0.09925 0.50267
i59S87.00000
1.01452
104
DUP050307626
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' LANCASTER LABORATORIES
Run Name: 9626806T61
Tube: 34
CCV
. 09/24/96
. INSTRUMENT ID: 0547S 23:39
ELEM
___Ag ___Al ___As ___Ba .....Be ___C3
Cd ___Co ;___Cr ___Cu ___Fe ___K ___Mg ___Mn ___Mo ___Na ___Ni ___Pb ___Sb ___Se ___Sn ___Ti _T1 ___V
Y ___Zn
AVG (ppm)
%RSD
. #1 ..
INTEGRATIONS. #2
.#3 REREAD REDIG
0.49844 0.899
0.50360
0.49622
25.04235 0.985
25.32475
24.86749
0.50335 1.001'
0.50743
- 0.50491
0.49383 0.797
0.49837
0.49160
0.49749. 0.917
0.50237
0.49679
25.24.721 0.9S8
'25.51770
25.19831
0.49716 1.039
0.50270
0.49632
0.47270 0.997
0.47757
' 0.4723S
0.49158 0.901 , 0.49987 0.949'
0.49630 6.50533
0.49094 , 0.49668
24.05558 0.908
24.28882
. 24.02210
25.67176 1.037
25.97438
25.47349
24:78173 1.017-
25.06969 ,
24.67432
0.49477 0.864
0.49948
0.49369
0.49909 0.426 .
0.49858
0.50143
25.72161 0.995
26.00544
25.50789
0.50057 1.028
0.50651
0.49788
0.49044 0.537
0.49333
0.48982
0.45889 0.362
0.45699
0.46003
0.49393 0.478
0.49498
0.49558
0.48616 0.751
0.49035
0.48449
0.49934 0.737
0.50349
0,49806
0.49929 1.057
0.49405
0.49920
0.49621. 0.806
O,50073
0.49477
167860.00000 0.715 0.50093 0.930
166528.00000 0.50609
168190.00000 0.49969
0.49550 24.934'SO
0.49772 0.49151 0.49332 25.02563 0.49247 0.46816 0.48750 0.49761 23.85581 25.56742 24.60118 0.49113 0.49727 25.65150 0.49732 0.48817 0.45966 0.49122 0.48364 0- 49647 0.50461 0.49312 16S862.00000 0.49702
'
105
DUP050307627
Page: 36
LANCASTER LABORATORIES
Run Name: 9626806T61
Tube: 35
CC8
09/24/96
23:44
INSTRUMENT ID: 0547S
ELEM
___Al AS Ba
___Be Ca
___Cd ___Co ___Cr
Cu Fe ' K'
....Md ___Mn ___Mo
Na ___Ni ___Pb ___Sb ___Se ___Sn ___Ti ___Tl ___V ___Y ___Zn
AVG
INTEGRATIONS
( ppm)
% RSD
#1
#2
#3 REREAD RE DIG
.0.00014 0.07520
-0.00106 . 0.00005
0.00015 0.13536 0.00021 -0.00023 -0.00001 -0.00106 0.05569 0.05504 0.07452 0.00004 0.00033 0.17263 -0.00028 0.00076 O.00153 0.00073 0.00000 0.00005 -0.00198 0.00031 169146.32812 0.00016
198.2 7.872 210.7 108.0 69.38 5.153 6.771 120.1 1193. 25.99 20.38 li .51
10.25. 52.12 81.78 11.25 7.541 49.67 70.64 64.49 32186 89.45 178.0 89.27 0.230 22.33
' 0.00047
0.07704 -0.00108
0.00011 0.00019 0.14132 0.00020 -0.00040 0.00016 .-0.00079 O.06871 0.06229 0.08090 0.00004 0.00061 0.19491 -0.00027 0.00060 0.00216 0.00024 0.00052 0.00002 0.00061 ' 0.00060' 169560.00000 0.00011
0.00003 0.07999 -0.00328 0.00006 0.00003 0.13707 0.00022 0-00008 -0.00014 -6.00135
0.05050 0.05059 0.07662 0.00001 0.00006 0.15922 -0.00026 0.00049 0.00214 0.00118 0.00046 0.00010 -0.00600 0.00030 168786.. OOOOO 0.00018
-0.000070.06858 0.00118 0.OOOOO 0.00024 0.12769 0.00021
-0.00038 -0.00005 -0.00104
0.04787 0.05223 0.06605 0.00006 0.00033 0.16376 -0.00030 0.00120 0.00028 0.00077 -0.00098 0.00003 -0.00055 0.00004 169093.00000 0.00018
A Data Reviewed by: WO\|zM5 0-35Aio
Data verified by: Q a 1--
Q-Q5.qU
' 106
DUP050307628
Paae: .Data Reviewed Bv:
.ancaster Laboratories
Q/q c >
Data Verified Bv:
Analvst:
142
q-an-qc*
Data File Name:
27001T61.DA
Run Name: 9627001T6I
Instrument Parameters:
Rinse Time: Individual Integration Time: Total Integration Time:
60 sec 10 sec 30 sec
Element- Symbol
Element Name
Wavelength(nm)
Ag A A1
Silver.' Aluminum
328.06 308.21
.
As
A rsenic
189.04
Ba
Barium
493.40
Be
Beryllium
313.-04
Ca
Calcium
317.93
Cd - Cadmium
226.50
Co A
Cr '
Cobalt Chromium
228.6.1 267.71
C-u CooDer 324.75
Fe I ron
271.44
K
Potassi urn
7fo6.49
Mg
Magnesi urn
279.07
Mn
Manganese
257.6.1
Mo
Molybdenum
'202.03
Na
Sodium
330.23
Ni Hieke 1 231.60
Pb Pb Sfo
A Sb Se Se Sn Ti `
l. ead t ead Antimony Antimony Selenium Selenium T in Ti tan.ium
220.35/1 220.35/2 206.S3/1 206.83/2 196.02/1 196.02/2 189.9S 334.94
T1
T haljium
190.86
V
Vanadium
292.40
Y
Yttrium
, 371.03
Z n 7. i nc
215.85 '
10 t;
DU PO50307629
lnW ***HtV-i&iniitlf .: l-vi-Lfe,... J' ' 2W|I|W'I;?'*1-V-. - y
&i
The c.) t i Ph i' t TCP i.t ;. r:h. a C- i' aw f o id-Kcnse ! i;i.-> i i Nii-i si- F(r< c. '.. i i
Tscnm o<le t o i" iead . < ;.nl j mony . 6no ss ) en) im .
i hio i <. iu j r n- : ii>? u '. . .: i ... . ;
ot t he* f j rat. and second o r u e i wave! engt. ns in it it c ca.icuj.ai j c mi q T o .j .c h o . t. i iti-th
ine tal daterminatians. Tn e> t E TRACE ICP a iso uti i i zes- V t i r i urn as an i nterna]
T> W
tandard to compensate for f j uct.uat.ions in nebu.1 isation and d 3 asma condition!.
11 Yttrium readings are expressed in counts.
Page: 2
LANCASTER LABORATORIES
Run Name: 9627001T61
INSTRUM ENT ID: 0547
Tube: 1
SO
09/26/96 '
00:47
ELEM
CONC ( ppm )
AVG INTENSITY .
RATIO.
%RSD
#1 '
INTEGRATIONS #2
#3
___Ag ___Al ___As ___Ba ___Se ___Ca ___Cd ___Co ___Cr ___Cu ___Fe
K ___Mg ___Mn ___Mo ___Na ___Ni ___Pb ___Sb ___Se ___Sn ___Ti ___Tl ___V ___Y ___Zn
0.000 0.000 0.000 - 0.000 0.000 OiOOO 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.'OOO 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000
N/A 0.000
-0.00055 0.00747
0.00027 0.00037 -0.05706 --0.00086 0.00071 -0.00040 0.00008 -0.00160 -0.00.005 0.00271 0.00005 0.00027 -0.00061 -0.00046 0.00011 0.00231 0.00009 -0.00172 -0.00015 -0.00045 -0.00121 0.00000 1-58S08.32812 -0.00005
6.815 1.537 .85.31 2.093 1.286 2.336 30.43 17.01 40.44 1.316 .21.67 6.400 109.0 15.52 59.32 49.24 33.47 37.88 585.7 32.88 39.08 5.,556 13.48 1183. 0.768 6.186
-0.00053 0.00759
0.00046 0.00038 -0.05790 -0.00086 0.00069 -0.00033 0.00004 -0.00159 -0.00004 0.00285 0.00011 0.00022 7O.00039 -0.00069 0.00015 0.00135 0.00054 -0.00214 -0.00008 -0.00044 -0.00103 -0.00009
157731.00000 -0.00005
-0.00052 0.00744 0.00034 0.00036
-0.05673 -0.00088
0.00093 -0.00047
0.00010 -0.00159 --0.00006
0.00252 0.00004 0.00027 -0.00041 -0..00046 0.00013 0.00252 0.00024 -0.00194 -0.00015 -0.00047' -0.00134 0.00001 158560.00000 -0.00005
-0.00059 0.00736 0.00001 0.00036
-0.05654 -0.00084
0.00050 -0.00039
0.00009 -0.00162 -0.00006'
0.00276 0.00000 0.00031 -0.00103 -0.00023 0.00007 0.00307 -0.00051 -0.00108 -0.00020 -0.00043 -0.00.126 - 0.00005 160134.00000 -0.00005
106
DUP050307630
Page:
LANCASTER LABORATORIES
Run Name:
Tuba
2
9627001T61
SI 5
09/26/96
00:52
INSTRUMENT ID: 0547'
ELEM
CONC (ppm.)
AVG INTENSITY
RATIO
. %RSD
#1
INTEGRATIONS . #2
#3
___Al ___Ca ___Fe
___K , ___Mg
Na ___Y
50.000 50.000 50.000 50.000 50.000 50.000
N/A
0.74450 0.79077 0.23392 1.29236 0.74804 0.11612 158188.32812
0.517 0.311 0.300 0.635 0.401 0.394 0. 143
0.74286 0.7S798 0.23317 1.29354 0.74558 0.11580 158248.00000
0.74138 0.79168 0.23402 1.28363 0.74714. . 0.11591 157937.00000
0.74866 0.79264 0.23457 1.29993 ' 0.75138 0.11664 158 380.00000
A
109
DUP050307631
page: 4
LANCASTER LABORATORIES'
Run lNlaute: Tube : 3
962 7D01T61 S2 5 .
09/26/96
00:55
INSTRUMENT ID: 0547
EL EM
CQNC (ppm)
AVG `in t e n s it y
' RATIO
%RSD
#1
INTEGRATIONS. #2
#3
___Aa ___As ___Ba
Be __Cd ___CO ___Cu ___Mn ___Ni
.Pb. ___Se ___T1 ___Y ___Zn
1.000 1.000 1.000 1-. ooo 1.000 1.000 1.000 1.000 1.000 1.000 i .oOo 1.000
N/A . 1.000
0.21662 : 0.24724 0.25137 .
4.49950 1.24150 0.24569 . 0.19565 1.01814 0.17172 0.30359 ' ' 0.12578 0.10101 158416.32812 0.09936
0.210 0.733 0.253 0.258 0.2390.277 0.202 0:211 0.268 0.591 0.376 3.438 0.370 0.174
0.2i696 0.24653 0.25227 4.49222 1.23977 0.24503 0.19595 1.01824 0.17172 0.30545 0.12632 0.. 09710 157870.00000 0.09932
0.21610 0.24588 0.25113 4.49336 1.23981 0.24565 0.19520 1.01595 0.17126 0.30187 0.12555 0.10219 159037.00000 0.09921
0.21680 0.24930 0.25220 '4.51293
1.24493 0.24639 0.19579 1.02024 .0.17219 0:30345 0.12546 0.10374. 158342.00000 0,09955
iio
DUP050307632
Page5
LANCASTER LABORATORIES
Run Name: 9627001T61
INSTRUMENT ID: 0547S
Tube: <4
SA
09/26/96
00:59
ELEM
___Or ___Mo ___Sb
Sn ___T i ___V ___Y
CONC f PDFT1 )
1.000 1.000 1.000 .1.000 1.000 1.000
N/A
AVG INTENSITY
RATIO
. %RSD
0.14023 0.42169 0.35304 0.09728 0.50048 0.14608. 1594 89.32812
1.533 2.146 3.376 1.558 1.631 1.504 0.924
.3 NTEGRATIONS 41 #2
0.13776 0.41150 0.33929 0.09553 0-49137 O.14356 161191.00000
O'. 14131
0.42479 0.36054 0.09825 0.50292 0.14709 158595.00000
443"
0.14163 0.42879 0.35929 0.09806 0.50715 0.14759 158682.00000
ill
DUP050307633
Page: o
. LANCASTER.LABORATORIES
Run Name: T ube: 5
9627O01T61 ICV
09/26/96
01:03
INSTRUMENT ID: 05478
ELEM
Aa ,___AI..
As ___8a ___Be
Ca ___Cd . ___Co ___Cr ___Cu ___Fe ___K ___Mg
Mn ___Mo ___Na ___Ni ___Pb ___Sb ___Se ___Sn ___Ti ___Tl ___V
Y Zn
AVG ( ppm )
,%RSD
#1
INTEGRATIONS #2
43 REREAD REDIG
0.65473 2.190 30.04846 2.223
0.63203. 2.737 0.62292 2.125 0.63095 2.593 30.28512 2.747 0.61944 2.588 - 0.62269 2.646 0.61512 2.635 0.63082 2.024. 30.13233 2.666 . 29.67363 1.430 30.18623 2.512 0.62608 2.488 0.62587 2.599 - 30.59942 1.776 0.62730 2.645 0.61954 2.350 0.60438 2.24 2 0.61884 2.104 0.61535 2.662 0.62577 2.362 O.62476 6.262 0.61157. 2.495 156779.32812 1.603 0.62401 2.435
0.62109 29.38157
0.61601 0.60977 0.61464 29.46532 0.60314 0.60631 .0.59965 0.61808 29.34440 . 29.26378 29.43643 0.61075 0.60919 30.09057
0.61127 0.60375 ' 0.59087 0.60457 0.59958 0.61126 0.5S03S 0.59681 159035.00000 0.60909
6.63422
0.64889
30.04573
30.71808
0.62918
0.65089
0.62274
0.63625
0.63083
0..64737
30.26113
31.12890
0.62001
0.63519
0.62250
0.63927
0.61371
0.63198
0.63074
-0.64362
30.10236
30.95025
. 29.65132 '
30.11178 '
30.16948
30.95277
0.62559
0.64190
0.62674
0.64170
30.53549
31.17221
0.62623
0.64440
0.62243
0.63243
0.60429
0.61797
0.62184- ' 0'61419
0.63010 0.63229
0.62523
0.64081
0.63965
0.65425
0.61060
0.62729
157233.00000 0.62347
154070.00000 0.63947
DUP050307634
,t' ' 7
LANCASTER LABORAlDRIES
,,,,,, Name: 9627001T61 1 to ICB
AVG (ppm)
%RSD
0.00082 32.14 0.02639 31.91 -0.00223 22.28 -0.00104 8.434 0.00030 8.767 0.09432 3.451 0.00000 1070. 0.00109 23.41 0.00010 471.9 0.00015 56.04 0.05480 15.31 0.07842 3.4210.04136 8'. 496 .0.00033 12.96-
0.00188 113.3 0.29597 18.26
0.00002 1763. -0.00128 62.03
0.00020 208.7 0.00195 77.53 0.00206 40.59 0.00050 26.49 0..00554 49.89 0.00066 40.45 159510.32812 0.201 .0.00037 18.68
09/26/96
INSTRUMENT ID:- 05473 01:07
. #1
INTEGRATIONS #2.
0.00106 0.03296
-0.00167 .-0.00095
0.00033 0.09767 ' -0.00007 0.00135 0.00013 . 0.00021 . 0.06091 0.07536 0.04541 . 0.00038-
0.00433 0.27S18 0.00047 -0.00037 0.00063 0.00309 0.00109 0.00066 0.00859 0.00044 9352.00000 0.00045
0.00053 . 0.02933 -0.00240 -0.00105 0.00028 0.09413 0.00011 0.00084 -0.00040 0.00005 - 0.04523 0.08037 0.03915
0.00032 .0.00084 0.25305 -0.00025 -6.00161 -0.00020
0.00253 0.00257 0.00041 0.00318 0.00057 159298.00000 0.00033
43 ' REREAD REDIG
0.00089
0.01689
-0.00262 _
-0.00112 ____, __ _
0.00030
0.09117' _________
-0.00001
0.00107 _____:
0.00057 _________________
- 0.00018
________
0.05827
0.07954
0.03951
. 0.00030
0.00046 _________________
0.35667 ________ _______
-0.00014
-0.00186
0.00018
0.00023
0.00250
0.00045
0.00486
0.00096
159SS1.00000____
0.00033 ________ ;
iis
DUP050307635
f/p: 7-^W '
Page: 8
LANCASTER. LABORATORIES'
Run Name: 9627001T61
Tube: 7
CRI
09/26/96
01:12
INSTRUMENT ID: 05478
ELEM
. Aq ;___A1 ___As ___8a ___Be
Cct ___Cd ___Co ___Cr ___CU
Fe ' K
___Mg Mn
___Mo Na
___Ni ___Pb ___Sb . ___Se ___Sn
Ti ___Tl ___V ___Y ___Zn
AVG (. ppm )
%RSD
0.02128 0.01640
0.01819 -0.00105
0.01035 0.08790 0.00996 0.104S9 0.01960 0.05256 0.03955 0.06015 '0.03252 0.03140 O.00029 0.20798 0.03282 0.00558 0.11325 0.01133
0.00155 0.00034 0.02207 0.10397 160292.32812 0.04147
3.188 21.82
2.055 8.128 1.797 1.500 3.499 1.630 0.744 1 .062 38.59 4.332 14.35 0.986 176.7 18.87 1.301 14.45 2.593 13.59
61.27 31.7 3 15.15 1.590 1.094 1 . 155
#1 '
0.02107 . 0.01400
0.01782 -o.ooioi
0.01035 0.08909 0.00960 0.10315 0.0.1944 0.05216 0.Q4565 0.05754 0.03529 0.03108 0.00063 0.21079 0.08161 0.00484 6.11477 0.01023 0.00091 0.00042 0.02039 0.10216 162108.00000 0.04097
INTEGRATIONS 82
#3 RREEREAD REDIG
0.02072 0.01469 0.01819 . -0.00115 0.01053 0.08813 0.00997 0.10496 0.01968 0.05232 0 .`02218 O'. 06275 0.02713 0.03144 -0.00030 O'. 16739 0.08316 0.00644 0.12056 0.01067. 0.00109 0.00022 0.02593 0.10434 160161.OOOOO 0.04152
0.02203 0.02052
0.01856 -0.00100
0.01016 0.08648 0.01030 0.10657 0.01970 . 0.05320 0.05082 0.06015 0.03515 0.03170 0.-00054 0.24577 ' 0.08369 0.00547 0.11943
0.01309 0.00264 0.00039 0.01990 0.10541 158608.. OOOOO
0.04192
`
DUP050307636
tvi/?rar 9
LANCASTER LABORATORIES
jinn Name: 9627001T61 ( i ibe : 8 ICSA
.09/26/96
01:16
INSTRUMENT ID: 0,5 47B
AVG
INTEGRATIONS
1 I-I'M
(opm)
%RSD
#1
#2
S3 REREAD REDIG
Ag ,__Ai
_As _6a ___Be _Ca
Cd ___Co
,,Cr ___Cu
,_Fe ,Jc.
'
^Mg Mn
____MO Na Ni
._Pb
,___Sb .....Be
Sn Ti T1 _V ,,__Y _7n
0.00009 570.0 520.73486 0.632
-0.00513 37.67 -0.00015 74.11
0.00198 6.071 508.92257 0.989
0.00003 527.1 0.00028 187.9
0.00873 6.655 0.00665 6.843 205.23049 0.860 0.04921 18.00 5.39.39044 0.824 0.00767 1.426 0.00067 83.07 0.21937 39.35 0:01263 2.725 0.00268 35.19
. -0.00597 33.13 0.00030 549.6 0.00049 329.6 0.01088 1.860 0.00591 19.60
-0.00127 20.86 153300.00000 0.635
0.00069 24.38
-0.00034 518.21203
-0.00694 -0.0002-5
0.00207 506.24517
0.00017 0.00000 0.00815 0.00634 204,14961 0.05781 536-. 67382 0.00761 0.00096 0.12332 0.01227 0 - 00364 -0.00467 0.00116 -0.00124 0.01073 0.00457 -0.00136 353489.00000 0.00067
-0.00003
0.00065
519.53149
524.46112
-0.00309
-0.00537
-0". 00002
-0.00019
0.00203
0.00185
505.79296
' 514.72961
-0.00016
0.00009
-0.00004
0.00083
0.00871
0.00931
O'.00643
0.00717
204.27267
207.26921
0.04010
0.04973
536.97186
544.52569
0.00759
.0-00779
0.00002
0.00102
' ' 0.24429
0.29050
0.01296
0.01265
0.00265
0.00175
-0.00826
-0.00500
' 0.00138
-0.00163
0.00200 '
0.00072
0.01081
0.01111
0.00657
0.00659
-0.00147
.-0.00097
154166.00000 ' 152245.00000
0.00087
0.00053
115
DUP050307637
Page: 10
LANCASTER LABORATORIES
Run Name: 9627001T61
Tube: 9
ICSAB
09/26/96
01:20
INSTRUMENT ID: 05473
AVG
INTEGRATIONS
ELEM r
( ppm )
%RSD
#1
- #2
#3 REREAD REDIG
:___As
1.06068 1.126
1.07323
1.05939
1.04943
___A1
517.27868 1.205
524.06158
515.97546
511.79901 ________ ;
___As
-0.00465 12.81
-0.00396
-O.0O498
-0.00501
___Ba
0.50306 1.066
0.50876
0.50229
0.49811 ________ .
___Be
0.47247 0.862
. 0.47633
0.47287
0.46822 __________________
Ca
. 505.51239 1.139
510.81079
506.34378
499.38259
___Cd .
0.92054 1.016
0.92990
0.92053
0.91119
1
___Co
0.47566 1.164
0.48112
0.47582
0.47005
___Cr
0.47607 0.967
0.48042
0.47654
0,47125 ______ ___________
___Cu
0.54039 1.159
0.54722
O;53905
0.53491 __
___Fe
203.29870 1.113
205.48196-
203.45169
200.96246
'
___K
0.05761 8.651
0.05897
0.06178-
0.05209
___Mg .
535.33935 1.075
541.13586
535.26275
. 529.61944
___Mn.
0.49012 1.033
0.49508
0.49034
. 0.48496
'
___Mo
0.00036 178.2
-0.00008
0.00111
0.00006 _
A
___Na ___Ni
0.22551 33.47 0.93547 1.156
0.1557.4.' 0.94618
0.30566 0.93569
0.21515 ________. 0.92455
___Pb
0.96702 0.723
0.97000
0.97203
0.95903
___Sb
-0.00668 35.65
-0.00397
-0.00845
-0.00762
___Se
0.00017 1226 .
-0.00129
-0.00085
0.00268. __
___Sn
0.00132 296.3
0.00559
-0,00209
0.00046 :'
___T i
0.01104 2.102
0.01116
.0.01118
0.01077
___T1 ___V ___Y ___Zn
0.00112 0.48530
153983.32812 0.97211
528.3 1.153 0.802 1 .104
0.00091 0.49114 .52722.00000 0.98273
0.00718 0.48479 154052.00000 0.97234
-0.00471 0.47998 _________________ 155191.00000 0.96126 _
116
DUP050307638
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LANCASTER LABORATORIES
Run Name: 9627001T61
T ube: 10
ccv
09/26/96
01:25
INSTRUMENT ID: 05478
E.LEM
AVG (. ppm.)
%RSD
#1
.INTEGRATIONS #2
#3-
REREAD REDIG
___Ag
0.52040 1.118
0.52365
0.52388
0.51368
___AI
25.92S06 1.375 .
26.11571
26.15173
25.51675
___As
0.51598 1.559
0.51892
0.52215
0.50688
___Ba
0.50780 1.217
0.51089
0.51183
0.50068
____8e
0.51245 1.149
0.51640
0.51527
0.50568
___Ca
26.10304 1.351
26.37229
26.23324
25.70359
___Cd
0.50939 11262
0.51432
.0.51173
.0.50212
___Co
0.51179 1.179
0.51551
0.51504'
0.50483
___Cr.
0.50126 1.109
0.50494
0.50399
0.494-86
___Cu
0.52413 1 . 184
0.52662'
0.52871
0.51707
' Fe
25.51128 1.326
25.71233
25.70081
25.12070
K
25.83.683 1 . 161
' 25.97335
26.04434
25.49280
___Mg
25.S6053 1.331
26.08057.
26.03691
25.46350 '
A ___Mn ___Mo
0.51503. 1.175 0.51022 0.930
0.51897 0.51190
0.51806 0.51391,
0.50806 ' 0.504S7 .
___Na
26.36300 0.925
.26.50925
26.49827
26.08149
Ni____Pb
0.5.1010 1 . 169 0.50798 0.768
0.51466 0.51086
0.51229 0.50954
0.50335 0.50354
___Sb
0.. 49749 0.456
0.49681
0.50003
0.49564
___Se
O.50103 0.830
0;49963
0-. 50571
0.49775
___Sn
0.50678 0.851
0.50781
0.51050
0.50205
___Ti
0.51401 1 . 156
0.51734
0.51754
0.50714
_J1
0.50842 3.680
0.4 8693. .
0.52113
0.51720
___V ___Y ___Zn
0.50651 1.242 157151.00000 0.339
0.51414 1 . 100
0.51082 1561.51.00000
0.51.740
Q.50942 156656.00000
0.51740
0.49929 158646.00000
0.50760
A
DUP050307639
Page: 12
LANCASTER LABORATORIES
Run Name: 9627001T61
T ube': 11
CCB
09/26/96
01:29
INSTRUMENT ID: 05478
ELEM
Aa _A1
As Ba ___.Be Ca Cd Co ___C.r ' ___Cu ___Fe K .. ___Mg ___Mn ___Mo _j__Na Ni ___Pb ___Sb ___Se ___Sn ___Ti . ___Tl ,__V ___Y - Zn
AVG
INTEGRATIONS
(ppm) -
%RSD
*fl
#2 .
#3 REREAD REDIG
0.00070 0.. 06.780
-0.00178 -0.00110
0.00038 0.14708 0.00000 1 0.00076 -0.00015 0.00055
o;06285 0.06i24
' 0-. 08923 0.00027 0.00143 0.29879
-0.00015 -0.00043
0.00073 -0.00030
0.00177 0.00037 0.00359 O-. 00066 160966.67187 0.00029
64.39' 13.26 156.6 9.323 21.11 6.661 3776. 93.41 339.6 67.06 29.64 7.793 11.79 32.01 133.2 53.93 541.2 190.8 85.43 244.2 27.95 68.05 227.9 98.71 1.111 32.96
0.00123 0.07348
0.00143 -0.00098
0.00046 0.15630 0.00006 0.00156 -0.00044 0.00098 0.08236 0.06011 0.09882 0.00034 v. 0 - 0036-2 0.28893
. -o.ooooi
. -0.00118 0.00006
-0.00035 0.001920.00066 0.01281 0.00086
162919.00000 0.00039
0;00042
0.00046
0.07249
0.05743
-0.00357
-0.-00322
-0.00115
-0.00118
0.00030
0.00039
0.14814 .
0.13679
-0.00021
0.00017
0.00018
0.00054
-0.00053
0.00052
0.00028 .
- 0.00040
0.06095
0.04524
0.05713
0.06648
0.09089
0.07797
. 0.00017
0.00030
0.00059
0 .-00008
0.14279
0: 46466
-0.00106
0.00060
-0.00059
0.00046
0.00082 ^
0.00130
0.00046
-0.00102
0.00122
0.00218
0.00022
0.00022
0.00080
--0.00283
-0.00006
0.00120
159404.00000 160577.00000
0.00027
0.00020
118
DUP050307640
r f>: 13
LANCASTER LABORATORIES
|,nn Name: 9627001T61.
,,/fje: 12
2583209 "BP'S 3 0
,!#* *, 100-100,DF10,962685720001. 8 > ,
09/26/96
01:34
INSTRUMENT ID:
r 1 <:M
J*9 ,A1 /^s Ha .. ^0 Jja ; Cd (-a ' f-: r _jCu '
Fe ,K ...Mg jMn Jio
f _Ni
Pto ,.st>
Se n
Ti .... T1 _V ..J ..... ^ n '
. AVG (. ppm)
%RSD
#1
0.00037 126.0 0.06234 8.608
-0.00222 25.16 ' 0.01432 1.423 0.00007 140.9 6.72471 1.432 0.00005 361.9 0.00030 238.9
' -0.00006 578.1
0.00032 72.50 0.08641 9.087 0.29910 0.932 2.79713 1.245 0.07850 1.275 0.00030 82.69 5.13857 1.567 0.00072 77.14. 0.00166 22.^7 0.00239 33.84 0.00000 1.3671 0.00133 117.0 -0.00004 196.9 -0.00553 25.44 0.00054 55.79 15S63S.67187 0.442 0.00463 4.701
-0.00011 0.05873
-0.00286 0.01409 0.00015 6.62229
'-0.00016 -0.00019 -0.00032 0.00005 0.08056 0.29588 2.75829
0.07742 '0.00003
5.10242 0.00036 0.00189 0.00314 0.00127 -0.00032 -0.00012 -0.00467 0.. 00036 159352.00000 0.00438
INTEGRATIONS tt2
#3 REREAD REDIG
0.! 00042
0.00081
0.06851
0.05979
-0.00184 -
-0.00195
0.01439
0.01448 .
0.00013
-0.00004
6.73843
6.81342
0.00009
0.00022
-0.00002
0.00114
-0.00022
0.00035
0.00040
0.00049
0.08334
0.09534
' 0.30081
0.30060
2.80752
2.82559
0.07868
0.07939
0.00053 5.08244'
0.00036 5.23036
0.00044-
0.00137
0.00187 0.00252 -0.00008
0.00123 0..00153 -0.00119
0.00154
0.00278
-0.00004
0.00004
-0.00715
-0.00476
0.00037
0.00089
158615.00000 157949.00000
0.00471
0.00479
-
11 &
DUP050307641
page: 14
LANCASTER LABORATORIES
Run Name: 9627001T61
Tube: 13 2583209 15>P*S3Dft .
UP**,100-100,DF10,962685720001.8,,
09/26/96
01:38
INSTRUMENT ID:
05478
EL EM
_Ag ___Al ___As `___Ba ___Be
Ca ___Cd ___Co
Or \ ___Cu ___Fe . ___K' ___Mg ___Mn ___Mo ___Na ___Ni
- Pb ___Sb ___Se ___Sn ___Ti ___Tl ___V ___Y ___Zn
AVG (ppm)
%RSD
#1 '
INTEGRATIONS #2
#3
REREAD REDIG
0.02108 1.038 0.47474 3.683 0.01732 .9-106 0.43503 0.772 0.01012 1.403 7.72682 0.555 0.01011 0.549, 0 i. 10375 1.043 0.02039 1.901
0:05281 0.484 0.26627 3.767 . 2.18034 0.589 3.78194 0.815 0.10962 0.550 0.19756 0.135. 7.24628 1.176 0.08303 1.263 0.01168 7.229 0.10774 0.209 0.00986 7.704 0.55275 0.684 0.10397 0.656 0.01504 12.43 0.10259 0.435 158222.67187 0.806 0.04281 0.415
0.02128 0.49480 0.01782 0.43811 0.00996 - 7.76613 0.01007 0.10463 0.02079 0.05310 0.27750 2.19459 3.81299 0.11013 Q.19776 . 7.34373 0.08373 0.01265 . 0.10798 0.00956 0.55659 0.10447 0.01720 0.10299 156815.00000 0.04295
0.02085
0.02111' _______________ __ ____________
. 0.46668
0.46273
0.01`858 .
0.01555 ________'
0.43144
0.43553
0.01013
0.01025 _
7.68097
7.73335 _
. 0.01017
0.01009 _
0.10254
O.10407 ________
0.02037.
0.02002 _
, 0.05262 .0.25819 V
0.05270 __ ' 0.26312
2.16961
2.17682 ;
3.75129
3.78155 ______:
0.10895:
0.10978 ___________________
0.19765 7.20959
0.19725 7.18552 .
0.08182 0.01128 0.10753 .
0.08354 __ 0.01112L 0.10773
0.00930
0.01072
________________
0.54902 O.10319 0.01399 O.10211'
0.55265 O.-10425 0.01393 0.1O26S
159302.00000 158551.00000
0.04261
0.042S6 _________
120
DUP050307642
11 gs: 15
LANCASTER LABORATORIES
|/nn Name,: 9627001T61
U,fc/e: 14 2583209
3D D
|,t**, 100-100 ,.DF10,962685720001 ,8, ,
09/26/96
01:43
,
INSTRUMENT
If EM
Ag A1 As 8a _8e Ca __Cd Co Cr Cu __Fe K ___Mg Mn Wa /_Na _Ni ...Pb ___Sb __Se Sn Ti __T1 ___V __Y ._Zr>
AVG
INTEGRATIONS
(ppm)
%RSD
ttl
#2
#3 R
0.00046 64.07
0.03533 11.28 -0.00251 35.67
0.01411 1.263 0.00001 2019. 6.S9697 0.8S5 -0.00014 16.56
0.00011 474.0 -0.00032 146.6
-0.00001 1009.' 0.06401 13.78 0.28615 3.418 2.71967 0.860' 0.07878 O.. 76,9 0.00049 38.37 5.08536 1.854 0.00158 63.92 0.00098 38.97 0.00195 23.11 0.00090 114.7 0.00140 59.61 0.00008 250.0
-0.00685 23.30 0.00042 31.83
159576.67187 0.795 0.01279 0.960
0.00079
0.00022
0.00037
0.03992
0.03282
0.03323
-0.00036
-0.00468
-0.00250
0.01431 ' .
0.01396 '
0.01406
-0.00024
0.00017
0.00010
6.63222
6.52957
6.62913
-0.00013
-0.00017
-0.00013
0.00042
^0 00053 j
0.00046-
'-0.00036
-0.00076
0.00017
0.00013
-0.00002
-0.00016
0.07417
0.05823
0.05962
` 0.28851
0.27540
0.29454
2.73848
2.69347
2:72706
0.07907
0.07808
0.07918
0.00069
0.00048
0.00031
5.09780
4.98543
5.172S4
0.00158
0.00057
0.00259
0.00118
0.00054
0.00123
0.00247
0.00173
0.00165
0.00090
-0.00013
0.00192
0.00167
0.00046
'0.00206
0.00029
-0.00010
0.00004
-0.00527
-0.00846
-0.00682
0.00045
0.00027
0.00053
158407.00000 1609 27.00000 159396.00000
0.01284
0.01265
0.01239
0547S REDIG
I2i
DUP050307643
Page: 16
LANCASTER LABORATORIES
Run Name: 9627O01T61
Tube: 15
D?:53D3 2583209
R*** , 100- 100,DF10,962685720001,>8, ,
09/2 6/96 ' ' 01:47
INSTRUMENT ID: 0547S .;
AVG
, INTEGRATIONS
ELEM
(ppm)
%RSD
#i
#2
S3 REREAD REDIG
___Ag
0.00562 9.649'
0.00554
0.00620
Al
0.23305 1.458
0.23400
- 0.23588
As
0.00204 49.05
0.00115
0.0Q313
8a
0.21744 0.449
0.21823
0.21774
' Be .
0.00494 2.731
0.00489
0.00484
Ca
7.04566 0.446
7.07729
'7.04531
Cd
0.00485 1 :465
0.00480
0.00493
Co
0.05081 1.498 .
0.05094
-0.05150
....Cr , .
0.02026 1.643 .
0.01991
0.02057
. Cu
0.02566 1.071
0.02557
-.0.02597
___Fef
0.16686 4.454 '
0.16834
. 0.17345
___K
0.63205 1.213 '
0.63763
0.63521
___Mg
2.91947 0.557
2.93235
2.92489
___Mn .
0.12851 0.480
0.12905
0.12364
JAo
0.20252 0.449
0.20151
0.20327
Na
5.50877 0.839
5.50913
5.55484
___Ni
0.05210 1.062
0.05247
0.05238
Pb
0.00252 19.40
0.00305
0.00243
___Sb
0.05121 3.545
0.05091
0.04956
___Se
0.00127 77.37
0.00237
0.00095
___Sn
0.41475 0.808
0.4154S
0.41769
___Ti
0.10293 0.416
0.10319
0.10316
___Tl
-0.00251 81.38
-0.00479
-0.00086
___V
0.05096 1.202
0.05086
0.05161
___Y
158951.32812 0.746 157604.00000 159408.00000
___Zn
0.05261 0.441
0.05276 .
0.05273
0.00512 O'. 22928 0.00185 0.21635 0.00510 . 7.01439 0.00482 0.04999 0.02029 0.02545 0.15880 0.62330 2'. 90118 0.12784 0.20278 5.46233 0.05147 0.00209 0.05316 0.00048 0.41110 0.10244 -0.00186 0.05040 159842.00000 0.05235
DUP050307644
I 17
LANCASTER LABORATORIES
ttlf\ Name: 9627001T61
8BS3DL
1 iiDe: 16
2583209'
Ml 100-100,DF50,,962685720001, 8, ,
t 1 EM
AVG (ppm)
%R5D
#1
09/26/96 .
01:51
-
INTEGRATIONS
' #2.
INSTRUMENT ID: 05478 #3 1REREAD REDIG
,A9
-0.00003 899.9
0.00027
-0.00025
-0.00011
,A1
0.02442 9.796
0.02185
0.02432
0.02659
As
-0.00239 19.80
-0.00284
-0.00189
-0.00245
Ba
0.00187 3.905
0.00194
,0.00179
0.00167
Be
0.00012 29.44
0.00009
0.00016
0.00012
Ca
1.39663 0.429
1.39577
i.39111
1 .,40302
^Cd
-0.00032 32 ..46
-0.00022
-0.00031
-0.00043
Co
-0.00024 65.83
-0.00010 '
-.0.00041
-0.00021
fir
-0.00053 24.94
-0.00040
-0.00053
-0.00067
'_Cu
-0.00030 '65.86
-0.00003
-0.00047 .
-0.00037
___Fe
0.04571 5.933 .
0.04788
0.04658
0.04267
K
0.10435 7.356
0.10868
0.09548
0.10888
,_jig
0.56896 0.045
0.56893
0.56872
0.56923
Mn
0.01557 0.411
0.01555:-
0.01551
0.01564
_Mo
-0.00018 175.3
-0.00040
.-O.00033
0.00018
A ..Na
1.07943 1.552
1.09755
1.07683
1.06412
,.Ni
0.00010 652.6
-0.00066
0.00061
0.00035
Pb
0.00163 33.98
0.00218
0.001-65
0.00107
i___Sb
0.00180 48.88
0.00135
0.00124
0.00282
_Se
0.00048**200.4
0 .'00145
0.00048
- -0.00048
Sn
0.00146 98.63
0.00206
-0.00018
0.00250
Ti
-0.00008 157.4
0.00007
-0.00017
-0.00017
,,T1 V
,y ___l n
-0.00451 0.00005
159813.32812 0.00357
9.509 221.7 0.369 2.762
-0.00432 0.00005
159131.00000 0.00361
-0.00500 -0.00007 160169.00000
0.00365
-0.00421 0.00018
160140.00000 0.00346
1 2-5
DUP050307645
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LANCASTER LABORATORIES
Run Name: 9627001T61
Tube: 17
2583206
AP
**** , 100-100, DFIO,96268572-0001,8 ,
09/26/96
01-56
. INSTRUMENT ID:
05478
.*
ELEM
Ag' Al.' As Ba Be Ca Cd Co , Cr Cu Fe K Ma Mn , Mo
2lNa
Ni Pb ___Sb " Se Sn ___Ti T1 V Y ___Zn
AVG (ppm)
%RSD
#1 `
INTEGRATIONS #2
. #3
REREAD REDIG
0.00061 48.94 0.05056 5.629. -0.00227 56.34 0.00447 1.461 0.00008 84.49 20.32574 0.937 -0.00017 69.40 0.00092 13.69 ' -0.00039 64.70 -0.00032 41.24 0.15149 7.375 0.38120 1.230 7..94437 0.826 0.06888 0.835 -0.00031 53.28 . 6.. 17558 1.115 0.00108 28.72 0.00112 38.27 0.00054 94.14 -O'. 00002 3900 . 0.00052 149.0 0.00066 3 8.07 -0.00403 34.20 0.00049 39.4 0 160219.32812 0.618 O - 0 0 7t 5 6 2.448
0.00029 . 0.05221 -0.00197 0.00444 0.00008 20.27176 -0.00023 0.00079 -0.00067 -0.00023 0.14047 0.37770 7.93246 0.06874 -0.00023 '6.14912 0.00076 0.00150 0.00045 -0.00090 0.00109 0 - 00056. -0.00505 0.00029 159774.00000 0.00251
' 0.00088 0.04723
-0.00116 . O . 00443
0,00015 . 20'. 16794 -0.00024 '
0.00092 -0.00032 ' -0.00025- .0.15119
0.37937 7.88546 0.06839 -0.00050 6 12303 0.00111 0.00122 0.00109 0.00112 . -0.00036 0.00064 ; - -0.00246 0.00051 161355.00000 . 0.00255
0.00066 0.05220 -0.00367 0.00455 0.00001 20.53752 -O'. 00003 0.00104 -0.00018 -0.00047 0.16281 0.38653 8.01519 0.06952 -0.00020 6.25380 0.00138 0.00065 0.00008 -0.00029 0.00083 0.00080 -0.00459 0.00069 159529.00000 0.00263
1O frj /
DUP050307646
l^ge: 19
LANCASTER LABORATORIES
1 f/un Name: 96270QIT61
INSTRUMENT ID: 05478
1 utoe:
18
2583207
DP
+ ** , 100-100.DF10,962685720001 , 8, ,
09/26/96
02:00
AVG
INTEGRATIONS
l-.LEM
(ppm)
%RSD
#1
#2
#3 R
Ag ___A1 '__As ,
Ba _Be
Ca Z_-Cd
__Co Cr Cu
",,fe
K '___Mg
;__,Mn Mo
5CNa
___Ni' Pb
___Sb ,._Se
Sn Ti ___Tl V .___V ^__Zn
0.00030 14.47
0.00027
0.00028
O'. 10143 14.59
0.11056
0.10937
. -0.00244 33.51
-0.00245
-0.00325-
0.00540 3.015
0.00545
0,00553
-0.00016 212.8
-0.00036 -
-0.00036
19.90632 2.405
20.01983
20,31830
-0.00015 74.79
-0.00023
-0.00009
0,00056 47.75
0.00060
0.00027
-0.00003 133.4
-0.00016
-0.00011
0.00011 102.0
0.00015.
. -0.00001
0.23043 1 . 169
0.23147
0.23245
0.40598 2.875
0.40101
0.41932
7.79379 2.477' ' 0.07100 2.415
7.84697 0.07147
7.95470 0'07244
-0.00065 82.22
. -0.00056
-0.00124
6.35961 1.023
6.3238S
6.43473
0.00130 115.3
. 0.00266
-0.00031
0.00156 59.48
0.00263
. 0.00091
0.00155 134.7
-0.00046
0.00370
0.00059 14 3.1
0.00069
0.00137
0.00212 23.64
0.00194
0.00174
0.00180 12.47
0.00197
0.00155
-0.00342 89.19
-0.00652
-0.00331
0.00073 43.99
0.00064
0.00046
. 156045.67187 2.323 154371.00000 153560.00000
0.00270 5.338
0.00256
0.00285
0.00035 0.08434 -0.00161 0.00522 0.00024 19.38083' -0.00007 0.00081 0.00004 - 0.00019. 0.22737 0.39762 7.57970 0.069.10 -0.00016 6.32021 0.00156. 0.00115 0.00141 -0.00029 . 0.00269 0.00189 -0.00042 0.00108 160206.00000 0.00268
REDIG
1 (J
DUP050307647
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LANCASTER LABORATORIES
Run Name: 9627001T61 '
.
Tube: 19
2583823 "
T>
100-100,DF10,962685720001,8, , .
09/26/96
. INSTRUMENT ID: 05478 02:05
ELEM
AVG (ppm).
%RSD
#1
INTEGRATIONS #2
' #3
REREAD REDIG
__Ag ___A1
As Ba 8S Ca' ;___Cd " Co Cr ___Cu ___Fe
___K ___Mg ___Mn ___Mo
Na ___Ni
Pb ___Sb ___Se ___Sn ___Ti ___Tl
V ___Y ___Zn
' ' 0.00070 50.30 0.01699: 62. 15
-0.00220 60.20 0.01059 2.734
' 0.00008 351.0 7.26962 2.188
-0.00016 61.40 0.00070' 98-. 76
-0.00019 114.4 0.00007 222.0
0.08658 12.19 0.51855 3.098 2.97514 2.294 .. 0.02539 2.532 -0.00014 434.5 4.99208 2.448 0.00047 117.5 0.00114 45'. 10 0.00204 48.46 0.00065 183.2 O.00199 26.07 0.00000 2360. -0.00292 69.19 0.00058 31.51 159766.32812 '2.176 0.01316 2.690
0.00072
0.00105
0,02870
0.01407
-0.00072
-0.:00261
0.01092 .
0.01046
-0.00023
0.00014
7.45315
7.17167
-0.00004
-0.00022
0.00025
0.00151
-0.00007
-0.00005
-0.00003
0.00027
0.08934
0.09550
0.53333
0.52088
3.05394
2.93718
0.02613
. Q.02507
-0.00048
-0.00054
5.12400
4.96963
0.00091
. 0.00067
0.00084 0.00286
0.00174 0.00232
-Q.00043
0.00045
0.00154
0.00256
0.00000
0.00014
-0.00379
-0.00061
0.00077
0.00057
155752.00000 161831.00000
0.01357
0.01301
0.00034 0.00819 -0.00328. 0.01039 0.00034 7.-18403 -0.00022 0.00035 -0.00045 -0.00001 0.074920.50145 2.93431 ' 0.02497 0.00059 4.88260 OF <5 -0-. 00015 0.00085 0.00094 0.00195 0.00186 -0.00017 --0.00436 0.00040 161716.00000 0.01290
DUP05 0307648
i-vKie: 21
LANOAS TER LA'BORATORTES
OI <N O
C
-C
i-Min Name: 9627001T61
2583824 100, DF.10.96^685720001.8, .
09/26/96
02:09
INSTRUMENT`TD: 054 7E
!: 1 f H
....f-Vj
A1
..
___i,i a _ jle
i :a ......cel __CD
:r CU ......I- e K pin ___Mn ___NO ^ Na
.. .Hi eh
_'.h
_.
_ cn
... i ' ii \j \
...n
AVG
INTEGRATIONS
( ppm >
%RSD
#1
42
#3 REREAD REDIG
0.00023 373.8 '
0.00000
0.03443 10.49
0.03144
-0.00215 52.73
-0.00263
0.00642 1.537
0.00639
0.00015 94.89
0.00020
19.11459 0.677
19.03349
-0.00018 82.17
-0.00007
-0.00003 2607.
-0.00042
-0.00043 162.5 .0.00034 97; id
-0.00009 0.00039
0.08355 16.08
0.07790
0.42207 1.957 7.68192 0.526
0.42868 7.64108
0.06761 0.644
0.06733
-0.000*1 97.25
-0.00072
6 - 00928 1.871
5.93643
0.00117 58.34
0.00109
'0.00043 143.0
0.0Q083
0.00236 44.95
0.00340
0.00185 27.11
0.00127
0 .. 00088 1 16.7
0.00013
0.00066. 57.81
0.00051
-0.00536 18.98
-0.00641
' 0.00014 386.9
0.. 00006
1.59799.67187 0.404 ' 0.00172 2.079
159685.00000 0.00170 .
-0.00050 0.03845
-0.00296 0.00635
' 0.00027
19.04625 -0.00034 ` -0.00067 -0.001.25 -0.00001
0.07387 0.41281 7.68272 0.06739 -0.00115 5.95263 ' 0.00053 0.00076 0.00127 0.00220 0.00045 0.00037 -0.00528. -0.00036 160495.00000 0.00169
0.00120 0.03339 -0.00085 0.00653 -0.00001 19.26402 -0.00012 0.00099 . 0.00003 0.00065 0.09890 0.42473 7.72197 . 0.06812 0.00002 6.13878 . 0.00190 -0.00028 0.00243 0.00208 0.00206 0-. 00110 -0.00438 0.00071 159219.00000 0.00176
DU P050307649
Page: 22
LANCASTER LABORATORIES
Run Name: 9627001T61
Tube: 21
CCV
09/26/96 \
02:14
INSTRUMENT ID: 05478 .
ELEN
Aq ___Al' '
AsBa ^Be Ca . Cd ___Co ' Cr. ___Cu_Fe . k. ___Mg ___Mn ___Mo ___Na ___Ni ___Pb -___Sb ___Se ___Sn ___Ti ___Tl ___V . _Y ___Zn
. AVG (ppm)
%RSD
'41
INTEGRATIONS 42
43 REREAD REDIG
, 0.51487 0.549 25.45551 0.285 0.51076 0.885 0.50183 0.564 0.50865 0.919 25.69828 0.878 0.50460 0.766 0.50798 0.836 0.49847 1.063 0.51812 0.335 25.31158' 0.912 25.53759 0.412 25.38333 0.607 0.51004 0.798. 0.50568 1.339 26.10069 0.337 0.50586 0.620 0.50425 1.005 0.49521 1.149 0.49741 1.263 0.50087 0.961 O.50366 0.726 0.50598 3.471 0.50299 0.874
158915.32812 0.724 0.50957 0.685
0.51168 25.40457
0.50810 0.49884 0.50325 25.43749 0.50013 0.50311 0.49235 0.51644 -25.04565 25.59648 25.20604 0.50534 .0.49796 26.00108 0.50235 0.49840 . 0.48873 0.49017 0.49534 0.50445 0.48592 0.49796 160238.00000 0.50554 .
0.51708 25.53877
0.51598 0.50447 0.51150 25.82464 0.50668 0.51098 0.50137 0.51991 25.46159 25.60020 25.48574 0.51256 0.51064'' 26.13267 0.50340 0.50747 0.49749 0.50137 0.50415 0.51139 0.51864 0.50612 158369.00000 O'. 51168
0.51585 ' - 25.42320
0.50819 0.50219 0.51119 . 25.83271 0.50698 0 ..50983 0.50170 0.51802 . - 25.42750 ' 25.41607 . 25.45820 0.51223 0.50843 ' 26.16331 0.50682 0.50687 0.49941 0.50070 .0.50313 0.51013 ,0.51337 0.50489 158139.00000 0.51150
128
DUP050307650
23
LANCASTER LABORATORIES
,,|jn Name: 9627001T61
1 ufoe
22 CCS
09/26/96
02:18
INSTRUMENT ID: 05478
l i tM
AO AJ As 6a Be "~C2H Cd Co .Cr Cu __Fo __K '
Jin MO Na Hi _pb __st> __se Sn ,._T i Tl i._V y __l n
l
AVS
*
(ppm)
%RSD
#1
INTEGRATIONS #2
#3 " REREAD REDIG
0.00022 22 '.4S .0.01230 16.42 -0.00185 73.63 -0.00113, 5.458 0.00033 22.11 0.09421 3.512 -0.0001-7 20.80 0.00075 30.88 -0.00065 63.43 0.00063 37.27 . 0.03959 16..88 G-. 06935 20.10
0.03772 10.12 0.00021 24.96 0.00160 24.41 0.23035 18.70 -0.00077 109.4 -0.00079 22.03 ' 0.00195 35.75 0.00106 332.1 0.00214 37.45 0.00031 21.52 0.00563 52.31 0.00032 147.0 159603.67187 0.' 452 0.00021 62. J 5
0.00026 0.01391 -0.00042 -0.00108 0.00041 0.09789 -0.00020 .0.00090 .-0.00053 0.00077 0.04135 0.080100.04195 0.00024 0.00190 0.20469 -0.00153 -0.00090 0.00275 0.00412 0.00122 O.00035 0.00678 0.00014 160294'; 00000 0.00034
0.00024 0.01003 -0.00199 -0.00112 0.00032 0.09323 -0.00013 0.00048 -0.00031 0.00076 0.04522 " 0.07435 0.03668 0.00024 0.00175 0.28009 0.00014 -0.00059 0.00143 0.00184 0.00271 0.00036 0.00784 0.00087 158852.00000 0.00007
.0.00016 .0.01296 -0.00314 -0.00120 . 0.00026 0.09150 -0.00019
0.00087 -0.00111
0.00036 0.03220 0.05360 0.03453 0.00015 0.00116 0.20626 -0.00095 -0.00090 0.00167 -0.00279 0.00251 0.00023 O.0022S -0.00003 159665.00000 0.00021
. .
129
DUP050307651
Page: 24
LANCASTER LABORATORIES
Run . Name: ' 9627001T61
Tube: 23
CRI
09/26/96
~ 02:22
INSTRUMENT ID: 054 it
ELEM.-
Ag A1 As _Ba' [Be _ca _Cd _Co . ~Cr "cu _Fe Ik _Mg _Mrv _Mo _Na ,,Ni __Pb
Sb
Ti
T1 V Y Zn
AVG (ppm) '
%RSD
.0.02162. 1.440 0.01036 48.57
0.01875 7.946 -0.00112 2.122
0.01038 1.271 0.09115 1.190 0.00982 2.162 0.10666 0.656 0.01999 1.276 0.05352 0.281 0.04076 14.50 0.05672 21.08
0.03334 4.313 0.03157 0.418 -0.00011 344.7 0.20442 7.970 0.08268 0.894 0.00466 10.12
0^. .11955 1.043
0.01128 13.20 0.00169 52.16
#1
0.02194 0.01605 . 0.01830 -0.00110 0.01025 0.09240 0.00976 0.10680 0.02000 0.05369 0.04690 0.05150 0.03472
O.03161 -0.00046
0.20090 0.08350 0.00415 0.11951
in t eg r at io n s
#2
0.02131 0.00854 0.02042
-0.00112
0.01037 0.09054 0.00964 0.10590 0.01973 0.05346 0.03510 0.04825'
0.03344 0.03142 -0.00016 0.19018 0.08206 0.00476 O:12083
0.00977 0.00264
O'.01131 0.00154
#3
REREAD REDIC
0.02161 . 0.00649 0.01754 -0.00114 0.01051 0.09050 0.01005 0.10728 0.02024 0.05341 0.04028 0.07040
0.03135 0.03167 0.00029 0.22219 0.08248 0.00507 0.11833
0.01275 0.00089
0.00020 4 72
0.01812 3.737 0.10494 0,264 158422.67137 0.493 0.04213 0.633
0.00027
0.01749 0.10471 158681.00000 0.04228
0.00024
0.01803 0.10486 159042.00000 0.04182
0.00010
0.01883 0.10525 157545.00000 0.04228
130
DUP050307652
i- ,.,e:
LANCASTER LABORATORIES
1:ifn Name: 9627O01T61
1 noe; 24
ICSA
09/26/96
02:27
INSTRUMENT ID: 0547S
1.1 CM
Aa ' A1 '
As Ba Be Cd Cd Co Or ,_CU Fa . ' _K
Mg Mn Mo Na Hi _Pb _Sb _5e Sn Ti _T1 __V ' _Y __Zn
AVG .
INTEGRATIONS
(ppm)
%RSD
41
#2
#3 REREAD REDIG
0.00045 68.02 515.85723 0.964
-0.00283 56.18 -0.00024 13.76
0.00189 3.868 503.09796 O - 366
0.00024 74.60 0.00043 52.38 0.00873 9.526 - 0.00696 3.498 203.36317 0.455 0.05056 .24.32
533.88616- 0.632 0.00760 1.271
-0.00125 31.07 0.29634 23.15 0.01282 6.273 0.00139 68.03
-0.00485 48. 37 -0.00041 336.7
0.00255 143.5 0.01082 0.947 0.00076 480.3 -0.00100 68 - 44 . 154161.6.7187 O ,, 442 0.00017 76.82
0.00080
0.00020
510.12066
518.47668
.-0.00459
-0.00241.
-0..00020
-0.00025
0.00187
0.00198
501.21170
' 503.18359
0.00024.
0.00006
0.00069
0.00034
0.00969
T 0.00836
0.00724
0.00680
202.31600.
-.203.70195
0.05752
0.03636
530.07580
535.07366
0.00771
0.00752
-0.00161
-0.00130
0.37527
0.26294
0.01374
0.01223
0.00164
0.00034
-0.00321
-0.00754
0.00046 '
-0.00203
0.00667
-0.00037 '
0.01090
0.01070
-0.00121
0.00498-
-0.00021
-O'. 00138
15,4859.00000 154130.00000
0.00011
0.00032
0.00037 518.97436
-0.00149 -0.00027
0.00184 504.89862
O.00042 0.00026 - 0.00815 0.00683 204.07156 0.05780 536.50903 0.00757 -0.00084 0.25082 0:01250 0.00219 -0.00379 0.00032 0.00136 0..01085 -0.00147 -0.00143 153496.00000 0.00007
'
13i
DU PO50307653
Page: 26
LANCASTER LABORATORIES
Run Name: 9627001T61
Tube: 25
ICSAB
09/26/96' -
02:31
.INSTRUMENT ID: 05478
ELEM
Aa ___AT ___As ___Ba' ___Be
Ca ___Cd ___Co ;__;cr
Cu ;___Ee .
K ___Mg ___Mn _Mo ___Na ___Ni ___Pb-
Sb :___Se _Sn ___Ti ___Tl ___V
Y Zn
AVG
-
INTEGRATIONS
-
(ppm)
%RSD
#1
#2 .
#3 REREAD.REDIG
1.05636 0.608 515.25201 0.685 . -0.00241 144.3
.0.49836 0.626 0.47031 0.480 503.74984 0.529
0.91223 0.474 0.-47351 0.492 0.47323 0.^34 0:53760 0.633 202.83786- 0.507 0.04949 11.51 .533.78179 0.515 0.48594 0.496 0.00038 135.8 0.2353S 20.71 0.92449 0.607 ' 0.95762 0.496 -0.00491 19.11 0.00115 263.0 0.00041 504. a 0.01080 0.519 0.00218 144.7 0.4SI 07 0.500 154384.00000 0.438 O.96613 0.478
1.05228 . 513.05895
-0.Q0536 0.49673
0.46315 501.19100
0.90829 0.4-7194 0.47071 0.53610 .. 201.96687 " 0.05602 331.87677 0.48394 0.00.048 0.20771 0.92060 0.95411 -0.00400 0.00016 -0.00199 0.0107& 0.00555 0.47892 154599.00000 0.96243
1.05302 513.37164
0.00142 0.49639 0.47012 503.54367 0.91154 0.47241 0.47321 0.53519 202.57188 0.04695 532.53112 0.48526 -0.00018 0.29168 0.92194 0.95572 -0.00486 0.00457 0.00195 0.01086 0.00168 0.48062 154928.00000 0.96466
1.06376 519.32550
-0.00329 0.50196 0.47266
506.51486 . . 0.91687
O'. 47619 0.47577 0.54152 ' ; 203.97482 0.04551 536.93743 0.48862 O.OOOB3 0.20675 0.93093 ' 0.96303 -0.00588 -0.00126 0.00130 0.01078 -0.00069 0.48367. 153625.00000 0.97132
13:3
DUP050307654
Page; 27
LANCASTER LABORATORIES
Run Name: 9627001T 61
Tube: 26
CCV
09/26/96
02:36
INSTRUMENT ID: 05478
ELEM '
Ag ... A1 ___As
Sa ___Be
Ca ....Cd ___Co ___Or' ___Cu ___Fe ___K_ ___Mg ' ___Mn ___Mo ___Na ___Ni ___Pb ___Sb ___Se ___Sn .
Tl ___Tl V
'Y ___Zn
AVG (ppm )
%RSD
' #1
INTEGRATIONS ' . #2
. #3
REREAD REDIG
0.51269 0.651
25.43849 0.477
0.50725 0.723'
0.49816 0.560
0.50554 0.675
25.72545 0.613
0.50113 0.691
0.50536 0.468
'0.49473 O. 708
0.51426 0.553
25.16716 0.65S
25.32871 0.301
25.43416 0.598
0.50620 0.613
0.50129 0.751
25.96751 0.589
0.50087 1.014
0.50228 0.846
0.49524 0.96-1
0 - 49
1.005
0.49874 1.241
0.50546 0.585
0.49705 3.837
0.49903 0.769
157661.67187 0.66 5
0.50626 0.640
0.51026 25.40324
0.50344 0.49605' 0.50313 25.66606 0.49S79 0.50409 0.49224 0.51197 25.09326 25.29812 25.57113 0.50411 0.49701 25.96374 0.49677 0.49902 0.49053 0.48B50 0.49593 0.50326 0.47503 0.49641 158389.00000 0.50371
0.51650
0.51130
25.57368
25.33354
0.51077
0.50755
0.50132
0.49711
0.50945
0.50404
25.90437
25.60591
0.50511
0.49949
0.50809
0.50389
0.49873
0.49320
0.51745
0.51335
25.35708
25.05112
- 25'. 41569
25.27233.
25.60778
25.32357
0.50976
0.50471
0.50413
0.50271
26.12256
25.81624
0.50656
0.49929
0.50709 '
0.50074
0.50005'
0.49514
0.49820
0.49519
O.50584
0.49445
O.50682
0.50430
0.50826
0.50737
0.50344
0.49726
A 56458.00000 153138.00000
0.50991
0.50515
135
DUP050307655
Page: 28
LANCASTER LABORATORIES
Run Name: 9627001T61
Tube: 27
CCB
09/26/96
02:40
INSTRUMENT ID:' 0547S
ELEM
AVG (ppm)
%RSD '
#1
INTEGRATIONS #2
#3 REREAD REDIG
Ac t
0.00061 75.10
0.00101
0.00010
- -O'00072 ___________________
___A1
0:07781 25.45
Q.09407
0.08362
0.05575
___As
-0.00312 17.68
--0.00367
-0.00311
-0.00257 ______.
___Ba
-0.00112 6.009
-0.00104
-0.00117
-0.00115;
___Be
0.00021 21.87
0.00022
0.00016
0.00026 _________
___Ca
' 0.14776 11.10
0.16487
0.14630
0.13213
___Cd
-0.00019 97.57
-0.00041
. -0.00006
0.00011- _______________. _________ _
___Co
0.00086 64.86
0.00148
0.00037
0.00074'
___Cr
-0.00.056 32.25
-0.00076
-0.00039
-0.00053
___Cu
0.00049 51.42
0.00065
0.00019
0.00061 _________________
___Fa
o:07199 14.97
0.08351
0.07032
" O'.06215
___K
0.06929 10". 50
. 0.07526
0.06119.
0.. 07142 _
A
___Mg
0.08990 17.45
0.10635
0.08824
0.07510 ______` :
___Mn
0.00021 25.29
0.00025
0.00023
0.-00015
A
___Mo
0.00078 7.875
0.00079
0.00084
0.00071
.__Na
0.19631 22.97
0.19339
0.24280
O'. 15274 J____________.
A ___Ni ___Pb
-0.0002S 52.67 -0.00216 .12 ; 18
-0.00039 -0.00193
-0.00032 -0.00210
-0.00011 -0.00245
___Sb
0.00096 38.01
0.00137
0.00066
0.00035 __
___Se
0.00121 30.91
0.00112
0.00088
0.00161
___Sn
0.00090 48.67
0.00115
0.00115
' 0.00039-________________
___Ti
0.00033 31.76
0.00044
0.00023
0.00034
___Tl
0.00610 56.10
0.01004
0.00391
0.00434 _______'
___V
0.00020 53.73
0.00032
0.00019
0:00010
___-y
158659.67187 0.983
.57787.00000 157730.00000 160462.00000
___Zn
0.00267 5.386
0.00281
O.0026S
0.00252
Data Reviewed by:
Data Verified by:
13
DUP050307656
J. Page: 1
1 i.
DUP0503 07657
The 61E TRACE ICP uses a Crawford-Kunselman Noise Reduction Technique for lead, antimony, and selenium. This requires the utilization of the first and second order wavelengths in the calculation of each of these metal determinations. The 61E TRACE ICP also utilizes Yttrium as an internal standard to compensate far. fluctuations in nebulization and plasma conditions All Yttrium readings are expressed in counts.
Page: 2
LANCASTER LABORATORIES
Run Name: 962/404T61
INSTRUMENT ID: 0547
Tube: 1 .
SO'
09/30/96
12:46
ELEM
CONC. (ppm)
AVG INTENSITY
RATIO
%RSD
' #1
INTEGRATIONS #2
#3
___Ag ___A1 '___AS ___Ba ___Be ___Ca __:cd ___Co .___cr ___Cu ___Fa ..
___K ;___Mg ___Mn ___Mo ___Na ___Ni ___Pb ___Sb ___Se ___Sn ___Ti ___Tl ___V ___Y
___Zn
.0.000 0.000 0.000 0.000 0. ooo 0.000 0.000 0.000 . 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000
N/A 0.000
-0.00046
0.00834 -0.00046
0.00002 -0.06633 -0.00085
0.00032 -0.00029
0.00001 -0.00159 -0.00010
0.00147 0.00009 0.00033 -0.00070 -0.00040 0.00010 0.00216 -0.00001 -0.00135 0.00001 -0.00047 -0.00116 0.00005 171449.67187 -0.00007
17.01 0.347 65.36 19.96 0.384 0.599 29.99 31.04 62.45 1.071 32.75 5.445 '44.14 5.763 4.290 11 .'48 24.14 8.625 1848. 3.981 347.7 lO. 18 18.59 40.46 0.117 8.552
-0.00043 - 0.00833 -0.00012
0.00002 -0.06645 -0.00085
0.00037 -0.00028
0.00002
-0.00157 -0.00011
0.00138'
0.00008 0.00034 -0.00073 -0.00035 0.00012 0.00237 -0.00005 -0.00129 0.00004 -0.00046 -0.00093 0.00002 171223.00000 -0.00007
-0.00039 0.00837
-0.00070 0.00003
-0.06651' -0.00085
0.00020 -0.00020 . 0.00000 -0.00159 -0.00006 ' 0.00149
0.00014 0.00030. -0.00067 -0.00040 .0.00008 0.00208 ' 0.00025 -0.00139 0.00005 -0,00043 -0.00120 0.00005 171607.00000 -0.00008
-0.00054 0.00832
-0.00057 O.00002
-0.06604 . -0.00086,
0.00037 -0.00038
0.00002 -0.00160 -0.00013.
0.00153 0.00006 0.00033 -0.00070 -0.00044 0.00009' 0.00202 -0.00024 -0.00138 -0.00005 -0.00053 -0.00136 0.00006 171519.00000 -0.00008
136
DUP050307658
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LANCASTER LABORATORIES
Run Name: Tube: 2
9627404T61 SI 5
09/30/96
12:50
INSTRUMENT ID: 0547
ELEM
QONC (PPm)
AVG INTENSITY
RATIO
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#1
INTEGRATIONS 42
' #3
___A1 ___Ca ___Fe ___K ___Mg
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50.000
50.000 50.000 50.000 50.000 50.000
N/A
0.66046
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nr.
DUP050307659
Page: 4
LANCASTER LABORATORIES
Run Name: 9627404T61
Tube: 3
S2 5
.
09/30/96
12:54
INSTRUMENT ID: 0547
ELEM
CONC (ppm)
AVG INTENSITY
RATIO
%RSD
#1
INTEGRATIONS it 2
#3
_Ag
1.000
___As
1.000
__J3a ' 1.000
Be 1.000
Cd .
1.000 ,
Co 1.000
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1.000
r. ooo
--___.YZh.
N/A
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1:910
3.527 2.647
0.17818 0.16955 0.24611 3.02933 0.79943
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dim
DUP050307660
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LANCASTER^ LABORATORIES
Run Name : Tube: 4
9627404T61
S3 3
09/30/96
12:58
INSTRUMENT ID: 05478
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__.Cr Mo .
___Sb Sn Ti
___V .___Y
CONC (ppm)
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N/A
AV6' INTENSITY
RATIO
%RSD
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' #1
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DUP050307661
Page: 6
LANCASTER LABORATORIES
Run Name: 9627404T61. Tube: 5 ' ICV
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13:02
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INTEGRATIONS
(ppm)
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#2
#3 REREAD REDIG
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0,60157
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27.74534
0.61777'
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0.59247
0.58380
0.60648
0.60608
28.00587
28'. 02292
0.59348
0.59418
0.59056
0.59022
0.61381
0.61310
. 0.59872 * ' ' ' 0.59307
. 27.83833
- 27.79644'
29.41302
29.15366
28.03933
27.89560
0.59670
0.59595
0.62079
0.62230
29.04394
28.64812 .
0.59766
0.59576
0.58622
0.58952
0.61098
0.61156
0.60120
0.6006S
'0.62234
0.61844
0.62980
0.62885
0.59605
0.59410
- 0.61252
0.61114
171263.00000 171444.00000
0.59969
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DUP050307662
LANCASTER LABORATORIES
fi(iD Name : (lilDe: 6
9627404T61.
IC8
09/30/96
13:06
INSTRUMENT ID: 05478
{ILPM
^1
iBa
f3a
~tx Ca
Ccd
T.co
^cr
---Cu ..r
'
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Se Sn " Ti ~ Tl
v
^zn
AVG (ppm)
%RSD
'
#1
0*00079 39.14 0.02576 121.9 0.00144 60.61 0.00054 30.75 0.00095 65.80 0.11153 2.984 0.00032 35.52 0.00081 20.82 0.00051. 62,61 0.00015 188.7' 0.06166 7.771 0.07616 7.391 0.04952 14.73 0.00025 61.70 0.00221 74.32 0.17438 26.05 0.00017 353,2 0.00138 42.50 '0.00308 9.527 0.00038 693.6 O.00042 174.9 0.00086 9.603 0.00319 44.03 0.00050 52.06 174566.00000 3.385 0.00091 16.16
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#3 REREAD REDIG
0.001id
0.02518 0.00071 0.00058 0.00090 0.10750 0.00037 0.00099 0.00087 0.00038 0.06718 0.07730 . 0.04855 0.00028 0.00184 0;22387 -0.00002 0.00073 0.00279 0.00084 0.00038 0.00092 0.00195 0.00081 173751.00000 0.00082
0.00081 -0.00537
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DU P050307663
page: 8
LANCASTER LABORATORIES
Run Name: Tube: 7
9627404T61 CRI
09/30/96
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-
Cr Cu
__ Fe
_jk
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___Ni ___Pb
' Sb
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___Sn ___Ti
___Tl ___V ___Y
Zn
AVG (ppm}
%RSD
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DUP050307664
Page: 9
LANCASTER LABORATORIES
Run Name: 9627404T61
Tube: 8
ICSA
09/30/96 .
13:15
INSTRUMENT-ID: 05478
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___Cu
__ Fe
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___Na
___Ni . ___Pb
___Sb
__ Se
___Sn ___Ti ___Tl ___V ___Y ___Zn
AVG (ppm)
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0.05599 487.56787
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LANCASTER LABORATORIES
Run Name : 9627404T61
Tube: 9
ICSAB
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%RSD
SI.
INTEGRATIONS #2 . ' S3
REREAD REDIG
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475.90548 '
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0.94373
0.94174
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0.49905
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188.54191
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490.58535
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DUP050307666
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LANCASTER LABORATORIES
Run Name: 9627404T61 Tube: 1-0 CCV
09/30/96
13:24
INSTRUMENT ID: 05478
ELEM
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%RSD
#1 - '
INTEGRATIONS #2
#3 REREAD REDIG
A
___,Ag ___A1 ' As ___Ba ___Be ___Ca - Cd 'TjCo :
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0.51069 23.99235
0.51226 0.49742 0.51300 24.42605 0.50778 0.49547 . 0.51853 0.50324. 23.36532 24.81412 24.05587 0,50718 0.52314 24.38476 0.51037 0.49553
0,50734 0.50286 0.52230 0.53009 0.50059 0.52346 169492.00000 .0.51070
0.50571 23.54494
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23.30572 ________ _
0.50918
0.48843
0.50903 :-- 24.07992 _________________
0.50420 _______:----------------
0.49155
0.51606
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23.40252 0.50293
0.52500--------------------------23.99730 ________ _______
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0.50535 _______:
O'. 49489 ________
0.51961 _________
. 0.52390 ______u. 0.49604
--
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145
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LANCASTER LABORATORIES
Run.Name: 9627404T61
Tube: 11
CCB
09/30/96
13:28
INSTRUMENT ID: 05478
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' T1 -___V ___Y ___Zn
AVG
INTEGRATIONS
Cppm)
%RSD
#1
#2
#3 REREAD REDIG
0.00092 30.48 0.09809 21.00
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0.07870 .
0.00031 __
. 0.00041 ________ i
O.00067
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0.15559 0.00024
0.00127 0.00069
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-0.00026 _.
0.09239
;
0.07650 _______: O'; 09762
0.00018 ; .
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146
DUP050307668
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LANCASTER LABORATORIES
INSTRUMENT ID: 05478
Run Name: 9627404T61
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09/30/96
13:33
Tube : 12
2583823
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ELEM
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%RSD
INTEGRATIONS - 82
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A __K .A
___Ag ___A1 --As ___Ba ___Be -s Ca
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Ti
__ Tl__ .V
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0.00259 3.772 9.66835 1.798 0.00144 48.63
0.00171 26.73 0.00240 65.68
-0.00005 1369. ; 0.00162 103-4
0.00032 62.26 0.00019 65.37 0.00034 35.29
170259.32812 1.111 0.00719 0.887
--0.00021 0.07067 0.00029 0.02402
-0.00014 14.14011
0.00007 O.OOQ32 0.00064 -0.00057 0.11034 1.06496 5.88809 0.05195 0.00252 9.84382 0.00225 0.00221 0.00329
0.00076 0.00311 , 0.00009 '0.00023 O.00046
168082.00000 0.00727
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0.00022
171509.00000 0.00715
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DUP050307669
RUN Mfil'IE s 96270021-05
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69/26/96 Cl* ASS
16`s 14 TVOL/WT 0
AVG (ppb) SSRPD -0.9800, 17.2
AVG abs0.000
LANCASTER' LABORATORIES INSTRUMENT IB: 04725 OP A A CLEMENT : SE
FVOL PF BATCH HUMBER "si
BURN 1 -0.081
BURN S "0.000
TUBES SAMPLE CRA
9 09/26/96 16 s 18 __________________Cl. ASS JV0L/U1T .&
. . iFVOL. PI&
BATCH `NUMBER
AVGCoob) 4.0500
2RP0 7.5
AVG abs 0.011
BURN 1 . 0.012
BURN 2 0.011
TUBES SAMPLE CCV 1
10
09/26/96 16:22 Cl. ASS TVOL/WT 8.
;
AVG(DDb) 'XRPD AVG Abs
24.8588
0.7
.0,059-
^RECOVERY = 99. 4
k
TUBE s SAMPLE CCB 1
11
09/26/96 CLASS*.
16s26 ` TV 01.../NT 0
AVGCDDb) -1.2300
'ZRPD AVG abs
17.5
-8.001
FVOL PP BATCH HUMBER
s i.
"i .
BURN 1 8.050
BURN 2 0.059 -
FVOL 0
PF BATCH JiUMBJER 1;
BURN 1 BURN g.` --0; 001. ' 0.801 ` .
A
TUBE:. 12
89/26/96 16:30
SAMPLE 2563825 b'Pi ft lt>
Cl. ASS
TVOL/WT 188
FVOL ,._RF__BATCH NUMBER - 108 ' 1 962681056081
x
AVG<Dt)b> -0.5380
JKRPP 8.2
AVG abs 0.001-
BURN 1. BURN r> RR r d
0.801
0.001
fUBEs' 13
09/26/96 11> * i o
SAMPLE
Pil.ASt: TVOL/WT
2583825 tbPifti\tsP[ A :< 100
AVG < DDb) 12.3100
JCRPD 1.7
AVG abs. 0. 830
J6REC0VERY 123.1
FVOL __PF__ BATCH NUMBER 100 1 962681056081
BURN 1 0.030
BJJilbL.3. 0.830 .
2Q
DUP050307722
RIJH NAME: 9627002F05
PAGE:
. 3
ANALYSTS
68
TUBE: 14
09/26/96 '16:39
SAMPLE 5583627 BRPi^F'
Cl ftSfi iyOL/UT
****
100
l a n c a s v.:r< l a b o r a t o r ie s
INSTRUMENT.ID: 84725 flFAA ELEMENT : SR
FVOL DF BATCH NUMBER
106
.1 962661056001
AUG < ppb> -0.7300
*RPD 56.2
AVG._ab.-3_ ' 0`. 000
BURN '(. BURN f> . RR 0.. 001 ' -0.000
RD
TUBEs 15
SAMPLE 2563627
- 09/26/96 16s43 .
. CL ftti: I VOL/NT \Hi sc-n-j: .100
-FVOL DF BATCH NUMBER
100
1 962661856001
' AVG < pp'b) 13.1800
*RPP 0.5
f
AVG abs 0.032
BURN 1 0.032
BURN 2 0.032
.
^RECOVERY = 131.6
".
TUBEs 16 SAMPLE 2665279'
.09/26/96 16s47
>.,yy
CL AS'li TVPL/UT
u ->: };>{ *
100'
FVOL . 180
DF BATCH NUMBER S 962691836051
V AVG'<ppb> %RPP AVG abs BURN 1. BURN 2 RR Rp
19.0700 ' 1.5
5.046'" 0.045
0.046
TUBE s 1?
SAMPLE 2565279 TZ
89/26/96 16a51
CL. ASS . I VOL/NT
UA*
lie
AVG < ppb) 30.8900"
XRPP 0.0
AVG abfe 5.873
5 RECOVERY = 116.2 . -
FVOL DF BATCH NUMBER
108
5 962691556881, ,
BURN 1 0.073'
BURN 2
'5.873
..
`
TUBEs 18
' SAMPLE 256527*9
89/26/96 16:56
C:l. ACC IVQL/MT
p * *.
100
FVOL ' 100
'
DF BATCH NUMBER "s 962691056881
V
AVG(ppb) & AVG ab-==
BURN L BURN t*' RR RD
28.2100
3.9
0.048 .0.049 "5.047'
TUBE: 19
SAMPLE. . 2565279
09/26/96 .17:00
t;i.ASC ;:* A-m
TVOL/UT 100'.
FVOL, _DF_ BATCH NUMBER ' - 180 ' 5 962691056007
AVG < ripb) 32.4180
%RPP 6.7
AVG abs BURN 1 0.076 " 0.073 '
BURN 2 "07060
^RECOVERY =122.0
----------- Mi-----
DUP0503 07723
I'riL'LS , nl-IALYST:
4 66
TUBEs SB
09/86/96 17sB4
SfD'lPLE .'563279
&&ZZZZ
Ct ASS
1 VDL/WT 100
SNSTRUMbN'l "IDs b-V/ir'D
o f a a c l c men r.: sc
FUOL PF BATCH HUMBER
100
5 962691056001
AUG <ppb) yiRPP AVO ab<
BURN I. BURN :1 RR RD
0-. 1300
2.0
0.046 . 0.049 0.047 . ___ ___
09/26/96 17:06 '
Cl ASS SV.PL/WT
R***ft*
.0
FUOL 0
DF BATCH NUMBER 5
AUG(ppb) 31.8400
tfRPD 1.7
AUG abs 0.073
BURN 1 0.072
BURN 2 ' 0.874
RECOVERY =' NOT APPLICABLE , .
i'UBE i SAMPLE CUV 2
09/26/96 c:l. ASS
17:12
1
IVOL/WT
0
FVOL.
.8
DF BATCH NUMBER
.1
AUG(ppb) "247?600
XRPP 2.4
AUG fibs 0.-8S9
BURN 1. 0.05S
BURN 2 0.060
^RECOVERY = 99.0
TUBE: S3
SAMPLE CCB
09/26/96 17s16
` CL` ftSS IVOL/WT ."
FUOL _..DF_ BATCH NUMBER
a. i
-
r
AUG(bob) -1.4600
*RPP- AUG abs
4 . .1
-0. 001
BURN 1 BURN.2 ~8.802"- -0.001
.
TUBE: 4 SAMPLE 8565276
09/26/96 17:20
CLASS 1 UDL./-UT
::);
100
V/ AVG(ppb) XRPP 'AUG abs
K
'
1.3708
3.3
.0.005
FUOL 100
DF BATCH NUMBER C 1 96269105680I"
BURN i BURN f! RR. RI>
5.085
8.005
UBEi 25
SAMPLE
635276
09/26/96. 17:24
CI._A.SH IVDL/UIT
188
AUG < ppb? 10.6900
XRPP AUG abs
1.9
0.027
^RECOVERY * 95.8
FUOL 100
I>F BATCH HUMBER 1 962691056001
BURN 1 0.027
BURN 2 0.026
SO-
DUP05 0307724
LANCASTER LABORATORIES GRAPHITE FURNACE ATOMIC ABSORPTION
DATA REVIEWED BY
DATA VERIFIED BYs /gl*6'1/'!
DATA FIU; NAME:; TL P690E RUN NAI'lEs 96O&90SF01
ANALYST s a'59
INSTRUMENT NOs 0S603 BKO CORA: BD
ELEMENT: TL
Concentration is used 'bo evaluate if -4 .am o I. calibration range.
20$
i-auU'i aro within
DUPO 50307725
RUM NAME s 9&&6902F0.1
PAGE::
:t
AHALYST s 6159
TUBES
i
SAMPLE
SO
09/25/96 05:S3 CL ASS :f VOL./WT a
AVG <ppb> %KPP AUG abs
0.0000 0.0
0.014
I. AM 0 A j i l:; i.. A y 11: a i u k i !.. I MSTK'UI'IEMT l'lt: 02603 GE A A GLEi'lEMlTL
FVOL PF BATCH HUMBER 0r
BURN 1 BURN 2 ~0.019 0.009
TUBES SAMPLE S10
09/25/96 05i87 CL ACC IVOL/UT 0
AUGlPPb) y-RPB AVG abs
10.0000" 7.3
0.049
FUOL PF BATCH HUMBER 01
BURH 1 BURN 2
0.047
0.052
TUBEs
SAMPLE
see
3
09/25/96 05s30 CL ASS 1VOL/WT 8
AUG<ppb> %RP:0 AUG abs
e0.00i. 9.6
0.116
FUOL. PF BATCH NUMBER 01
BURH 1. BURH 2
0.11
0.126
TUBEs SAMPLE S40
09/25/96 05s 34 CLASS. 1UOL/WT 0
FUOL. PF BATCH HUMBER 01
AUG < pob> JiRPO AUG abs
40.0000 3.1
0.22
BURN 1 BURH 2 . 0.217 0.227
TUBE t SAMPLE
09/25/96 85 .:33 Cl a s s :; 1UOL/WT
FVGI-." PF BATCH NUMBER
i
H
AVG(ppb) 3SRPD AUG abs
,-60.0000 0.1
0. 336
BURH 1 BURN 2
0. 336
0.336
TUBES
SAMPLE
sae
09/25/96 85 s 4 1. Cl. ASS 1UOL/WT 0
AUG(ppb) JiRPB AVG abs
60.0000 7.1
0. 399
FUOL PF BATCH HUMBER 01
BURH 1 BURN 2 0.420 . 0.379
TUBE s {SAMPLE ICU
09/25/96 05 s 45 CL ASS I UOL/WT 0
FUOL PF BATCH HUMBER 0. 1
AUG < DDb) tfRPD AUG abs BURN 1
49.348(3
1.2
0.276
0.276
BURH 2 0.274
^RECOVERY == 96.7
RUN NAMl PAGE !i ANALYST!
96269021-01 as9
TUBE : SAMPLE ICB
8
89/25/96 05:46 c l a s s IVOL/WT 8
, AVG < DPb> JiRPD AVG ab& --0.9B00 95.6 -0.804
LAWCAOTER I..HIsORA TOK1E INS'f'RUMtM'f Il>: 0c:&Bis GFAA ELEMENT; TL
FVOL KF HATCH NUMBER 01
BURN 1 BURN -0.001 -0.007
TUBE: .SAMPLE CRA
9
09/25/96 05:51 Cl. ASS IVOL/WT 0
AVIS (pub) XRPD AVG abs
12.3608 6.0
0.063
FVOL DF BATCH HUMBER
BURN 1 BURN a
0. BE?
0.060
TUBE: 10 SAMPLE ZZZZZZ.
09/25/96 05:55
CLASS: IVOL/WT
x -#h (
0
AVG < pb) JiRPD AVG abs
31.5900 4.2
0. 160
FVOL DF BATCH NUMBER 0' 3
BURN 1 BURN a
0. 185
. 174
TUBE: 11 SAMPLE CCV :l
09/25/96 05 s 56 Cl. ASS IVOL/WT 0
AVG(DDta) XRPD AVG ab&
41.0000 3.9
0.226
RECOVERY - 102.5
FVOL _JDF__BATCH NUMBER 0 i.
BURN 1 0.234
BURN 8 0.222
TUBE;: 12 SAMPLE CCB 1
09/25/96 06:02 Cl. ASS ;i VOL/WT 0
AVG < (Job) XRPD AVG
0.2000 99-9
0.001
FVOL. DF~ BATCH NUMBER 01
BURN 1 , BURN g
0.002
0.000
TUBE: s a mp l e ; PBW ft
13
' 09/25/96 06:05
CLASC IVOL/WT
*: >; *>: >; )! 4;
100
X
AVG < ppb) *RPD AVG cl O ':>
-0.6900 49.6
-0.004
FVOL DF BATCH NUMBER
100
1 962681856081
BURN l BURN f> RR RD -0.003 -0.006
DUP050307727
RUN NAME* 962&988F01
PAGE:
3
ANALYSTS 859
TUBEs 14 SAMPLE PBW
09/85/96 86 s 89
ct a s s :i VOL./WT
ii- >: Ax
180
1
AVG {DDb) RPD AVG abs
-88.0680 18. 3
8. 189
^RECOVERY - 110
LANCASTER LMbuRAl UK.1.LS INSTRUMENT IDs 088W3 GFAA ELEMENTj TL
FVOL i>F BATCH NUMBER
100
i 96e6sies&0Bi
BURN 1 0.140
BURN 8 0.118
TUBES 15 SAMPLE LCSW
09/85/96 66 s 18
Ct ASS :r VOI.../WT
3; i
X,VJ*
AVG < b p W JSRP& AVG afo-.-;
47.8880 8.4
0.864
FVOL 1>F BATCH NUMBER
T i " sca&aiis&itji
BURN 1. BURN 8 RR fiB
8.865 8.863 __
_
TUBE s 16 SAMPLE LCSW fi
09/85/96 06 s IS .
Cl. ASS TVOL/WT
ilfy-V.
1
AVG(Dob) *RP0 AVG abs
68.5180 0.9
0. 368
^RECOVERY = 106.8
FVOL PF BATCH NUMBER 1 9686ai0S6iil
BURN 1 8.366
BURN 8 0.371
TUBES 17
89/85/96 86 s 19
SAMPLE
C:l. ASS J VOL/WT
8583885 bW\5S / 5*
188
X
AVG<DDb) #RP AVG abs* ,-8.0808 38.0 -0.810
FVOL BF BATCH NUMBER "180 ~ 1 968681856881
BURN I. BURN 0 RR Rj> -0.007 -0.013 ___ ___
TUBES 18 SAMPLE 8583865
09/85/96 06 s 88 Cl. ASS T VOL/WT A* 180
AVG < DDb) ItfR.PP. A ^ G b
19.8508 i.a
0. 118
^RECOVERY = 96. 8
FVOL. ' i>F BATCH HUMBER-
188
1 968681096001
BURN 1 0.110
BURN 8 0.113
TUBE s 19 SAMPLE 2583806
89/85/96 06 s86
Cl. ASS TVQL/WT
*** %
188
AVG (ppb) KRPD AVG auvi -0.9700 18.9 -0.08 5
FVOL DF BATCH NUMBER
180
1 968681056801
BURN 1 BURN 8 RR Rj> -8.005 -0.004
206
DUP050307728
RUN NANG:;
pag e s
/\
ANALYST: 859
LANCASTER 1.. A B 0E AT U E i E INSTRUMENT IDs 88803 GFAA ELCHEN f;; TL
TUBE s 20
9/5/96 06: 9
SAMPLE
Cl. ACC IVOL/WT
i5S3sei& 'BBfMP - >:ufiM
100
FVOL DF BATCH NUMBER
108
i 962&81056001
AVCtoob) 19.3700
/RPD a. 4
AVG abs 8.113
BURN 1. 8.115
BURN 8 0. Ill
tf.RECGVERY 96. 8
-- -- --....;............................
................. .... .................... ............. ....... -- -------------------- --
TUBE: 21
09/E5/96 06 a 33
SAMPLE
CLAWS XVOL/WT
858328? I3W P L> *>:->c *k k
108
FVGL 188
DF BATCH NUMBER 1 962681856001
VJ X'
AVG(sob) -1.2700
/KPD 18.4
AVG eifcfc'ri -8.086
BURN 1 -0.006
BURN 8 -0.887
RR RD ----- --
TUBE: 88 SAMPLE '583207
89/85/96 86 s 36
CLAWS XVOL/WT
DDR k i:A*
:l 88
'FVOL 180
DF BATCH NUMBER 1 962681856881
AVG < Bpb> 19.5900
I*RP &. 9
AVG abs 0.114
BURN '!. 0.189
BURN r> 0. 188
/RECOVERY = 98. 8 .
'
TUBE: 83 SAMPLE ccv a
... ................ . .. .. ... .... -
09/35/96 86:48 Cl. ASS XVOL/WT 8
FVOL DF BATCH NUMBER 01
AVG(DRb) 36.g.Pfi. AVG abs BURN . 1.
44.8008
7.6
0.245
8.238
BURN a
0. 858
/RECOVERY' 118.0
TUBE s 84 SAMPLE CCB a
09/815/96 06 a 43 CL ASS XVOL/WT 0
" ** ~ .......--
.
--
FVOL DF BATCH NUMBER 81
AUG < DDb) /RPD AVG abs
8. 17(38 99.9
0.081
BURN 1 0.004
BURN 2 -8.802
TUBE: 85
SAMPLE 8583288 DWDAG)
.......... `
89/25/96 06:46
Cl. ASS JVOL/WT
FVOL
i
100
100
* ..... *" - -----..
--
DF' BATCH NUMBER 1 962681056001
Vy X
AVG <DDb> --1.8888
56RPD 58. 5
AVG ab-:i' --0l006
BURN 1 BURN 8 RR RD -0.084 -8.009
RUH Hill'll:..: 9626902F81
PH 6b: ANALYSTs 659
TUBE: 6
89/25/96.06:50
SAMPLE
A CLASS JUPt/WT
2563006 BP>545Hi *mk *A
100
AVO(ppb) KRPP AUG abs
"16.6000 7.'ft.
0.106
^RECOVERY = 93.0
TUBE.:. 27
09/25/96 06:53
SAMPLE
Cl. ASC JUDL/MT
2583209 BPS 51>
. 100
V . AUGtppb) i*RPD AUG abs -1.5400 99.9 -0.006
LAMCA5 1
1_Hi.11 j r r I UK .1. t...
INSTRUMENT It): 02603
OFftA ELEMENT; TL
FUQL DF BATCH HUMBER
100
1 962661056001
BURN 1 0.112
BURN 2 0.101
FUOL 100
..........
DF BATCH NUMBER 1 962661656001
BURN L BURN Stli) R 0.004 -0.019 r?
TUBE: 26
09/25/96 06:57
SAMPLE
Ci. ACC - SUOL/WT
563209 pTS-)B DfV
100
AUG(ppb) %RPD AUG abs
20.0100 23.2
0.116
^RECOVERY = 100.0
FUOL DF BATCH NUMBER
100
1 962681856001
BURN 1 0.098
BURN 8.137 :
TUBE! 29
09/25/96 07:00
SAMPLE
_ Cl. ASS IVOL/NT
2583269
**
100
X
AUG ippbV *RPD AUO abui
0.7500 23.0
0. 004
FUOL DF BATCH NUMBER
100
1 962661856081
BURN L BURN 2 RR RD
0.004
0.003 ___ ___
TUBE: 30
09/25/96 07:03
SAMPLE
Cl. ACC fVOL/WT
2583209 BP)531)IlB Dx -):>: Ax -
100"
flUG (ppfa) .XftPP AUG abs
16.7000 li. 1
B. 107~
^RECOVERY = 93.5
FUOL DF BATCH NUMBER
100
1 962681056001
BURN 1. 0. 115
BURN 0. 100
TUBE: 31
09/25/96 .07:06
SAMPLE
Ck ACC TVQl/WT
2563209 OB'POVS R* **;* ~ 3 60
AUG(ppb) *RPP AUG abs
44.0300 "8 7i
0.245
FUQL DF BATCH HUMBER
100
1 962681056001
BURN I. BURN 2 RR ' RD 0.246 0.244
RUN NAME* 9&26902F01
PAGE s
6
ANALYST s 859
L ANCA 0 T ER LA B OR A T OR X t" S INSTRUMENT IPs 0288; OF A A ELEMENT TL
TUBE a 32 SAMPLE ZZZZZZ
89/25/96 07:18
CL. ASS J VOL /WT
R **}< A*
8
AVG<DDb> !KRPD AVG abs
57.5900
1.6
0.324
FVOL PF BATCH HUMBER 01
BURN t. 0. 328
BURN a 0. 320
/RECOVERY WOT APPLICABLE
TUBE!; 33
09/25/96 07 8 13
SAMPLE
Cl. ASS 1VOL/WT
2583218 `DBftcj'S ****
' 188
V. X
AV G < p r b) XRPD AVG sb'-s
"3.9880
7.3
-0.019
FVOL DF BATCH NUMBER
108
1 962681856001
BURN 1. BURN
RR Ri)
-0.018 -8.020 ___ ___
TUBE! 34
89/35/96 87 x .1.7
SAMPLE.
CL ftUS; 1 VPI../WT
5583210 UftA'^S'A .k A.'
100
FVOL PF BATCH NUMBER
100
1 962681856001
AVG<ppb> - /RPP AVG abs 17.3980 11.i 0.097
BURN 1 0.098
BURN 2 8.105
/RECOVERY = 87.0
TUBE 5 35 SAMPLE CCV 3
09/25/96 07 s20 CL ASS TVOL/WT 0
AVG < d pb) JiRPD AVG &bs
42.3000 4. 3
0.835
/RECOVERY = 105.8
FVOL PF BATCH HUMBER 01
BURN 1 0. 848
BURN 2 0. 826
TUBE; 36 SAMPLE CCS 3
.09/25/96 87s23 Cl ASS' TVOL/WT 0
AVG<pb> 54RPP AVG *b<&
1.8808 .99.9
8.085
FVOL DF BATCH NUMBER 01
BURN 1 BURN S
8.002
0.089
TUBE; 37
09/25/96 07:: 27
SAMPLE
` CL ACC TVOL/WT
2583823 B'&f'iSt)
*'**
100
AVGtppb) /RPP AUG aba -2.8908 52.8 -0. 0.14
FVOL PF BATCH HUMBER
188
1 968681056801
BURN I. BURN 2 ER RD -0.819 -0.009
~&d
DUP050307731
RUN NAMES 9626902F01
PAGES
7
ANALYSTS 059
TUBES 30 SAMPLE p ^ 2563623
89/25/96 07s3' n Cl. ASS JVOL/WT
100
AVG(ppb) *RP AUG abs
20.2200 0.9.
0.119
^RECOVERY = 181.1
LAHEh ST"! '.i>: i..Ai.u j RAVu K .i. i:./,:. INSTRUMENT 1 D: 026Uo GFAA ELEMEN I i TL
F VOL DF BATCH NUMBER
100
1 962661056801
BURN 1 0. 120
BURN 2 0.116
TUBIrls. 39
09/25/96 07 a 33 .
SAMPLE
Ct. ASS l.UOL/UT
503024 BPyP)<9,S *5***k
10
AUG <ppb) ffRPD AUG ab-j -2,3700 13-9 -0.012
FUQL DF BATCH NUMBER
180
1 962001056081
BURN 1 BURN ? RR RD -0.010 -0.013
TUBE s 40
09/25/96 07:37 l
SAMPLE
Cl ASS '.i'UOL/UT
2563624 T3YtfVaSPi ' i:KJ!4tA
15
FUQL DF BATCH NUMBER
188
1 962661 @56001*
'AUGtppb) I&RPD AUG abs.
20.9680 13.9
0. 123
BURN i; 0. Ill
BURN 3 8. 13 5
^RECOVERY
104.6
'I
A
TUBEs 41
09/25/96 07 340
SAMPLE
CLASS TUOL/WT
FUOL DF BATCH NUMBER
A
2583625.
***#
108
180
1 962661856681
.AUG(cob) *RPD. A MtJ. ' AlLi*n
BURN 1 BURN 2 RR RD
A
-2.5400 99.9 ""-eT-aie
-0.803 -0.022
TUBE; 42
89/25/96 07s 4';
SAMPLE
Ci. ASS :t:uoL/yT
3583625 N5Tai<?1i\'Op^
-i: A
188
AUG (mah) JCRPD- AUG afos
21.8580
1.0
0. 1.24
/.RECOUERY 185 .2
FUOL DF BATCH HUMBER
100
1 962661856001
BURN 1, 0. 123
BURN 2 8. 124
TUBE: 43
09/25/96 07 s 47
SAMPLE
Cl. ASS JUOL/WT
2583826 \5Rft \5
108
FUOL DF BATCH NUMBER
188
1 962681056801
A
*
AUG < pb> *RPD AUG ab-v
BURN 1. BURN n Rj RD
-0.3080 99.9
---------------- - _ .. -------------------- ------------ -------------- ... ..
-0.001
-8.807
8. 084
. ............. ,, .......... . ......... .......____
O / Ti *A JLfJ
DUP050307732
RUN NAMES 96a6902F01
PAGEs
ft
ANALYST s 859
l.AN C A I' EU L A I't '1 R A T U K 1 L INSTRUMENT IBs 0!'r Aft ELEMENT ;; TL
TJJ.BE s_ 44 SAMPLE _
09/25/96 67s SI
Kft-ii
100
FVOL 180
BF BATCH.. NUMBER 1 962681856001
J4RPD AVG afas
BURN l
19.6706 9. 4
0.115 . 0. 123
BURN 2 0. 107
^RECOVERY * 98. 4
TUBE; 45 SAMPLE
258382?
'25/96 07s 54 Cl. ASS JV0L/WT \ 180
k
AVG < ppb) *RPD AVG ab-i 0.9900 80.3 . 0.005
FVGL. DF BATCH NUMBER
.180
1 962681056081
BURN V BURN r> RR RjO 0.002 8. 888
TUBES 46 SAMPLE
ras/9& 07 a 57 Cl. ACC IVOL/WT
A 100
ftVB (Plata) %RP> AVG afos
ai.7900
1.2
0.122
. 104 .0
FVOL I>F BATCH NUMBER
18
1 962681856001
BURN 1 0.123'
BURN 2 8. 121
TUBE s 47
.SAMPLE
bev A '
'25/96 06 a 01 Cl. ASS TVOL/WT
0
FVOL Df- BATCH NUMBER 01
A AVG <ppb) flRPU AVG abs
BURN 1
BURN 2
A3-5500
2.0
0. 242
0.. 239
0.246
^RECOVERY
10ft. 9
TUBE: 48 SAMPLE CCB 4
89/85/96 06 s 0-5 Cl. ASS '.fVOL/W'f' 0
FVOL DF BATCH NUMBER
.0
1
AVG(DDb) Sift PD AVG abs BURN 1 BURN 2
A
-0.2900 67. 1
-0.001
-0.002 -0.001
TUBEs 49 SAMPLE PBU
09/25/96 08 n 87
Cl. ASS JVOL/WT
;**s; -K -3v *>;
180
FVOL DF BATCH NUMBER 180
vs
\
AV G (nob)' ftRPD -1.7200 30. 7
,, ....... . ............
AVG --8.008
BURN 1. BURN 2 RR -8.010 -0.007 ----
.............. .. .. _________
RD ----
21
A
DU P050307733
LANCASTER LABORATORIES GRAPHITE FURNACE ATOMIC ABSORPTION
DATA REVIEWED BY
DATA VERIFIED BY
DA l A HUE NAMES JL2&909 RUN NAME: 96E&903KT91 ANALYST :r &09
INSTRUMENT HO: tJEttOS BKi'j CijRR i Bi>
ELEMENT; TL
'/
Concon fcT,t.*b i on ii ia s 0 d to ^v s Iu a c ^ i. \ calibration ramie*.'
21u r*J
$> Lv*:j.u I, b' .> c^vwxtKiln
jttCift DUP050307734
ANALYST: 609
TUBE: SAMPLE B0
1
09/25/96 12s2S Cl ftSC JVOL/WT 0
AVG(DDb) JiRPS)' AVG aba 0.0000 0.0 -0.017
in s t r u me n t i d : feiciiiu: OF A A CLEMENT : TL
FVOL I>F BATCH NUMBER 01
BURN 1 BURN 2 -0.019 -0.014 -
TUBEs SAMPLE SIB
2
09/25/96 '.1.2 s 28 C.l. A SC :r v o l /w t 0-
FVOL 0
1)F BATCH NUMBER 1
AVG<DDb) *RPO AVG abs
10.0000 2.5
0. 067
BURN 1 BURH 2 0.068 0.065
TUBE s SAMPLE S2B
3 09/25/96 12 s 32 Cl ACC :f VOL/WT 0
t
AVG (DDb) 20.0000
JCRPD 5.2
AVG aba 0 1&1
FVOL I)F BATCH NUMBER 01
BURN 1 BURN 2 0.125 0.116
TUBES SAMPLE S40
4
09/25/96 ias'36 Cl ASS TVOL/WT 0-
FVOL DF BATCH HUMBER 01
AVG (DDb) ` J6RPD 40.0000 5.4
AVG abs BURN 1 0.227 , 0.236
BURN 2 0.219
TUBEs SAMPLE S60
5
09/25/96 12s.59' Cl ACC :r v o l /w t 0
AVG(DDb) #RP3t> AVG abs
6,0.0000
1.6
0.313
FVOL DF BATCH NUMBER 01
BURN T. BURN 2
0.317
0.310
TUBEs SAMPLE S80
6'
09/25/96 12s43 t::t ACC TVOL/WT 0
AVG(ppb) ?-FP:0 AVG abs
80.0000 3.0
(3.395
FVOL d f BftTCH NUMBER 0. 1
BURN 1 BURN 2
0.387
0.404
TUBEs
SAMPLE icv
7
09/25/96 12s46
Cl. AOO TVOL/WT "0
WG(pp.b) i*RP& AUG a bib
46.7100 0.5-
0.259
'^RECOVERY * 93. 4
FVOL 1>F BATCH HUMBER 0i
fiUKJbLJ. id; 258
BURH 2 .7260
R U M N AML: 9626 9 0 3 F u .1. PAGE: ANALYST: 609
TUBE:
SAMPLE ic b "
6
89/25/96 12:50
Cl ASS IUOL/HT 0
AUG <ppb> *RPP AUG abs -0.3500 23.6 -8.002
Lh Ma i-iS (: i..h b u Ri 11 ui-- > i.. INSTRUMENT II) : w26vJ3 Or ftA i-Ll-HENT ; TL
FVOL DF BATCH NUMBER 01
fcURN 1 'BURN 2 -0.002 -0.003
TUBE:-
SAMPLE CRA
9
9/25/96 IE:S3
Cl ASS ' IUDL/NT FUOL
e` / '
(3
PF vBATCH NUMBER 1
AUG < ppb) y-RPto AUG abs
9.6408 19.6
0.06-4
BURN 1 BURN'2 8.855 0.873
TUBE: 3.0 SAMPLE 2ZZZ2Z
89/25/96 13:56
CLASH IVPL/WT
*******
0
FUOL DF BATCH NUMBER 1'&
AUG< apb) #RPD 30.3680 3.0
AUG abs BURN 1 BURN 5
8.160
0.134' '0.1V?
TUBE: 11 SAMPLE CCU I
89/35/96 13:00 Cl ASH 3UOL/NT 8
AUG (pab) yiRPB AUG abs
42.1500 2.9
0.233
^RECOVERY = 105.4
FUOL PF BATCH NUMBER 81
BURN 1 0.233
BURN 3 8.242
TUBE: 12 SAMPLE CCB 1
09/25/96 13:03
Cl. ASS JUOL/WT 0
FUGL PF BATCH NUMBER 0r
AUG (ppb> *RPD AUG abs
.0.6100- 68.3
8.004
BURN 1 BURN 2 0.006 0.002
TUBE: 13 SAMPLE 533209
09/25/96 13:86
Cl. ASH JVCL/WT'
l.u: )'.>; * >:
100
X'
AUG <DDb> 1.8900
5CRPD 31.1
AVC Ck O s 0.007
FUOL PF BATCH HUMBER
100
1 962661056001
BURN L BURN 2 RR kj)
0,809
0.086
4Q X*3 X-
A
DUP050307736
RUM NAME i: 962690 JI-fell PAGE ! ANALYST! 809
TUBE: 14 SAMPLE 2563209
09/25/96 13:10
Cl. AGS JVPL/WT
Uih :*-A-x
180
ALG < p ij b) ' XRPP AVG abfe
20.0100l
0.5
0.121
'^RECOVERY = *34.6
LAMCAG rs;i< LABORA'i uR ILL'S INSTRUMENT Il>s 02303 g f a a e l e me n t .: t l
FVOL. DF BATCH NUMBER
100
1 962&81&56081
BURN 1. 0.120
BURN 2 0.121
TUBE.! 15 jftMPLE
09/25/96 13:13
Cl. ASS JVOL/WT
2583630 -r-r-ww *##*#
mtm*
...
100
AVGtppb) *RPP AVG
2.1300 16.4
0.014
FVOL DF BATCH NUMBER
100'
1 962681056002
BURN 1. BURN 2 RR Rj>
0.016
0.013
TUBE: 16
'09/25/96 13:: 1?
s a mp l e
; a a s :-:: j v o l /w t
2583330 ZZZ1XZ. **A*. . - 100
AVG C ppb) XRPP AVG abs
20.590(3 1.0
0.124
^RECOVERY * 92.3
FVOL DF BATCH NUMBER
180
1 962681056802
BURN 1. 0. 125
BURN 2 B. 123
TUBE?. 17
09/25/96 13:28
SAMPLE
CL ftGG JVOL/WT
2583831 r7??'TT ***** .* .1.00
AVG < ppb? XRPP AVO aiw -0.3780 99.'9 -0.002
FVOL DF BATCH NUMBER
100
1 962681056002
BURN 1 BURN 2 RR RD 0.,003 -0.003 ____
TUBE : 18 SAMPLE 2583631
09/25/96 13s20
CL ACC TVPL/UT
4; A
100
AVG < DDb> gRPD AVG Abs
20.1100 0.2
0.121
'^RECOVERY = 100.6
FVOL DF BATCH NUMBER
100
1 962681056002
BURN l 0.122
BURN 2 0.121
TUBE: 19
09/25/96 1.1:27
SAMPLE
Cl. AGO 1VPL/HT
2533832 iXtZZ* ****:
100
FVOL ' 100
DF BATCH NUMBER 1 962681056002
0.yiiiR&fei..' i^r p p A.yL._jj.5
0.7400 55.0
0.805
BURN I, - BURN 2 RR K'P 0.083 0.007"
p-j r
DUP050307737
r u n h > i h ;c t 962&V03FW1
P )"1 i> L s
4
ANALYST; 609
' I..h NCh :;IVk LMBu k h i uK.i t.S
INSTRUMENT 1 i> s iJciaUi
GFAA ELEMENT : I'L
TUBE; 0
09/25/96 13:31
SAMPLE
Cl. ASS' IUOL/WT
as6363e ZZXZSL' **a
100
FVOL PE BATCH NUMBER
100 1 gea&aiss&Biag
AUG' < ppb) XRPP AUG abs 16.7300 4.0 \ 0.114
BURN 1 0.110
BURN 2 0.111
/RECOVERY = 93.6
TUBE; .1 '
09/25/96 13:: 3 4
SAMPLE
CL AUG? ' 1VOL/WT
2563633 ZZ-u^Ig UttUtttHt
100
. FVOL : 100
PE BATCH HUMBER 1 962661056002
AUG < ppb) . ZRPD AUG ab-i BURN 1. BURN 2 RR Rl)
. 0.6100 99.9.
0.004.
0. 806 . 0.081
TUBE: 22
09/25/96 13s36
SAMPLE
CL ASS JVCL/WT
2563633 Z2Z22S >=** a *
180
FVOL _DF BATCH NUMBER
108
1 962661056082
- AUG < ppb) XRPD AUG &bs . BURN t BURN 2
19.7100 5.1
0.119
0. 115
8. 124
/RECOVERY = 96.6
TUBE; 23 SAMPLE CCU 2
. 09/25/96 13:41 CLASS T VOL/WT 8
AUG(BDb) 5SRPD AUG &bs
40.6100
1.2/
0.238
/ RECOVERY = 181.5
FUOL DF BATCH NUMBER 81
BURN 1 8.232
BURN 2 0.228
t u b e :: 24
SAMPLE
ccb a
09/25/96 13#44
CLASS JVGL/WT
FUOL PF BATCH HUMBER
B.ei-
AVG <ppb> ZRPO' AUG abs -0.3600 69.4 -0.003
BURN 1 BURN -5.001 "-0.004
TUBE; 5 SAMPLE 563634
09/25/96 13a 46
CL A Sit J VPL/UIT
KK4f
3 00
FUOL 100
PF BATCH NUMBER 1 962661056002
A
AUG < ppb) /RPD AUO Abs
BJsjrtN I. BURN 2 RR RJ>
-57804 " I0.2700 99.9
0.002 ' ""a"'006"
2-
DUP050307738
Mercury Data
21
f (
DUP050307739
S... 1-11'l s..: i 1 b r !: I-; L A .1.1 KIH 111 ; .1. L.... MERCURY ANALYZER-
DATA REVIEWED BY: /l/^ M 2 2-3
^ j2-4 [ &
DATA VERIFIED BY
DATA FILE NANEs 3&r&93. PRN RUN NANEs 96E6983MB3 ANALYST i; /a i.1
"3S>
INSTRUMENT NO: uicici ELEMENT: HG
21l
DU PO 50307740
r u n i infii...
PAGE ;
;i
ANALYST: Cifi
TUBE s 1
SAMPLE SB
09/23/96 17:14
CLASS
TVDL/WT
5i* ** **
0
AVG<ppb> 0,, 0000
Intensity 773-. 0
FVOL. .0
I.HHLl-V-j 1 I -k 1 Ii m.-.i 11 ui-. INC l K UNLIT 1 .1 0 BE CV I'LCflLM i : !IG
DF 1
BATCH NUMBEh
TUBE: a
SAMPLE
so .a
09/85/96 17.>16
. Cl. ASS
TVOl. /LH
FVOL
DF
*
0.0i
Bu t CM MUM BE K
"17a 0
~ 20i atf." 0
TUBE: 3 SAMPLE gyTM*}.... .
09/23/96 17816
Cl. ACC. fVUL/WT
**#
0
AVG <ppb) 0.3000
Intensity, ' . 54198.0
-FVOL 0
DF 1
BATCH NUMBER
TJ.JBE: 4
SAMPLE Si. 8
09/85/96 .17 Tat
Cl.. ACS
IVOL/UT
. >}~k
0
!9.y.S.jLl5i?J.3.L 1.0000
Intensity 103361.0
FVOL. ~0
DF . BATCH MUM BE R 1
TUBE a 3 SAMPLE S2. 3
89/85/96 178 2-1
CL ASS
:i VOL/WT
0
FVOL 8
DF 1
BATCH NUMBER
A
AVG < ppb)
intensity
8.5008
849425.8
TUBE v. 6 SAMPLE S3.B
TUBE a 7 SAMPLE, 1CV
09/85/96 17:: 26
Cl..ASS
TVCU. /LIT
**
0
9.70.^.1111111.. 5.8808
IntensE -by 4 S'6 09C., 0
FVOL '0
DF 1
BATCH HUMBER
Correlation Coefficient - 0.99996
. -69/85/96 17s 86
. Cl. ACC :i VDL/UT
FVOL,
DF
WKK-ltK'K-K
001
BATCH HUMBER
AVG(ppb)
a.0400
Intensity 80484.7. 0
^RECOVERY * 102. 0
0 4 C.
<v..*........................................................................................................................................
j..
DUP0503 07741
RUN NAMEs 9626903M03 PAGE s ANALYSIS 823
TUBE* a ' SAMPLE ICB
09/25/96 17s 31
Cl. ASS
II V01. /WT
#*
8
-"~-a~0 i?&
iaiyiiisJr.ix
sag. 0
FUOL 8
LAI-iOAG i: ; Au h Ai Ok j i IM'o 1 RUMEN t u; V!'...
cu iLLLMLM1 . 1 Uj
DF i
BATCH MUM BEK'
TUBE is 9 SAMPLE CRA
09/85/96 1?:: 3.1
'
Cl. ASS
3 VOL. /P I
;;* .
0
AVG< p ij h) 0.1900
lL0i!:?.`;2-iiX. il052.0
FUOL 0
DF . BATCH NUMBER 1
TUBERS 10 SAMPLE
CCU 1
.
09/25/96 17 s 35
Cl. ASS
3 UftL/WT
KMKK*KK-
0-
FUOL 6
....!>... 1
BATCH NUMBER
8.yiiiiil?Ja.L
7.0408
1 irberi & 1. ty `..105717.8
^RECOVERY = 104.0
TUBE s ii SAMPLE CCB 1
09/25/96 17:33 CLASS '. JUOL/WT 0
FVOL 8
DF 1
BATCH NUMBER
AUG < cmb) -0.8200
Intensity 229. 0
TUBE s SAMPLE PBUI
/
12
89/25/96 17.: 48
Cl ASS
IU0L/W7
u k <k
AUG<BJ?b> 0.0100 .
"is is ."a
FUOL 6
DF 1
BATCH NUMBER 962638321801
RR RD
TUBES 13 SAMPLE LCSW .
09/25/96 1742
C:>. ASS
11 UOL./WT
1
FUOL
i
.DF . 1
BATCH NUMBER 962630321881
y
AUG<Dob> 8.3828
81322J o'
A A RD
TUBES 14 SAMPLE 2563205
.89/25/96 17i:-45
CLASS :i UOI../ UT
>; >: n >: k
3
U
AUG <ppb)
I viLen-al by
-8.0020
2806.0
FUOL 3
DF 1
BATCH NUMBEh 9 6263 3(Hi 81
BR
DUP050307742
RUN NAMES 96869031't(33
PAGES
3
ANALYST: 823
TIJPE a 15 SAMPLE 8563806
09/85/96 17:47
CLASS
IVDL/WT
x***
6
LANCASTER LABRATCRIES INSTRUMENT IPs (35280 CV ELEMENT: 1 ID
FVOL. 8
PF 1
BATCH NUMBER 968680881001
010060
I Vi Lii-m-.-ri- fey iV&7.0
RD
TUBE a 16
SAMPLE SsSsee? brU Dp
09/85/96 17 a 40
ci. a s s
:rvoi. /wr
S.
. FMOL a
BATCH NUMBER 968680881 001
0,,SiS.tEi2.!a2. 0.0110
i22.te.u02li.i2iL '"'3243.0
RD
TUBpIs 17 SAMPLE 2533206 HRS45
09/25/96 17a 51
CLASS ; IVOL/WT
*!;*: 5h ;
'6
F90L .8
PF. 1
BATCH NUMBER 968680621001
AUG< ppb) ... 0.-'0(350
I t i l by 2670'(3
RD
TUBE a 16
SAMPLE 8583809 BBS 3-0
89/25/96- 17 a 54
<LljggS
IVOL/WT '
U"-><8
FVOL '..PF 61
BATCH HUMBER 968600621001
V '(/
AVG<ppb> 0.0030
1 nU^n-A'i. fey 2494.(3
lift RD __ ___
A TUBE;: 19
09/25/96 17 s 56
r
SAMPLE
Cl. ACS
JVPL/UT
FVOL.............PF
BATCH. NUMBER
2583209 'feB.SBDP
&*:* :*
6 8 1 968680821001
V/
A 'x/
8te!i.L\.P.Ei3.L " 0.(304(3
Silte.UL!^i.teiL 8631.0
k
' Rft ~
RD
TUBE a 80 'MlMIM ! 8563809
09/85/96 1?;:58
Cl. ASS
:i VOl / wr
8
FVOL .
6
PF BmJCH -n u mb e r
T 968680881001
AVG C g_pji.
Inbian-ti by
A
1. (3900
11(3152.(3
A
RD
-2-2-i
DUP050307743
RUN NAME: 96S6903N03
RAGE a
t\
ANALYST t Iia3
TUBE a 21
SAMPLE 2563810 T>BA5S
09/85/96 10* 00
Ul.. ASS :t VOL /WT
!; }: >:
{ ,
0.0170
I Vi L'r?ri-:> i 'ey ... 3606". 0
i .h Nc m', i i i .iU.'Rh i ul. i.t ! Hu t RLil'iu N l i. u: tr> . l .i CV ELEMENT . HU
F VOL, ' Ll6X
BATCH NUMBER
9ti 81>0 0681001
RD
TUBE; SB SAMPLE
ccu"'i"'"
TUBE a 83 SAMPLE CCB 8
09/85/96 10:: S3
Ul.. ASS
'.I VOL./UT
-****
.
FVOL 0
DF i
' BATCH NUMBER
AVG<PDb)
i.8500
Intens ILy
"*106109. fcJ
WRECOVERY ~ 105.&
09/85/96 10-S05
CLASS . 3 VOL /WT
****
0
FVOL 0
DF 1
BATCH NUMBER
AVG < ppb) " 0~. 0880
Intn& siiTo
TUBE a 8 4 SAMPLE a5&3&3 &bPV3l''t>
x
09/85/96 10;: 07
UL ASS
:i VOL/WT
**
0
FVOL 0
AVG(Dab) 0.0690
Illkl-ijLiiLSCL 3000.0
DF 1
BATCH NUMBER 96863008100).
RR RD
TUBE a SS SAMPLE 2563084
09/85/96 10:09
CL ASS .
J VOL /LIT
-i: a
FVOL 0
DF 1
BATCH NUMBER 968600021' 001
V/ y
AVG jL&HbL. . ""''0010"
ILTl'Ll-LLLLidL/. .... "aasa.'e
RR RD
TUBE a 86 SAMPLE 8503025 '
>/
09/85/96 10s18
CLASS
:iVUL/UT
8
AVG(ppb) 0.0010
L L;y ' 8803.0
FVOL 0
DF 1
BATCH NUMBER 968600081001
RR RD
TUBEa 27 BAMPLE 2503086
Pi \$
09/85/96 10;: 1 -V
CL ASS-
1 VCH. /UT
>: >: -j :
0
AVG(ppb) -0.0010
L.Ii.&'iLL.ckjil'. 8079.. 0
FVOL . 6
DF 1
BATCH NUMBER
96860008
..
6* >-j \i
RR KD
DUP050307744
HUH NflrtL
9C2&903M03
AMALYSIs 623
TUBE: 26 SAMPLE 2563627
09/25/96 16s 16
Cl. ACC
I VOL/WT
\ Si &
St/
y
AUG fools) 0. 0030
In'tm-.ii'fcy , 2466.0
TUBE 5 a9 SAMPLE PBW
09/25/96 16.: .1.6 . I VO!. /WT
-i; -it
AUG <ppb) . 0.0000
In b=3m->i by 2237.0
i..h Wk -h , i:
i .1 c r i i i
us.
INSTRUMENT 1 D:: to 32 21->
CV CLEMENT ; !IG
FUCiL a
DF i
BATCH NUMBER 96266U62iui
RR R D
FVQL a
DF i
BATCH NUMBER 9u e c av.i a a i u u a
Kp
TUBE s 30 SAMPLE LCBW
. c'/l _
09/25/96 16a21
Cl. ACC
!i UOL/WT
.*** '
:i
5/
' AUG ippb? 1,,0700
Inb^rns 1 by 106765.0
FVOL 1
1)11
BATCH NUMBE R 962660621002
RR RD
TUBE; 31 SAMPLE 2533222
^janu* ioc........
.09/25/96 13 a 23
Cl ASS
TVUl / WT
&
y/ '>'
[WB/. jJijbjL 0.0030
'
Inb^iisLt.y 2469.0
FVOL a
DF BATCH HUMBER 1 96 a & a 0 a & 1 00 a
RR RD
TUBE; 32 SAMPLE 2563223
09/25/96 16a 25 CL ASS , IVOL /m ft
FVOL a
DF 1
BATCH HUMBER 9&a,aaaitj0a
AUG < ppb> 0.0010
I ni;:-nv> i. by 2244.0
RR RD
TUBE: 33 SAMPLE 2563224
09/25/96 16.s27
Cl. ACC
) VOI. /WT
AUG < ppb) 0.0070
In t;..-nv.i. i. fay 2906.0
FVOL 6
DF 1
BATCH NUMBER
HR Rp f) '.Tu> CO,
DU P05 0307745
RUN NAMES 9626903N03
PAGE::
('
ANALYSTs 623
TUBES 34 SAMPLE CCV 3 "
09/25/93 13:30
Cl. AGS
TVOL. /WT
ttKXHXK*
it
LANCAG l`LK Lb SKA 1 UK.I,.
:i. NS TRUMEM'i ;U):
cv l :i,,; :i!i .Li i . u g
FVOL 0
PI-' 1
BATCH HUMBER
AVO < pofa) 0.9660 .
` Inter:sity 96044.0 tfRECOVERY = 96.6
TUBE : 35 SAMPLE CCB 3
f
09/25/96 16:32
CL ACE:
3 VOL /WT
.0
AVG <opb> -0.0310
T. interns i ty -670.0
FVOL 0
PF ' 1
BATCH NUMBER
TUBE s 36 SAMPLE
2563225-
09/25/96 16.1-3 4
C:l. ASS
3 V CL/LIT '
- X'XXKXKX'
6
FVOL. '6
PF 1
BATCH NUMBER 962660621002
AVG <ppb> (dT (3470
I*n L^vrvi. by 6653.0
k j .)
TUBEs 37 SAMPLE
2563226
`09/85/96 16;:37
Cl, ACC
TVOL /LIT
U-k *k
6
FOOL. 6
DF 1
BATCH NUMBER 962660621008
AUG <ppb> -0.0010
. I n L:m-> i. l;y E096.0
1'6< RB
TUBE: 36 SAMPLE 2563226
'i/y
09/25/96 16:: 39 .
CLASS
1VGL/WT
p-x->i
6
AVG<ppb) 8.0030
T n ben-ri. by 2467.0
TUBE: 39 SAMPLE 2563226
09/25/96 .16:: 41
CL AGS
TVOL /WT
>: 6
FVOL 6
PF '1
BATCH NUMBER 962660621002
* 1C R D
FVOL. 6
PF .1
BATCH NUMBER 962660621008
V/
AVG <e.pb) 1.8600
IJlfcliBlIJL-k/. ur/aiirW
RA RD
TUBE s 40 Wl|
09/25/96 16.: 4 4
Cl. ASS
TVOl. /UT
-X ~
6
4
AVG < nob) -0.0010
I-.jjJi'iBLLL'F-/.. 8126.0
FVOL 6
DF 1
BAY UH THOMBER 96266d&2'i 0 0 2
U! < Is '0
DUP050307746
Extraction/Distillation/Digestion Logs
&p.oO tt_: DUP050307747
Wafer Digestion Logbook ICP-20
1151 Rev. 08/22/95
O4L
CM
DUP050307748
Water Digestion Logbool: Graphite Furnace - 20
DUP050307749
limn
.3 i
Analysis #0821 Water Digestion Logbook
DUP050307750
Chain-of-Custody Record
DUP050307751
DUPO 50307752
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DUP050307753
DUP050307754
Lancaster Laboratories
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Sample Administration Receipt Documentation Log
Client/Project: _______ CO/SO CV
Date of Receipt:
}-
Time of Receipt:__________Q
0
Source Code: ______________ F~ I
COC Seal: Pre^t / Not Present on cooler Broken / farfsact
Package: Cf^^d / Not Chilled Unpacker Emp. No.: _ Yy
Thermometer ID:
Corrected Temp.: Bertie / Air
#1
16 f0 3
e)v *7
/ Dry Icfe / Ice Packs Ice Present? (y) I N
. #3 Thermometer ID: Corrected Temp.: Bottle / Air Wet Ice / Dry Ice ! ice Packs Ice Present? Y / N
Temperature of Samples #2
Thermometer ID: Corrected Temp.: Bottle f Air Wet Ice / Dry Ice / Ice Packs Ice Present? Y / N
#4 Thermometer ID: Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / ice Packs ice Present? Y / N
Paperwork Diserepancy/Unpacking Problems:
Name 11....
Sample Administration Chain of Custody
Date
Time
Reason for Transfer
f'/A f i
/A 9 f-.
/e f ^ . //
/<too
Unpaektng-- felace in Storage__j)or
Entry
Remove from Storage^
Place in Storage or Enty
Entry
1
Rev. 2174 09/09/96
DUP050307755
3425 WwHoO>ndPitoUncMt; w 15601-5994
Sample Administration Receipt Documentation Log
Client/Project: Date of Receipt: Time of Receipt: Source Code:
OM/~0 CO
0 <pf Bl
COC Seal: Pr^fent / Not Present on cooler Broken^/ Inject
Package: Cl^pd I Not Chilled Unpacker Emp. No.: _
ThermometerID: Corrected TemD.:
#1
f0f
it f
B^e / Air
We^jjie / CVy Ice / Ice Packs
Ice Present? $) / N
#3
Thermometer ID:
Corrected Temo.:
Bottle / Air
Wet Ice / Dry Ice / Ice Packs
Ice Present? Y / N
Temperature of Samples #2
Thermometer ID: Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs Ice Present? Y / N
#4 Thermometer ID: Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs Ice Present? Y / N
Paperwork Discrepartcy/Unpacking Problems:
Sample Administration Chain of Custody
1
Name
Date
Time
Reason for Transfer
|
Cax j u ia x *
$'19-%
/on Unoackina //flK Place in Storage) or
'laofi Remove from Storage^
Entry
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Rev. 2174 09/09/96
23
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zlfr Lancaster Laboratories
3925 NewHoOmd Pike* Lancaster, FA 176CM-59W
Locked Storage Chain of Custody Original Sample
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Preservative: _ t M'/O 6 3_________ Matrix: //) /, )_________
Sample 8 Range of Entry Group: A? A"
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SDG: rrAL 0 I
Bottle Type:
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Sample Numfaer(s) Released Received
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By By
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Date of Time of Transfer Transfer
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Reason for Change of Custody
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Dist.r Extr., or Digest Chain
Created (X)
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2016 Rev. 09/05/95
DUP050307757
2425 New Holland Wee UncMler, 04 17601-5994
Locked Storage Chain of Custody Original Sample
Client/Project: C)h PnrCf'
H-Pfa/Ai/ffiti z1 O i/r.S._____ jEof--C.--l23.fi
Preservative:
___________
Matrix: ju UJ___________
SDG: j^lDO !
Sample # Range of Entry Group:
3 5~ P 33-3 /"
Bottle Type: SQO
Sample Number(s) in Custody
351^-2^-XI
Released Received Date of Time of By By Transfer Transfer
Reason for Change of Custody
S* * .1C5^rv(t4-* wSW-j*
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DUP050307758
Als.) ancaster Laboratories
l|r 3425 Hew Ho*Kl Pfl* UrKJIltr. M. I760!-59>*
Locked Storage Chain of Custody Metals
Client/Project: ______-f^) PC. PyvOt___________________________:______________________ __
Sample#:
Q5-)0 ) 3- SS- 3^>3-3/7_________
Digest Type (circle one): Hg PMetals^ GF Hydrides
SDG: F rvifo 0 1
Trial No: (If not 1, fill in)
Batch No:
Ml . 3- le
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Sample Number(s) in Custody - no
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2231 Rev. 09/21/95
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DU P050307759
iaiv^oter Laboratories J425 Ntw Holland N *UnuSttr. Bfc 17601-5994
Locked Storage Chain of Custody Metals
Client/Project:
E>
Sample #:
% >flS "10 ;
Digest Type {circle one}: Hg Metals
-zn Hydrides
SDG: --P m Dot
Trial No: (If not 1, fill in)
Batch No:
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Sample Number(s) in Custody
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2231 Rev. 09/21/95
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DUP050307760
#1 anraderl ahoratories 2c2S New Motoyj Pike Unastet PA 17601-5994
Locked Storage Chain of Custody Metals
Client/Project:
tx- Pcndr
Sample #: ^5ynog-10 ; 3-gg 3fr>3 - 7 Digest Type {circle one): Hg Metals ^GF) Hydrides
SDG: -----F nfl C>Ot Trial No: (if not 1, fill in)
Batch No:
3-
1 0S
Sample Number(s) in Custody
Released By
Received By
Date of Time of Reason for Change
Transfer Transfer
of Custody
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2231 Rev. 09/21/95
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DUP05 0307761
./lx I ancaster Laboratories
Locked Storage Chain of Custody Metals
wiient/Project:
/$>#? r_____________________________
Sample #: ^ Digest Type (circle one): Hg
i ^5^ 3ji?3
Metals ,
Hydrides
SDG: F/?7?^y
Trial No:
9 (If not 1, fill in)
Batch No:
:z_
/ a 36
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Sample Numberfs) in Custody
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Released By
Received By
Date of Time of Reason for Change
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2231 Rev. 09/21/95
Pase__>of DUP050307762
^Lancaster Laboratories
^5 2<25 Newhofiand fik* Lancaster, PA l?60t-594
Locked Storage Chain of Custody Metais
Client/Project: VU P&n/T
u' fU,m cd* a-e*
Sample if: 2.S2 molT-J* . 9.^
__________
Digest Type (circle oneh^Hg^? Metals GF Hydrides
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SDG:
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Trial No: (If not 1, fill in)
Batch No: <? SL %
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Sample Number(s) in Custody
3.^3 3 P-os-/>
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Date of Time of Reason for Change
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of Custody
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DU P050307763