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January 28, 1972 ! AKRON FORMULA AK-502 NEW AKRON, NEW YORK, PLANT FORMULA DRYWALL ADHESIVE AK-502 DESCRIPTION - Drywall stud adhesive FORMULA Raw Material Water Calgon-T Ethylene Glycol Advawet-33 Atomite Limestone Clay BPG3 Asbestos SG210 Resin EB-12 Emulsion RA-315 Propasol Dibutyl Phthalate Water Acrysol ASE-60 AMP-95 Biocide 290 Function RK Spec. Solvent Wetting Agent Solvent Wetting Agent Filler Filler Filler Adhesive Adhesive Filming Agent Plasticizer Solvent Thickening Agent pH Buffer Fungicide 11 182 220 217 225 Percent Lbs./Batch 12.0 0.1 3.0 0.9 27.0 9.0 0.8 8.0 30.0 1.6 0.8 2.8 3.8 0.5 0.3 617.0 (74 gals.) 5.0 154.0 (16.6 gals.) 46.0 (5.5 gals.) 1398.5 462.0 41.0 410.0 (55 gals.) 1541.0 (173.0 gals.) 51.0 (7.0 gals.) 41.0 (4.7 gals.) 144.0 (17.3 gals.) 195.0 (22.4 gals.) 26.0 (3.3 gals.) l.S 100.0 5133.0 YIELD One batch yield 480 gals. MIXING PROCEDURE 1) Add water (first .addition) Calgon-T, Ethylene Glycol and Advawet 33 2) Add Atomite, Clay, Asbestos and mix for 30 minutes Add the following Ingredients allowing each ingredient to be thoroughly blended before addition of the next ingredient: Resin EB-12 Emulsion RA-315 Propasol Dibutyl Phthalate 4) Add water (second addition) and Acrysol ASE-oO (may be added simul caneously 5) Add AMP 95 Biocide-290 Lehnert 10.3.01-87 SGP 0016188 IV -tz January 28. 1972 AKRON FORlfelA AK-502. NEW CONTINUED VISCOSITY - Refer to Plant Testing Procedure No.'109 Specifications: 460 - 10 Brabender unit Brabender Viscosity 480 - 10. Viscosity can be adjusted by addition ,, of water, reduction of mix. water, or by addition of ASS-60 in small amounts. It is best to hold back a small amount of water to be added if the viscosity is too high. ASE-60 may be added to chicken the nix should too much water have been added. Should it be necessary to add ASE-60, Che pH must again be checked since ASE-60 is acidic and its addition will lower pH. Remember, changes in the water content affect flow properties as well as the wet density; WORKING CHARACTERISTICS: Shall extrude easily from tube and form a uniform bead chat does not sag oc run. OPEN TIME - Refer to Plant Testing Procedure No. 114 WETTING CHARACTERISTICS: Refer to Plant Testing Procedure No. 115 TENSILE STRENGTH - Refer to Plant Testing Procedure No. 116 ALKALINITY - Refer to Plant Testing Procedure No. 34. Adjust ' with small quantities of AM? Specifications: Maximum Minimum Average 8.0 7.7 7.9 DENSITY Specifications: 10.75 lbs./gal 10.65 lbs./gal 10.7 lbs./gal Case weight should be 35 lbs, l lb. ED0:elz Lehnert 10.3.01-88 SGP 0016189 August 15, 1972 Supersedes AK-502 Dated 1/23/72 AKRON, NEW YORK, PLANT FORMULA DKYWALL ADHESIVE AK-502 DESCRIPTION - Drywall stud adhesive FORMULA Raw Material Water Calgon-T Ethylene Glycol Advawet-33 Atomlte Limestone Clay BPG3 Asbestos SG210 Resin EB-12 Emulsion RA-315 Propasol Dibutyl Phthalate Water Acrysol ASE-60 AMP-95 Biocide 290 Function RH Spec. Percent Lbs./Batch Solvent Netting Agent Solvent Wetting Agent Filler Filler Filler Adhesive Adhesive Filming Agent Plasticizer Solvent Thickening Agent pH Buffer Fungicide' 11 182 220 - * 217 225. ;' 12.0 0.1 3.0 0.9 27.0 9.0 0.8 8.0 30.0 1.0 0.8 2.8 3.8 . 0.5 0.3 100.0 617.0 (74 gals.) 5.0 154.0 (16.6 gals.) 46.0 (5.S gals.) 1398.5 462.0 41.0 410.0 (55 gals.) 1541.0 (173.0 gals.) 51.0 (7.0 gals.) 41.0 (4.7 gals.) 144.0 (17.3 gals.) 195.0 (22.4 gals.) 26.0 (3.3 gals.) 1.5 5133.0 YIELD - One batch yield 480 gals. MIXING PROCEDURE -v * 1) Add water (first addition) Calgon-T, Ethylene Glycol and Advawet 33. 2) Add Atomlte, Clay, Asbestos and mix for 30 minutes 3) Add the following ingredients allowing each ingredient to be thoroughly blended before addition of the next ingredient: Resin EB-12 Emulsion RA-315 Propasol Dibutyl Phthalate 4) Add water (second addition) and Acrysol- ASE-60 (may be added, simul taneously 5) Add AMP 95 Biocide-290 Lehnert 10.3.01-89 SGP 0016190 August 15, 1972 Supersedes AK-502 page 2 Dated 1/28/72 VISCOSITY - Refer to Plant Testing Procedure Ho. 109 Specifications: 430 to 46Qsrabender unit Brabender Viscosity 430 to46Q Viscosity can be adjusted by addition of water, reduction of mix water, or by addition of ASE-60 in small amounts. It is best to hold back a small amount of water to be added if the viscosity Is too high. ASE-60 may be added to thicken the mix should too much water have been added. Should it be necessary to add ASE-60, the pH must again be checked since ASE-60 is acidic and its addition will lower pH. Remember, changes in the water content affect flow properties as well as the wet density. WORKING CHARACTERISTICS: Shall extrude easily from tube and form a uniform bead that does not sag or run. OPEN TIKE - Refer to Plant Testing Procedure Ho. 114 WETTING CHARACTERISTICS: Refer to Plant Testing Procedure Ho. 115 TENSILE STRENGTH - Refer to Plant Testing Procedure No. 116 ALKALINITY . . - Refer to Plant Testing Procedure No. 34. Adjust with small quantities of AHP Specifications: Maximum Minimum Average 8.3 7.7 8.0 DENSITY Specifications: 11.00 lbs./gal 10.75 lbs./gal 10.85lbs./gal Case weight should be 35 lbs. ^ 1 lb. , - ED0:elz Denotes change Lehnert 10.3.01-90 SGP 0016191 r-2scr,i?Ttos Supersedes AM-502 Dated 8/15/72 AMROK, JEW TO3K, 3LAKT FCRXUIlA DStWALL ADHESIVE AK-502 Dryvall stud adhes ive Saw Material Function EX S--=c . Percent lit. 'larch Water Calgor.-T Ethylene Glycol Acvowe t-33 Aictrito Limestone Clay 3PC3 Asbestos SG210 Hesin E3-12 Emulsion Elvace 1873 Proposal Dibutyl Phthalate Water Acrvsol ASE-60 a>:?-95 biocide 290 Solvent Wetting Agant Solvent Wetting Agent Filler Filler Filler Adhesive Adhesive Filming Agent Plasticiser Solveat Thickening Agent pH Buffer Fungicide 11 182 .220 217 223 12.0 0.1 3.0 0.9 27.0 9.0 O.S 8.0 30.0 1.0 C .8 2.8 3.8 C.5 0.3 617.C (74 gals.) 5.0 .oA.v v.j.o gals.) Ac.O (5.5 gals.) 139c.. i 462.3 41.0 410.0 (55 gals.) 1541.2 (173.0 gals.) 51.0 (7.0 gals.) \*r / ^l) 144.0 (17.3-gals.) 195.0 (22.,4 gals.) 26.3 (5.J gals.) 1.5 100.0 wS* Aw V".1LD One batch yield 4S0 gals. MIMIMO PROCEDURE - i) Add water (first addition) Caigon-T , Ethyl:ine Glycol and Leva:-, at 33. 2/ Aid A c orr.ite, Clay, Asbestos and aix for 30 minutes 3} Add the following ingredients allowing each ingredient rc be thoroughly blended before addition of the next ingredient: Jtesir. ES-12 Emulsion RA-315 Propasal Dibutyl Phthslate Add water (second addition) and Acrysol ASS-60 (may be added situlcaneously o; d AK? 93 Eiocide-290 -/ dar.obas change Lehnert 10.3.01-91 --'C: elz SGP 0016193