Document aJpjVyvra7xGg33EbNbNw5G5e
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C.VT 260
D.V - 31 5) 317, 322/3230
? 0$ 40
CODE 'RT-531 -D
iLmJfA
( DATE )
PKG __
PROCESSES
APPROVED BY:
< ) RT-531 ~D (P > EWK 03/02/82
COMTY.P JOB NAME: 40.RT531BMP
E.ST * NT.
HR S'. ____________ TIME 4
issssssssussss::
EQUIP ME NT
MI-.BLEED I NO
SHS SZ ZZ zz zz zz zz zzzzzzzz zz
i i ACCT N-COBE i LBS
PREP 1
1 4 -NITR0 ~ 2 - AMIN 0TOLUENE FOR 6 i 3-H Y B R 0X Y - 2 - N APTHY L AM IDE FOR 318 1 3-4^tXEAN, BRESS, CLOSE 24" CLARIF PRESS 1 I PS FRAMES '
?0* (700 G> WATER INTO V-..SS.7___
__JL.___m"RUN IN HYDROCHLORIC ACID FROM V-324^ ,,
HJMP IN FROM SI 4~NITR0-2-A.M INOTOLUENE
54,--C 150-C
jS^O.
. 28-D :j 504-C
DJTi'lL JlCiWgipipW
' WWBMQHWWIOLC:
.1
^DJ TO 42" (1470
jps330 I
SIPHON IN SOD>IUM NITRITE IN 7-10 MIN, ,
i I
n_A____________J&j i?.J
\I jk, *4L\
pyrT STIR 5 MIN 6 RECORD: CR.i:__< + ) ,
_..( + > I
i
j I NOTE: <1>. IF CR-, KI- ADD 200 "AS IS*
Ii
i 1 INCREMENTS HYDROCHLORIC ACID ASSUME 32% I_________|
i * RECORD: CR,,_____(+) K.I________ .< + )
!!
I ! (2) IF CR+, KI- ADD 'IBS- "AS IS" INCREMENTS i
j
j ! SODIUM NITRITE
ASSUME 33% . j_______ j
1 J^RffCORD: CR_< + >
KI<*.)
1l
\T \ STIR 10 MIN ATkfrAjptF MAINTAINING ;S-CgL +KI J
j
i I FOR SI 3 RECORD : TIME START.J/J.iil.I
!
' 57-*a ]A6&>
725-A I 138
28-D *1 i
725-A
\ I i
tj
!I 11
MISC 11 3
SLURRY DIC.ALITE FILTER AID IN 40 GAL WATER j
IN DRUM & PRECOAT CLARIF PRESS
I
777-A
DV .4
WHEN ..511 STIR COMPLETE DUW
0^... IN DICAt ITE FILTER AID STIR 30 MIN AT3^4^DEG F
I MAINTAINING +KI FOR 523. ' RECORD: START.,___________ KI___
l 10 1 ASSUME 33 A.!_______ ;
, (+)
777-A i 10
725-A |______ 57-A 1______
f9111*}$}&jW -TER INTO V~2>i3
SLURRY TRISULPHOIL SOAP D IN 250 WATER &
S^OrTIN
DUMP IN 3-HYDR0XY~2"NAPTHYLAM:[DE FROM S2 &
TIR 30 MIN OR LCNGERy TO WET. J..QT
RECORD' START
A A -J&Li
3R-A 3A-
13#~C j 336
*:! Co
,, <r NOV 151982
EOMTYP JOB NAME : 40RT531DHP
PAGE 02
DATEf PRINTED : 8/03/82
EQUIP MENT
""T~'...............
i PAGE 2
'
OF 3
CG 40
""".
CODE RT~S3i~D (P>
i USE I LBS
302 f jiiN 2" (1 44G) WATER INTO V-302
2^j3QU IN SODIUM HYDROXIDE
ASSUME 50%
84
3KT RUN IN ACETIC ACID THRU PMEETER. & SSTIR 3 MIN I -- . I
7/ M___ _____
RECORD PH,,Z:J.,< 6.7-?,,5)) IF NECESSARY ADJ TO I
]
6,7-7,5,
ACETIC ACID ASSUME 70%i_____ _
i RECORD PH_____ SODIUM HYDROXIDE ASSUME 50%I
ON V- W' AGITATOR. & ADD ICE, THEN
I2X330
'*ZJP0SWT OFF AGITATOR
Z3AI PUMP DV THRU CLARIF PRESS XRTO DV USED IN 1 I i S 23, MAINTAINING TEMP AT 3*S~#*F'. RECORD: j
*i i START: .AhllhtSi-
TOTAL rttN__*3L.
1 i^OTE: DO NOT USE V-303 - .TOO- SMALL
ir i
}2#t WHEN S23A CLARIF COMPLETE WASH DV (S4)
!
i 1 LINES PUMP 6 PRESS FOR 20 MIN OR TO A -CR ! I f TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT f
1 I WHICHEVER COMES FIRST, COLLECT WASHINGS IN'!
DV (S23) RECORD: STARTJjMjtfjtXLJSLC-OR+ > I
WHEN S24. IS COMPLETE TEST DVCS23) ASSUME 33% |_______ CORD: KXj*fef_C+> TEMP.,,J&_( 40-45* F) i_______
WEIGH SULFAMIC ACID IN RUBBER BUCKET AND !
i
j^frffRSE IN - AND STIR'5 MIN,
. ! 1-5 {
2Wn RECORD: KI, MUST BE - & IF NECESSARY I
i
TOP-KI WITH SULFAMIC ACID
!___
i
AJCUKTO. 55? <1925 G) AT 40-45 DEG F
[1X330 1
i-COE
7-D 30-D 30-D
7-D
! ACCT i LBS i... ..... 1 i 42 i j 1 63 i
1------- --
57-A f -44.6
725-A j ____ _ 57-A 1______
1 395-D [ 15 '
ii 395-D ]_____
57-A [______
260
N 33" <3300 G) WATER INTO V-260
.1
I
8
WHEN SI 8 STIR COMPLETE, POUR IN SODIUM
\/
260 10
! PjdYDROX-lDE IN 3-4 MIN,
ASSUME 50% [ 320
}3*THEAT' TO 128-132 DEG F AFAP & STIR 5 MIN TO i
-[ I DISSOLVE, STOP AGITATOR.
L
------- ----------------------------------------------------- --------------- ---- ------------------- ---
--------------------------------- ------------------------------------------------------------------------- --
133KT IMMEDIATELY 'RUN V-fflk AFAP INTO CV7*N0 ;
!
*1 AfrJWimON IN CV, RECORD: STARTJLUwftjT ' v !
e*AT' TOTAL* MIN
!
[3*7<r .RUN IN ACETIC ACID THRU METER SU!R 5 MIN ' m............................... &&*.%
RECORD :
10.5-11.0)
ASSUME 50%
[ | I NECESSARY ADJ TO PH ,10.5-11.0
SCOR'D: PH,,.Z0'.1C
ASSUME 70%
13
i --. to
7-D { 160 f i!: *
30-D ] 218 7-D I.........
30-D
Wwffirwrrr*nr r nri iri n^iyrr.
') f
73-82 DEG F AND RECORD:
i
?J*__DEG F AND REC_.J`:CLJ,..,_.DEG F
I
WHEN Swr'COMPLETE, COUPLE DV UNDERSURFACEj i
IN^-70 MIN. 41AIMIAIN CV AT 78-32 DEG Ft l
RECORD: STARTNXJ^r?2fTOTAL MIN ~70
t
N
STIR 5 MIN, DISCONNECT TRANSFER UNE AT CV i
i & RECORD: DIA.ZO_________ <3fcr_. <+A"26t.
I
J^FftSE ___ (MUST BE +) PH..?lv_7.Y<4 - 2~4.6)
I
f4H IF NECSSSAeXSTIR TO " DIAZS -RECORD:
I
i ' 1 STmTgfcJ&JZzL., TOTAL MlN^/iC?___
!
i J RECORD: DIA20
v* | j
BASE
% PH
_ MUST BE MUST BE + (4.2-4.6)
I :i
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DUP050061197
EQUIP I < NENf
HI SC '1 1
260 12
NAME : 40RT53TDMP
PAGE 03
DATE PRINTED; 8/03/8;
USE i
t ACCT
OF CG 40 CODE RT-53.1-D (P-) | LBS I N-CODE f LBS
ADD 30G WATER AT 130-140* TO DRUM FROM HOT
I | ' 43 | 567-B | 43
i W&XERJ1IXER ADD 'BLANCOL N &STIR FOR S43 ,1
f
|
IN N-S67-B SOLUTION FROM S42 HE^WP TO 194-196 DEG F ' IN 55-60 HIN AW "RECORD: HT^g_.^.__DEG F AND REC/^fCl_DEG F
WHEN S44 HEATING COMPLETE, RUN IN ALUMINUM SULFATE" SOLUTION THRU BADGER METER* NOTE:'
[NSE.IN. LINE AFTER N-115-D SOL 'N RUN IN*
:R 30 MIN AT 194-196 DEG F 'FLOOD TO 8" (7928G) AND STOP AGITATOR
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