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ARRKG -- 1RES Telomer Research Program yz AGC -------- = Claria-- nt. WHER Analysis of Telomer-Based Products and Telomer-TreatedArticles Scope and Rationale coTfonhresmuaTtmeieloornmaaernrtdi/RcloeersseraterrlcaeahtseePdorwfoigptreharfmslu(ucThoRrpPor)oo'cdtuhcaatnsso.istauTcdhki]ees(puPunrFpdOoeAsr)ewafoyrftothmoistinewvooemrsetlrig-iabsta1es0tedhdeetopeodrtumeinctntieaslwahnetdher aerntviicrleosnmterenattaeld ewxipthosruerperetsoenPtFaOtAiv.e tTehleomfeurll-bsacsoepdeporodfhuectpsrcoognrtarmibuteouttolisniegndifinicsahnet ThRuYmaLnevoerr of Intent? Project Overview siTnchrteeheTenmiRnagjhosarustdcesolnowtmirlealrc-itbneavdseewstdiitgphartoaednuloceuvtteslssiindoefcorPemFsmeOeaArrcchienltaahnbeodrtaahrtrtoeirecylmefsaojcaonaratleeyndzde-wfuiosteh tcthahetoeupgsroerpsireeonsduccetcsao.mfpPerTFsh,OeeA pmeoexlimylbmeeesrrsas,nmdwhapianpcehur.frerpTrsheesaepnnrtdisemplap.rryoxTpirhmodapulrceotldsyu8tcht5at%cltoahfseteThsRe0Ptlmboeemmebeesrrbcassermaerpkheotdeufsothretthveshoe asrprpelTpiceoatnisonsare TRP member companies manufacture as actual items of commerce. psWtrhuiedlsyeewntithllertpehreaorpveriidmemaanryycoppmroptoredneuthciteanlcsltiaevslseoemsneirina-cbloasmpeimdcetpurorceleyom(fe1re2ixcpporpsorduourdceutcspt)o.st,enaTtihraeellarbtyeivlfeloeycusosmfiatnlhgliosnnsucmerbeneeenring aamrcattjiucoallresmeni0dl-buceosnetdepistoteildoynmaserrcwiiactcthputraholdecuscautrbspjeea,cntdtetxtethioelmec,eorar-nrbdeaspspaeopdnedprionslguybamsrettriaictlceessportofrdecuaoctmtedmseurncdee.r reTphreetseesmtaetdve or Approach and Methodology Method Development and Validation A significant amooufwnortk was required to develop and coordinate the appropriatesampling, ecspoxehnpritefprrlmatuecsotnrftolroaaobcsntm.datnahoTneiahcTleyaRsciPiinsdimtpaaelnlaamnlwbysoetraircksacwlboeysmltlptaahnaednsaicr1eod0nssst.yrinnactTpthhaeirasasbillzienewilitaliwlnaildtrwhecqoheurafikrfraoecrwttmaseesr(ti0chzoeosnodpldirudciicemttvaeberdilydobsapynmfderanon[tma1y,opt2orc-t"aeqnlCtu]iail a. tive determination of PFOA in th various article matrices and clomer-based products ae wel ac Nhemeouomspa&niCcosmppaarniyc.ipating n he TRP include Asai Glass, Clan GH, Dakin Industries nd 1 ufons de ReLtatAe3ro2f6n.en forthe Tlomer Research Program submited toStcphen Johnson (US EFA) on March 14,2003 553 55 BoSn + =8 2 a2g5 Does not contain TSCA CBI 1 TRP (31-Mar-03) a - -- dvaelviedlaotipomneonftthanedmmeetthhooddolvoaglyidfaotriodneti erdmiisnciunsgsePdFbOelAowi,n treated articles. More on method ArcStoaimmcmplelerecsAoinaaflltymhsaeins1u2fatcetluormiern-gtrfaecaitleitdieasrtaincldesanwialllybzeedcoflolrePctFeOdAfruosminpgiltohtepdleanvtelfoapcielditaensdorvaflriodamted aptnrhaeolssyeetnirtceaiplnormeteaetcdhholdte.vreelastT.ehdearsttiucdley ciosldleesctiegdn,eadnadsifa istcirseperneisnegnts,tuatdywthoatdleetveerlmsinaendwhtehtehceornfPiFdOenAceisof TypesofArticles: representative textile, carpet and puper articles (12 total) upAesnredbLifOlolMriotSnhIe(spMepSba)nmawelitythsheoasdohrlaeolvagitynigvuestihsentgaonbdj[ae1rcd,t2id-vee'viCoa}ftiapotentrafoilnfuiolnregsosaoctlthoaawnneori2c0l%ia.mciitdoifntqeurannatlifsitcaantdiaorndowfi|lpbaert fM7oe0rtt-ih1foi1cd0a%tdieofnvorelletovheprlemseeonmtaft1wriiplcplebsb,e-1-c0coapnrpdpubectat(nenddylw1oi0nt0)h,ptpthebex.tgiloeal(opoflyheasvtienr)g aexntdrapcatpieorn -e-ffatictiheenctihcrseefalPlFwOitAhin `mfOoernnetthsheusmnhdeortwehdoadcscidexetpyvtaetbllwoepomree(1cn6ot2v)earunindetrsmeaeatttehtdhoedslhveaavvleelisdda-ntcoiatorenpdt,po,trthteeixoctnoilnoetfratanhcditsplsaatbpuedwyri.lslapImfrpsolcceoesuetwdienwrgietchgxpemenerertr-hatoedd validation, MTanhedethm1o0ed0thpVoapldbidfiaonrteitoahncehfodoefrtePcraFmriOpneAatt(iinnoynAlorotfnic)l,PesFp:aOpAerin(cterllautleodsea)rtaincldesfawbirlilcb(epovlayleisdtaetre)duantd1erppGbo,od10 ppb asLenapdbaorpraratetecoirdsayiyosPn.roafcHteitcnheecsem,(eGt3Lh6Po)s.dambpyMleaetnsahflooydrzicvnaaglcihsdiaaxrttisioacnlmepw-illels6csoepamicpkhreidasteaot1 fepadpcbeh,mof1no0srttpirpfaibctaiatnniogdnt1lhe0ev0ealpcopcunbrtoanucygach ofdvaaalyirdt-aitciwloeins.lhbaAesnaablneyaeslniyszoaepfdprfaoorvrteiadc.loetsawlilolfo1t08parnoacleyesdesunotvielrmethtehotdwov-adlaiydapteiroinoadnodfptrhoetomceotlhfoodr analysis Spbrlaoomdcpuklcetd.se:siSgEinxaca(hp6o)prfsoutabhc-ehs.a1m2Spealrvetesinctwleiysl-lttwebsoetea(d7n2aw)lilyslzuebbde-sftaorrmepaetlaeecdshwfaiortrthiacralteis/cilpnergsolde(u1tc2telptoarmierea,tre-sdbealasercetitdceldpeosulxsymi6enrsagiubcpsfaoaiumrsrp.luensIi)nqcuwleiuldcleabdrepfegoterpnereaorcadhtuecodtf aptanheidtrw1,2eslairxvteiucn(lie1qs2u)weipltrleoxbdteuicl4tes/upnwrtiorldeluacbtteedpcaosilarlsmepacltneedds tffwoorobauennauilsqyesudiesapsraepcseournltitrpionrlgodaiunncdt for extraction efficiency verification. TPLhrCio/sdMuscSctr/eAMenSnailmnyegstishstoudd.y sMadtersiixgnceodmptloedxeitteircmsimneaythmealkeveelthoefsePFanOaAlysinescapcarhtipcruoldaurlcytcchlaalsleunsgiinngg.an Product Types: acrylate and urethane polymers (12 product formulations) Docs not contain TSCA CBI 2 TRP (31-Mar-03) ``mSceaotmmhppoladenosioleosfgttyhoeitsh1eb2eciopnnrgtirmuaascretydlatfbeorlfootmrheearsn-eablayasnsiaesld.yspeoAsloysfmtetarenidlcaormpderrao-ddbduuictstiesodnwipalrplopdbruecotapscr,hovhuiasdvieindnggbLyloCTwRMerPSlMmimeSimtboefr pq(ur1ao,nd2tu-icftCi}csaaptmeipronlflefusoorraorPeoFcatOnaAanloyoizefe|dap,cairedxttiprneatcertrnimaoilnllseitfofanincd(iaeprnpdcmiw)eislwlwiibtlehl abusereecdlvaattlhivureaotusegtdhaonoudntaratdtheldeesavtsiutadtty.ioonoBoerffto2hr0ree%et.heA cpornodduuccttegdrouunpdserusGiLnPg.modified methodologies supplid by the TRP. Product analyses are being Results "The resuls ofthis screcning study wil be prepared as a report, including the following details: SMautmemrairayloufseMdethod and Resuls REeqaugiepnmtesnatnudsesdtandards used APnraelpyatriactiaolnPorfoscteodcukresstandard calibration standards solution, preparation of fortification of articles and preparation of prepr-eppraorcaetsisoinngproofcseadmuprleess, sample fortification procedures, analyte extraction and final sample ILnCs/trMuSmecnotnadtiitoinons LC/MS Calibration and Samples Analysis Calculation Methods Resulis and Discussion DCoenttercotloranrde/sopronBsleank RExetcroavcetriioensEfficiency Limit ofQuaniification and LimitofDetection Conclusions Schedule asWnhoailrpykmtiecbnaytl tashtneadnTadRnaaPrldyassniafsolrypttirhcoealcperexdoppueorrsateessdbwweeoglralkn.asipnIrnJiacmnoaunarcreyryat2nw0di0t[3h1,tto2hi-ds"eCve}fefloporetpr,ftplhouetoeranoptopicratolapcnroicnaittcreaacsctiadmapblsi.ng, awTneRdrPescaiodmmepnpltaeinfriieeedqsuaianrndedmbdeiendltsisvweienrreeFdestboorliutcahireteydl.2ab00Ti3nh. eMaTsrehcleehcit2net0de0r3ln.aablosrtaatonrdyarrdecweaisvepdretphearfeidnalbystoundey opftlahnes Does not contain TSCA CBI 3 TRP (31-Mar-03) HH pTMrahoredcuihcn-tiAtspalwriiwllolr2bk0e03i1.0nidtieaTvteheldeoipannaaAnlpydrsiilvsao2l0fi0dt3ae.tleomaTneharle-yttfriiecnaaallteradenpadorrtstiacimlsepselxeapnmedcettteehdloodbmsyerwJ.iulbnlae.sbeedJcupolonyldy2um0ce0t3re.idc iTnhe results wil be provided to EPA as soon as they become available. Docs not contain TSCA CBI 4 TRP (31-Mar-03)