Document Z4O271Q4Bv4EBa5yEYrb6vY5V
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RREEPPOORRTT OONN TTHHEE M MAANNUUFFAACCTTUURREE,, UUSSEE,, AANNDD RREELLEEAASSEESS
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OOFF PPFFCCss AATT TTHHEE 33MM CCOOTTTTAAGGEE GGRROOVVEE FFAACCIILLIITTYY
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CCOONNFFIIDDEENNTTIIAALL AATTTTAACCHHM MEENNTTSS
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Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000011
Exhibit 2764
33MwAAG0S252277115544
`MMSauabddjeeecAAtvvtaaoiillPaarbbollteeecbbtyyiv33eOMMrdffooerrrIIInnnssppePeccaitilioomnneaavrnn.dd3CMC,ooppyNyoii.nnggG2aa.ss0CC4o-on6nf3ifid0de8enntitiaall IInnffoorrmmaatitioonn::
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000022
33MMAAC022552277115555
131 ml
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Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000033
3MA02527156
`MMSauabddjeeecAAtvvtaaoiillPaarbbollteeebcbtyyiv33eOMMrdffooerrrIIInnnssppePeccaitilioomnneaavrnn.dd3CMC,ooppyNyoii.nnggG2aa.ss0CC4o-on6nf3ifid0de8enntitiaall IInnffoorrmmaatitioonn::
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000044
33MWAAC022552277115577
CONFIDENTIAL BUSINESS INFORMATION Contains Non-PuNic Trade Secret Information
Attachment 3 Typical PFOA Flowsheet
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SieteProecieOrde palmer. G2 040008 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22776644..00000055
ssosarise 3MA02527158
`MMSauabddjeeecAAtvvtaaoiillPaarbbollteeecbbtyyiv33eOMMrdffooerrrIIInnnssppePeccaitilioomnneaavrnn.dd3CMC,ooppyNyoii.nnggG2aa.ss0CC4o-on6nf3ifid0de8enntitiaall IInnffoorrmmaatitioonn::
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000066
33MWAAC022552277115599
CCOoNntFaIiDnsENNoTmIAPLaBcUSTIrNadEeSSSeIveNrFOiRoMmAToInON CONFIDEN~ItAL BUSINESS INFORMAI ION Contains Non-Public Trade Secret Information AAtttaacchhmmeenntt 44 TTyyppiiccaall PPFFBBAA FFlloowwsshheeeett
FT F-7977
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HHYYDDRROOLLYYSSIISS TTOO CCRRUUDDEE AACCIIDD
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RR--2211557799 I1-1t 117766 DDRRYY PPHHOOTTOO CCOOUUPPLLEERR
Sibi Protect Orr 1 Falmer Wo. 53-04-8308 Made
Made
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Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000077
w3MAA205225727116600
`MMSauabddjeeecAAtvvtaaoiillPaarbbollteeecbbtyyiv33eOMMrdffooerrrIIInnnssppePeccaitiiloomnneaavrnn.dd3CMC,ooppyNyoii.nnggG2aa.ss0CC4o-on6nf3ifid0de8ennttiiaall IInnffoorrmmaattiioonn::
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000088
33MUAAC022552277116611
CCCOOoNnNtFFaIiIDDnsEENNNoTTnI-IAPAuLLblBBiUUcSSTIIrNNadEEeSSSSSecIIrNNeFtFOIOnRRfMoMrAAmaTTtIIiOOonNN
Contains Non-Public Trade Secret Information
AAtttaacchhmmeennt 5t5 CCaotStttuaamggmeeaGGrrryooovvfeeCPPeFElClC OMMuatanpnuuuftafac(ct1tuu9r7rii6nn-gg19FF9aa5cc)iil'liittyy
S ummary of Cell Output (1976-1998)~
Base PPFPFBFaPBsPeAAA. PPPPFFMFOBSOAAFA PEPPPBMBCSSSHFFFS PPPPODEOSSCSFFHF S
PDSF
TTOOTTAALL
CCeclllI OOuuttppuutt((iinn tthhoouussaannddssooffppoouunnddssooffFFiinniisshheeddGGooooddss))"z
11907766-85100) 11998511-68550
04a77707361960
400733 360433
68300 13900
36 0
0
3
16
11998666-99007 11999911.-99555 11999966-9988oTTOOn TTAALL
5a159227 7w 151075 ads91s0 ao10sm31:32
547020 75ooe00 245%040 2m52s266
48 302 s56803
2a46w900
325
0252
sms 0
0
0
53
101
57
x23000
995533 661188 s80o4 11009%4 9o1n1 a 4380
LLeeggeenndd:: PPPFFFPPBAAA.PPPPFFFMOBOSAAAF.PPPPBBMESSCSFFHF-SPPPOEOCSSFFH-S PPDDSSFF-
PPPeeerrrffflluluouoorrroooppbrruootpapanaenneeCaCCraabrrobbxoyoxlxyayltlaaettseess PePPPreeefrrrlffflluuulooourroroooroboocmuctettaatanhnnaccenCCeCaraaSbrruboblxfoooyxnlyyaallatatetteeessss PPeePPrrceffrrllfftluuuuoooorrrrooooebbmtuuhtetyatalhnneaeeynScSeululoSflhufooelnfxnaoaatnnteaeesstSeuslforates PPPeeerrrffflluuluooorrrooooeoctchttayannlceeySScuulollfhfooennxaaartneeess Sulfonates PPeerrfflulouorrooddeeccaannec SSuullffoonnaatteess
l2T}~he evTc"TelhTlheheseecfretfaalrrenacocgciftetroitdoovnfnfoolurrofoiforPniPmnEaFCatCft-iirboo-abanncastcciseoeeedndillsocclooafotmmCCpppooootutuetanangdgdesresiGGi0nncrsr"ouo"FbvvFeiseeintnaiwwninssetehhrireteeeaddlGssGhohpueouortotdcdddesosno"w"twavvnngaaeniisrnni.eed1d1w99Awi9c9dc88ioe.drledyliy.n. gDlDey,pepeeni nddiiwnneggiogonhntththoefepFrporiodnducuhtce,t,dyt~op3c)uiacaldl
indicated a his able includes significant levels ranged from a fraction of a percent
indicated in this table includes significant
percentages of on-PFC consis. to substantia[ percentages, Accordingly,
percentages of non-PFC consliments.
the
weight
of"Finished
Goods"
`MMSauabddjeeecAAtvvataoiillPaarbbollteeebcbtyyiv33eOMMrdffooerrrIIInnsnsppePeccaitiiioomnneaavrnn.dd3CCMo,oppyNyoii.nnggC2aa:ss0CC4o-on8nf3ifid0de9enntitiaall IInnffoorrmmaattiioonn::
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00000099
33MwAAn02s52277116622
`MMSauabddjeeecAAtvvtaaoiillPaarbbollteeecbbtyyiv33eOMMrdffooerrrIIInnnssppePeccaitilioomnneaavrnn.dd3CMC,ooppyNyoii.nnggG2aa.ss0CC4o-on6nf3ifid0de8enntitiaall IInnffoorrmmaatitioonn::
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00001100
33MWAAC022552277118633
CC`OOCoNNnFtFaIIiDDnsEENNNoTTnI-IAPAuLLblBBiUUcSSTIIrNNadEEeSSSSSecIIrNNeFtFOIOnRRfMoMrAAmTaTtIIiOOonNN
Contains Non-Public Trade Secret Information
AAttttaacchhmmeenntt 66 `SSuummmmaarryyooffCCototttaaggee GGrroovvee PPFFCC PPrroodduuccttiioonn RReeccoorrddss
PMA M4b Frodtueestion LeMveglsa Omer PFMA-based PMSF based 0 PMSF-based PPA 10 _ PFPA-based TBA bed Ts i PFBA-based FBS bed TE PFBS-based FrOR bed wT 5 PFOA-based FECTS Tod 5 7 PECHS-based Tiegh Foun 7 o Fire-Fighting Foam FRO hued Iie 3 v PFOS-based
iVllb 19.4 0.2
1,0 16.5 0.3 95.1 3 2,7 312,7
Production Levels
Lots
Mgal
1
0,06
0.7 2.3
Oiher Y
Pla
12
v
PFMA-bwed
17.2
Y
a PPMSSFF] -bbassedd
w 0i.59 o10T w0.1
FA bad
Ti
v
2
[rns ted PFBA-based
PFHxg-based
EE21.4
Y
2.4
g2 [[PPPFOrrocAmH-bsbaebsxuededd
I E31L0).0 5 ....~J........ ow261,1
Y v
FPEocCFHgSb-biansgedPom Ta1e7.2
TT4 30,004011
Y v
PROSwaed ~ire2Fighting Foam wes 146,3
B08 11
204.1
Y v
FDA bad PFOS-based
0S 1,466.6
250
49.6
Y
PFDA-based
O. 5
LLeeggeePnnddE:MA Prfluoromethanscarbonate:
PPFPFFFEMMPMASSA P--eP_PPreeerhrrfotlflurulouoororporormomomeepetttahhbnauanenneeecsscauaarlrflbbooonoxnanytseela:te
PPPPFFFEPBBGASAA --PPPPeeeerrrfffllu]luucooorrmrooopbbbruuuoatapannnaseneescccaauartberbbonooxrxyayylailateete
PFBS -
PPFFOAS PFHxS
--PPePPerefefrlrlfululcuourorooonrbcoocubhiteeasxxnnaaeenneescuasslrufubollofnofxaynotleantee
FiPPPrEFEeOC.CFHAiHSg-Sh--tPiePPnreegfrrlfuulFouoroomorneoodcehtCtahyonylnetytcccyaalcirlonboheohexdesyxsalamannateeellssuuallcffootnniaaottene: POS:based andor PFHS-based mateisls
PFPPRFiFrOOeD-SSAF-i*gPPhPeteeicrnftlgllhuiooForrorooaooomdccettc-aaannCneeoecssnauutrlalffbionoonnenadastteeslmataell fraction PFOS-based and/or PFHxS-based materials
PDS Peeorodecane sulfone PFDA - Perfluorodecane carboxylate
PFDS - Perfluorodecane sulfonate
NNootteess.:: This atachnens provides sumomfcaurcay availabe records fom he tmperiodsspecifid
HH21".oowTwnehfeviosveerrarm,t,taacrtceohicromorddeisnnsctaauprrrreeoenonvotitdtlecycsuasranvre~atnudltmlsyybmalvavarrayeilcl~aolbfrldecesufrfioroserrnnoaotlllt]lysmmaovoosanfihtlhasisby/alyeeeafraroerscssopierndcisthhffeeylsoswerhatteimttheheeerpptieemtrrhiieeooddpmsse.a.rniuofdascstpuerciinfgieodf. merits
n2rTe.edccohowrnfdfodoeerrddkmeiianndtihtuohopnossaieen
currently available records
rCeocroirdewGarsovneied in he records was initiated in the
eerooriatidoeln 31 is not sufficient to specify
eleclxofluormation cells at
Cotage whether
Cottage
Groveo nid isewbere the manufacturing of materials
Grove or initiated elsewhere
a3M5n.adEElwxapoplrhhaknoaeuadttsiouaonpnndaoostffUoCUfnoingttitatal.sgl:eonMMGs;hrlboOvt-ehtt.heohr-usoPanudrssooofafppdonouuondunfddrsssc:;iLLetooirtssis--nNNooutunmedbmerboorfefekctoorrrtds,sspbpeteciefvidoe.dq,uabbnuutttitnoyo fvvooorllumumamteei/owwnee.iigghht.;
Mgal - thousands of gallong; Other- Production of materials noted in record, but no quantity information_
`MMSauabddjeeecAAtvvtaaoiilPaarbbollteeecbbiyyv33eMMOrffodorrerIInnIssnppePeccattliiomonenraavnn.dd3CCMo,oppyNyoii.nnggC2aa.ss0CC4o-on6nf3ifid0de9ennttiiaall IInnffoorrmmaattiioonn:
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00001111
33MwAAo0z2s52277116644
CORTRNTFIALeBUTSoHeESSenOWRAoTInON CONFIDENTIAL BUSINESS INFORMATION Contains Non-Public Trade Secret IJffonnation
PPFIMMAA-Dbaesedd
PMSF-based
Fir: PFPA-based
PFBA-based
o [Fr ~ PFHxS-based
| 2 [Fronmmes '7 PFOA-based
| ~ |VEPECCHHSS-Bbaasseedd
on R--_Tone ......
MIb
e16s.3
62.7
-- 0.6
418.3
hr2.2
IY v 96.3
Production Levels
Lots
Mgal
]
37
2
117
0.3
Other
Y Y
113300,99
8
606.0
Y v
Fire-Fighting Foam
5,438.9
48 2,852.1
Y
PFOS-based
Troy PFDA-based ToPFDS-based
1,165.7
117
31,4
Y
= 15.3
2
a4.4
i PFMA-based
; v 1
Y
PMSF-ba~ed ................ 142.7
16
PPFFPPAA--bbaasseedd
C336.6
: [Per PPFFBBAAb-absaseedd
~ [PFPOroAA-bbaaseedd
~ PECHS-based
6 269. I
155
w668s.9
w8T1
78.2
30
2 |TFiirrceF-Fiigghht'iii~nga~F'foooamm
E45E3).8
8
PPFOOSS-bbaasseedd.
2 822,3
71755
y
Y Y
vY v
Y
Y
882244.77
Y
23 i~'o~ ............. YY
PFDA-based
16,9
2
PFDS-based
trLegend: Tos ete cate PFMA - Peffluoromethane carboxylate Fe PFMS - Perfluoromethane sulibnate hoe PFPA - Perfluoropropa.ne carboxylate HER Fone PFBA - Perfluorobutane earboxylate ee PFBS - Perfluorobutane sulfonate i Foe, PFIq_xS - Perfluorohexane sulfonate re i, PFOA - Perfluorooctane carboxylate SF wire PECHS - Perfluoroethylcyclohexane ~ulfonate ves Fire-Fighting Foam - Contained small fraction T mie e, PFOS - Perfluorooctane sulfonate
26.1
HOS ie PFOS-based and/or
ikr PFHxS-based materials
PFDA - Perfluorodeeane carboxylatc
PFDS - Perfluorodecane sulfonate
-Notes: cnt ovis mya ero er i 1. This altachment provides a summary of currently available recorc~ fi'om the time periods specified. dbee et However, records are not currently available for all months/years in these time periods. mtr 2. Information in currently available records is not sufficient to specify whether the manufacturing of materials LR To Co Er recorded in those records was initiated in the electrofluorinadon celia at Cottage Gro've or initiated elsewhere previa and worked up at Cottage Grove. TT tonsLsNanmatohiss, 3. Explanation ofUmts: Mlb - thousands of pounds; Lots - Number of lots specified, but no volume/weight;
Mgal - thousands of gallons; Other - Production of materials noted in record, but no quantity information.
2
Ws Ailey 5 r or scE ionard Coping5Csonn oman Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22776644..00001122
swansriss 3MA02527165
(CCCOOoNNmFFtIIiDDnEENNNoTTnLIAAPeLLlBiBUUTSSrIIaNNdEEeSSSSS eIINNrFFOOfRRorMMmAAaTtTiIIoOOnNN Contains Non-Public Trade Secret Information
TT MPMiSSFFb-baasseedd
FrPFPA-based i PFOA.based
| 3 [rece PECI IS-based
[ecrammrom Fire-Fighting Foam FroStons PFOS-based Freer PFDA-based
vrei Production Levels
Mb Las Mes ower Mlb
Lots
Mgal
Other
5 1166,55
3 3
2
27.8
5
To Ii.9
10
50+ 255.0
6
Ee124.0
20
50.1
Y
wv 0.4
Y
tepnt Legend: Vika -Feturometare caters: PFMA - Perfluorometha~e carboxylate FINS tomaslro PFMS - Perfluoromethane sulfonate FETA Foro aoc PFPA - Perfluoropropane carboxylate [mt PFBA - Perfluorobu~ane carboxylate FESFeroosme PFBS - Perfluorobutane sulfonate PLS ethane alfnge PFHxS - Perfluorohexane sulfonate FHOR: Paani abomine PFOA - Perfluorooctane carboxylate FECHS Peeshpkoeobelannce PECHS - Perfiuoroethylcyclohexane sulfonate Fach Fon Coresoo cen FOS bs to FSS bus mails Fire-Fighting Foam - Contained small fraction PFOS-based and~or PFHxS-based materials FEO heave ote PFOS - Perfluorooctane sulfonate FDA Peltodecne cohort PFDA - Perfluorodecane earboxyIatc FED Fees lone PFDS - Perfluorodecane sultbnate
Now:Notes: hs ste provi sry comedy ible crs omeve pends peed 1. This attachment provides a summary of currendy available records fxom the rime periods specified. Tower eto rt cen ssl for sl mbes hs ie ere However, records are net currcmly available for all months/years m these time periods. 2 min aren sag es ot efg o cls bees acing of marl 2, Information in currently available records is not sufficient to specify whether the manufacturing of materials hind bt eens ed 1 no cb + Cong Gov ob recorded in those records was initiated in the electrofluorination cells at Cottage Grove or initiated elsewhere the Competroe and worked up at Cottage Grove. laionf Un. Mb. ss of pounds Lot - Sur ffs spf, ut volevcghs, 3~ Explanation of Units: Mlb - thousands of pounds; Lots - Number of lots specified, but ne volume/weight; in mand oflon, Gis Prd ofls acd chord. doy oti Mgat - thousands of gallous; Other - Production of materials noted fl~ record, but no quamity iifformation.
3
SMWuaabddjeeecAAtvviaialFabrbltleeebboyyw33eMOrffodorrerIInnIsstppePecactitiimooennrava.nrdd3CC.ooppyNyoii.nngg2aa.ss0CC4o.o8nn3fdi0dn8etntaiall
Information
Information:
Subject to Protective Order In Palmer v. 3M, No. C2-04-6309
22776644..00001133
swaszsariss
3MA02527166