Document a1YYkz8XjLVBgzy05mMpX0Gxb

AR226-2498 j 1 "5 i ; |l 1 l 1j "x ifls . i] ^ P ^ n ^0 r- ^ ^1 ^ ^ : s^ . ft ^ 1 1 ^" S | 0 h-- I i 5& N 'sy ' - j^l 5"' > i r c w r ^ .3 sl 1 r1 5 |iI 5 1 1V s2 ? g ^ ' - 1 0 ^ ^ 3 = d8 m5 jiif illl (s! ^IISIS -^ /?t ^a.1S 1 ?^ 2-g ft' S *- s-t ^ 0 ^ 0 ^ H ^ ^ t i C< T^, ^ 1j j <^ S, ' | | ?i ^ 1^ i? > i ^ ^ / ^ :/ c3 :? ^ >-^ 1 1 1 / 1'^ v / i ^"& s j i i |] |J! ,,. -S 0 / & I 1 /:/ 1 .! 1 < / ^ ^ C! 51 ,'w" J5 S & S BirH43235 ^Lancaster Laboratories HK WhensquaStyEasdence. ^ On 07/27/01. 1. *aple muhtUted to Uluaatef Laborotoric* Belov are lifted pur JMple nmfMif itft your corrtupondiog dcBCrlptlon ud tode. Pleimc refer to your Lanc--ter Liboiftorl.t* client *ccoimC lumber when BtibalCt;li>g B&Bple* or correBpondlog with fcha lbt>i?st0ty. Account tlurfmt-t 0703} KDM AP SKWICES ORS - DUMONB6 SSWtS KlU. KAZh BLM 37 IWaSTBH PtKK 6 KOOTB UX MimSOGTOtt DB 19BOS Phonei 30a-l)3-OS9$ FAX < 303-2-153? BILL TOi ABQM AF SSilVlOtS CSfl-B I BCTOttT C8 tIEMOOTS & CO alXUst KtU, PiAZA fiLtX} i? lAHcxs-rgK ?IKB 6 iioore 1*1. nwowsmv m IIBS_ ShDties 302-9M-M66 y.o. stasis: uio>3i7 COPIBS t0 1 Wa - Plcnda . MDCK JU> Service- totley Mill n*, Bidg. 27 Lancaatcr Pik* (i Route Hi lllLlngton DB 19805 KB. KWBEX; 1^7(7 SfSOXb SOB W>s OOOTS ITOHBEX; 135803 A IAI ) fiMiple eode/Dencrlptioo eiBCS531,R MX-HilISSittR SJS tW 8--plc CatttfiEHlUt MBA 7/91 Collected oa 67/3t/01 at mS by SO MMlylr )dbemil141 0495 1MO 2001 2334 2335 4C13 Hiahlngton ' Job Mg.f 703; ** ISStlMAtBD lOKM, ~oTii5SaKO'O' 0.00 0,00 TT Anlyal.yi day Wt OKI 39 W SUMMxy 1 t 04*5 IS W/HS Coofl; 7 I. 15(0 3 tjb Chronicle 3002 39 Buah Fax/C.11 3 3 rC-l3 HiS 4< tetl,<iidB Altctwte Water Kittr 4(13 1 OlakBtce ttAvcrble Ml; trice 6,06 29S-00 0.00 0.00 335.00 0.00 0.00 DiBConnc nice 0.00 395.00 0.00 0.00 335 .,00 0.00 0.00 6x080 MttHt6 0.00 295,00 0.00 0,00 325100 0.00 0.00 Diacouoe 0.00 o.oo 0.00 0.00 . 0,00 0.00 0.00 ?6 Eatimte 0.00 295.00 0.00 0.00 22S.OO '0.00 0.00 Totl Juulyl* md Pr<-p charge* 530.00 S2t>.dO SOB tVCUiS 530.00 0.00 520.00 MarUagtoa oriw chrtna Well 3cb tto. ; 7035-S0709S-77IOOB 7/61 0.00 0.00 *** assvmxm woo. 5520.00 ?0*00 $530.00 ^ 'OKIBMUIIB4l.MHUMKoB!g .o..( All teai ie charged w a third party will BOC billed directly to be accepted without the client, * BtBtecot, signed by UIB third p*fty, tlll^ aAnowledgea and accepts payment reaponslbllty. The paperwoxk irobinltted with you? l^>l wtlX be --auud to dencribB the testing protocol you dtulre. Atly chaigw to elliB protocol vwV. be ubalfcted to U,t la writlncj. If testing i9 lre<iy la progTM*, you illl be billed. (Our yAX BUMbef Jiff 717-t5t-2(ai. a Send cbliges bai ClienC ServlCca - mEStfil) t* i(t-aBCBBtet Latooftoriea resexvea (.he rl9ht to .u>ei>d thio acknowledgeiKftt the Da-pic (fl) fta received require additional preparation charges. ^nU.r U^agM^^243^i^tfo^^g^^^^^ IBMiaEH ^^^^y-^jffOfi. ^ 717-6S6-268t Q 2217 Hl^WW E101A3236 Lancaster l^oratories Where quaRtyis a science. ANALYTICAL RESULTS PitpMtdfon CRO-BJIDuPont de NflKHB3 ft Co BtikyMiUPIiia.Bld5.27 LiiricstcrP&e& Route 141 WilmingtonlDB 19805 302-W2-6768 -. ItqaKdby: I.tttciSttT Laboratories 2425 New Holland Pike lAne3aCT,rAl76)S-2425 SAMflJBQHOtffi Tie saaspkigroup for his subnuUal is 77187S. .Samples iicdved at the laboratory on Saturday, July 28, 2001. The P0# for &H group.is LBIO-64237 aad the release number B LB748. ' Client I>BSaM><ioiL_ ]LTM-SJlUnspate4WiitetSaiBple LTL-^MrAPWster&Bnjple 1-TLA.SJ.TAP-DW Water Sainpte LaBcaaterJ^bs Nram^er . 3656026 . 3656027 3656028 ' ^IgmQDpiOOY 1'he specific methodologies used in obtaining the enclosed analytical tesute are indicated on the laboratory chronicles. 1COPYTO URS.. Diamonds Ate: ADQMAP Services. Questions?Contact your Client Sendees Representative NMityBoinlolnxat(717)656-2300. * - Respectfully Submitted, -* ;-> y.-yw-t it.-'- ^ - "^.^^P% Christine M-DuIaney ^i?: Sc. Chemist \-; ME-M-"--B--S-R-- Uiixa?tBTlBbt>*toflttlne. iCSHWiWtodrei* totwQXS LXKUtft. PA 0605.2WS ?T.tS6,a< fiK:?W<56-2W1 EIP143237 ^Op^/^Repdrf ^ LaiKaster Laboratories ^|r M^erequaJKycascfencB I.&ncaatar ,iLaboratorieB Sa^fia 6. DM Collected*07/26/2001 14t00 by KM Subiaitbedt p-y/29/2001 l0s05 Reported; 08/22/2001 at 13;28 Discard; 09/22/2001 Krti-0-Sri Unspiked Water Sample STSVW TORDOIT NBttS 7/01 3656026 rage 1 of I Account number; 07032 CRO-B.l.DiiPont do Heniours & Co Barley. Mill Plaza/ Bidg". 27 Lancaster pike & Route l4l Wilmington DB 19805 SJOOl Wt Mo. oaaa-t 064SS gDO#i XiOeOl-OlBKQ 2j( Reoaivod AH SBClv*d Mathod Analy.l.ia Hawi aa Mvith*^ K*ulb Datactios I4illAt 1FC-K3 32S-26-1 0,685 3 6.038 The reeovtiy ot fcha wrogatea PFPinn. jmd 11H-PETA afB outsidt the QC Units, a re-1.43 ico*i(y i outtidB the Vft H-alf (or i** MS/MSD, the Wo tetwecit the MS/MSD in oafcutdB the fie cxlterla. Tl! PC-M3 wcowiKcy M?t QC wflte csrictoila (or tlio aBeoeiafced tics. BC/t COttfaa ol EC-143 3825-36-.A .D. 0,090 Tbe recwery of K-143 wi0 thl sample. Sui wf x*ltim <> fiC llattn to vcmsat aiCfvWWs ttoc .tor M8 Aoclated FC-143 belweeB the MS/USD <a XBO ootaids ot Qe HnitB. The icwcKy was wtfcliin QC linJltB ia the I/as. ttnitu "9/1 1*3/1 Dlltitloa lrotor CAT 1(0. 02334 00495 02325 .MmlyalB Mat tC-143 CC/HS ccanTM ot rc-143 pBBticide Alt*eaate Hafcnr BXtt Laboratory Ift&ad FC.S.43 by GC/BCD* 10/91 FC-143 by OC/HS re*l4a 10/91 Chronicle nlyfli m*-l DifeB Dad ttBrt I oa/o?/200i 10-.ot I 08/15/2001 11;45 i oa/ol/zool oa:oo lUialyafc ttfchell* J. KolodtieJBhi filoothy Tifes Deborah M. Zi*neziMli Dllntloo y<!to- I Acn lantMttT Laboiirtorte^ ln<2ttSNiWHo*adrtt* rO<nt1M l>c6a.,Wf?5-225 -M-ew-'>-wn sw'TKMi-'*'ii 0 >--' -* -1 <-t> " ai$ itmi.WWOO EIP143238 'ArmtysK^por^ " . -.-. . : ':: . '..-' .''.- .'.. .. ., ;. ,' ^Lancaster Laboratories ^ir WhensquaStyGasdence. &anc&at;x Laboratories sample HO, tnt Collected;07/26/2003L l5i45 by KM SUbttitteilt 07/28/2001 10;OS Reporteds 08/22/2001.at 13t28 Dittcard; 09/22/2001 It'Sttt-o-Siir-TAP Hater sample STBVSW TORDOMt WBI.liS 7/01 3656027 Pagis 1 ofl Account lluinbcirs 07032 cro-B.I.Dufonb d tieitfBUys & Co BMley Hill Plaza, Bidg. 27 Lancaatei* Pike k Route 141 wiliningbon OB 1S80S . SJTAP eft wo, 02324 OM9S Aa Xi>clVd JL RBCaivd K*tiod aaj,yala Mano Cftfl Wunb*r ttOlUlt D*t*ctic"> IJit FC-M3 382S-2<-1 0*045 J 0.039 ItoB tecovexy at the Bniwogatee S-CTCA ad UM-PCHA as ouflAB tte. QC llaif. Bitt FC-H3 reccrwiy ia outulte tt BC lld6 (oc arts HS/MSD. the K> Ixittrtttai thd MS/tKD t> outaid* the OC elflteicltk- '(he PC-H3 reeoyery et .QC CKltwia (CK the afloclatril . eC/IB Contin* ft yC-143 9t2S-26-l B-B. 0.090 n tecowsty ot TO-3 wa oufldB of QCdliitwtcifrceBnclae JeEluWs HreS -Al*f3lnobeeitawteeden the with thtr aanplfc, ThB Wslaeive percent: MS/MSD ww alao oBCside o( QC llmltii; Ttt reeoery nas -witbtn W liBltB in the l-GS. 'BteiM ug/l USA Dtlntloa yaetor CAT Ho03334 0049S 02325 airlyl*' Has&a l?C.l*3 fiC/tIS COBfira o rc-l3 frcsticlde Altcrnatt HatAr Bxcr Laboratory Ktho4 pc-143 by ec/o 1B/91. FC-K3 by W/HS FC-lO 10/91 Chronicle nl7flla Trll Dstti 1 TJJMI 1 08/06/2001 12; 10 I 08/1^/2001 IStH .1 oa/ei/2001 oa;oo Xnalyat; Michelle 3. KolodxieJBki T.lanolAy IrecB Deborali M. Zil^nMU Dilution raebor l MBMBBiR -\CIL *b0ftort* tot. 22SNwHofal"lt roiwmus ti^tiaw.fAifsos-nas rty:CTft.'w *' ' ' .-Thrr (;'i:c 1K*^ > 0 5>- 0 r>i* ; uni/oo BID143239 ^Lancaster Laboratories ^K WherequaBtyiSa science. ggnai^.^pbrr I>ancast;ei? Xmboratoslos Sampio Ho. Mtt Collected8<7/26/200l 15;4S by TO Submitted: 07/2B/2001 10; 05 Reported? 08/22/2001 at l3s%8 Discard: 0&/22/2001 ITti-e-SJ-TOJP-DTO Hater Sample STHVEH iXOfifiON WEI.lyS 7/01 3(59038 Page lofl Account number; 0703% ill CRG-B.I.Dupoot de Hennours & Co Barley Mill. Plaza, Bidg^ 27 Lancaster Pike s Koute Milroinston DE 19805 .TAPDP CKt SUn 0332 Aa Kiird Xx froBld MBtbod Jftdywin Mww FC-M3 taa Mis-ixr 3BaS36l Xfule 0.053 J BBtootlon idale 0.036 TIB z-tcWeaey o( tte ltirKOflrate IPiroDA tiful IIH-PFOA in* outBide the QC XJtaifcil. 0003 ShB PC-10 recovery 1 Outride tbo QC llttlfc* tor the KS/HSD. Tbe RH> bebveen the MS/MSD la oUtniite the QC Critdrla. The PC-143 recovdry inet QC critferi* for fcha aBODci&Ecd LCS, GC/H3 Confirn of K-U3 . 3825-26-1 M.B. 0.090 The rccowtiry of PC-143 OUUlde 6X QC liMita lu eha MS ABBociat.rf with lehia BanplB. 'Bi* relative parefeot alffBrencB .for PC-143 betweeft fche HS/HSO.>aB *IBO outaltift Of QC Itaiea. TbB recovery waa within QC lllfiCil in febe LCS. ^ f^3/1 "a/i Pilufcion yetor CAT Ho. 03324 60495 02325 Anlysj. (Uwia PC-143 GC/MS Caaciilk of rc-143 peaticide AlternatB Mater Bxtir Laboratoxy litbo4 rc-143 by GC/BCD 10/91 rc-143 by GC/MS rc-143 10/91 Chronicle ^Qalyalji Sxll D&fca and Tia* 31 08/06/2001 12:42 09/1^/2001 15853 oa/oi/2001 08:oo Mialyat Micbelle .7. Kbiodzlejilei TiBothy Trees Deborah M. Sioaeimaa Dllufclon yaetoe I Laiioeter Laborirtotti^ Inc. -\Cl! M EM BE R 2e5HmVH6ftndrft PO.BoxtttS Hrtt.HtttFAT760S.2C5 I" lt*-eTC 1~nn tT-* -- *TM < fe S at--t. -4 EID1432AO Lancaster Laboratories WhefequaRtyisasdence. Quality Control SwoceKa.vy Page 1 of2 Client Hames C&O-E.X.DuPont de Hemourp & Co Group Number; 771875 Reported* 08/22/01 afc Oli28 W Laboratory Coiapliaiace Quality Control teaiynia. Saitch mstbor: 01313006A PC-US Blaafc KUlt BiBlik ?1. SM^le BUbc(f) ! 0.076 J .09 "^ ttwort tCS gni.f 36;$$026-365fi038 U9/1 16 E 'use l3/MS3n Htt 3-5S WP jt?P HJI Much ldtT> 01312WkX026 CC/KS CCfflflxn oe PC-143 Saapl6 aurix;r(B)t 36S6026-365602B M.D. .1 ug/X <S 3-S5 tealyi- * BafctA wiabef: 013120009A PC-H3 Batcit EUiabtO-1 012?.3HX02< ee/iB OMrfAf *>< PC-MS Saaple Matrix QualdLty Contro.1 m wo m/iisa wi uoa sv POP mile %IMC miAht giro HME egne cone TOg Sample XS* fiauzple 37* nuaHxtt-l") i 36SI>036-3(,5602fl 21.* SO-160 32* 30 / aufl6>er()i 36en6-36SSOM .5-7 SO^lOO S* 30 surrogafce Quality CoutTol tealywia Matte iFC-M3 la Wtw Batch Bwribeti 012120009& vsw. iiit-yroii smoK. 3656026 3656027 3SS6028 Blank IiCS US HSD 19 6 9 12 . '16.. I* 21 2* X* 3* 2* a* 2* O" 16* $* . 17* 11* 14*' M* 20* Lfifi 1*W 13-8 Analyal HMM( 001S CBttfilxw of fC-U3 / tM Batch ouatoeri 01213HAX036 ?n SO-1SO ; 36S626 33 3656027 28 36S602B S . Blank 1<C3- HS ?0 - 14 19 17 37 ...' . ' . .. . *~ Outside of specification (1) TheiBsult for one or btoA deteoninatioiB was less than five times (he LOQ. '"' 'ItcbaclcgnHind result was DaOle than four tiines the ^iice added. u'"if>u'"n"n-i-a" LtnciBttr lAtloratorio, he, 2425 NEW Hctendl f09wWS twm.ta.w.rfwws . . EID143241 ^ir ^g.q^tea^nSoiiBtr^o,l S,,u.t_tB_Baxy Pa? 2 of 2 Client flaws: CRO'B.I.DnPont Reported* 08/22/01 at Ol;28 " . (Anitas l-SO de Nemours & Co 3PH (hwrogate Quality Group Control Number; 771875 *- Oubide of specification(1) The result for onti or bofl dcttinnadons was less than five tiroes the LOQ. /'" The baclcgrt>undresult was ffloiB than fow (HDCS the qike added. -U--B"-U""R-SS-BR-a -\C1L Uncastel Ijibonrtwfei, kic. 2425 riiH6M>^ rft pQBox'QCB U-WMtKiA 170&24!$ 3BXD143242 f^/^W l^A^/ ^)"^"\ "^ o0 <w ^S ^^"^^^^ -" -^N^^ I 1 ; ; ^Of ' [ ( ^ . | . ( P t " ^ l ^ ^ T^O^ \ \ .wiwwi ^ ^ x Y ,, , aKfe ^9/" <! 7' ^y^d/--y--i'^--M^S/i--'l --iA--(i--pw--iw-- --s--\ ----------Bi:l--UB--llQ-- '^\ \,. \ \Aqpiwy ^^c^ .JiL ^-^ fi^ g; 's-^^tXMIW^ wf^ fc >-*-/K t >M wtwwl W i -- i - - --'- ^^ ^^ S^t/ ^^ ^x/ :,;f^ ^^ ^-f .0081 000) MM MM. fffA/^'f ' djfj SIK tdAj (OjCt Aawio WMBI(; ianp) SI&OTS -u ------------------------------------------------,,,,,,,,,,,,,,..-,.... ,. - awpaocdd awdS'StWOS ''"< r < \ BtqafljiS^pciaoH to(i. s-r"QN rwa-'afcr re/ ^ iwsasssw^e ----------------------ssvsmss^' 1.----------------Jj^.t--f^--ti--j^----------,....----.^^^o ' "e^ssozos-seoi U' CT&ts ,,, ,, , . ''--3 S.8!.eZ AM ''jKiU:(K)t!Efi .fttuw'' M"a"*"ti""tt".- ttd<g, FBJP^ OOOT300WG o' ^V7^f'/yf? /yHr99" .sE-sMavd-.iaS ^I^Lanc^erlJMratories ^Ir W^enscfjality'Basdenoe. Oa 67/21/01, & uple* irexo milwlttrt CO it*HCfltef I.lx>rtorlcB BelfKt M; llittd OW Md^lo maitoen* Kith oor corrMpcioding dorcrlptlon and coda, Please refer to yottr Laacuttr !Abortorle client ccoMBt Ruabw tWA flutifclettog ;Hq>l> or coireirpowU.ag *1A tha lAortory. *ceTMst IhsbCT, 6)633 WGK M SVSW1CKS VS3 DUMOaS Buaar wtt. fuuo. wes z? IABCASTB TITS IIORX 1L iramnwrcw D mos DiOWl Ba-2-8S5 Hff ; 303*?2-1S33 ?.0. MCKMa* UXO-Sa37 COiPiSS TOs 1 OllS - BlUMOto . MflK SttCVlef Xwley Mill. Molt*. Mg. ? I^BcartKf nt" It Route 1.41 WUMtegtm OB WOS RB. tItMSBBi I^7 BlUb TO: XOgH ftP EBWtCBS OtC-B X DOTOTT DH MoeDItS & CO KB GAMJH MIU. fUZk BIOQ 27 tSltWStSS. A HODTIt 141 immGTO BB isaos"'., BbOBOt t2..3-l6'S- SfBOXJO. TO MOt : CIIOOrt mMWtfc USt3 A BME No. Supl Code/OfilpHoai 1M}CSf63C LTL-0-&n Dnapllctd M6r Sl>l sxBvxjf mnxt MaAs 7/91 C6lUett4 OD <17/2S/tl e 1*00 by XH lnly*l* MUdnf61l 09S 1566 1S61 3324 3335 v 's(Ba7 lai^o-sa-'Biff Mttr fi--fie \ SIWB) TOffiON MK1AS 7/61 la coinicted w (ft/at/oi fc i5s toy lot 1' uulyia IM&miiOUl MM 1560 2334 332S - -0(5 Knr^l*W.-B IhtW . SIBVIB JOjiPOW SBU-S 7/91 collected OB /2^'o^ft Xaalynl* ubt;fi0 iCU SOB WSKUS KUUngefm tforka Stcvia cordon Weir - 7/01 JOb HOt I 7035-SO-C3S-?7aOOt * KSTIMATSO tOTAI. 0.66 1S60.00 9.W 0.09 >--MW------WHw4*Wi (1MB.BB rT telyif iwf <lW OK am 3 oc swiMixy 3 I6fC5O 3306 eLCab/MSOuCrtOutlttefilRf: << ?-10 3 1S(1 39 BSD TO/CAM, 1 M14 3 FC-H3 3 ailS 3 FfBticide Altctil.te Katcr Kxtic 3 413 3 Dl^lcettc Beliyeiabit 1 t>i*K rce 0,06 '2S .00 0 .06 0 -0 32S 00 0 .00 .00 Dincount Ptice 0 00. 235 66 6 66 B 00 335 00 0 00 9 00 Tocal Aanlynla. ml l?rcp charges . $OT tOTAliS oxtxia gatiitata 0.00 15'.00 6 .00 6 .00 SfS 06 0 .60 0.00 15(0 > 00 , 1S60.00 Mashingtoo Horki* Stcvctt Jordoa Nell* - 7/01 biBcamfc 60 00 00 00 00 60 6 60 0.00 let BelM>6e 0.00 (15.60 6.60 O.Oli S7S-60 0.00 0.00 X560.00 1S60.00 0.00 Lancatter laboratories, Inc 2425 Wew Holland Pike. 90 Box 12425. laficMter, fA T760S-Z42S 717-656-2300 Fax: 717-<56-2m E S B M g M gP g6 JB f**^ -->--... 4>r>r>mmAA ^ ^(ttr EID1432AA ^LancasterLaboratories ^K Wr(pa%y&a5crenoa ACCOCBf HO; 07B32 xoert AJP sBWicsB TOS - DMMOtDS RAluanc HIU. FIAZA BLOG 37 LHKAStBl IKB . IhlWIB 141 muDannxi w ios ?ag* a job No.; 7035-5 !)70SS-7-?30()0 ... xsrmkiED TOTM. tissa.oo '""iS'oS B.OO ?S^ST?S' TheBbZiUUllMag .o..e All tec* alct d>ug4 w tMl pwtr will aot billed ilinetly to lw cceptcd withoot UK; cllcnE-- tttteiocne, -igned by the thiri pArty. widch aetaottladge* ad cefcp'f p*y.6at rMponalbilty. till fbe pjpemiork mAtlttoS with ywr Mnplf toe ined to <teeib tfeft 6M6la9 mufc bfl i6Blttd to lpH IAI t<K la l w ywt itlo d g. M Ii f f . t e jtny rtto ch g mi ! ge* ale to exd h y hlJ In PKOtOcol pwgw, y< 'rtll 1'iUw*. (ow rax oin-b^ l 717-tSt-asn; Send cluui9c< tot Client; Sefvleen - WBssft) . ' i ttai ncaa tb<! tniu ljit>o iptet n ) ew m l r e c kCTeic eived vw cq tfca Hlx r ight ddl t to lD e crl nd pre thl par ^ck iiCion aovlv^cvc dmrge?. i t t . TOR liM OSBi 771B7S Bll P t 30 97/3/0l 100S ASROOO M 3S1 634 SO 00.00 C t-- S ' . tancastet laboratories. Inc. * 2425 New Holland Pte. fO Box 12425. laneastef. (% 1760S-242S 7l7-S52300 Fax: 717-56-268t IMBSfl EID143245