Document a1YYkz8XjLVBgzy05mMpX0Gxb
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BirH43235
^Lancaster Laboratories
HK WhensquaStyEasdence.
^ On 07/27/01. 1. *aple muhtUted to Uluaatef Laborotoric*
Belov are lifted pur JMple nmfMif itft your corrtupondiog dcBCrlptlon ud tode. Pleimc refer to your Lanc--ter Liboiftorl.t* client *ccoimC lumber when BtibalCt;li>g
B&Bple* or correBpondlog with fcha lbt>i?st0ty. Account tlurfmt-t 0703}
KDM AP SKWICES ORS - DUMONB6 SSWtS KlU. KAZh BLM 37
IWaSTBH PtKK 6 KOOTB UX
MimSOGTOtt DB 19BOS
Phonei 30a-l)3-OS9$ FAX < 303-2-153?
BILL TOi
ABQM AF SSilVlOtS CSfl-B I BCTOttT C8 tIEMOOTS & CO
alXUst KtU, PiAZA fiLtX} i?
lAHcxs-rgK ?IKB 6 iioore 1*1.
nwowsmv m IIBS_
ShDties 302-9M-M66
y.o. stasis: uio>3i7
COPIBS t0 1 Wa - Plcnda . MDCK JU> Service-
totley Mill n*, Bidg. 27
Lancaatcr Pik* (i Route Hi
lllLlngton DB 19805
KB. KWBEX; 1^7(7
SfSOXb SOB W>s
OOOTS ITOHBEX; 135803 A
IAI )
fiMiple eode/Dencrlptioo
eiBCS531,R MX-HilISSittR SJS tW 8--plc CatttfiEHlUt MBA 7/91
Collected oa 67/3t/01 at mS by SO MMlylr )dbemil141 0495 1MO 2001 2334 2335 4C13
Hiahlngton ' Job Mg.f 703;
** ISStlMAtBD lOKM,
~oTii5SaKO'O'
0.00 0,00
TT
Anlyal.yi
day Wt
OKI 39 W SUMMxy
1
t
04*5 IS W/HS Coofl;
7 I.
15(0 3 tjb Chronicle
3002 39 Buah Fax/C.11
3 3 rC-l3
HiS 4< tetl,<iidB Altctwte Water Kittr
4(13 1 OlakBtce ttAvcrble
Ml;
trice
6,06 29S-00
0.00 0.00
335.00 0.00 0.00
DiBConnc
nice
0.00 395.00
0.00 0.00 335 .,00 0.00 0.00
6x080
MttHt6 0.00
295,00 0.00 0,00
325100
0.00 0.00
Diacouoe
0.00 o.oo 0.00 0.00 . 0,00 0.00 0.00
?6
Eatimte 0.00
295.00
0.00 0.00
22S.OO
'0.00
0.00
Totl Juulyl* md Pr<-p charge*
530.00
S2t>.dO
SOB tVCUiS
530.00
0.00
520.00
MarUagtoa oriw chrtna Well 3cb tto. ; 7035-S0709S-77IOOB
7/61
0.00 0.00
*** assvmxm woo.
5520.00
?0*00
$530.00
^ 'OKIBMUIIB4l.MHUMKoB!g .o..(
All teai ie charged w a third party will BOC
billed directly to
be accepted without
the client,
* BtBtecot,
signed
by UIB third p*fty, tlll^ aAnowledgea and accepts payment reaponslbllty.
The paperwoxk irobinltted with you? l^>l wtlX be --auud to
dencribB the testing protocol you dtulre. Atly chaigw to elliB protocol
vwV. be ubalfcted to U,t la writlncj. If testing i9 lre<iy la
progTM*, you illl be billed. (Our yAX BUMbef Jiff 717-t5t-2(ai.
a
Send cbliges bai ClienC ServlCca - mEStfil)
t*
i(t-aBCBBtet Latooftoriea resexvea (.he rl9ht to .u>ei>d thio acknowledgeiKftt
the Da-pic (fl) fta received require additional preparation charges.
^nU.r U^agM^^243^i^tfo^^g^^^^^
IBMiaEH
^^^^y-^jffOfi. ^ 717-6S6-268t
Q 2217 Hl^WW
E101A3236
Lancaster l^oratories
Where quaRtyis a science.
ANALYTICAL RESULTS
PitpMtdfon
CRO-BJIDuPont de NflKHB3 ft Co BtikyMiUPIiia.Bld5.27
LiiricstcrP&e& Route 141 WilmingtonlDB 19805
302-W2-6768
-.
ItqaKdby:
I.tttciSttT Laboratories 2425 New Holland Pike lAne3aCT,rAl76)S-2425
SAMflJBQHOtffi Tie saaspkigroup for his subnuUal is 77187S. .Samples iicdved at the laboratory on Saturday, July 28, 2001. The P0# for &H group.is LBIO-64237 aad the release number B LB748.
'
Client I>BSaM><ioiL_ ]LTM-SJlUnspate4WiitetSaiBple
LTL-^MrAPWster&Bnjple 1-TLA.SJ.TAP-DW Water Sainpte
LaBcaaterJ^bs Nram^er
.
3656026
.
3656027
3656028
'
^IgmQDpiOOY
1'he specific methodologies used in obtaining the enclosed analytical tesute are indicated on the laboratory chronicles.
1COPYTO
URS.. Diamonds
Ate: ADQMAP Services.
Questions?Contact your Client Sendees Representative NMityBoinlolnxat(717)656-2300.
*
-
Respectfully Submitted,
-* ;-> y.-yw-t it.-'- ^ - "^.^^P%
Christine M-DuIaney ^i?:
Sc. Chemist
\-;
ME-M-"--B--S-R--
Uiixa?tBTlBbt>*toflttlne.
iCSHWiWtodrei* totwQXS
LXKUtft. PA 0605.2WS ?T.tS6,a< fiK:?W<56-2W1
EIP143237
^Op^/^Repdrf
^ LaiKaster Laboratories ^|r M^erequaJKycascfencB
I.&ncaatar ,iLaboratorieB Sa^fia 6. DM
Collected*07/26/2001 14t00
by KM
Subiaitbedt p-y/29/2001 l0s05
Reported; 08/22/2001 at 13;28 Discard; 09/22/2001
Krti-0-Sri Unspiked Water Sample STSVW TORDOIT NBttS 7/01
3656026
rage 1 of I
Account number; 07032 CRO-B.l.DiiPont do Heniours & Co
Barley. Mill Plaza/ Bidg". 27 Lancaster pike & Route l4l
Wilmington DB 19805
SJOOl
Wt
Mo. oaaa-t
064SS
gDO#i XiOeOl-OlBKQ
2j( Reoaivod
AH SBClv*d
Mathod
Analy.l.ia Hawi
aa Mvith*^ K*ulb
Datactios
I4illAt
1FC-K3
32S-26-1
0,685 3
6.038
The reeovtiy ot fcha wrogatea PFPinn. jmd 11H-PETA afB outsidt the
QC Units,
a re-1.43 ico*i(y i outtidB the Vft H-alf (or i** MS/MSD, the Wo
tetwecit the MS/MSD in oafcutdB the fie cxlterla. Tl! PC-M3 wcowiKcy M?t QC
wflte csrictoila (or tlio aBeoeiafced tics.
BC/t COttfaa ol EC-143
3825-36-.A
.D.
0,090
Tbe recwery of K-143 wi0 thl sample. Sui
wf
x*ltim
<> fiC llattn to
vcmsat aiCfvWWs
ttoc
.tor
M8 Aoclated FC-143 belweeB
the
MS/USD <a XBO ootaids ot Qe HnitB. The icwcKy was wtfcliin QC linJltB
ia the I/as.
ttnitu "9/1
1*3/1
Dlltitloa
lrotor
CAT 1(0.
02334
00495 02325
.MmlyalB Mat
tC-143
CC/HS ccanTM ot rc-143 pBBticide Alt*eaate Hafcnr BXtt
Laboratory
Ift&ad FC.S.43 by GC/BCD* 10/91
FC-143 by OC/HS
re*l4a 10/91
Chronicle
nlyfli m*-l DifeB Dad ttBrt
I oa/o?/200i 10-.ot
I 08/15/2001 11;45 i oa/ol/zool oa:oo
lUialyafc
ttfchell* J. KolodtieJBhi filoothy Tifes
Deborah M. Zi*neziMli
Dllntloo
y<!to-
I
Acn
lantMttT Laboiirtorte^ ln<2ttSNiWHo*adrtt*
rO<nt1M
l>c6a.,Wf?5-225 -M-ew-'>-wn sw'TKMi-'*'ii
0 >--' -*
-1
<-t>
"
ai$ itmi.WWOO
EIP143238
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: '::
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^Lancaster Laboratories
^ir WhensquaStyGasdence.
&anc&at;x Laboratories sample HO, tnt
Collected;07/26/2003L l5i45
by KM
SUbttitteilt 07/28/2001 10;OS Reporteds 08/22/2001.at 13t28 Dittcard; 09/22/2001 It'Sttt-o-Siir-TAP Hater sample STBVSW TORDOMt WBI.liS 7/01
3656027
Pagis 1 ofl
Account lluinbcirs 07032
cro-B.I.Dufonb d tieitfBUys & Co
BMley Hill Plaza, Bidg. 27
Lancaatei* Pike k Route 141 wiliningbon OB 1S80S
. SJTAP
eft
wo, 02324
OM9S
Aa Xi>clVd
JL RBCaivd
K*tiod
aaj,yala Mano
Cftfl Wunb*r ttOlUlt
D*t*ctic">
IJit
FC-M3
382S-2<-1
0*045 J
0.039
ItoB tecovexy at the Bniwogatee S-CTCA ad UM-PCHA as ouflAB tte.
QC llaif.
Bitt FC-H3 reccrwiy ia outulte tt BC lld6 (oc arts HS/MSD. the K> Ixittrtttai thd MS/tKD t> outaid* the OC elflteicltk- '(he PC-H3 reeoyery et .QC
CKltwia (CK the afloclatril .
eC/IB Contin* ft yC-143
9t2S-26-l
B-B.
0.090
n tecowsty ot TO-3 wa oufldB of QCdliitwtcifrceBnclae JeEluWs HreS -Al*f3lnobeeitawteeden the
with thtr aanplfc, ThB Wslaeive percent: MS/MSD ww alao oBCside o( QC llmltii; Ttt
reeoery
nas
-witbtn
W
liBltB
in the l-GS.
'BteiM
ug/l
USA
Dtlntloa yaetor
CAT Ho03334
0049S 02325
airlyl*' Has&a
l?C.l*3
fiC/tIS COBfira o rc-l3 frcsticlde Altcrnatt HatAr
Bxcr
Laboratory
Ktho4 pc-143 by ec/o 1B/91. FC-K3 by W/HS FC-lO 10/91
Chronicle
nl7flla Trll Dstti 1 TJJMI
1 08/06/2001 12; 10
I 08/1^/2001 IStH
.1 oa/ei/2001 oa;oo
Xnalyat; Michelle 3. KolodxieJBki
T.lanolAy IrecB Deborali M. Zil^nMU
Dilution raebor
l
MBMBBiR
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*b0ftort* tot.
22SNwHofal"lt
roiwmus ti^tiaw.fAifsos-nas
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BID143239
^Lancaster Laboratories
^K WherequaBtyiSa science.
ggnai^.^pbrr
I>ancast;ei? Xmboratoslos Sampio Ho. Mtt
Collected8<7/26/200l 15;4S
by TO
Submitted: 07/2B/2001 10; 05
Reported? 08/22/2001 at l3s%8
Discard: 0&/22/2001 ITti-e-SJ-TOJP-DTO Hater Sample STHVEH iXOfifiON WEI.lyS 7/01
3(59038
Page lofl
Account number; 0703%
ill CRG-B.I.Dupoot de Hennours & Co
Barley Mill. Plaza, Bidg^ 27 Lancaster Pike s Koute Milroinston DE 19805
.TAPDP
CKt SUn 0332
Aa Kiird
Xx froBld
MBtbod
Jftdywin Mww FC-M3
taa Mis-ixr 3BaS36l
Xfule
0.053 J
BBtootlon
idale
0.036
TIB z-tcWeaey o( tte ltirKOflrate IPiroDA tiful IIH-PFOA in* outBide the
QC XJtaifcil.
0003
ShB PC-10 recovery 1 Outride tbo QC llttlfc* tor the KS/HSD. Tbe RH>
bebveen the MS/MSD la oUtniite the QC Critdrla. The PC-143 recovdry inet QC
critferi* for fcha aBODci&Ecd LCS,
GC/H3 Confirn of K-U3
.
3825-26-1
M.B.
0.090
The rccowtiry of PC-143 OUUlde 6X QC liMita lu eha MS ABBociat.rf
with lehia BanplB. 'Bi* relative parefeot alffBrencB .for PC-143 betweeft fche HS/HSO.>aB *IBO outaltift Of QC Itaiea. TbB recovery waa within QC lllfiCil
in febe LCS.
^ f^3/1
"a/i
Pilufcion yetor
CAT
Ho. 03324
60495 02325
Anlysj. (Uwia PC-143
GC/MS Caaciilk of rc-143 peaticide AlternatB Mater
Bxtir
Laboratoxy
litbo4 rc-143 by GC/BCD 10/91 rc-143 by GC/MS rc-143 10/91
Chronicle
^Qalyalji
Sxll D&fca and Tia* 31 08/06/2001 12:42
09/1^/2001 15853 oa/oi/2001 08:oo
Mialyat Micbelle .7. Kbiodzlejilei
TiBothy Trees
Deborah M. Sioaeimaa
Dllufclon yaetoe
I
Laiioeter Laborirtotti^ Inc.
-\Cl! M EM BE R 2e5HmVH6ftndrft PO.BoxtttS Hrtt.HtttFAT760S.2C5 I" lt*-eTC 1~nn tT-* -- *TM <
fe
S
at--t. -4
EID1432AO
Lancaster Laboratories
WhefequaRtyisasdence.
Quality Control SwoceKa.vy
Page 1 of2
Client Hames C&O-E.X.DuPont de Hemourp & Co
Group Number; 771875
Reported* 08/22/01 afc Oli28 W
Laboratory Coiapliaiace Quality Control
teaiynia.
Saitch mstbor: 01313006A PC-US
Blaafc KUlt
BiBlik
?1.
SM^le BUbc(f) !
0.076 J
.09
"^ ttwort tCS
gni.f
36;$$026-365fi038
U9/1
16
E
'use
l3/MS3n
Htt
3-5S
WP jt?P HJI
Much ldtT> 01312WkX026 CC/KS CCfflflxn oe PC-143
Saapl6 aurix;r(B)t 36S6026-365602B
M.D.
.1
ug/X
<S
3-S5
tealyi- *
BafctA wiabef: 013120009A PC-H3
Batcit EUiabtO-1 012?.3HX02<
ee/iB OMrfAf *>< PC-MS
Saaple Matrix QualdLty Contro.1
m
wo m/iisa
wi uoa
sv
POP
mile %IMC miAht
giro HME egne
cone
TOg
Sample XS*
fiauzple
37*
nuaHxtt-l") i 36SI>036-3(,5602fl
21.*
SO-160
32* 30
/
aufl6>er()i 36en6-36SSOM
.5-7
SO^lOO
S* 30
surrogafce Quality CoutTol
tealywia Matte iFC-M3 la Wtw
Batch Bwribeti 012120009& vsw.
iiit-yroii
smoK.
3656026 3656027 3SS6028 Blank IiCS US
HSD
19
6
9
12 .
'16.. I*
21
2*
X*
3*
2*
a*
2*
O"
16* $* .
17* 11* 14*'
M*
20*
Lfifi 1*W
13-8
Analyal HMM( 001S CBttfilxw of fC-U3 / tM
Batch ouatoeri 01213HAX036 ?n
SO-1SO
;
36S626
33
3656027
28
36S602B S .
Blank
1<C3-
HS
?0 -
14 19 17 37
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. '
.
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.
*~ Outside of specification (1) TheiBsult for one or btoA deteoninatioiB was less than five times (he LOQ.
'"' 'ItcbaclcgnHind result was DaOle than four tiines the ^iice added.
u'"if>u'"n"n-i-a"
LtnciBttr lAtloratorio, he, 2425 NEW Hctendl
f09wWS twm.ta.w.rfwws
. .
EID143241
^ir ^g.q^tea^nSoiiBtr^o,l S,,u.t_tB_Baxy
Pa? 2 of 2
Client flaws: CRO'B.I.DnPont Reported* 08/22/01 at Ol;28
"
.
(Anitas
l-SO
de Nemours & Co
3PH
(hwrogate
Quality
Group
Control
Number;
771875
*- Oubide of specification(1) The result for onti or bofl dcttinnadons was less than five tiroes the LOQ. /'" The baclcgrt>undresult was ffloiB than fow (HDCS the qike added.
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Uncastel Ijibonrtwfei, kic. 2425 riiH6M>^ rft
pQBox'QCB U-WMtKiA 170&24!$
3BXD143242
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^Ir W^enscfjality'Basdenoe.
Oa 67/21/01, & uple* irexo milwlttrt CO it*HCfltef I.lx>rtorlcB BelfKt M; llittd OW Md^lo maitoen* Kith oor corrMpcioding dorcrlptlon and coda, Please refer to yottr Laacuttr !Abortorle client ccoMBt Ruabw tWA flutifclettog
;Hq>l> or coireirpowU.ag *1A tha lAortory.
*ceTMst IhsbCT, 6)633
WGK M SVSW1CKS VS3 DUMOaS
Buaar wtt. fuuo. wes z?
IABCASTB TITS IIORX 1L
iramnwrcw D mos
DiOWl Ba-2-8S5 Hff ; 303*?2-1S33
?.0. MCKMa* UXO-Sa37
COiPiSS TOs 1 OllS - BlUMOto
. MflK SttCVlef Xwley Mill. Molt*. Mg. ?
I^BcartKf nt" It Route 1.41
WUMtegtm OB WOS
RB. tItMSBBi I^7
BlUb TO:
XOgH ftP EBWtCBS
OtC-B X DOTOTT DH MoeDItS & CO
KB GAMJH MIU. fUZk BIOQ 27
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BME No.
Supl Code/OfilpHoai
1M}CSf63C LTL-0-&n Dnapllctd M6r Sl>l sxBvxjf mnxt MaAs 7/91 C6lUett4 OD <17/2S/tl e 1*00 by XH
lnly*l* MUdnf61l 09S 1566 1S61 3324 3335
v 's(Ba7 lai^o-sa-'Biff Mttr fi--fie
\
SIWB) TOffiON MK1AS 7/61
la
coinicted w (ft/at/oi fc i5s toy lot
1' uulyia IM&miiOUl MM 1560 2334 332S -
-0(5 Knr^l*W.-B IhtW .
SIBVIB JOjiPOW SBU-S 7/91
collected OB /2^'o^ft
Xaalynl* ubt;fi0
iCU
SOB WSKUS
KUUngefm tforka Stcvia cordon Weir - 7/01
JOb HOt I 7035-SO-C3S-?7aOOt
* KSTIMATSO tOTAI.
0.66 1S60.00
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'2S .00 0 .06 0 -0
32S 00 0 .00 .00
Dincount Ptice 0 00. 235 66 6 66
B 00 335 00
0 00
9 00
Tocal Aanlynla. ml l?rcp charges
.
$OT tOTAliS
oxtxia
gatiitata 0.00
15'.00 6 .00 6 .00
SfS 06 0 .60 0.00
15(0 > 00 ,
1S60.00
Mashingtoo Horki* Stcvctt Jordoa Nell* - 7/01
biBcamfc
60
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6 60
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let
BelM>6e 0.00
(15.60 6.60
O.Oli S7S-60
0.00 0.00
X560.00
1S60.00
0.00
Lancatter laboratories, Inc 2425 Wew Holland Pike. 90 Box 12425. laficMter, fA T760S-Z42S 717-656-2300 Fax: 717-<56-2m
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