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October 29, 1968 NEW FORMULA ACME. TEXAS PLANT FORMULA PLAINTIFF'S EXHIBIT READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS') ( READY MIX "X") DESCRIPTION OF PRODUCT - White Ready Mixed Joint Compound used for taping, covering tape, filling cornerhead and spotting nails FORMULA Raw Material Water Filler TEX-970 Ucar WC-130 Benzoflex 50 Source Solvent R.M. Spec. % Act. Ingr. . Body Adhesive PIasticizer 185 183 91.5 8.00 0.50 100.00 Lbs./Batch 400.00 H*.2(48 gal.)* 700.0 2oo.o 58.3 ti.^7 4 0 /. i4- 1162.3** *Approximately 52 lb./lOO lbs. of active ingredients (this may vary + 2 gallons per batch.) **One batch yields 17(+)- 5 gallon pails of Ready Mix Joint Compound at 65.6 lbs./pail. TESTING PROCEDURE Working Consistency - Refer to Plant Testing Procedure No. 32. Specifications for Paste: If paste is not proper working consistency, a maximum of 5 c. c. water per 150 grams of paste may be added to adjust. Barbender ~ - 580 + '.2- /O Working Properties - Refer to Plant Testing Procedure M) . 33. Compound shall be plastic, buttery working, and free of any coarse, gritty, or undispersed particles. Material shall be free from lumps due to incom plete mixing. Bonding Properties Refer to Plant Testing Procedure No. 35. Specifications: After compound has dried, tape shall show at least 90% fiber tear when delaminated. Crack Resistance Refer to Plant Testing Procedure No. 37. Specifications: There shall be no large fissure cracks in the wedge, and no cracks in the thinner half of the wedge. Color Specifications: - White Dried compound shall match color of standard sample. RRB:kgc SGP 0018028 July 6, 1972 TEX-977 NEW FORMULA ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (MACHINE TOOLS) DESCRIPTION OF PRODUCT - White Ready Mix Joint Compound used for taping, covering tape, filling corner beads and spotting nailheads. FORMULA Raw Material Nalco 71-D5 Water Preplasticized PVA Emulsion Filler TEX-978 Function R.M. Spec Anti-foaming agent Solvent - ldhesive 185 - Percent Lbs/Batch 0.1 - 7.4 92.5 -5t00 4. > -Hie-rtK) (2-gal) Uo 148-rQO X / 3 7.0 0 1841.00 / 7 cj o 100.00 3104.00 ** One batch yields 51 - one 5 gallon pail WORKING CONSISTENCY Specifications Brabender Viscosity - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. - 385" 20 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery working, and free of any coarse, gritty or undispersed parti cles. Materials should be free of lumps caused by incomplete mixing. BONDING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 35. - After compound has dried, tape shall show at least 757 fiber tear when, delaminated. CRACK RESISTANCE Specifications There shall be no large fissure cracks in the wedge, and no cracks in the thinner hal'f of the wedge. COLOR Specifications - White - Dried compound shall match color of standard- sample. EDO:elz C, SGP 0018029 August 25, 1972 Supersedes: TEX-977 Dated 7/6/72 v ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (MACHINE TOOLS) ... : i I DESCRIPTION OF PRODUCT - White Ready Mix Joint Compound used for taping, covering tape, filling corner beads and spotting nailheads. FORMULA Raw Material Function R.M. Spec Percent Lbs/Batch Nalco 71-D5 Water Preplasticized PVA Emulsion Filler TEX-978 Anti-foaming agent Solvent Adhesive - - 185 - 0.1 - 7.4 92.5 .4.60 996.00 (120 gals) 137.00 4 1700.00 -/ ** One batch yields 45* one 5 gallon pail 100.00 2837.60 WORKING CONSISTENCY Specifications Brabender Viscosity WORKING PROPERTIES Specifications BONDING PROPERTIES Specifications CRACK RESISTANCE Specifications . COLOR Specifications ,, - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. - 385" ^20 3^5 .- Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery, working, and free of any coarse, gritty or undispersed parti cles. Materials should be free of lumps caused by incomplete mixing. - Refer to Plant Testing Procedure No. 35. - After compound has dried, tape shall show at least 757 fiber tear when delaminated,. . There shall be no large fissure cracks in.the wedge, and no cracks in the thinner half of the wedge. - White . - Dried compound shall match color df' standard sample. ; f i ,, j './. ` ` EDO:elz --S SY*'7 -/ denotes change if /4-3/<f. fa/ ' *6/ 0 * * Pa at/*/ / ^ SGP 0018030 April 12, 1973 Formula TEX-977 NEW ACME, TEXAS, PLANT FORMULA READY MIX FILLER TEX-977 DESCRIPTION OF PRODUCT - Filler for Ready Mix Joint Compound TEX-972 and TEX-973. FORMULA Raw Material Gendriv 492S Dowicil 100 Gelvatol 6000 Attagel 40 Mica p80-H Land Plaster TEX-25 Function RM Spec Thickener Fungicide Adhesive Fiber Filler Anti-cracking agent Filler 223 126 126 9 11 Percent Lbs/Batch .50 .15 1.60 4.00 9.00 84.75 40.0 12.0 128.0 320.0 720.0 6780.0 100.00 8000.0 WORKING CONSISTENCY Specifications: - Refer to Plant Testing Procedure No. 32 Maximum Minimum Average 62 58 60 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33 - Filler shall be very heavily bodied and possess fair plasticity. It shall be free of any coarse gritty or undispersed particles. COLOR ' Specifications - White - Dried compound shall match color of standard sample. NOTE: A wet mix of the filler shall be prepared according to Formula TEX-974 at least twice a day or with every sixth or seventh batch of filler manufactured. This prepared mix shall be tested and shall meet all the specifications required of Ready Mix Joint Compound - Formula No. TEX-971. WNG:elz SGP 0018031 March 8, 1974 NEW FORMULA TEX-977 ACME, TEXAS, PLANT FORMULA READY MIX TOPPING COMPOUND NO. TEX-977 ` DESCRIPTION OF PRODUCT - White Ready Mix Joint Compound used for covering tape, filling corner beads and spotting nailheads. To be used in 4-gallon cartons and 5-gallon pails. FORMULA Function RM Spec Percent Lbs/Batch Nalco 71-D5 Water Preplasticized PVA Emulsion Filler TEX-973 Antifoaming agent Solvent Adhesive -- -- -- 185 -- 0.1 -- 6.0 93.9 2.00 929.60 (112 gal) 111.00 (12.3 gal) 1733.00 100.00 2775.60 One batch yields 60 + one 4-gallon carton or 45 + one 5-gallon pail. WORKING CONSISTENCY Specifications < - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. Brabender Viscosity 560 + 20 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery working, and free of any coarse, gritty or undispersed particles. Materials should be free of lumps caused by incom plete mixing. BONDING PROPERTIES Specifications Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall show at least 75% fiber tear when delaminated. CRACK RESISTANCE Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge, and no cracks in the thinner half of the wedge. COLOR Specifications White Dried compound shall match color of standard sample. WNG:elz SGP 0018032 Supersedes: May 29, 1975 Formula TEX-977 Dated: 3/8/74 ACME, TEXAS, PLANT FORMULA READY MIX TOPPING COMPOUND NO. TEX-977 DESCRIPTION OF PRODUCT - White Ready Mix Topping Compound used for finishing, filling corner beads and spotting nailheads. To be used in 4-gallon cartons and 5-gallon pails. FORMULA Function RM Spec Percent Lbs/Batch Nalco 71-D5 Water Preplasticized PVA Emulsion Filler TEX-973 Antifoaming agent Solvent Adhesive -- 125 0.1 -- -- 185 6.0 -- ___< L9 2.00 929.60 (112 gal) 111.00 (12.3 gal) 1733.00 10.00 2775.60 One batch yields 60 + one 4-gallon carton or 45 + one 5-gallon pail. WORKING CONSISTENCY Specifications - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. Brabender Viscosity 560 + 20 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery working, and free of any coarse, gritty or undispersed particles. Materials should be free of lumps caused by incom plete mixing. BONDING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 35. - After compound has dried, tape shall show at least 75% fiber tear when delaminated. CRACK RESISTANCE - Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge, and no cracks in the thinner half of the wedge. COLOR Specifications - White - Dried compound shall match color of standard sample. WNG:elz -/ denotes change SGP 0018033 September 20, 1977 Formula TEX-977 NEW ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS) DESCRIPTIONS OF PRODUCT - White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4 gallon cartons and 5 gallon pails. For selected market trials and shipment to Memphis only. FORMULA Raw Material Dowacil Filler TEX-976 Elvace EP-. 00 Nalco 71D-5 Acrysol ASE-60 Water Function RM Spec Preservative Filler Adhesive Defoamer Thickener Solvent 193 -- 185 125 147 Percent Lbs/Batch .35 94.35 5.00 .10 .20 -- 7.0 1958.0 100.0(11 2.0 4.0 847.0(102 100.00 2918.0 One batch yields 64 1 1 four gallon carton or 52 1 1 five gallon pail. SPECIAL MIXING INSTRUCTIONS - Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler TEX-976 5) Mix until filler is dispersed 6} Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 480 20 to allow for 24 hour viscosity build of 100 pts. WORKING CONSISTENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (580 1 20) For machine tools add 7 gallons H2O (400 + 20) pH Minimum - 9.0 Maximum - 9.5 WORKING PROPERTIES - Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. HCF:jg Continued on Page 2 ... SGP 0018034 . ^ -cr BONDING PROPERTIES Specifications CRACK RESISTANCE Specifications COLOR Specifications September 20, 1977 Formula TEX-977 Page 2 NEW - Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall show at least 90$ fiber tear when delaminated. - Refer to Plant Testing Procedure No. 37. Rating shall be 4 or better. - White Dried compound shall match color of standard sample. HCFjjg SGP 0018035 October 26, 1977 Supersedes Formula TEX-977 Dated 9/20/77 ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS) DESCRIPTIONS OF PRODUCT - White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4 gallon cartons and 5 gallon pails. For selected market trials and shipment to Memphis only. FORMULA Raw Material Function RM Spec Percent Lbs/Batch -/Proxcel CRL Filler TEX-976 Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Preservative Filler Adhesive Defoamer Thickener Solvent 193 -- 185 125 147 .115 94.585 5.00 .10 .20 2.23 1962.77 100.0(11.73gal^ 2.0 4.0 847.0(102 gals) 100.00 2918.0 One batch yields 64 1 1 four gallon carton or 52 1 1 five gallon pail. SPECIAL MIXING INSTRUCTIONS - Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler TEX-976 5) Mix until filler is dispersed 6 Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 480 20 to allow for 24 hour viscosity build of 100 pts. WORKING CONSISTENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (580 1 20) For machine tools add 7 gallons H2O (400 + 20) PH WORKING PROPERTIES -/ denotes change HCF:jg Minimum - 9.0 Maximum -9.5 Refer to Plant Testing Procedure No. 33Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. Continued on Page 2 ... SGP 0018036 October 29, 1968 NEW FORMULA ACME. TEXAS PLANT FORMULA N_, READY MIX JOINT COMPOUND TEX-977 (EM&- TOOLS) ( READY MIX "X") DESCRIPTION OF PRODUCT - WhjUte *5!ea3y^Mixed Joint Compound used for taping, covering tape, filling cornerhead and spotting nails. FORMULA Raw Material Water Filler TEX-970 Ucar WC-130 Benzoflex 50 Source Solvent R.M. Spec. % Act. Ingr. . Body Adhesive Plasticizer 185 183 91.5 8.00 0.50 100.00 Lbs./Batch 400.00 H+*2 (48 gal.)* 700.0 2oo.o 58.3 ti.*7 4.0 I.t4- 1162.3** *Approximately 52 lb./lOO lbs. of active ingredients (this may vary + 2 gallons per batch.) **One batch yields 17(4-)- 5 gallon pails of Ready Mix Joint Compound at 65.6 lbs./pail TESTING PROCEDURE Working Consistency - Refer to Plant Testing Procedure No. 32. Specifications for Paste: If paste is not proper working consistency, a maximum of 5 c. c. water per 150 grams of paste may be added to adjust. Barbender - 580 +-3&-/0 Working Properties - Refer to Plant Testing Procedure Kb . 33. Compound shall be plastic, buttery working, and free of any coarse, gritty, or undispersed particles. Material shall be free from lumps due to incom plete mixing. Bonding Properties Refer to Plant Testing Procedure No. 35. Specifications: After compound has dried, tape shall show at least 90% fiber tear when delaminated. Crack Resistance Refer to Plant Testing Procedure No. 37. Specifications There shall be no large fissure cracks in the wedge, and no cracks in the thinner half of the wedge. Color Specifications: White Dried compound shall match color of standard sample. RRB:kgc SGP 0018037 July 6, 1972 TEX-977 NEW FORMULA ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (MACHINE TOOLS) DESCRIPTION OF PRODUCT - White Ready Mix Joint Compound used for taping, covering tape, filling corner beads and spotting nailheads. FORMULA Raw Material Nalco 71-D5 Water Preplasticized PVA Emulsion Filler TEX-978 Function R.M. Spec Anti-foaming agent Solvent - Adhesive 185 - Percent Lbs/Batch 0.1 -5-r00 4, , - -HdtO-rfK) Ct32-gal) 7.4 92.5 14 8 rOO X / 3 7,0 0 1841.00 /7oO 100.00 3104.00 ** One batch yields 51 - one 5 gallon pail WORKING CONSISTENCY Specifications Brabender Viscosity - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. - 385* - 20 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery working, and free of any coarse, gritty or undispersed parti cles. Materials should be free of lumps caused by incomplete mixing. BONDING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 35. - After compound has dried, tape shall show at least 75% fiber tear when, delaminated. CRACK RESISTANCE Specifications There shall be no large fissure cracks in the wedge, and no cracks in the thinner half of the wedge. COLOR Specifications - White - Dried compound shall match color of standard- sample. ED0:elz H /4 <a^ SGP 0018038 August 25, 197.2 Supersedes: TEX-977 Dated 7/6/72 ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (MACHINE TOOLS) DESCRIPTION OF PRODUCT - White Ready Mix Joint Compound used for taping, covering tape, filling corner beads and spotting nailheads. FORMULA Raw Material Function R.M. Spec Percent Lbs/Batch Nalco 71-D5 Water Preplasticized PVA Emulsion Filler TEX-978 Anti-foaming agent Solvent Adhesive - - - 185 0.1 .4.60 - 996.00 (120 gals) 7.4 92.5 137.00 1700.00 100.00 2837.60 -/ ** One batch yields 45 - one 5 gallon pail WORKING CONSISTENCY Specifications Brabender Viscosity WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. - -365^ t 20 36$ - Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery- working, and free of any coarse, gritty or undispersed parti cles. Materials should be free of lumps caused by incomplete mixing. BONDING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 35. - After compound has dried, tape shall show at least 757 fiber tear when delaminated. CRACK RESISTANCE Specifications . There shall be no large fissure cracks in.the wedge, and no cracks in the thinner half of the wedge. COLOR Specifications - White - Dried compound shall match color of standard sample. EDOielz -/ denotes change / . ./ . / SGp 0018039 April 12, 1973 Formula TEX-977 NEW ACME, TEXAS, PLANT FORMULA READY MIX FILLER TEX-977 DESCRIPTION OF PRODUCT - Filler for Ready Mix Joint Compound TEX-972 and TEX-973. FORMULA Raw Material Gendriv 492S Dowicil 100 Gelvatol 6000 Attagel 40 Mica p80-H Land Plaster TEX-25 Function RM Spec Thickener Fungicide Adhesive Fiber Filler Anti-cracking .agent Filler 223 126 126 9 11 Percent Lbs/Batch .50 .15 1.60 4.00 9.00 84.75 40.0 12.0 128.0 320.0 720.0 6780.0 100.00 8000.0 WORKING CONSISTENCY Specifications: - Refer to Plant Testing Procedure No. 32 Maximum Minimum Average 62 58 60 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33 - Filler shall be very heavily bodied and possess fair plasticity. It shall be free of any coarse gritty or undispersed particles. COLOR Specifications - White - Dried compound shall match color of standard sample. NOTE: A wet mix of the filler shall be prepared according to Formula TEX-974 at least twice a day or with every sixth or seventh batch of filler manufactured. This prepared mix shall be tested and shall meet all the specifications required of Ready Mix Joint Compound - Formula No. TEX-971. WNG:elz SGP 0018040 March 8, 1974 NEW FORMULA TEX-977 ACME, TEXAS, PLANT FORMULA READY MIX TOPPING COMPOUND NO. TEX-977 DESCRIPTION OF PRODUCT - White Ready Mix Joint Compound used for covering tape, .filling corner beads and spotting nailheads. To be used in 4-gallon cartons and 5-gallon pails. FORMULA Nalco 71-D5 Water Preplasticized PVA Emulsion Filler TEX-973 Function Antifoaming agent Solvent Adhesive -- RM Spec --- 185 -- Percent Lbs/Batch 0.1 2.00 -- 929.60 (112 gal) 6.0 93.9 111.00 (12.3 gal) 1733.00 JO.00 2775.60 One batch yields 60 + one 4-gallon carton or 45 + one 5-gallon pail. WORKING.. CONSISTENCY Specifications - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. Brabender Viscosity - 560 + 20 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery working, and free of any coarse, gritty or undispersed particles. Materials should be free of lumps caused by incom plete mixing. BONDING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 35. - After compound has dried, tap3, shall show at least 75% fiber tear when delaminated. CRACK RESISTANCE - Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge, and no cracks in the thinner half of the wedge. COLOR Specifications - White - Dried compound shall match color of standard sample. WNG:elz SGP 0018041 Supersedes: May 29, 1975 Formula TEX-977 Dated: 3/8/74 ACME, TEXAS, PLANT FORMULA READY MIX TOPPING COMPOUND NO. TEX-977 DESCRIPTION OF PRODUCT - White Ready Mix Topping Compound used for finishing, filling corner beads and spotting nailheads. To be used in 4-gallon cartons and 5-gallon pails. FORMULA Function RM Spec Percent Lbs/Batch Nalco 71-D5 Water Preplasticized PVA Emulsi m Filler 1 :X-973 Antifoaming agent Solven t Adhesive -- 125 " 185 -- 0.1 --" 6.0 93.9 2.00 929.60 (112 gal) 111.00 (12.3 gal) 1733.00 100.00 2775.60 One batch yields 60 + one 4-gallon carton or 45 + one 5-gallon pail. WORKING CONSISTENCY Specifications - Refer to Plant Testing Procedure No. 32. - If paste is not of proper working consistency, a maximum of 5 cc of water per 150 grams of paste may be added to adjust. Brabender Viscosity - 560 + 20 WORKING PROPERTIES Specifications - Refer to Plant Testing Procedure No. 33. - Compound shall be plastic, buttery working, and free of any coarse, gritty or undispersed particles. Materials should be free of lumps caused by incom plete mixing. BONDING PROPERTIES Speciiications - Refer to Plant Testing Procedure No. 35. - After compound has dried, tape shall show at least 757. fiber tear when delaminated. CRACK RESISTANCE - Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge, and no cracks in the thinner half of the wedge. COLOR Specifications - White - Dried compound shall match color of standard sample. WNG:elz -/ denotes change SGP 0018042 September 20, 1977 Formula TEX-977 NEW ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS) DESCRIPTIONS OF PRODUCT - White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4 gallon cartons and 5 gallon pails. For selected market trials and shipment to Memphis only. FORMULA Raw Material Function RM Spec Percent Lbs/Batch Dowacil Filler TEX-976 Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Preservative Filler Adhesive Defoamer Thickener Solvent 193 -- 165 125 147 -- .35 94.35 5.00 .10 .20 -- 7.0 1956.0 100.0(11.73 g 2.0 4.0 847.0(102 gal 100.00 2916.0 One batch yields 64 1 1 four gallon carton or 52 1 five gallon pail. SPECIAL MIXING INSTRUCTIONS Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler TEX-976 5) Mix until filler is dispersed 6) Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 460 t 20 to allow for 24 hour viscosity build of 100 pts. WORKING CONS IS PENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (560 t 20) For machine tools add 7 gallons H2O (400 j; 20) pH Minimum - 9*0 Maximum - 9.5 WORKING PROPERTIES - Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. Continued on Page 2 ... HCF:jg SGP 0018043 BONDING PROPERTIES Specifications CRACK RESISTANCE Specifications COLOR Specifications September 20, 1977 Formula TEX-977 Page 2 NEW - Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall show at least 90$ fiber tear when delaminated. - Refer to Plant Testing Procedure No. 37Rating shall be 4 or better. - White Dried compound shall match color of standard sample. HCFrjg SGP 0018044 October 26, 1977 Supersedes Formula TEX-977 Dated 9/20/77 ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS) DESCRIPTIONS OF PRODUCT - White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4 gallon cartons and 5 gallon pails. For selected market trials and shipment to Memphis only. FORMULA Raw Material Function RM Spec Percent Lbs/Batch -/Proxcel CRL Filler TEX-976 Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Preservative Filler Adhesive Defoamer Thickener Solvent 193 -- 135 125 147 -- .115 94^535 5.00 .10 .20 -- 2.23 1962.77 100.0(11.73 ga 2.0 4.0 347.0(102 gal 100.00 2913.0 One batch yields 64 1 1 four gallon carton or 52 1 1 five gallon pail. SPECIAL MIXING INSTRUCTIONS Blend ingredients in following order: 1) Water 2) Elvace EP-200 3; Nalco 4) Filler TEX-976 5) Mix until filler is dispersed 6) Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 430 20 to allow for 24 hour viscosity build of 100 pts. WORKING CONSISTENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (530 1 20) For machine tools add 7 gallons H2O (400 f 20) pH Minimum - 9.0 Maximum -9.5 WORKING PROPERTIES -/ denotes change Refer to Plant Testing Procedure No. 33Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. Continued on Page 2 ... HCF:jg SGP 0018045 January i/, ^> /tS Supersedes formula TEX- 977 Dated-: 10-26-77 ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS) DESCRIPTIONS OF PRODUCT - White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4 gallon cartons and 5 gallon pails. FORMULA Raw Material Function RM Spec Percent Lbs/Batch -/Proxcel CRL Filler TEX-976 Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Preservative Filler Adhesive Defoamer Thickener Solvent 193 -- 135 125 147 .115 94.535 5.00 .10 .20 2.23 1962.77 100.0(11.73gals 2.0 4.0 347.0(102 gals) 100.00 2913.0 One batch yields 64 1 four gallon carton or 52 1 five gallon pail. SPECIAL MIXING INSTRUCTIONS - Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler TEX-976 5) Mix until filler is dispersed 6) Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 430 20 to allow for 24 hour viscosity build of 100 pts. WORKING CONSISTENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (460 20) For machine tools add 7 gallons H2O (400 20) pH Minimum - 9.0 Maximum - 9*5 WORKING PROPERTIES Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. -/ denotes change Continued on Page 2 ... HCF: SGP 0018046 May 2, 1973 Supersedes Formula TEX- 977 Dated: 1/17/73 ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS) DESCRIPTIONS OF PRODUCT - White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4 gallon cartons and 5 gallon pails. -/FORMULA Raw Material Function RM Spec Percent Lbs/Batch Proxcel CRL Filler TEX-976 Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Preservative Filler Adhesive Defoamer Thickener Solvent 193 --- 185 125 147 ---- .113 94.83 4.863 .097 .097 ___ " 2.32 1950.00 100.0(11.73ga: 2.0 2.0 861.68 (104 gal: 100.00 2918.0 One batch yields 64 1 1 four gallon carton or 52 1 1 five gallon pail. SPECIAL MIXING INSTRUCTIONS Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler TEX-976 5) Mix until filler is dispersed 6} Add Acrysol ASE-60 7; Mix until Ready Mix is smooth - pumping viscosity should be 480 + 20 to allow for 24 hour viscosity build of 100 pts. WORKING CONSISTENCY Specifications for Paste Brabender: (460 i 20) Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. For machine tools add 7 gallons H2O (400 20) pH Minimum - 9.0 Maximum - 9.5 WORKING PROPERTIES - Refer to Plant Testing Procedure No. 33Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. -/ denotes change Continued on Page 2 ... HCF:jg SGP 0018047 December 13, 1978 Supersedes Formula TEX-977 Dated: 5/2/78 ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 (HAND TOOLS) DESCRIPTION OF PRODUCT - White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4 gallon cartons and 5 gallon pails. FORMULA Raw Material Function RM Spec Percent Lbs/Batch / PMA-30 Filler TEX-976 / DuPont JCM Nalco 71D-5 Acrysol ASE-60 Water Preservative Filler Adhesive Defoamer Thickener Solvent 193 - 185 125 147 - .112 94.864 4.83 .097 .097 - 2.32 1964.68 100.00 ( 12 gal.) 2.0 2.0 1000.0 (120 gals.) 100.00 3071.0 One batch yields 61+1 four gallon carton or 49 j- 1 five gallon pail. SPECIAL MIXING INSTRUCTIONS Blend ingredients in following order: 1) Water 2) DuPont JCM 3) Nalco 4) Filler TEX-976 5) Mix until filler is dispersed 6) Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 480 + 20 to allow for 24 hour viscosity build of 100 pts. WORKING CONSISTENCY Specifications for Paste - Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (460+20) For machine tools add 7 gallons 1^0 (400+ 20) pH Minimum - 9.0 Masimum - 9.5 WORKING PROPERTIES - Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. -/ denotes change SGP 0018048 NEW Formula TEX-977 July 13, 1979 ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 DESCRIPTION: FORMULA: Raw Material Water DuPont JCM Nalco 7ID-5 PMA-30 Filler TEX-976 White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4-gallon cartons and 5-gallon pails for selected market trials only. Function Solvent Adhesive Defoamer Preservative Filler RM Spec 185 125 193 Percert 2.08C .IOC .111 97.705 Lbs/Batch 1120.2 41.5 2.0 2.3 1950.0 C135 (4.6 gal.) gal.) - Yield: 100.000 3116.0 One batch yields 62+1 four-gallon cartons at 50 lbs/ carton or 50+1 five-gallon pails at 62 Ibs/pail. SPECIAL MIXING INSTRUCTIONS: Blend ingredients in the following order: 1) Water 2) Adhesive 3) Nalco 4) Preservative 5) Filler 6) Mix as required WORKING CONSISTENCY: Brabenaer: of Plant Testing Procedure No. 32. As manufactured - 600 + 20 at 75F. After 3 months - Maximum of 730 at 75F. Minimum - 9.0 Maximum - 9.5 WORKING PROPERTIES: Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. -/ denotes change riCF: pS Continued on Page 2 ...................... SGP 0018049 t NEW Formula TEX-977 July 13, 1979 Page Two BONDING PROPERTIES: CRACK RESISTANCE: COLOR: BACTERIA GF )WTH: Plant Testing Procedure No. 35. When dried, tape shall show at least 90% fiber when delaminated. Plant Testing Procedure No. 37. Rating shall be 4 or better. White Dried compounds shall match color of standard sample. Plant Testing Procedure No. 119. Current Production: Maximum of 6 colonies in 48 hrs. Retain Three Months: Maximum of 20 colonies in 48 hrs. KCF:ps SGP 0018050 February 5, 1980 Supersedes Formula TEX-977 Dated: 7/13/79 -/ DESCRIPTION: ACME, TEXAS, PLANT FORMULA READY MIX JOINT1 COMPOUND TEX-977 White Ready Mix Joint Compound used for taping. topping and texturing. To be used in 4-gallon cartons and 5-gallon pails. FORMULA: Raw Material -/ Water DuPont JCM Nalco 71D-5 PMA-30 Filler TEX-976 Function Solvent Adhesive Defoamer Preservative Filler RM Spec 185 125 193 Percent 2.080 .100 .115 97.705 Lbs/Batcl 938.2 41.5 .0 2.3 1950.0 (113 gal (4 .6 gal -/ Yield: 100.000 2934.0 One batch yields 58+1 four-gallon cartons at 50 lbs/ carton or 47 +1 five-gallon pails at 62 lbs/pail. SPECIAL MIXING INSTRUCTIONS: Blend ingredients in the following order: 1) Water 2) Adhesive 3) Nalco 4) Preservative 5) Filler 6) Mix as required WORKING CONSISTENCY: Brabender: -/ pH Plant Testing Procedure No. 32, As manufactured - 600 + 20 at 75 F. After 3 months - Maximum of 730 at 75 F, Minimum -8.0 Maximum - 9.0 WORKING PROPERTIES: Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. -/ denotes change HCF:ps Continued on Page 2 ..................... SGp 0018051 February 5, 1980 Supersedes Formula TEX-977 Dated: 7/13/79 BONDING PROPERTIES; CRACK RESISTANCE; COLOR; BACTERIA GROWTH: Plant Testing Procedure No. 35. When dried, tape shall show at least 90% fiber when delaminated. Plant Testing Procedure No. 37. Rating shall be 4 or better. White Dried compounds shall match color of standard sample. Plant Testing Procedure, No. 119. Current Production: Retain Three Months: Maximum of Maximum of 6 colonies in 48 hrs. 20 colonies in 48 hrs. HCF:ps SGP 0018052 May 1, 1980 Supersedes Formula TEX-977 Dated: 3/24/30 DESCRIPTION: ACME, TEXAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4-gallon cartons and 5-gallon pails. FORMULA: Raw Material Water DuPont JCM Nalco 71D-5 PMA-30 Filler TEX-976 Function Solvent Adhesive Defoamer Preservative Filler RM Spec 185 125 193 Percent '1.986 Lbs/Batch 99 8.0 "(12 1 gal) 43.61. <4.9 gal) . 105 97.909 2.3 2150.0 Yield: 100.000 3193.91 One batch yields 64+1 four-gallon cartons at 50 lbs/ carton or 51 + 1 five-gallon pails at 62 lbs/pail. SPECIAL MIXING INSTRUCTIONS: -/ Blend ingredients in the following order: 1) Water 2) Adhesive 3)* Nalco - 0 to 50 mis, 4) Preservative 5) Filler 6) Mix as required as required to break foam. WORKING CONSISTENCY; Brabender: PH Plant Testing Procedure No. 32. As manufactured - 600 + 20 at 75F. After 3 months - Maximum of 730 at 75F. Minimum -8.0 Maximum - 9.0 WORKING PROPERTIES: Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. -/ denotes change HCF:ps Continued on Page 2 SGP 0018053 September 24, 1980 Supersedes FORMULA TEX-977 (dated: 5/1/80) ACME, TECAS, PLANT FORMULA READY MIX JOINT COMPOUND TEX-977 DESCRIPTION: White Ready Mix Joint Compound used for taping, topping and texturing. To be used in 4-gallon cartons and 5-gallon pails. FORMULA: Raw Material Water DuPont JCM * Nalco 7ID-5 Proxel CRL Filler TEX-976 Function Solvent Adhesive Defoamer Preservative Filler RM Spec -- 185 125 -- --------- Percent -- 1.986 -- .109 97.905 100.000 Lbs/Batch 998.0 (121 43.61(4.9 -- 2.39 2150.0 gal) gal) 3194.00 Yield: SPECIAL MIXING INSTRUCTIONS: One batch yields 64+1 four-gallon cartons at 50 lbs/carton or 51 + 1 five-gallon pails at 62 lbs/pail. Blend ingredients in the following order: 1) Water 2) Adhesive 3) Nalco - 0 to 50 mis. as required to break foam. 4) Preservative 5) Filler 6) Mix as required. WORKING CONSISTENCY: Brabender: pH WORKING PROPERTIES: -/ denote change BGR: ps Plant Testing Procedure No. 32. As manufactured - 600 + 20 at 75F. After 3 months - Maximum of 730 at 75F. Minimum - 8.0 Maximum - 9.0 Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritting or undis persed particles. Material shall be free from lumps due to incomplete mixing. Continued on Page 2 .... SGP 0018054 SGP 0018027