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; , CR 456 ,^CO|E YT-562-D PKG '-':felJsi^I-KgK4a--
< DATE ) :
(LOT NUMBER)
c9'fHS E$T. WT. SSai^ LBS *
P'EEPARAT I OH NOTES:
PROCESSES < > YT-5'62-D (P)
APPROVED BY: EWK 12/23/81
COMTYP JOB . NAME: 50YT562DMP 7J STANDARD HRS. _______ TIME ^MCJ1*
EQUIP MENT
IE: GREEN GOLD
IN 2,4 DIHYDROXY QUINULINE FOR. OBTAIN P-CHLORO ANILINE FOR S 9"
RUN 3?" (2*63? G) WATER INTO V-2S3 &
HEAT TO 85-96 DEG F-
DUMP 4,:- RINSE IN 2,4-DIHYDROXY QUINOLINE
FROM SI /jj
NOTE
.ji.# .<V9J
100%
--Art5f*1*?>--
.JjSUm.*
WEIGH AND
RECORD ALL
N-44-C
NON-BLEEDING
*"*** ~~ ss *
I USE ( LBS
# ACCT N-CODE i LBS
44-C I ' 613-C I
J? / 7
44-C J .1186 i l
*DUMP IN SODIUM CARBONATE ADJ TO 54" (2836G)'AT 35-96F A STIR TO SOLN
>/ i 8
EjLPT 17 " (595 G) WATER INTO v-_X/2:_
iUN IN HYDROCHLORIC ACID FROM' V 32%
M,, _____
[EAT TO- 68~72 DEG F &
FROM
NOTE (1) THE RESOURCE CONSERVATION ,,OT
RECOVERY BILL HAS CLASSIFIED PARA-_jjtl[____ |
CHLORAN ILINE <N-613-C) A HAZARDOUS,__________ j
WASTE MATERIAL. THIS REQUIRES
____________ I
EMPTY :N6i3U CONTAINERS TO BE GIVEN 3 WATER [
RINSES WITH \135-1 45# F WATER FROM HOT WATER I
MIXER INTO DV- BEFORE DISPOSING.
I
NOTE (.2) H-613-C IS EXTREMELY TOXIC DESTROY!
RUMS PER STANDARD PRACTICE
j
STIR 36 MIN OR LONGER TO DISSOLVE FOR g
RECORD: START..,
28-D 61 3-C
0011151982
:
--f -
RUNS <98 G) WATER INTO V_.4<tEfi?-
INST AL
STfP CHARTS.
WHEN S 6 STIR COMPLETE, RUN IN DV THRU
SCREEN
616 8?3
V
DU P050103893
MAKING' TUtTROCfIONS': BATCH" UNIT
EQUIP HENT
ii- 3 CG 56 CODE T~562~D
I USE CP) | LBS
N-COBE
a 5c t LBS
WHEN S 1 STIR COMPLETE, ADJ TO 58" C20OG>i <f
|
,| AJ*5tS~60 BEG F. ICE
j 4x33 I
SIPHON IN IN 10-12 MIN, SODIUM gTRITj^^ } ^
/(|
5 MIN 6 RECORD: KMUST-?! + l_ZZIIIl
STIR 3 MIN P,T%6~12 BEG F 'MAINTAINING
[
[
+CR, +KI FOR S 2T0. RECORD : TIME STARl/^^ I_________i
CR_afc=__< + ) KTZ-kr?-.___< + )
"1
1
NOTE: M) IF CR-, KI~, ADD 204 "AS IS*
1
i
INCREMENTS HYDROCHLORIC ACID RECORD: CR ;<+.), KI< + >
ASSUME 32%1_________I
__Ja >
I
(2> IF CR-:-, KI-, ADD 204 "AS IS" INCREMENTS[
i
SODIUM NITRITE
ASSUME 33% 1________i
RECORD: CR _____< + > KI_________ < + >
|i
57-A f%%]?_
I 72 5-A
725-A
481
57-A
28-D }_.,
725-A
RUN 15" <760 G 5 WATER INTO V 283 & HEAT TO 6~B& DEG F W IN NICKEL SULFATE 6 STIR TO DISSOLVE
SIPHON IN IN 10-12 MIN 6 STIR FOR S 29
I AMMONIUM HYDROXIDE
!
1033 561
707-B i 22-D
1033 561
i WHEN S 16 STIR COMPLETE, TES
6 RECORD:
I CR<+ 5, KI,,TL_<+ >>, TEEMMPP.././.Jfe* (60-72*F ) 1.
i 1NOTE: <1) IF CR~, KI-, ADD 204 "AS IS"
I
i I INCREMENTS HYDROCHLORIC ACID
ASSUME 32%'}.
j } RECORD: CR ___<+> KI__________1 + )
1
i | (2) IF CR+, KI -, ADD 204 "AS IS" INCREMENTS}
I I SODIUM NITRITE
i ASSUME 33%!.
1 J^-RECORD: CR JXZ^z. I+i KI_.Tl-_T-LD.---Z/
1
SETTLE 15-3.0 J1IN FOR S 23 .|@
/
|
i - I RECORD: ,, Jl * DV, $\Pm J&Jz Zj T
I
ADJ CY TO 82-80 DEG F AT 42" (4074 G5
RECORD: HT
F & .REC^2l___F
WHEN S 21 SETTLING COMPLETE, COUPLE DV
UNDERSURFACE IN JJD-70. MIN
ORB : STAET__J/.a>l., TOTAL MIN,,/j^____
RAIN IN DV 5 MIN h WASH IN LINE ONLY
STIR 30 MIN, 6 DISCONNECT TRANSFER LINE AT
RECOIMRMDE: DIADTIAEAZLCYZCr-L<r<.--)) ,, BASE___lt_ < + ) ,
PH_._jfLt.fU_ < 8,9-9,0)
1<1) IF DIAZG +, BASE -, 6 PH BELOW 3.0
(A) ADJ TO PH 8,0-9.0 SODIUM CARBONATE
(B> RECORD: PH___________
<2> IF DIAZO+, BASE-, 6 PH 3.0 OR ABOVE
(A) ADD 104 100% N-44-C TO A 55G DRUM
2,4-DIHYDROXY QUINOLINE
<B5 ADJ WITH WATER TO 0,~> 25 G '
(C) STIR TO DISSOLVE
<D> POUR INTO CV
I . (E) STIR 10 MIN
1(3) REPEAT U> & (2) ABOVE AS NECESSARY I TO - DIAZO, + BASE
3-A
___j 44-C
' V' hk
DUP050103894
eq u ip
KENT
MAKING INSTRUCTIONS:BATCH UNIT
PAGE 3
USE 50 CODE YT-562-D CP') i LBS
"h -c o d E
AC~CT LBS
yEAT- TO P&IBj^-DEG F IN_32-38 MIN STIR 20-25 MIN AT 17#W$fUl)E& F, DURING STIR WASH DV TO SEWER RUN IN_ V 2S3 IN 20-25 MIN MAINTAINING
'STIR 5 MIN & RECORD: "UMP IN BARIUM SULFATE STIR 60 MIN AT jf-Tligg DEG F
e ^?"* f
(?*8-8,8)
/So^x
/ /LS>
STOP-AGITATOR
TAKE i QT SAMPLE
S 33
V-105
V-i S6
94" 96 s
GAL (91 ?4G.) ( 9322G)
V-i 0.0 S3"
(S250G)
V-1S2 84"
(8300G5
START/i
FINISH
iiMr^ limm
QPTJ
SUPERVISOR NOTE:
<1) IF DIAZO + AFTER IMITAL COUPLING 1S26)
ADVISE PROCESSING TO: (A) LOAD IN DRUMS 8 3254- NET AS PRESSCAKE
TAKE 1 QT SAMPLE, DO NOT DRY, (B) HIGH PRESSURE HOSE PRESS AND BOX AFTER
DROPPING BEFORE FILLING NEXT BATCH,
SUPERVISOR_______________ _________ ________________ DATE_____ ___________________________
DUP050103895
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DUP050103896
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DU P050103897