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AR R26 -- 1193 JULY 2002 SURFACE WATER MONITORING REPORT FOR WASHINGTON WORKS FACILITY AND LOCAL, LETART AND DRY RUN LANDFILLS WASHINGTON, WV Date: September 2002 Project No.: D6WW7423.01 18983635.20000 `CORPORATE REMEDIATION GROUP DuPAonntAlalniadncUeRbSetDwieaemnond BWairllmeiyngMtiolln,PlDaezlaa,wBaurieldi1n9g80257 SONTBIN NE OR = 85 } =-- RECEIVED SEP 23 gp, ELeuTony prog 000243 Surtac vate Monitoring Report TABLE OF CONTENTS Tableof Contents PX oRFUTLY TERT OR ---- J 3.0 Washington WOrKS FACHILY .......cccoorsuummmsmssssssssssssssssssssssssssssssssssssssssssssessssssnd [XJ 5,72 SR F071 OT 7.0 REFETONCES corr -------------- nnn] Table 1.0 Table 2.0 Table 3.0 Table 4.0 Figure 1.0 Figure 1.1 Figure 12 Figure 2.0 Figure 2.1 Figure 2.2 Figure3.0 Figure 3.1 Figure 3.2 Figure 4.0 Figure 4.1 Figure 42 TABLES C-8 in Surface Wate--r Washington Works Facility C-8 in Surface Wate--r Local Landfill C-8 in Surface Water -- Letart Landfill C-8 in Surface Water -- Dry Run Landfill FIGURES Site Location Map-- Washington Works Facility Surface Water Sample Location Map -- Washington Works Facility C-8 Concentration Map July 2002 -- Washington Works Facility Surface Water Site Location Map - Local Landfill Surface Water Sample Location Map -- Local Landfill C-8 Concentration Map July 2002 -- Local Landfill Outfalls Site Location Map -- Letart Landfill Surface Water Sample Location Map - Letart Landfill C-8 Concentration Map July 2002 - Letart Landfill Outfalls Site Location Ma--Dpry Run Surface Water Sample Location Map -- Dry Run Landfill C-8 Concentration Map July 2002 - Dry Run Landfill Outfalls ewes an 08 000444 Surace waler Monitoring Report Table of Contents Appendix A Appendix B Appendix C Appendix D Appendix E Appendix F Appendix G Appendix H APPENDICES Laboratory Analytical Data Reports ~ Washington Works Facility Chain-of-Custody Records ~ Washington Works Facility Laboratory Analytical Data Reports ~ Local Landfill Chain-of-Custody Records -- Local Landfill Laboratory Analytical Data Repo~rLettasrt Landfill Chain-of-Custody Reco--rLedtasrt Landfill Laboratory Analytical Data Reports ~ Dry Run Landfill Chain-of-Custody Records ~ Dry Run Landfill Waneiglwone, OsF e mz 000445 i `SurfacewaterMonitoring Report Introduction 1.0 INTRODUCTION A`WemsutlVtiir-gmiendiiaaDceopnasretnmteonrtdoefr (EOnrvdierronNmoe.nGtaWlR-P2ro0t0e1c-ti0o1n9()WwVaDsEPen)t,ertehdeiWnetostbeVtiwregienniathe DepartmentofHealth and Human Resources ~ Bureau for Public Health (WVDHHR- BPH) and DuPont on November 15, 2001 (Consent Order). The Consent Order identifieda series ofrequirements and tasks to be performed by the parties to determine `whether there has been an impact on human health and the environment as a result of releases ofammonium perfluorooctanoate (C-8), CAS Number 3825-26-1, to the environment from DuPont operations at the Washington Works facility and the associated landfills (Local, Letart and Dry Run). The Consent Order established the C-8 Groundwater Investigation Steering Team (GIST) to oversee investigations and activities that will be conducted to assess the presence and extentofC-8 in drinking water, groundwater, and surface water at and around the `Washington Works facility and the Local, Letart and Dry Run Landfills. An additional componentofthe Consent Order relates to the National Pollutant Discharge Elimination System (NPDES) permit sampling requirements. In this portion ofthe Consent Order, specific outfalls and outlets (outfalls) are to be sampled monthly for C-8 by DuPont. Pursuant to Attachment Aofthe Consent Order, three tasks will be performed by DuPont and evaluated by the GIST, Tasks A, B, and C. Task A: Groundwater Use and Well Survey/Groundwater Monitoring has been completed (DuPont, 2002a; 2002b). Task B: Assessmentof Existing Groundwater and Surface Water Monitoring Data includes the compilationofhistorical C-8 data, monitoring all wells at the landfills and the development ofa Groundwater Monitoring Plan (GMP) for the Washington Works facility. The first partofthe task, the historical C-8 data compilation report has been submitted to the GIST for evaluation (DuPont, 2002c). The second part of this task, `monitoring C-8 in groundwater at the landfills, began in December 2001 and was performed monthly for four months and quarterly thereafter. The third part ofthe task, the proposed GMP for the Washington Works facility, was submitted to the GIST for evaluation (DuPont, 2002d) and groundwater sampling on the Washington Works facility began in January 2002. Groundwater sampling at the Washington Works facility was. conducted monthly for four months and continues quarterly. Task C: Plume Identification/Groundwater Assessment is ongoing. This report presents the results ofthe C-8 sampling that was performed in July 2002. Surface water results are presented for the Washington Works facility and the Local, Letart, and Dry Run Landfills. fo 000446 i SurtacewaterMoning Report C-8 Analytical Reporting 2.0 C-8 ANALYTICAL REPORTING `The has analytical method, changed over time. method detection limit, Prior to 1991, DuPont and laboratory performed C-8 utilized analysis for C- analysis at the DuPont IEnxvpeesrtiimgeatnitoanlwSatasticoonndiuncWtield,mitnhgetaonna,lyDseilsawwaarsec.onItnra1c9t9e1d,twohtehne CtHhe;MRHCiRllALVaebriofriactaotriyonin DMeotnetcgtoorme(rGyC,-AElCaDb)ambaa.sedBoatnhallyatbiscaulsmedetahoGdaswiCthhrodmeatetcotgiroanplhiym/iEtlsefcotrrCo-n8Ctahpatturraenged from 0.10 1.0 ug. CcHea;sMeHdiolplercatoinodnu.ctAetd tCh-at8 tainmael,ysDiusPfoonrtDuhPaodnctomipntloettehde foanlleorfou1n9d98ofwhaneanlytshieslfaobrotrhaetory LRaCboRrAatoFraiceisl,itLyaInncvaesstteirg,atPiAo,n f(RoFrIt)h.e RTFhIesaenacloyntdicraoluwnodraknawlayssitsriannsMfaerrrcehd t1o99L9a.ncaster uLnatniclaOsctetrobLearbo2r0a0t1o,riwehsecnondteivneuleodptmoecnotnadnudctteCs-t8inganwaalyssicsomupslinegteGdCo-nEaCnDewforanDaulyPtoinctal u`tmieltihzeosd LdieqvueildopCehdrobmyaEtxoyggreanphRye/sTeaarncdhe,mIMnca.s(sExSypgecetnr;olmoectartyed(LinC/StMaSt/eMCSo)l.legDeu,PPoAn)tthat adopted Exygen the was regular use contracted of LC/MS/MS t0 perform the for C-8 analysis in water analyses for DuPont. in November 2001 and aErxeyegveanluraetpeordtfsoCr-p8rerceissuilotns bfoyrctohmeplaarbionragttohrey frieeplldicsaatmeopfleearcehsulftioeldtshaemcpolrer.esTphoensdeinrgesults laboratory replicate result. Q sIfabmoptlherfeosrultthsataraenalleystsetihsacnotnhseidprearcetdictaolhqauvaentpiatastsieodntlhiemiptre(cPiQsLi)on, ctrhieterreipal.icate Q cfoonnsiedeorrebdottohhraesvueltmseatrethbeeptrweeceinsioonnecraintderifaivief tthiemetswtohreePsuQlLts,dtihfeferrepblyiclaetses itshan the PQL. Q dIiffofneererdesbuyltasvalleuses ltehsasntthhaenPtQheLPaQnLd,tthheeortehpelriciastneotis, saanidd itfothheavtewmoertestuhlets acceptance criteria. Q tFionhalalvye,imfebtotthhercersiutletrisaiarfetahtelreealsattfiivveepteirmceesntthdeifPfQerLe,nctehe(RrePpDl)icbateetwiseecnontshiedetrweod dreisfufletrsenisceloefsts wthoanmoerasequuraelmetont2s0%di.viTdhede bRyPtDheiisrtahveeraabgseo.lute valueofthe f`iWehlednsatmheplpereacnidsiloanbcrreitpelriicaatoeutrleisnuletdsarbeopvoertaerdebmyett,heElxaybgoreantorreyp.orItfcsrtihteeraivaerfaogreporfectihseion warheeenxcoeneedereds,ulEtx(yfgreonm rtehpeosrtasmptlhee/hliagbhererpolfitcahtee psaaimrp)lies aabnodvleabthreepPlQicLataenrdesuolntse.beFlionwal,lyt,he rEensvuiltrotnhamtenitsaalboDvaetatbhaesPeQ(LCsEDi )raepnodrtaerde.reCp-o8rtreedsualstsFCar-e14r3ecoforrdecdonisnitshteenCcoyrpwoirtahte historical results. WWimengioen, OsF eme 008aer--; SSurfau ce watter onaodncg ReoportwstervontoWiaWasshnhiinngggttooRnnWWe oorrkkpssFaFoacciilltiittyy 3.0 WASHINGTON WORKS FACILITY Fouitgfuarlels1w.0ersehoswasmptlheedlofcoartCi-on8 o(f00t1h,e 0W0a2s,h0i0n3g,to00n5W,o0r0k7,s afnacdili1t0y5.).OAnllJuolfyt2h3es,e 2ou0t0f2a,llssix collect process water and stormwater runoff. Samplingofthese outfalls is required by the Consent Order outfalls are shown and WV NPDES in Figure 1.1. permit No. WV0001279. The locationsof these. `liTsatbeldei1n.0thpirsotvaibdlee,shtihsetoCr-i8calandaaltyatiicsalsurmesmualrtsizfeordswuirtfhactehewamtoesr.t rFeocrenctarcehsuslatsmpllsitnegd pfoirisntt FLiagbuorreat1o.r2yparneasleynttiscatlhedaCt-arecpoonrctesntarnadtitohne mChaapinf-oorft-hCeuosuttofdayllrescaomrpdlseadreininJculluyd2e0d02in. Appendix A and B, respectively. Teweesd s SReEe 0000448 IE 000449 TABLES 000450 0917/02 Table 1.0 Summary of Analytical Results: C-8 in Surface Water DuPont Washington Works Facility Washington, WV ome CUAL007 COTE | COAL Tow meTeam ww [-- omeee7-- -- p--e] er m Coommmee T e sm se I [ ome-- e -- e a a-- mr C" a oser s -- i as e-- [ oomseeme aaeneee m [ masem r e o ae r m meer m oi o }| [m m m emoT e e os mes ame [omme e Ta om mr]| -- ase-- T -- e -- Co omes 1e m ] [m [ [ mmm r es e oae wms ] n I emmeT -- e--; aaemmoer wees [ [ mev er m oressso e me s eemen see e Se r aw } ] e emmeor e ae ] e e ame e w an 1of2 000451 Table1.0.doc Table 1.0 Summary of Analytical Results: C8 in Surface Water DuPont Washington Works Facility Washington, WV [spe OUTLET 105 Note: Analytical method T T b cowon | ew Tos [easoo a z| SeveToa nee Tose [eeeToms | Tsoe m | [s | o os e [mzTos [amoor Tis | ewe TR eas Tae [s 1 mo6o r z| wee T7550 we15 ome asf Ee emoor 1 ers changed as of November 2001 (see Section 2.0 for deta). os/t7i02 000452 2012 Table1.0.doc Table 2.0 Summary of Analytical Results: C8 in Surface Water Local Landfill Washington, WV CeCHTPe ALL OOF ToT w] w eo Te r m; ------ C7 o omwe -- 5 rars] -- CTPA Tr wemee T ia se ] 77 ---- ame r-- -- v-- m 7 me-- e -- a e x--e STALL GE FE TS C[ [ owiC eo 5 o m 5 e--e s ----] i [e -- a--r [amreem [ F mz| i --coS hoonofnowdT canoton-- ss----]] 7 me EX ws-- I I-- -- ------ -- re-- -- -- Cam7e-- -- --1 ---- we--= -- owe si] CoTET ToT [m [ m rv C -- o n-- sm| 1 seer ---- [ ameo 1 e % s oommeer swso [ Im -- en -- --a [am I mor--e --5 s -- [o7 ma -- -------- --) Ce ome m Tu] Note: Analytical method changed as ofNovember2001 (see Sectio2n.0 for deals). 000453 osrt7i02 Toft Table 2.0.doc SummaryofTAanballey3t.i0cal Results: C8 in Surface Water Letart Landfill Letart, WV SS S 7 T TT --meTT a0 S.C-- f----msawoeT 1 a ew y| NS |---- ise f--tese TT aes sr zorTee --hzmssot moot Ts [--Tes2000Tas] --dmz000Te --neooeTeo ome 1 sao | meeTFloo wConaibons ---- szw0s z TT s T NTotw anoao e ize z s"| moe TT oes ase Toe RT 33 STREAM. E [e T rS Tom X -- | ssw Ts f----Ta T ma ones oz emer Ti 7SI -- ese a |--Fromoor 0 mio Toss [me TTTr aes 1A I -- {wees Tis [ses --T otAnanzes f--ssoerTam | meeeTae [zs TT WoiSampied | CT Iwesee7 er Te = 0 Note: Analytical method changed as of November 200 (sce Sectio2n.0fdoetails). c+ oSaaurprlheesiswaeemperlet,sakeanmiavtehdetrthee asb wpsaurrmefsacncedwwaettreeiolooctvatailoeynzse.dH.owever,duefoan eror by the os/t7i02 000454 Tot Table 3.0.60 o9n7i02 Summary Table 4.0 of Analytical Results: C- in Surface Water Dry Run Landfill Lubeck, WV. sme TwTam OUTLET 001 OUTLET 003 see7S TT hT e 0 -- | ES E-- ese Te mse ----mme Ee T aT s----------| ----i2n Rofi2 owcond0 ions r -- zeo e T m TT a e aio s e 0| --snaiessTq _amnoosTes1 mee Toss --------] I 1S S-- | =O XE -- mee Te 2250 9280 TT Notiow congiions TT No lowconaibons | | "OUTLET 004 neeTo --e I mm Woiow o conditz ions| [ S804 T TT m NNooflloowwccoonnddi2 ibtioonnss || eso 17 5 2280 TcT onNd ofi owtions| 7J 7 -- PROPERTY BOUNDAR[ Y mm32o 1207T 17 e Noflowcondita ions | mmesee Ts me e| soz TT se mez TT emoTse f--[ jeaz goosE 1 s 0 n3 3e s--e --s1| nares Tom STREAMSAMPUNGPOINTAT I__aonessTo | spwop | 165 1 emerTom EmerTee immsmeeTo esee| f--iznzo Te [----joaan0g0e0sT T 07o 58s| STREAMSAMPLNGPONT#Z |__shonsssTy | Soap | sip fE --smT wezE Tass T -- -------- mee 7 S-- nao [oma 26s ars [[ --zaes nesh s1 T en r e as ss| 000455 102 Table 4.0.doc Table 4.0 Summary of Analytical Results: C-8 in Surface Water Dry Run Landfill Lubeck, WV [Swe 1 dme TT Coen | [Smee Tse [spw ayea Teese Ts ease os [meee1508] ana ee [omeooe 127d [ozenees Ts [snanses [56 [reer |e] POND UNDERDRAIN [ awsem merea e [eso 1667| TeeseTors mmo Res Note: Ray Seal method ha3nofgNoveeambdmearr201 01 (sc Section 230 f5or4demi). 7] 000456 oan 202 Table 4.0.doc 000457 FIGURES 0003158 , BEL. Fn EB o ee Pt i poi 2 TE SU pe ) CTT / Sa WASHINGTON WORKS FACILITY eeSe 4 i ' RTaEwEarN\T-- Te : : gcpmasse RIVER es LY Ce" ny a o N SW B4 -- on # ne Aa Lag en msTe whe % oo fo -- oF LerEeuEenRsSV / . sLood:Si r Fin, ialND WANSWwW By . & a 0 en :J3 o.H . LLUs BE - BERR . C.: K, ' oe;. : 4 Wortia: Ln ~- am & SITE LOCATION MAP open USGS QUADRANGLE. Corporate Remediation Group | DuPont Washington Works Facility a| to fomo, daton [e Eeg mee TE Simon: Dinars 13605 FoeGouzde. Lo . Lanaon / wee E ~9 : ite ANNES TE See, Nou i ee scate ee) 700 0 700" doP pe oO rer Ee [Co| ws| CT] mrss Somers =] Corporate Remediation J Group SAMPLE LGCATION wae [ouPoWnetshWiansghtionn,gtownestWorvikgsinFiooci| 000460 - i hspeerm a -- : =5 i Ne SCALE Eee fp e] a ==] 7] 0e 0 l00 csm Corporate Remediation nl tr Group ammosserny [DuPoWnatshWiansghtionn,gtoWnestWorVkisr.gFinaicaility ETSY CE tra ES - oo ; --_ oo . 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NN id U% Sol i i Kero) 000466 ENG a) as No lhit ea EN A= / 7 \\ i 00046; rs Tree ma 000468 r j 0 VAeN ) : } = o /{ go we 5 A " mA a0 g8 \ \ QR : = K i g Tu (E==N ruise NE NNT i ; it lf S$ -- . rons i$ il ile lq? WET FiEr LE i i F ad APPENDICES 000470 APPENDIX A LABORATORY ANALYTICAL DATA REPORTS WASHINGTON WORKS FACILITY 1! XY8 ESEARCH Peper Ars ese Was Vie CO Sarg TE Dupont Sample entiation aero oot) YJ-- r zio-- emee ne oe22 e2=so ete YSEozuor, ine Outabs w=pni 3 Link of Detect (00) rth process pointy 10751 Lint of Ouariaton L0G) or hs prsodive is 50751 J NQ Compound dot at aleve betwen 1 LOD nd LOG. Fs et cst Ni Rests se cca scaring he loing (tPDms)stampeeleerann aerencupas as grrcetrtan222800ggl.aand ltelt porreeaftrre eSescammepreaon briy cCptwse fseseha22205 51,aaro hsolabsstiforrrocnonien 000472 Xe _Ron. 0007 BHER APPENDIX B CHAIN-OF-CUSTODY RECORDS WASHINGTON WORKS FACILITY 000473 z9 NEE|OE) EL f EEENETIE> PT5T3) | 2I I 108 Lote 3 g Ehls|2 o 3g) TF Se | Ela |B ic Q LFEE2 IEm EE1R2 EIS mmr if[[2]Ew 2h biFbTFlEEeEHEH OSne [|S2hE LEFLE[EEiH oimm [3B FEhk 2 (T S1 C Ful SHE BERR | it BSTlEaEdRe Tat [O LL 0[J0 e1]1|22 TrebrrreEe F E235221) 2Sl2i2 oy BERG aR AHHH] ETRE Nn TE EEE rl ZR SEE PPE il EAN ERY R[EF Feliit s= Hed] Ty 2N S N REET fiof ~3 Be nenh e : SEELREFNE: i2E frEdtoeh 3t iH BBEE iv ooooooE Bf F FT E = RJ ; lSlgfereeeeeesrss| MSOf FRFPRRRAToH H.C BI Esvtebeyd SHP I HOT HHFl & 28 BHIEFE ERRE ERFTo eo s MW!Hf S2 0009 APPENDIX C LABORATORY ANALYTICAL DATA REPORTS LOCAL LANDFILL 000475 E en XYE ESEARCH FrecPhreovReenseReasruclhts. a Analytical Results Local Landfill C8 Sampling 7/02 DuPont Sample Identification APFO (ng) LOL-K-QBLK1 238 LLCCLL-ZZ--OOuuttaallll 000044 ONledwWWeessttSSttrreeaamm 1111280000 LLCCLL--ZZ--OOuuttaeltl100015 Old Central Stream 3623100000 Limit of Detection (LOD) for the procedure is appoximately 10 nglL Limit of Quantiation (LOG) for the procedure is 50 nglL. ND - Compound not detected NQ - Compound detected at a level between the LOD and LOQ. Result is not quantifiable. ND <LOD <NQ <LOO Results are calculated according to the following criteria I the sample and laboratory duplicate are greater than 250 ng/L, and the relative percent difference v(aRlPuDe)isisrleopsosrttehda.n 20, the average value s reported. If the APD is greater than 20, the higher 1 the sample and laboratory duplicate are less tha 250 ng/L, and the absolute difference is less than r50e,potrhteedaverage value is reported. i the absolute difference is greater than 50, the higher vale is 0007 000476 Soneencth OKVveeaon, usa L8`1ee4n2ag72c1ro0n0)0 APPENDIX D CHAIN-OF-CUSTODY RECORDS LOCAL LANDFILL 000477 . Ke10O 3 {E NgY IT7E3 ioFFm r 5 TEE EAE gl ] : 3 9 a Zl l9a 2 EEE HY 22 :3 :ig RRERE:H2B g = a SH iEg > | :|i {E4 TE tH :- je Zoe| 18 i TTHe eo RTE iniiiriflig iFS|g 3: :| [Es HE : 3 ; 8 : i: 2% 2 H 1H[[[Hl] e i T)/5 8 F 8 if:xr [I les]al|iW Hs1 lg "| EEE [ Ii BE bso EaLt; he= olbe ERS Bik C mE l gr5i5s5gs5t2s8di: ZHHz g 2ic:iz =H y 509 E HF | : 3 : i: A ! g i: i2 :2 LA;gs | - 3 ir F:X p| HE], ; MA J F uH H l H -- fi: .0 HfIz3 Er =-- g (TeT er T 0009 : IS [Si=g "wm 3 Ikii I |FE2 2aI |H|P EZ dR % a 5 BBNIglSo a E DEh E Gales LlaR Hide TR |S 2 HE EES 2 |(i 32H: izmzTER f $ (E LITRE SB is AEE (TARR HgQa |3S SER LITTEE |[if] RE iass C T Te Teer]|1)22en 5sf:BgEsE: 2Q2 [| [emer] HEE] : 3R BiE g0 EgTARiNSlo FH `Mig a E edC i 1 3 N F 1 RYNiEll H iBi S [{ReEa HE i2aa S FooRoEcoEoRp CIE HH [T TTTI TTH NT Zr/sT cmmme, N"pm 5cH5mC SoEEg RA AH MH ETI INTF HE =--=--g == 8 ff HOTOerTEHI 2 0010 z1 oRhS gZd| gBk agZsz ES g c0 BaL 3n H 8 a Bil Tfdaiilnoeenso LFoiHs aIeis A i is] dS pee i ES FE |. [rn 3F ef T cH A mTT E|F) is B > |t||FPRNEE 9 N *Z2I[E 2 H {PRS E BH ESem PRE |S 3 || BERR 2 LIER 1] Mise & R l(LiUmE )|: |f]c [TTT H [TTT TTTTMemEoRemmS]ie] 3g Ih fii 1|223 3 30: C (5152 253)| 22z1n1 8 =5 WES BMEEF FRIGNINE SE File IRD NEN: HE IN BA HEHBERSS T2S AT lEsitg 3fll HbiEl iE oooooog glggezzrd 2 IEEEZS & Eeseecsf i 2 Ff HON Aw cHEmS =H HTT zeese EM HOT = B< 3, g oB f I I H O [ "HI % 3 HOE H LTTE Zee. H [2 ee gor] < ' TG EINEESsf L FUHE TTIEETS EES || -e237) 2Hon YG | :g tl) m20 ole |f Ff1i>m [|E= tH RLeRpRPEEHH = Coc REE|I>Z ||g2 F WERiTHH 2cm Nel"--o\ 2Fl 2 b fElga |8 Bk SKA x= a RN o wa 3 3 =< [eB $ LN. BTlEoEg fll uN BSi RS ih fas 1I TTB Js i [O TTTe en 2(i2e9s 5) | aEli EE ee | F 2 anG BE 3|PPnb RFRlRE3 WETo $IED Lhe li: = RE EH N : Is 52 if { L HSEs ) 2 iLinai:s EIRE P E2 BE iLI p 3 ERi 5s FREE 282208 Sg glll eesse ieeie cisz loerred Ff 2 : [E-- E- FH [I h sI r reT me ]BH C siegHMC H [ HH ( OO H -- T fblzHC&: HHH eeewer [= RT amT S 0012 : 9BiA E2nN FFSITRTRESwv | 2o7m5 sf I BH4 NEeP ZZ dAdd g s = 5 FLIPS B= =H[a f:H g g ea cSloE|HEd RREAS H Ee = a LLG Els |: fs RE Heth fBE e BERT |S F5 EEg TR v SL i ILTEEH [51]: RiEas EE iE CI ikon Kee |2 28 3) 238 [comper|e | Eu B| | 3 MET B A 4) i: Cenhes|| 5 51 a5 o ch ERTIES b aSAhE EFH ) II> Hss s | Head PH N gs RAersesM:i: <CO {ais 2 Ll Sia ifeth eisd @ Mii 3d2 f sNl:NE il Ei:D22 tei3 8 8 8= [Hrgetss 5 S ghlkPEN FS :2 das: A : HE coooooE geeesff BBE) ER I TITJsT wemeeIeINHB ga5 HC Ssthriepn eg M I o Tr IBF gO J g sibs CREO OE HITE mae, HHEI: 83 2 BOT aes Ml 2 0013 APPENDIX E LABORATORY ANALYTICAL DATA REPORTS LETART LANDFILL 000433 E \tgeenn, Analytical Resulis LeTart Landfill C8 Sampling 7/02 DuPont Sample Ideniification APFO (nghl) LTL:Z-Outlet 002 LTLK-EQBLKA 14100N0D0 Limit of Datocton (LOD) for th procedure is appoximtely 10 nglL Limit of Quartiation (LOG) for the procadure is 50 nglL ND - Compound not detected NQ - Compound detectedat a lovel between the LOD and LOQ. Results not quantifiable. ND<LOD<NQ<LOQ Resuls aro calculated according to the following criteria (iRtPhDe)saismlpelses atnhadnl2a0b,ortahteorayvedurpalgiecavtaeluareeisgrreoaptoerrtotdh.anIf2t5h0e RngP/LD, iasgnrdetahteerretlhaatnive20p,ortchaenhtidgihfeirerance value is reported. 5i0,hethsoaamvpelreagaendvalalbuoriastroerpyordtuepdl.icaItfethaereablsooslsutthead2if5i0ernegnicLa.iasngdratahterabtshoalnut50e,dithfeerheingcheerisvlaelsuse tishen reported. 0007 000484 X= Bison, us ShHonH APPENDIX F CHAIN-OF-CUSTODY RECORDS LETART LANDFILL 000485 9 I =] gl I wo 3EE: Rol 2 i < FR RR EE2R | r ETH HH l 23HB <a g3 ET SE 2 SELEEES SRREIZ 2(E [EIER I E F R=RE E oMee stun &bl i EEIES 3(BSHBEER ER =a= NEO 3 Qo EIS [2h EE g FIRE YN P =< 2 S i iF TERE [51 Bes 2 PLL |7 2 2 $3 7 Bz TFA |: of CT hl, T E Ie E p R(|ieg i85 58, E2}: YE3S&2 41 NGRIE5 Teme] | 3FEISNh IgfS)SEREE FH S NS ALE I2 ERFpaLRhLeS :82sYC Fl k 2 RgSERIE adiBl ge : [sss[2 HIE 34 : HER iS[oles aEiht|p f[| o HIGH sk tl BE: BE: =2Wii5 C HR z z a 3 = HM ZU gx cogoeoeonoeorz8gy| BH1F9TT[ TOEH ET o =fu FH A|Pd 82 s| p BiH H T OO CT R, HS Sl Bll 0g5ineY HH O O mew E 8 H3Z i HB TENE ar] | 2 009 APPENDIX G LABORATORY ANALYTICAL DATA REPORTS DRY RUN LANDFILL 000437 X) sFooen. Precise Research. avait Fosut ry un Lana C3 Samping 702 DuPont Sere taps sero 0) Tzornaas: 25>20 it ofOotcton LOD) rh rca pint 075. Lit of Guta 100) or hs process 551 I 40- Compmdntntes aioe beget LOD EL RaSh BIS NT Route ro celoated sing te aloingtrs Sarain SRea, n wanes esa I the sample and laboratory duplicate are less ee ea tha 250 ng/L, and the absolute difference is less than 000438 X=Bion, ue 0007 eHaEm, APPENDIX H CHAIN-OF-CUSTODY RECORDS DRY RUN LANDFILL 000489 3:%[) BGeEl S>>29S :0 TSTA gL RlHT REe EERE1 S22 |[I =23 7&eT r 7C L.FB5E 2 H0BE! ren EH fe 3 arp 2118ls wcv PERLREL ES IiBRI ema. SN THER | oq SES 2 VES [CE HAHA E- F[2El< EH|: ssa81|$B wa THIEN: i ERE 8 FILER aC B: FE = aa m RERE 1, E D ee e ee (iiEodem 3T, iiThPleTe sel HER hDl n ples aH Lhht: ESTE 3 cocoons IH seepefd| sR ERR] EER yii S(3 RL E ETRE [F SIRF KE 5 A HE HE 1 ELE NER : K FI BE] 2 T TTH LN cro ime rBgH f|G gOhf ff CB jRrmemO eme--eT--T --"--H--MrlHl 0009 9 B&Q SETI ERR ep F EVERETT 23gl ENE 2=rlo gaa BtlZTe |:[2LR 3A| AEFRp RRE:EciH KF BE Rr i] 2H 2 HEAR 8 P a Tae dl 13] ER 1LSE Elz [2 RREIECHSF| lll 5H 0 LECH gEm PIS HY 5 fx Iki IIE [51] F 2 3 g 5 R 25 2 2 Usth re R B C i SeEeA ! e Cr= emeh l|H S 0 ferili#l fAoge ; k L TELNE ENIESBie mEYER sss LgANE i ' HEI HE RF Sl HA 4 Ik E tile- o 3E:E I SIE RER2TEQS E a gih : - H: PN iEp RS hese gr Bl 3 SsoeorcneonoyyHlof.ff Eee gE O [d II c= oI osTEB g52HS mB, 5 fii Fo HF; 1 0 HHH 0070 -