Document Z4GwwNgB08VkZL1b9n52Ezjop
FILE NAME Brakes BRK
DATE 0000
DOC BRK306
DOCUMENT DESCRIPTION AIA - Recommended Work Practices - Fabrication and Use of Asbestos Friction Materials
ae S,
BS
Speer
Street
USPHS Membrane Airborne Asbestos Fibers
Vacuum Cleaning Stations
Filter
Method
For
Page 1 Page 2 Page 3 Page 5 Page 7 Page 8 Appendix A
Appendix B Appendix C
Introduction
The Occupational Safety and Health Act was signed into and became effective on April 28 1971. The Act has the
every American worker a safe and healthy workplace
law on December
stated objective of
29 1970 assuring
On December 7 1971 the Secretary of Labor issued an emergency standard for exposure to asbestos dust As required by the Act a permanent standard for
asbestos exposure was promulgated six months later on June 7 1972. The present OSHA Asbestos Standard discussed in this booklet became effective July 7 1972 Thorough understanding of the standard is important to management of any company utilizing asbestos in its manufacturing or processing operations
The work practices on the following pages have been prepared by the Standards and Technical Committee of the Asbestos Information Association America They are intended as general guidance for safe and clean workplace conditions in keeping with the spirit and intent of the OSHA Standard for Occupational Exposure to
Asbestos Dust :
These practices have been developed through careful study and consultation and are recommended as good procedure It is recognized that manufacturing conditions vary Implementation of the practices contained herein cannot be considered as a guarantee of OSHA compliance Where there may be a question of compliance OSHA personnel should be consulted
A proposed revision to the OSHA Asbestos Standard was published in the Federal Register on October 9 1975. This work practice booklet will be revised as necessary to reflect any approved changes to the standard
:
Products and Operations
The types of asbestos friction material products covered by these work practice recom-
mendations are
Brake eat
band
6:
Operations to which these work practices may apply are
Clutchassemblyandrebuilding operations
4 transmision ex
asaembslysembly
Automatictaransmission assembly
Summary of OSHA Asbestos
Standard
General Comments OSHA published a Standard for Exposure
to Asbestos Dust in the Federal Register Vol 37 No. 110 dated June 7 1972. The
standard was recodified from 1910.93a to
1910.1001 in the Federal Register Vol 40 No. 103 dated May 28 1975. The standard is reproduced as Appendix A. The standard applies to any manufacturing fabricating or handling process or operation utilizing asbestos fiber or materials containing asbes-
tos fiber
The standard is divided into eight major
sections
1. 1910.1001 -Permissible Exposure
Limits Sets maximum allowable asbestos fiber
concentration in the workplace air 2. 1910.1001 -Methods of Compliance Recommends procedures to meet permis-
sible exposure limits
3. 1910.1001 PersonaPlrotective Equipment
Specifies types of personal protective equipment and defines circumstances under which they are required 4. 1910.1001 -Method of Measurement
1910.1001 -Monitoring Specifies monitoring procedures to determine if work places meet permissible expo-
sure limits
5. 1910.1001 -Caution Signs and
Labels
States when caution signs and labels are required and wording to be used
6. 1910.1001 -Housekeeping Specifies results to be obtained from housekeeping and methods of waste disposal 7. 1910.1001 -Recordkeeping Specifies type and duration of monitoring
recordkeeping States requirements for employee notification of monitoring results if exposure is in excess of permissible exposure limits and of corrective action being
taken
8. 1910.1001 -Medical Examinations Details requirements for medical examina-
tions and duration of medical record-
keeping
Specific Comments
1. Exposure Limits 1910.1001 b It is the employer's responsibility to assure that exposure of employees to airborne
concentrations of asbestos fibers does not
exceed the limits prescribed by the stand-
ard
The OSHA standard maximum permissible ex-
posure limits of asbestos fiber in the work-
place air are
a Eight weighted average 1 At present 5 fibers longer than 5 micrometers per cubic centimeter 2 Effective July 1 1976 2 fibers longer than 5 micrometers per cubic centi-
meter
b Ceiling concentration 1 At present 10 fibers longer than 5
micrometers per cubic centimeter
2 Effective July 1 1976 No change
2. Methods of Compliance 1910.1001 c
Engineering Methods Engineering controls such as isolation en-
closure exhaust ventilation and dust collec-
tion shall be used to meet the prescribed permissible exposure limits
All hand operated and power operated tools which may produce airborne asbestos fibers in excess of permissible exposure limits _ shall be provided with local exhaust sys-
tems
Wet Methods
When practicable asbestos products shall
be handled in a wet state sufficient to pre-
vent the emission of dust to the atmosphere This procedure is not required where the usefulness of the product might be diminished by wetting The applicability of wet methods is limited In most situations engineering controls provide more efficient pro-
cedure
3. Personal Protective Equipment and Clothing 1910.1001 d
e Respiratory Protection
Respiratory protection is required whenever the airborne concentrations of asbestos fiber exceed either the permissible time weighted average level or permissible ceiling concentration The type of respirator to be used is determined by the fiber concentration in the workplace
a Fiber concentrations up to but not ex-
ceeding 10 times the allowable limit Air purifying respirator- reusable or single use
b Fiber concentrations up to but not ex-
ceeding 100 times the allowable limit Powered air purifying respirator
c concentrations excee1d00itnimges
the allowable limit Type C supplied air respirator
Protective Clothing
Whenever airborne fiber concentrations ex-
ceed the prescribed ceiling level the employer shall provide and require the use of special clothing such as coveralls or similar whole body clothing head coverings gloves and foot coverings When the employer provides and requires the use of special clothing he shall also provide for the laundering or disposal of the special clothing
Whenever airborne fiber concentrations ex-
ceed either the permissible weighted average concentration or permissible ceil-
ing concentration the employer shall provide change rooms for his employees Change rooms shall be equipped with two
separate lockers or containers for each
employee so separated or isolated as to prevent contamination of the employee's
street clothes from his work clothes
4. Measurement and Monitoring 1910.1001 e f
The standard requires that all workplaces
where asbestos fiber may be released shall be monitored to determine exposure levels After initial determination of airborne con-
centrations monitoring shall be of such frequency and pattern as to represent with
reasonable accuracy the levels of exposure
Monitoring must be repeated at no less than
month intervals where exposure to
asbestos dust may reasonably be foreseen to exceed permissible exposure limits
All monitoring shall be done by the membrane filter method Appendix B provides a description of this procedure
Affected employees or their representatives shall be given a reasonable opportunity to observe any required monitoring and shall have access to the monitoring records
Any employee found to have been exposed
at any time to airborne concentrations of
asbestos fibers in excess of the prescribed limits shall be notified in writing of the exposure as soon as practicable but not later than five days of the finding
5. Caution Signs and Labels 1910.1001 g
Caution signs shall be displayed at each workplace where asbestos fiber concentrations exceed permissible exposure limits Caution labels shall be applied to all materials and products which during any rea-
sonably foreseeable use might release con-
centrations of asbestos fibers in excess of
permissible exposure limits
Signs and labels are described in detail in Appendix A.
6. Housekeeping 1910.1001 h All external surfaces machinery and equip-
ment shall be maintained free of asbestos
fiber accumulations that might if dispersed
create asbestos fiber concentrations above
permissible exposure limits
For recommendations on housekeeping procedures see Housekeeping section
under General Recommendations
7. Recordkeeping 1910.1001 ) Every employer shall maintain records of personal and environmental monitoring required by the standard Records shall be maintained for a period of at least three
years
8. Medical Examinations 1910.1001 ) Preplacement annual and termination medical examinations must be provided or made available by the employer for any employee . engaged in occupations exposed to airborne concentrations of asbes-
tos fibers These medical records must be
kept for 20 years and are available to the employee's physician
General Recommendations
Exhaust and Dust Collection
Systems
The OSHA Asbestos Standard requires that exhaust and dust collection systems be designed and maintained in accordance with American National Standard Fundamentals Governing the Design and Operation of Local Exhaust Systems ANSI Z9.2-1971 This publication is available from
American National Standards Institute
1430 Broadway New York N.Y. 10018
The National ^ missionsStandards for Haz-
ardous Air Pollutants NESHAPS as published by the Environmental Protection Agency in the Federal Register Vol 38 No. 66 dated April 6 1973 and amended Octo-
ber 14 1975 state that there must be no
visible emissions to the outside air from as-
bestos mills or from buildings in which com-
mercial asbestos is used in the manufacture of textile materials
cement products fireproofing and insulating materials friction products
paper millboard and felt floor tile
plastics and rubber materials
chlorine shotgun shells
asphalt concrete paints coatings caulks
adhesive and sealants
Visible emissions are defined as emissions which contain asbestos and which are visu-
ally detectable without the aid of instru-
ments Rather than meet the visible-
emission requirement air cleaning proce-
dures using a fabric filter collector may be
employed When the use of fabric filters creates a fire or explosion hazard use of a high energy wet collector may be authorized by EPA
For small and intermittent production and fabrication operations major dust collection systems of the high volume low velocity type design described in the references
above may not be necessary Instead sys-
tems of the low volume high velocity type utilizing as their exhaust air source a high efficiency vacuum cleaner could be suitable For design information on these sys-
tems attention is invited to the AIA booklet Recommended Work Practices on
Shop and Field Fabrication of Asbestos
Sheet Products This booklet is available
on request to AIA
All exhaust and dust collection systems
should be inspected periodically for proper
functioning For continuous operations it is recommended that the system operation and the interior of the baghouse be checked daily A scheduled maintenance program that includes bag replacement should be prepared and followed
Wherever possible operations involving
containing materials should be
isolated from other work areas by partitions
curtains or other means If central exhaust
systemarse utilized the work areas should
be
gn pres- under maintained
maintained
maintained
as as
gn negative negative presnegative negative negative
sure
sure
Housekeeping
Housekeeping is an essential part of any manufacturing operation is even more essential in an asbestos plant because airborne dust created by lack of good housekeeping has the potential for harm to employees
The OSHA Asbestos Standard stipulates
that all external surfaces ainn anyplace of
of fiber asbestos asbestos fiber A WAN WAN
would be excessive
with asbestos dust It is important that both new employees and employees with tenure have information concerning the safe use of asbestos brought to their attention at periodic intervals Each employee should
be informed of
a Operations which could result in exposure to excessive asbestos fibers b Engineering controls and workplace practices for employee protection c Purpose and proper use of respiratory
equipment equipment
equipment equipment equipment
andMedical examination requirements
e Provisions of the OSHA asbestos
standard
A copy of the OSHA Asbestos Standard
should be available to employees The AIA pamphlet What Every Employee Should Know About Asbestos and Health
is recommended for distribution to em-
ployees The pamphlet is available at mini-
mal cost from the Association Posters may
an
et et 808SIOS et et
posters
808SIOS
et posters
Surface cleaning should be accomplished
by a vacuum process Portable vacuum
cleaning units should be equipped with
internal filtration and disposable dust bags
Single or hose stationary vacuum
cleaning systems designed for use with |
A Oa
tian
wel
TL
A record of employee training should be
kept The record may appropriately include
for each employee name social security
number and job title along with the date
including and description of training
ma-
terials distributed
Vase Demes
No visible emissions to the outside air may
result from collection processing packaging transporting or deposition of any ascontaining waste material Alternatively wastes may be mixed with water
and sealed in a labeled tight container and deposited at a disposal site or they may be formed into friable forms and deposited at a disposal site
Specific Recommendations
Normally friction materials should be ob-
tained from the manufacturer in finished form cut machined and drilled to fit
particular requirements This procedure avoids additional fabricating operations
Fabricating equipment such as grinders lathes drill presses working on large capacity operations should be equipped with
high volume low velocity exhaust and dust
mendations on page &
Intermittent short duration machining op-
erations might be equipped with hign velocity low volume exhaust and dust collection systems All dust control systems which discharge exhaust air to atmosphere must be equipped with fabric filter collection devices U.S.
Environmental Protection Agency National
Emission Standards for Hazardous Air Pol-
Asbestos Federal Register Vol 38 No. 66 dated April 6 1973
If dust control by means of exhaust ventilation is not feasible or practicable wet machining utilizing fluid cutting lubricants might be a suitable alternate
Dust and chips generatedby the machining
operations shoC 2 ved aquar preaby ) VETLUT methods ED 3.8-
preaby
paragraphparagraph
tions
After fabricating and before shipping all excess dust and chips should be removed
from the surfaces of friction material to prevent dust contamination of the fabricator's
workplace and no customer's workplace
Information and Training
Employees assigned to a work area where
exposure to airborne concentrations of as-
bestos fibers may exceed the maximum
permissible permisble
permissible permis ible
limitslimits
should
be
fully
informed
of the possible hazards to health associated
theNESHAPS amend-
ment dated October 14 1975. The OSHA OSHA
Asbestos Standard requires that asbestos waste which when handled or transported could generate airborne fibers in excess of the permissible exposure limits be disposed of in sealed bags or closed con-
tainers impermeable to asbestos fibers
Personal Hygiene
In the preparation of containing products unless good procedures are fol-
lowed dust conditions can result Employees must be aware that inhalation of asbestos dust may be a serious risk to
health Every effort should be made to
eliminate dust conditions and avoid exposure to dust
Good personal hygiene practices are important in every working situation When working with asbestos workers are urged to observe the following personal hygiene practices for their own health protection their families and those with whom they
work
Do not smoke
Wash before eating
Shower after work
Respirators and special clothing are provided for worker protection under
certain excessive dust level conditions
These items of personal protective equipment deserve the highest respect
of the worker and should be worn prop-
erly when required Change to work clothes upon arrival at work and change from work clothes at conclusion of work Use change rooms
for this purpose
If work clothing is taken home carry in a bag impermeable to asbestos fibers and wash separately from other clothing Never shake dusty clothing Use a washing machine
Appendix A
RULES AND REGULATIONS
Title LABOR
Chapter Occupational Safety
and Health Administration Depart-
ment of Labor
PART OCCUPATIONAL SAFETY AND HEALTH STANDARDS
Standard for Exposure to Asbestos
Dust
On December 7 1971 an emergency
_ temporary standard concerning exposure to asbestos fibers was published in the
FEDERAL REGISTER 36 F.R. 23207 In ac-
cordance with section 6 3 of the WilSteiger Occuptaional Safety and Health Act of 1970 a notice of proposed rulemaking regarding a permanent
standard for exposure to asbestos fibers was published in the FEDERAL REGISTER ON
January 12 1972 37 F.R. 466 The no-
tice invited interested persons to submit
both orally and in writing data views and arguments concerning the proposal
On or about January 24 1972 the Advisory Committee on Asbestos Dust was established and requested to make written recommendations with regard to the proposed standard on asbestos On or about February 1 1972 the Department of Health Education and Welfare transmitted to the Secretary of Labor a criteria document containing Recommendations for an Occupational Exposure Standard for Asbestos by the National Institute for Occupational Safety and Health NIOSH Public notice was given of the receipt of the recommendations
and their availability for inspection and
copying On or about February 25 1972 the Advisory Committee on Asbestos Dust submitted its written recommendations to the Assistant Secretary of Labor for Occupational Safety and Health
Note Federal Register Vol 40 No. 103
May 28 1975 p 23072 announced that the OSHA standard for Exposure
to Asbestos Dust was recodified from 1910.93a to 1910.1001
Pursuant to the notice of rule making a hearing was held on March 14 through 17 1972 for the purpose of receiving oral data views and arguments concerning the proposed standard On or about March 31 1972 the presiding hearing ex-
aminer certified to the Assistant Secre-
tary of Labor for Occupational Safety and Health the record of the proceeding The record includes prehearing written comments a transcript of the oral presentations made at the hearing and numerous exhibits received during the course of the hearing or within the pe-
riod allowed after the close of the
hearing The proposed standard dealt with 1
permissible concentrations of asbestos fibers 2 methods of compliance 3 warning signs 4 monitoring 5 medical examinations and 6 recordkeeping Each of these major proposals elicited comments arguments objections and counterproposals They all have been examined and considered
1. Acceptable concentrations of asbestos dust The proposed standard would limit occupational exposure to hour weighted average TWA airborne concentrations of asbestos dust not exceeding five fibers longer than five micrometers per milliliter Concentrations above five fibers but not to exceed 10 fibers ceiling concentration would be permitted up to 15 minutes in an hour but for not more than 5 hours in any one hour day
NIOSH in effect has recommended that the fiber TWA and fiber peak concentrations be permitted only
for 2 years thereafter TWA concentra-
tions should be not more than 2 fibers
per cubic centimeter cm.of air and peak concentrations should not exceed 10 fibers with no time restriction Numerous objections and counterproposals have been made with regard to both the limits of asbestos fiber concentrations and the time periods to comply with them Some for example have recommended return to a fiber standard of an earlier day i.e. a level adopted under the Healey Public Contracts Act in 1969. Others have recommended a fiber standard to become effective in 6 months then a fiber standard for 2 years and finally a zerofiber standard after 3 years These recommendations give a fair indication of the wide spread of the counterproposals
No one has disputed that exposure to asbestos of high enough intensity and long enough duration is causally related to asbestosis and cancers The dispute is as to the determination of a specific level below which exposure is safe Various studies attempting to establish quantitative relations between specific levels of exposure to asbestos fibers and the appearance of adverse biological manifestations such as asbestosis lung cancers and mesothelioma have given rise to controversy as to the validity of the measuring techniques used and the reliability of the relations attempted to be established Because of the long lapse of time between onset of exposure and biological manifestations we have now evidence of the consequences of exposure but we do not have in general accurate measures of the levels of exposure occurring 20 or 30 years ago which have given rise to these consequences There
are also controversies concerning the
relative toxicity of the various kinds of asbestos and varying hazards in different workplaces
It is fair to say that the controversy
has centered in the area between a twofiber TWA concentration and fiber TWA concentration with variations on the time needed for compliance Many
employers support a fiber TWA Most medical opinion is divided between
a fiber standard and a fiber
standard
In view of the undisputed grave con-
sequences from exposure to asbestos fibers it is essential that the exposure be
regulated now on the basis of the best evidence available now even though it may not be as good as scientifically de-
sirable An asbestos standard can be re-
evaluated in the light of the results of ongoing studies and future studies but cannot wait for them Lives of employees
are at stake It is concluded that there should be
one minimum standard of exposure to
asbestos applicable to all workplaces exposed to any kind or mixture of kinds of asbestos Reasons of practical administration preclude a variety of stand-
ards for different kinds of asbestos and of workplaces Also while the evidence tends to show that crocidolite for instance is more harmful than chrysotile the evidence is not sufficient to establish separate standards for varieties of asbestos
Because there must be one standard governing exposure to all varieties of asbestos and in workplaces apparently more hazardous than others because
some present employees with regular exposure to asbestos have probably already accumulated great doses of asbestos fibers due to higher levels of exposure in the past because it appears that levels of exposure which may be safe with regard to asbestosis are not safe with regard to mesothelioma because the statute requires the protection of every employee even of one who may have regular exposure to asbestos during a working life which may reach or even exceed 40 years and because of several other considerations which have been urged and are reflected in the record of the proceeding the conflict in the medical evidence is resolved in favor of the health of employees As of July 1 1976 TWA concentrations of asbestos fibers longer than 5 micrometers will not be allowed to exceed two fibers with a ceiling value of 10 fibers The current TWA concentrations of five fibers and
ceiling concentrations of 10 fibers will be permitted until July 1 1976 during what will be a transitional period deemed necessary to allow employers to make the needed changes for coming into compliance with the more stringent standard
The record shows that the many work operations subject to the single asbestos standard textile manufacturing industrial and marine installation etc. will meet varying degrees of difficulty in complying with the standard In some plants extensive redesign and relocation of equipment may be needed It appears however the delay in the effective date of the fiber standard will provide all employers a reasonable time to comply At the same time so long as the celling limit is complied with no harm is reasonably expected to result from exposures during the transitional period
2. Methods of compliance It has been pointed out by many persons that protection against asbestos fibers is best obtained by controlling the generation of fibers first and secondly by controlling the dispersion of released fibers into the ambient air of the workplaces Therefore the standard requires feasible technological controls and appropriate work practices as the primary means of compliance Rotation of employees as a way of meeting the TWA concentration requirement is allowed only in stated exceptional circumstances because as a general rule it would be difficult to implement Personal protective equipment such as respirators cannot be relied upon because among other reasons they
may be so uncomfortable as to be bur- also many helpful comments The recom-
densome except for short periods of mendations of NIOSH and of the Advi-
time Therefore it is expected that respirators and shift rotation will be used during the period necessary to install en-
sory Committee on Asbestos Dust were
much more specific with respect to both frequency and type of medical examina-
gineering controls and to train employees in sound work practices but after
tions to be required The comments vary as to the class of employees to be ex-
technological compliance has been achieved their use must be limited to
amined and as to the frequency of the
examinations
special work situations and emergencies Where both are practicable shift rota-
The adopted standard requires medical
examinations both at the beginning and _
tion is required
the termination of employments exposed
3. Labeling The proposed standard to concentrations of asbestos fibers and
stopped short of requiring labeling as- also requires annual medical examina-
bestos and containing products tions of every employee exposed to air-
The proposed standard would have re- borne concentrations of asbestos It has
quired only warning signs at locations been pointed out that in certain indus-
where asbestos hazards are present tries such as construction an employee
However labeling rather than warning may work for several employers during
signs has proved to be a point of con- the same year Accordingly the standard
troversy Both NIOSH and the Advisory does not require either preemployment
Committee on Asbestos Dust recom- or termination or periodic examinaton
mended labels for asbestos products and of any employee who has been examined
containers and these recommendations in accordance with the standard within
became very controversial in the course the past year
of the proceeding Many counterpro-
One question which has been raised
proposals have been made as to the language of the warning as well as to the
goes to whether the employer or the employee should be allowed to choose the
products to be subject to the labeling examining physician The standard
requirements Employers in general gives the option to the employer Since
strongly contend that 1 finished prod- some employers already have a medical
ucts which effectively entrap asbestos
fibers so that these would not be released
in the normal use of the products should
examination program in operation and also have medical departments with some expertise in the diagnosis of abes-
not be required to be labeled and 2 related diseases it seems more
words such as danger and cancer are reasonable to permit them to utilize the
unwarrantedly alarming Both contentions have merit and the
standard has been changed accordingly
present programs and expertise than to permit an employee to choose a private general practitioner
4. Monitoring The proposed standard would have required personal monitoring and environmental monitoring Many issues have been raised concerning the availability and reliability of measuring instruments frequency of monitoring and conditions in which monitor-
6. Records The standard as proposed and as adopted requires maintenance of records of monitoring and of medical examinations Most of the controversy in
this area has revolved around the question whether an employer should be allowed to have access to the results of
ing should be required The adopted standard takes the objections into consideration It requires periodic monitoring at intervals no longer than 6 months thus allowing considerable time and dis-
the required medical examinations The apprehension of those who have argued against employer access is based on the expectation that some employers will use the medical examinations as a means of
cretion and prescribes the use of the screening employment applicants and
er?
membrane filter method which is an ac- worse as grounds for discharging current
ceptable method for determination of employees who show signs of being af-
asbestos fibers
fected by exposure to asbestos Since the
It has also been recommended that purpose of the medical examinations is
employees or their representatives should to monitor the health of employees ex-
have an opportunity to observe the posed to the hazards of abestos em-
monitoring The recommendation has been accepted
5. Medical examinations The pro-
ployees cannot in reason be granted the privilege of refusing to disclose to their employers results of occupational expo-
posed standard would only require an sure It does not make sense to require
appropriate medical examination on a employers to provide medical examina-
periodic basis The generality of the pro- tions if they cannot know and use the
posal has attracted many objections and results of the examinations For these
reasons the standard provides that employers may have a restricted access to some medical information
On the other hand there is no intention to allow employers to abuse medical information obtained pursuant to the Act to the detriment of employees Therefore the administration of the medical records requirement will be closely watched and in cases of abuse appropriate action will be considered
The issues discussed above are believed to be the major ones Numerous other issues have been raised in the rulemaking proceedings Some have been referred to incidentally Many recommendations for instance about work practices are so obviously meritorious that their adoption needs no exposition here Other recommendations and many objections have not been adopted for a variety of reasons which should be manifest Several for instance have recommended the use of respirators only pursuant to a variance or in cases of emergency and occasional short exposures The
recommendation with respect to vari-
ances undoubtedly has many merits but is considered administratively im-
practical Accordingly after consideration of the
whole record of the proceeding and
pursuant to sections 6 b and c and c of the Williams Occupa-
tional Safety and Health Act of 1970 84 Stat 1593 1596 1599 29 U.S.C. 655
657 29 CFR 1910.4 and to Secretary of Labor's Order No. 12-71 36 F.R. 8754 Part 1910 of Title 29 of the Code of Fed-
eral Regulations is amended as set forth
below
1910.1001 Asbestos
a Definitions For the purpose of this section 1 Asbestos includes chrysotile amosite crocidolite tremolite anthophyllite and actinolite
2 Asbestos fibers means asbestos fibers longer than 5 micrometers
b Permissible exposure to airborne concentrations of asbestos fibers Standard effective July 7 1972. The hour weighted average airborne concentrations of asbestos fibers to which any employee may be exposed shall not exceed five fibers longer than 5 micrometers per cubic centimeter of air as determined by the method prescribed in paragraph e of this section
2 Standard effective July 1 1976 The hour weighted average airborne concentrations of asbestos flhers
to which any employee may be exposed shall not exceed two fibers longer than 5 micrometers per cubic centimeter of air as determined by the method prescribed in paragraph e of this section
3 Ceiling concentration No employee shall be exposed at any time to airborne cencentrations of asbestos
fibers in excess of 10 fibers longer than 5 micrometers per cubic centimeter of air as determined by the method pre-
scribed in paragraph e of this section
c Methods of compliance Engineering methods 1 Engineering con-
-
trols Engineering controls such as but not limited to isolation enclosure exhaust ventilation and dust collection
shall be used to meet the exposure limits
prescribed in paragraph b of this section
ii Local exhaust ventilation a
Local exhaust ventilation and dust col-
lection systems shall be designed constructed installed and maintained in accordance with the American National Standard Fundamentals Governing the Design and Operation of Local Exhaust Systems ANSI Z9.2 1971which is incorporated by reference herein
b See 1910.6 concerning the availability of ANSI Z9.2 1971and the maintenance of a historic file in connec-
tion therewith The address of the American National Standards Institute is
given in 1910.100
iii Particular tools All hand erated and operated tools which may produce or release asbestos fibers
in excess of the exposure limits pre-
scribed in paragraph b of this section such as but not limited to saws scorers abrasive wheels and drills shall be pro-
vided with local exhaust ventilation systems in accordance with subdivision ii
of this subparagraph -
2 Work practices- Wet methods Insofar as practicable asbestos shall be handled mixed applied removed cut scored or otherwise worked in a wet state sufficient to prevent the emission
of airborne fibers in excess of the ex-
posure limits prescribed in paragraph b of this section unless the usefulness of the product would be diminished
thereby
ii Particular products and operations No asbestos cement mortar coating grout plaster or similar material containing asbestos shall be removed
from bags cartons or other containers
in which they are shipped without being either wetted or enclosed or ventilated so as to prevent effectively the release of airborne asbestos ^...bersin excess of the
limits prescribed in paragraph b of
this section
iii Spraying demolition or removal Employees engaged in the spraying of asbestos the removal or demolition of pipes structures or equipment covered or insulated with asbestos and in the removal or demolition of asbestos insulation or coverings shall be provided with respiratory equipment in accordance with paragraph d 2 iii of this section and with special clothing in accordance with paragraph d 3 of this
section
d Personal protective equipment1 Compliance with the exposure limits prescribed by paragraph b of this section may not be achieved by the use of
respirators or shift rotation of em-
ployees except
i During the time period necessary to install the engineering controls and to institute the work practices required by paragraph c of this section
ii In work situations in which the methods prescribed in paragraph c of this section are either technically not feasible or feasible to an extent insufficient to reduce the airborne concentrations of asbestos fibers below the limits
prescribed by paragraph b of this
section or
iii In emergencies
iv Where both respirators and personnel rotation are allowed by subdivisions i ii or iii of this subparagraph and both are practicable personn^'lrotation shall be preferred and used
2 Where a respirator is permitted by subparagraph 1 of this paragraph it
shall be selected from among those ap-
proved by the Bureau of Mines Department of the Interior or the National Institute for Occupational Safety and Health Department of Health Education and Welfare under the provisions of 30 CFR Part 11 37 F.R. 6244 Mar. 25 1972 and shall be used in accordance with subdivisions i ii iii and iv of this subparagraph
i Air purifying respirators A reusable or single use air purifying respirator or a respirator described in subdivision ii or iii of this subparagraph shall
be used to reduce the concentrations of
airborne asbestos fibers in the respirator below the exposure limits prescribed in paragraph h of this section when the ceiling or the hour weighted average airborne concentrations of asbestos fibers are reasonably expected to exceed
no more than 10 times those limits
ii Powered air purifying respirators A full facepiece powered air purifying respirator or a powered air purifying respirator or a respirator described in
subdivision iii of this subparagraph
shall be used to reduce the concentrations of airborne asbestos fibers in the
respirator below the exposure limits prescribed in paragraph b of this section when the ceiling or the hour timeweighted average concentrations of asbestos fibers are reasonably expected to exceed 10 times but not 100 times
those limits
iii Type C supplied respirators continuous flow or pressure class A type C continuous flow or presdemand supplied respirator
shall be used to reduce the concentrations of airborne asbestos fibers in the
respirator below the exposure limits prescribed in paragraph b of this section when the ceiling or the hour timeweighted average airborne concentrations of asbestos fibers are reasonably
expected to exceed 100 times those limits
iv Establishment of a respirator pro-
gram a The employer shall establish
a respirator program in accordance with the requirements of the American National Standards Practices for Respiratory Protection ANSI Z88.2 196w9hich is incorporated by reference herein
b See $ 1910.6 concerning the availability of ANSI Z88.2 196a9nd the maintenance of an historic file in connection therewith The address of the American National Standards Institute is given in 1910.100
c No employee shall be assigned to tasks requiring the use of respirators if based upon his most recent examination an examining physician determines that the employee will be unable to function normally wearing a respirator or that the safety or health of the employee or other employees will be impaired by his use of a respirator Such employee shall be rotated to another job or given the opportunity to transfer to a different position whose duties he is able to perform with the same employer in the same geographical area and with the same seniority status and rate of pay he had just prior to such transfer if such a different position is available
3 Special clothing The employer shall provide and require the use special clothing such as coveralls or similar whole body clothing head coverings gloves and foot coverings for any employee exposed to airborne concentrations of asbestos fibers which exceed the
ceiling level prescribed in paragraph b
of this section 4 Change rooms i At any fixed
place of employment exposed to airborne concentrations of asbestos fibers in excess of the exposure limits prescribed in paragraph b of this section the employer shall provide change rooms for employees working regularly at the place
ii Clothes lockers The employer shall provide two separate lockers or containers for each employee so separated or isolated as to prevent contamination of the employce's street clothes from his work clothes
iii Laundering a Laundering of asbestos contaminated clothing shall be done so as to prevent the release of air-
borne asbestos fibers in excess of the ex-
posure limits prescribed in paragraph b
of this section
b Any employer who gives asbestoscontaminated clothing to another person for laundering shall inform such person of the requirement in a of this subdivision to effectively prevent the release of airborne asbestos fibers in excess of the exposure limits prescribed in paragraph b of this section
c Contaminated clothing shall be : transported in sealed impermeable bags or other closed impermeable containers
and labeled in accordance with paragraph g of this section
e Method of measurement All de-
terminations of airborne concentrations of asbestos fibers shall be made by the
membrane filter method at 400-450 X
magnification 4 millimeter objective with phase contrast illumination
f Monitoring- Initial determi-
nations Within 6 months of the publi-
cation of this section every employer
shall cause every place of employment
where asbestos fibers are released to be monitored in such a way as to determine whether every employee's exposure to asbestos fibers is below the limits prescribed in paragraph b of this section If the limits are exceeded the employer shall immediately undertake a compliance program in accordance with
paragraph c of this section 2 Personal monitoring Sam-
ples shall be collected from within the breathing zone of the employees on membrane filters of 0.8 micrometer porossity mounted in an open filter
holder Samples shall be taken for the determination of the hour timeweighted average airborne concentrations and of the ceiling concentrations of
asbestos fibers
ii Sampling frequency and patterns After the initial determinations required
by subparagraph 1 of this paragraph samples shall be of such frequency and pattern as to represent with reasonable
accuracy the levels of exposure of employees In no case shall the sampling be done at intervals greater than 6 months for employees whose exposure to asbestos may reasonably be foreseen to exceed
the limits prescribed by paragraph b
of this section
3 Environmental monitoring samples shall be collected from areas of a work environment which are represent-
ative of the airborne concentrations of asbestos fibers which may reach the
breathing zone of employees Samples shall be collected on a membrane filter of 0.8 micrometer porosity mounted in an open filter holder Samples shall
be taken for the determination of the 8-
hour weighted average airborne concentrations and of the ceiling concentrations of asbestos fibers
ii Sampling frequency and patterns After the initial determinations required by subparagraph 1 of this paragraph samples shall be of such frequency and pattern as to represent with reasonable accuracy the levels of exposure of the employees In no case shall sampling be at intervals greater than 6 months for employees whose exposures to asbestos may reasonably be foreseen to exceed the exposure limits prescribed in paragraph b of this section
4 Employee observation of monitoring Affected employees or their representatives shall be given a reasonable opportunity to observe any monitoring required by this paragraph and shall have
access to the records thereof
g Caution signs and labels 1 Caution signs i Posting Caution signs shall be provided and displayed at each location where airborne concentrations
of asbestos fibers may be in excess of the exposure limits prescribed in paragraph b of this section Signs shall be posted at such a distance from such a location so that an employee may read the signs
and take necessary protective steps before entering the area marked by the signs Signs shall be posted at all approaches to areas containing excessive concentrations of airborne asbestos
fibers
ii Sign specifications The warning signs required by subdivision i of this subparagraph shall conform to the requirements of 20 x 14 vertical format signs specified in 1910.145 4 and to this subdivision The signs shall display the following legend in the lower panel with letter sizes and styles of a visibility at least equal to that specified
in this subdivision
Legend Asbestos 2a ..2---n~ e. e
Notation
" Sans Serif Gothic or
Block
Dust Hazard " Sans Serif Gothic or
Block
Avold Breathing Dust Wear Assigned Protective
Equipment
Do Not Remain In Area
Unless Your Work Re-
1/4 Gothic ...Gothic
...Gothic
quires It Breathing Asbestos Dust
May Be Hazardous To Your Health
14 point Gothic
Spacing between lines shall be at least equal to the height of the upper of any
two lines
2 Caution labels Labeling Caution labels shall be affixed to all raw materials mixtures scrap waste debris and other products containing asbestos fibers or to their containers except that no label is required where asbestos fibers have been modified by a bonding agent coating binder or other material so that during any reasonably foreseeable use handling storage disposal processing or transportation no airborne concentrations of asbestos fibers in excess of the exposure limits prescribed in paragraph b of this section will be released
ii Label specifications The caution labels required by subdivision i of this subparagraph shall be printed in letters
of sufficient size and contrast as to be readily visible and legible The label shall state
CAUTION
Contains Asbestos Fibers
Avoid Creating Dust Breathing Asbestos Dust May Cause
Serious Bodily Harm
h Housekeeping- Cleaning All external surfaces in any place of employ-
ment shall be maintained free of accu-
mulations of asbestos fibers if with their dispersion there would be an excessive concentration
2 Waste disposal Asbestos waste scrap debris bags containers equipment and contaminated clothing consigned for disposal which may produce in any reasonably foreseeable use handling storage processing disposal or transportation airborne concen-
trations of asbestos fibers in excess of the
exposure limits prescribed in paragraph b of this section shall be collected and disposed of in sealed impermeable bags or other closed impermeable containers
) Recordkeeping Exposure records Every employer shall maintain records of any personal or environmental
monitoring required by this section Records shall be maintained for a period of
at least 3 years and shall be made available upon request to the Assistant Secre-
tary of Labor for Occupational Safety and Health the Director of the National Institute for Occupational Safety and Health and to authorized representa-
tives of either
2 Employee access Every employee and former employee shall have reasonable access to any record required to be maintained by subparagraph 1 of this paragraph which indicates the employee's own exposure to asbestos fibers
3 Employee notification Any employee found to have been exposed at any time to airborne concentrations of asbes-
tos fibers in excess of the limits pre-
scribed in paragraph b of this section shall be notified in writing of the exposure as soon as practicable but not later than 5 days of the finding The employee shall also be timely notified of the corrective action being taken
j Medical examinations- General The employer shall provide or make available at his cost medical examinations relative to exposure to asbestos required by this paragraph
2 Preplacement The employer shall provide or make available to each of his employees within 30 calendar days following his first employment in an occupation exposed to airborne concentrations of asbestos fibers a compre-
hensive medical examination which shall include as a minimum a chest roent-
genogram posterior 14 ^ 17 inches a history to elicit symptomatology of respiratory disease and pulmonary function tests to include forced vital capacity FVC and forced expiratory volume at 1 second FEV )
3 Annual examinations On or be-
fore January 31 1973 and at least 1nually thereafter every employer shall provide or make available comprehensive medical examinations to each of his employees engaged in occupations exposed to airborne concentrations of asbestos fibers Such annual examination shall include as a minimum a chest roentgenogram posterior 14 x 17 inches a history to elicit symptomatology of respiratory disease and pulmonary function tests to include forced vital capacity FVC and forced
expiratory volume at 1 second FEV ) 4 Termination of employment The
employer shall provide or make available within 30 calendar days before or after the termination of employment of any employee engaged in an occupation exposed to airborne concentrations of
asbestos fibers a comprehensive medical examination which shall include as a minimum a chest roentgenogram posanterior 14 x 17 inches a history to elicit symptomatology of respiratory disease and pulmonary function tests to include forced vital capacity FVC and forced expiratory volume at 1 second FEV
5 Recent examinations No medical
examination is required of any employee if adequate records show that the employee has been examined in accordance with this paragraph within the _ past year period -
6 Medical records- Maintenance Employers of employees examined pursuant to this paragraph shall cause to be maintained complete and accurate records of all such medical examina-
tions Records shall be retained by
employers for at least 20 years
ii Access The contents of the records of the medical examinations
required by this paragraph shall be made available for inspection and copying to the Assistant Secretary of Labor for Occupational Safety and Health the Director of NIOSH to authorized physicians and medical consultants of either of them and upon the request of an employee or former employee to his physician Any physician who conducts a
medical examination required by this paragraph shall furnish to the employer of the examined employee all the information specifically required by this paragraph and any other medical information related to occupational ex-
posure to asbestos fibers
1910.19 Special provisions for air con-
taminants
a Asbestos dust Section 1910.1001 shall apply to the exposure of every employee to asbestos dust in every employment and place of employment covered by 1910.12 1910.13 1910.14 1910.15 or 1910.16 in lieu of any dif-
ferent standard on exposure to asbestos
dust which would otherwise be applicable by virtue of any of those sections
Note Following defines additional occupational areas affected by sec-
tion 1910.19 above
1910.12 - Construction Work
construction alteration and repair including painting and decorating 1910.13 . Ship Repairing 1910.14 - Shipbuilding 1910.15 - Shipbreaking 1910.16 - Longshoring
Appendix B
USPHS Membrane Filter Method
For Evaluating Airborne Asbestos Fibers
Nelson A. Leidel
Stephen G. Bayer Ralph D. Zumwalde
U.S. Department of Health Education and Welfare
Public Health Service Center for Disease Control
National Institute for Occupational Safety and Health Cincinnati Ohio 45202
November 1975
This report describes the equipment and procedures for collecting mounting sizing and counting asbestos fibers on cellulose ester membrane filters for the evaluation of breathing zone samples of airborne asbestos fibers The purpose of the method presented is to determine an employee's exposure to airborne asbestos fibers
This is the method of test referenced in the Federal standard on occupational
exposure to asbestos 29 CFR 1910.1001 formerly 29 CFR 1910.93a and the MESA Mining Enforcement Safety Administration air quality standards 30 CFR 55.5-1 b
It is used by the National Institute for Occupational Safety and Health NIOSH and the Occupational Safety and Health Administration OSHA
Preface
f
f
It has been almost seven years since the last detailed information was published by NIOSH concerning an asbestos counting method Edwards and Lynch 1968 In the interim this method passed from a recommended status to one required by federal occupational health standard 29 CFR 1910.1001 formerly 1910.93a
This report was prepared to expand on the 1968 paper It incorporates much of
the sampling and analytical experience of the last seven years accumulated by counts made by NIOSH laboratories and the OSHA Analytical Services Laboratory The report attempts to answer many of the practical questions concerning the method A draft of
this report has been used for the last two years by the NIOSH Division of Training in a course on asbestos sampling and analysis
Recently a report prepared by the Joint ACGIH Aerosol Hazards Evaluation Committee was published in the AIHA Journal Recommended Procedures for Sampling and Counting Asbestos Fibers AIHAJ 36 pp 83-90 1975 The ACGIH report was not submitted for technical review to either NIOSH or OSHA personnel responsible for technical procedures of the USPHS asbestos count method The ACGIH report contains conflicting and possibly confusing guidelines This NIOSH report contains the NIOSH technical guidelines and procedures referenced in the Federal asbestos standard 29 CFR 1910.1001 formerly 29 CFR 1910.93a
The guidelines of this NIOSH report should be carefully and consistently followed by personnel collecting and evaluating asbestos samples in order to yield accurate
results
,
Table of Contents
oT)
Scope Summary of Method Significance
Definitions Interferences
Apparatus Reagents Safety precautions Sampling
Calibration and Standardization Procedure XII Calculations of Airborne Concentrations
XIII Precision and Accuracy
XIV References
| SCOPE
A. This method describes the equipment and procedures for collecting mounting sizing and counting asbestos fibers on cellulose ester membrane filters in the evaluation of breathing zone samples of airborne asbestos fibers The
purpose of the method is to determine an em-
ployee's exposure to airborne asbestos fibers The method is primarily a personal monitoring
technique but can be used for area monitoring
B. The method has been successfully applied using 37 mm Millipore AA filters and small battery operated personal sampling pumps at a flow rate of 1.0 to 2.5 liters per minute Ipm for time periods of a few minutes to 150 minutes at concentrations of 1 to 20 fibers longer than 5 micrometers centimeter Large deviations from these conditions may result in samples with either too few or too many fibers which will yield air concentration estimates of low statistical precision and
accuracy
C. This method considers only fibers with a length to width ratio of 3 to 1 or greater and a length greater than 5 micrometers
|| SUMMARY OF METHOD
The sample is collected by drawing air through a membrane filter by means of a battery powered personal sampling pump The filter is
transformed from an opaque solid membrane
to a transparent optically homogeneous gel The fibers are sized and counted by phasecontrast microscope at 400-450X magnification
III SIGNIFICANCE
This type method was first used by the Asbestosis Research Council in Great Britain ) and
later was slightly modified by the U.S. Public
Health Service for asbestos dust studies in the
United States 2 It has been referenced as the method of test 3 for the Federal standard for asbestos in industrial air 29 CFR Part 1910.1001 formerly 29 CFR 1910.93a and the MESA air quality standard 30 CFR 55.5-1 in the NIOSH Criteria Document on occupational exposure to asbestos 4 in sampling procedures of the Occupational Safety and Health Administration Department of Labor 5 It is the method used by NIOSH and taught in NIOSH Division of Training Course 582 Sampling and Evaluating Airborne Asbestos Dust Finally the procedure has been submitted to
the ASTM for consideration as an ASTM Meth-
od of Test
IV DEFINITIONS
Asbestos fibers means asbestos fibers longer than 5 micrometers Asbestos includes chrysotilo amosite crocidolite tromolite anthophyllite and actinolite For definitions of terms used in this report refer to ASTM Definitions D 1356 Terms Relating to Atmospheric Sampling and Analysis
V INTERFERENCES
All particulates with a length to width ratio of 3 to 1 or greater and length greater than 5 micrometers should in the absence of other
information be considered to be asbestos fibers and counted as such
VI APPARATUS
A. Sampling Equipment The personal sampling equipment train consists of ) personal sampling pump 2 tubing 3 clothing spring clip 4 tubing monitor metal adaptor and 5 field monitor collecting filter and holder
1. Personal sampler pump The pump must be battery powered and weigh less than 2 pounds 0.9 kg The pump must be capable of sampling at 1.0 to 2.5 1pm against a flow resistance of 7.5 inches of water 1.4 cm Hg for 8 continuous hours on a fully charged battery
2. Tubing Laboratory tubing such as rubber or plastic with 6 mm bore ...inch and about 90 cm length 3 feet
3. Clothing spring clip This clip attaches the rubber tubing to the lapel or shirt of the individual being monitored Large spring paperclips will also work
4. Tubin monitor adaptor A short adaptor with ridges on one end to grip the inside of the tubing The other end is designed for a pressure fit into the field
monitor
5. Field monitor collecting filter and holder The only field monitor currently considered acceptable by NIOSH is manufactured by the Millipore Corporation The unit consists of 1 a section styrene plastic case designated Millipore aerosol Monitor Case 2 a 37 mm diameter plain white cellulose ester membrane filter designated Millipore AA nominal pore size of 0.8 micrometer 3 a support pad and 4 two plastic sealing caps If a large number of samples are to be taken it will be less expensive to reuse
the plastic cases Great care must be taken in the cleaning and reassembly process The outside mating surfaces of the field moni-
tors should be covered with shrink
sealing bands to seal the units and provide a writing surface for filter identification
B. Optical Equipment 1. Microscope body with binocular head
2. 10X Huygenian eyepieces are recommended Other eyepieces can be substituted
if necessary
3. Koehler illumination preferably built in and having provisions for adjusting light intensity
4. A Porton reticle is recommended Others such as the Patterson Globe and Circle can
be substituted if necessary
5. Mechanical stago
6. Abbe and Zernike condenser fitted with
phase ring or Heine with a numerical aperture N.A. equal to or greater than the N.A. of the objective
7. 40-45X N.A. 0.65 to 0.75 positive phase
contrast achromatic objective
8. Phase centering telescope or Bert-
rand lens
9. Green filter if recommended by micro-
scope manufacturer
10. Stage micrometer with 0.01 _mm sub-
divisions
For general guidance on microscopes consult Needham 6 and Clark 7 under phase contrast microscopes and accessories
C. Filter Mounting Equipment Experience has shown that certain equipment is useful for efficient sample mounting The following items are recommended for extracting and mounting a portion of the filter onto the
microscope
1. Microscope slides 2.5 by 7.5 cm one inch by three inches glass slides are most commonly used Sample number data initials etc. can be conveniently written on a
frosted end slide
2. Cover slips Cover slips are a necessary
part of the slide mount and optical system The shape should be appropriate for the size of the filter wedge The appropriate cover slip depends upon the objective to be used Ordinarily objectives are optically corrected for 10.17 millimeter thickness cover slip Improper cover glass thickness
3. Scalpel A scalpel is needed to remove a portion of the filter to be examined A number curved blade scalpel works very
well
4. Tweezers A pair of tipped tweezers
is used to remove the membrane filter slice from the field monitor and place it upon the slide
5. Lens tissue To insure cleanliness use
of a free tissue is recommended This
tissue should also be used for wiping mounting tools and for cleaning slides and cover slips
6. Glass rod or spatula A spatula or firepolished glass rod is needed to spread the mounting solution on the slide
7. Wheaton Balsam bottle This special glass container has a glass top which prevents contamination of the mounting solution A glass rod is included for dispensing the
solution
.
VII REAGENTS
Chemicals should be reagent grade free from particles and color conforming to the specifications of the Committee on Analytical Reagents of the American Chemical Society where such specifications are available Chemicals required are A. Dimethyl phthalate B. Diethyl oxalate
VIII SAFETY PRECAURONS Avoid getting the mounting solution on the skin Wash skin promptly with soap and water if skin contact occurs
IX SAMPLING
A. General Information
:
General guidelines for the monitoring of omployee exposures to industrial atmospheres are given in reference 8 The Federal requirements regarding employee exposure monitoring for airborne asbestos are given in 29 CFR
1910.1001
B. Calibration
The personal sampling pump should be recharged prior to calibration and then calibrated 9 against a bubble meter wet test meter spirometer or smillar device at 1.0 to 2.5 1pm The sampling train used in the calibration pump hose filter should be the same
as the one used in the field The calibration should be of sufficient accuracy that the 95
confidence limits on the flowrate are 10
( two standard deviations
C. Mounting the Sampling Pump on
the Worker
Fasten the sampling pump to the worker's belt and fasten the field monitor to the lapel or shirt front as close to the face as is practical
Remove the top cover of the plastic monitor
then invert the monitor making certain the
exposed filter is facing downward Turn on the
pump and adjust to the previously calibrated flowrate 1.0 to 2.5 1pm Immediately record the following information in a logbook
1. Filter number
2. Pump start time and date
3. rate Flow
4. Subject's name
operation
5. Type of operation
ap roved for worker 6. Ventilation controls
is
wearing a respirator approved for asbestos
The pump should be checked periodically dur-
ing the sampling period for proper operation
and flowrate
D. Optimum Sampling Times The requirement for a minimum count of 100 fibers or 20 fields in Section XI below
was determined to be the optimum chioce to
achieve low variability of the fiber count as approximated by the Poisson distribution and reduced counting times Another way of looking at this requirement is that the optimum fiber density on the filter should be one to five fibers per microscope counting field To estimate optimum sampling times one must know in advance the approximate field area of the counting scope and the pump flow rate
folowing equation
The following optimum sampling times calculatecan
then be plotted on log paper
Minutes MFA
1000
where FL == 1 to 5 fibers ECA = effective collecting area of fil-
ter 855 mmfor 37 mm filter MFA =: microscope field area gener-
ally 0.003 to 0.006 mm FR - Pump flow rate generally 1.0
to 2.5 1pm
AC = Air concentration of fibers in fibers
Figures 1 and 2 show typical sampling times
for a pump flow rate of 1.7 1pm Figure 1 is for
a microscope field area of 0.003 mmIn Fig-
ure 2 we see that the sampling times which yield optimum fiber density on the filter are in the range 40 to 80 minutes for a 1.7 1pm sampling rate and 0.006 mmfield area Each individual responsible for sampling asbestos should prepare a similar chart for his particular pump flow rate and field area before sampling is performed to avoid filters that are too light for reliable statistics or too heavily loaded to count However note that the upper limit on
_
the optimum counting density of 5 fibers is an arbitrary one This upper limit is highly dependent on the background particulate density Under very light background conditions
the upper limit for reliable counts may extend to 25-30 fibers
From Figures 1 and 2 it can be seen that there are certain sampling times which will yield optimum fiber densities on the filter for almost
all airborne fiber concentrations from 1 to 10
cu.cm These optimum times have been calculated and are presented in Figure 3. Note that the optimum times given by Figure 3 are approximate and can be varied by as much as 25 percent The nomogram is intended as a guide to be used where no prior knowledge of the air concentration is available If after
sampling for the times recommended by Figure 3 the sample is very heavily loaded greater than 10 fibers then the air concentration
probably greatly exceeded the ceiling standard
of 10 cu.cm Conversely if the filter fiber
density is very low less 1than fiber then
concentration standard than the air
probably was
the 1976 Federal hour average standard standard of
2 cu.cm 29 CFR 1910.1001 b effec-
tive July 1 1976 The nomogram gives the
sampling times which produce optimum fiber
densities on the filter 1 to 5 fibers for
air concentrations of 1 to 10 fibers
E. End of Sampling Period Remove the field monitor replace the plastic top cover and the small end caps and store the monitor Always shut off the pump when changing monitors to avoid contaminating or
damaging the pump Record the pump shutoff time and flowrate in the logbook
F. Blanks
With each batch 25 to 50 filters of samples submit two unopened filters which have been subjected to the same handling as the samples
except that no air has been drawn through them Label these as blanks If the blanks yield fiber counts greater than about 5 fibers
fields then the entire sampling procedure should be examined carefully for the cause
of contamination
Figure 1 - Optimum sampling times for airborne asbestos where microscope field area = 0.003 sq mm
10 t Ceiling std
Air
Air T
1972 hr.TWA std
|
heavy heahveyavy
ttooo
Maybe
Maybe
~
Plant
Plant of
fiber
Optimum
Optimum
fibers
/
fibers
CC
field-
field-
CC
field-
field-
Fibers N
_
1976 hr.TWA std
light Fibers
Fibers
Too
,
t
10 15
{
100 200 500 1000
Sampling Time in Minutes @ 1.7 Ipm
Figure 2 Optimum sampling times for airborne asbestos
where microscope field area = 0.006 sq mm
10 i Ceiling std
heavy
too Air
Air
Maybe
Air 12 l-
1972 hr.TWA std
Maybe
_
Plant
Plant
of
fiber
of
fiber Optimum
CC
field- Optimum
field-
1976 field- /
Fibers 2
hr.TWA hr.TWA
~
Fibers light
Fibers
light
Too
1'
10 15
;
100 200
500 1000
Sampling Time in Minutes @ 1.7 Ipm
Figure 3 - Nomogram for optimum sampling times for airborne asbestos fibers
a
30EXAMPLE = 1.7 1pm
4 A = 0.00302 mm
-0.007
4 READ OPTIMUM TIME = 120 min
a
-25 %
1pm minutes
-0.006
1 minutes 50-
minutes
m
TIME
RATE TIME
AREA SAMPLING 4
-0.005 ,
FLOW FIELD SAMPLING 4
-0.004
-0.004
SAMPLING 100-
SAMPLING 4
OPTIMUM
PUM 4 OPTIMUM 4
,
FR
OPTIMUM
0.003
MICROSPE a OPTIMUM
-
7
A
200-
4
NIOSH / Leidel
1.0 300-0.002
G. Shipping The field monitors in which the samples are collected should be shopped in a rigid container with sufficient packing material to prevent crushing
H. Numbers of Samples When sampling for the ceiling standard 29 CFR 1910.1001 effective July 7 1972 only one sample minute maximum duration is theoretically necessary However sev-
eral samples should be taken during expected
periods of peak air concentrations to allow for detection of gross sampling or counting
errors
When sampling for determination of noncompliance with the hour TWA standard one should continuously sample as large a portion of the work day as is feasible 29 CFR 1910 1001 or b Normally this would mean 6 to 10 consecutive samples on the same man However if this is not feasible the hour TWA air concentration can be estimated from fewer than 6-10 samples Leidel and Busch 10 have shown an optimum number would be 4 to 7 Refer to reference 10 for treatment of the
data for the determination on noncompliance See the NIOSH handbook 8 and Jones and Brief 11 for how to treat data taken for an employee exposure monitoring program
^ CALIBRATION AND STANDARDIZATION
A. Porton Reticle and the Counting Field The asbestos fiber count procedure consists of comparing fiber length with calibrated circles and counting all fibers greater than 5 micrometers in length within a given counting field
area It is recommended that a Porton reticle be used for this purpose The Porton reticle is
a glass plate inscribed with a series of circles and rectangles The square on the left divided into six rectangles is defined as the counting
field
B. Placement in Eyepiece The Porton reticle is placed inside the Huygenian eyepiece where it rests on the fieldlimiting diaphragm The reticle should be kept clean since dirt on the reticle is in focus and will complicate the counting and sizing process For mounting in other eyepieces such as a Ramsden a counting collar must be used
C. Stage Micrometer The Porton reticle cannot be used for counting until it has been properly calibrated with a stage micrometer Most stage micrometer scales are approximately two millimeters long and are divided into units of hundredth of
a millimeter or ten micrometers
D. Microscope Adjustment When adjusting the microscope follow the manufacturer's instructions while observing the following guidelines
1. The light source image must be in focus
and centered on the condenser iris or annu-
lar diaphragm 2. The object for examination must be in
focus
3. The illuminator field iris must be in focus centered on the sample and opened only to the point where the field of view is illumi-
nated
4. The phase rings annular diaphragm and shifting elements must be concentric
E. Porton Reticle Calibration Procedure
Each eyepiece combination on the microscope must be calibrated Should any of the three be changed disassembly replacement zoom adjustment etc. the combination must be recalibrated Calibration may change if interpupillary distance is changed For proper calibration the following procedure should be
,
followed closely With a 10X objective in place place the stage micrometer on the mechanical stage focus and center the image Change to the 40-45X objective and adjust the first scale division to coincide with the left boundary of the Porton rectangle Count the number of divisions between the left and right boundaries of the long horizontal dimension of the largest rectangle estimating any portion of the final division This measurement represents 200 L units and one divides the measurement by 200 to find L The large rectangle is 100 L units long on the short vertical dimension The calculated L is inserted into the formula = 2N where N is the circle number indicated on the reticle and D is the circle diameter Since
the circle diameters vary logarithmically every
other circle doubles in diameter For example
number three is twice the diameter of number one number four is twice the diameter of number two When the circle sizes have been
determined the counting field area consisting of the left six smaller rectangles can be calcu-
lated from the relation 10,000 L. This completes the reticle calibration for this specific
objective combination
XI PROCEDURE
A. Preparation of Mounting Solution A very important part of the sample evaluation is the mounting process This process involves a special mounting medium of prescribed viscosity The proper viscosity is important in order to expedite filter clearing and minimize particle migration Once the sample has been mounted an elapsed time of approximately fifteen minutes is needed before the sample is ready for evaluation
Combine the dimethyl phthalate and diethyl oxalate in one to one ratio by volume and pour
into a Wheaton balsam bottle Add 0.05 gram of new membrane filter per milliliter of solution
to reach the necessary viscosity The mixture must be stirred periodically until the filters have dissolved and a homogeneous mixture is formed The normal shelf life of the mounting solution is about six months Twenty milliliters of mounting solution will prepare approximately 300 samples
B. Sample Mounting Cleanliness is important A dirty working area may result in sample contamination and erroneous counts The following steps should be followed when mounting a sample
1. Clean the slides and cover slips with lens tissue Lay the slide down on a clean surface with the frosted end up It is a good practice to rest one edge of the cover slip on the slide and the other edge on the working surface By doing this you keep the bottom surface the one which contacts the filter from becoming contaminated
2. Wipe all the mounting tools clean with lens tissue and place them on a clean surface such as lens tissue When mounting a series of filters the scalpel should be wiped clean before cutting each sample
3. Using a glass rod which is supplied with the Wheaton balsam bottle apply a small drop of mounting solution onto the center of the slide It may be necessary to adjust the
quantity of solution used or the size of the
wedge The correct amount will result in the
solution extending only slightly beyond the filter boundary If the quantity is greater than this adverse particle migration will occur
4. With the spatula or a supplemental glass rod spread the mounting media into a tri-
count in either direction from circumference to wedge tip Random fields are selected
without looking into the eyepieces by slightly
advancing the slide in one direction with the mechanical stage control
angular shape The size of this triangle
should coincide with the dimension of the
filter wedge
D. Achieving Comparable Results 1. Size only fibers with a length to width ratio greater than or equal to 3
5. Separate the middle and bottom sections of the field monitor case to expose the fragile filter Cut a triangular wedge from the center to the edge of the filter using the scalpel The size of the wedge should ap-
proximate eighth of the filter surface
6. Grasp the filter wedge with the tweezers
in the outer area of the filter which was
clamped between the monitor case sections Do not touch the filter with your fingers Place the wedge sampled side up upon the
2. Count only fibers greater than 5 micrometers in length Be as accurate as possible in accepting or rejecting fibers near this length Measure curved fibers along the curve to estimate the total length
3. Count as many fields as necessary to
yield a total count of at least 100 fibers Exceptions a count at least 20 fields even if you count more than 100 fibers and b stop at 100 fields even if you haven't reached
100 fibers
mounting medium
4. Select the field of view without looking
7. Pick up the cover slip with the tweezers
through the microscope's eyepieces to elimi-
a)
and carefully place it on the filter wedge
nate unconsciously selecting heavy or
Once this contact has been made do not
light areas
a2
PaCS reposition the cover slip
mote
5. The fields are selected along the entire
34
Bs.
Ge 3. Label the slide with the sample number
length of a radial line running between the
a d and current date before proceeding to the
outside perimeter and the tip of the wedge
next filter
6. When an agglomerate mass of material
9. The sample should become transparent
covers a significant portion of the field of
after about fifteen minutes If the filter ap-
view approx 1/6 or greater reject the field
pears cloudly it may be necessary to press
and select another Do not include it in the
very lightly on the cover slip This is rarely
number of fields counted However report
necessary
the fact as it may have meannig to sampling
10. Discard the sample mount after three
days if it has not been counted Crystals
which appear similar to asbestos fibers may
begin to grow at the mounting media interfaces They seldom present any prob-
lems if the slide is examined before three
days In any case stay away from the filter's edges when counting and sizing
C. Counting and Sizing Finding and inspecting counting fields Place the slide on the mechanical stage and positoin the center of the wedge under the objective lens and focus upon the sample Nearly all of the particulates particles and fibers will be
found in the upper ten to fifteen micrometers
of the filter surface When counting and sizing
continual use of the fine focus control is re-
quired to insure that nothing is missed Start
counting from one end of the wedge and progress along a radial line to the other end
or medical personnel
7. Bundles of fibers are counted as one fiber
unless both ends of a fiber crossing another can be clearly resolved .
8. For fibers that cross either one or two
sides of the counting field the following procedure is used to obtain a representtaive count First arbitrarily select a the left and bottom sides and b the upper and lower
left corners and vertical direction as decision aids
Then count any fiber greater than 5 micrometers in length but only if the fiber
a lies entirely within the counting area or b crosses the left or bottom sides or
c crosses the upper or lower left corners or d crosses both the top and bottom sides
Reject and do not count all other fibers Refer to Figures 4 through 9
Figure 4. COUNT fiber crosses both top
and bottom sides
Figure 5. COUNT as one fiber
et a Yan,
4
es Nk
tad
RSgSt
take peumeg dee
Pe 2
en
Be Ar 7 ae oe
3a Gs tet Care a
Ks
ake yal sea
corner
Figure 9. COUNT fiber crosses upper left
corner
Po Nees CN Ee
a parasio: (|
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enn AY Ee EY
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ai
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EAS ares
AE
XII CALCULATIONS OF AIRBORNE
CONCENTRATIONS
Asbestos fiber airborne concentration may be
calculated from the following formula
C FB A
Where C = Airborne fiber concentrations in fibers
. > cm F = Average fiber count in fibers > ...m
field
B = Average fiber count of blank or con-
trol filter in fibers > field It is
subtracted to eliminate the error or
background contamination W _ 855 mmfor 37 mm diameter filter the
portion of the Millipore filter which is exposed when mounted in the field monitor case i.e. the effective filter area A = The area of the counting field of a calibrated reticle expressed in field V Total air volume collected through filter expressed in milliliters
XIII PRECISION AND ACCURACY
A. An accuracy and precision study of the membrane filter counting procedure for asbestos has been conducted by Conway and Holland 12 They conducted an intralaboratory study involving six counters Three of the counters were experienced while the other three had only a short familiarization with the rules for fiber counting The conclusions of the study included
1. The precision of the procedure for filters not containing an abundance of fine fibers can be estimated by a standard deviation of
16.2 This value includes variation among counters and observed interaction effects
2. The accuracy of the procedure for similar
filters may be estimated for a fiber count
by a standard deviation of 21.4 This
assumes that the contribution of the overall variance from the nonuniform fiber distribution is additive
3. The fiber concentration varies significantly between angular sectors on a given filter Where approximately 100 fibers are
counted the standard deviation of the fiber
count distribution for the whole filter appears to be represented by 1.6 rather than
which is a property of the Poisson distribution where n is the total number of
fibers counted
4. A high percentage of very fine fibers on the filter can significantly affect the standard deviation and confidence limits for counts by different counters After combining variations
in fiber concentrations over the entire filter
with those for different counters it was con-
cluded
.
a For filters with a low concentration of
the fibers the standard deviation is estimated at 21 and the 95 confidence
interval is 43
.
b For filters with a high concentration of fine fibers the standard deviation is esti-
mated at 25 and the 95 confidence
interval is 50
B. Lynch Kronoveter and Leidel 13 have also reported on the precision of the method Their intralaboratory study utilized the data from a large number of dust counts made by different methods by experienced counters over a period of years in an ^'pidemiologic study of the asbestos products industry They
concluded that the standard deviation of counts
of fibers longer than 5 micrometers on mem-
brane filters could be estimated from the rela-
tion = 0-591 Thus for counts of about 100 fibers the standard deviation could be esti-
mated at about 15.2 and the 95 confidence limits at 30.4 These values are lower than
the precision values reported by Conway and Holland 12
C. Systematic inaccuracies can be introduced by the improper choice of microscope or by
not checking a particular individual's counts in
relation to other counters Leidel and Busch
14 found that one particular microscope tested yielded counts that were approximately 45 higher on the average than counts from four other microscopes in a phase contrast michoscope evaluation Also one particular counter produced counts that were 27 higher on the average Leidel and Busch 14 concluded that a significant difference in asbestos
fiber counts can result when the same filters are counted on different makes and models of
microscopes Significant differences can also exist between trained counters They concluded that any laboratory counting asbestos
on membrane filters should be part of an interlaboratory collaborative quality program This participation will insure that 1 equipment is propertly adjusted and calibrated 2 counters are properly trained and their counting efficiency is continually evaluated and 3 com-
parable results are obtained from each labora-
tory This type of quality control program is conducted by NIOSH as the Proficiency Analytical Testing PAT program The PAT program is used by the AIHA as part of their Laboratory Accreditation Program which is partially funded by NIOSH
XIV REFERENCES 1 Asbestos Research Council The Measure-
ment of Airborne Asbestos Dust by the Membrane Filter Method Technical Note Dr. S. Holmes Secretary P.O. Box 40 Rockdale Lancashire Great Britain 1969 Edwards G. H. and J. R. Lynch The Method Used by the U.S. Public Health Service for Enumeration of Asbestos Dust on Membrane Filters Annals of Occupational Hygiene 11 1-6 1968 Federal Register 39 23543-23545 June 27 1974
U.S. Department of Health Education and Welfare Public Health Service National Institute for Occupational Safety and Health
Criteria for a Recommended Standard-
Occupational Exposure to Asbestos HSM 72-10267 1972 U.S. Department of Labor Occupational Safety and Health Administration OSHA Sampling Data Sheet No. 2- Asbestos Unpublished - Jan. 1972
Needham G. H The Practcial Use of the Microscope Charles C. Thomas Publish-
ing Corp. Springfield Illinois 1958
7 Clark G. .: The Encyclopedia of Micros-
copy Rheinhold Publishing Corp. N.Y.
1961
;
8 Handbook for Compliance Determinations
of Employee Exposure to Industrial Atmos-
pheres USPHS NIOSH Technical Publica-
tion to be published 1975
American Conference of Governmental In-
dustrial Hygienists Air Sampling Instru-
ments for Evaluation of Atmospheric Contaminants Fourth Edition Section K Air Movers and Samplers pp 26 P.O. Box 1937 Cincinnati Ohio 1972
10 Leide N. A. and K. A. Busch Statistical Methods for the Determination of Noncompliance with Occupational Health Standards NIOSH Technical Publication 75-159 1975
11 Jones A. R. and R. S. Brief Evaluating Benzene Exposures AIHA J. 32 610-613 1971
12 Conway R. E. and Holland W. D Statis-
tical Evaluation of the Procedure for Count-
ing Asbestos Fibers on Membrane Filters LFE Corporation Richmond CA. Prepared for Asbestos Information Assoc./North America New York N.Y. 1973
13 Lynch J. R. K. H. Kronoveter and N. A. Leidel Validity of the Poisson Distribution in Dust Counting USPHS NIOSH unpublished house report TR
14 Leidel N. A. and K. A. Busch An Evaluation of Phase Contrast Microscopes for Asbestos Counting presented at the 1974 American Industrial Hygiene Conference Miami Beach Florida 18 May 1974 NIOSH unpublished house report TR
1
-
Notes
;
an
A. SOURCES OF PERSONAL SAMPLER PUMPS 1. Mine Safety Appliance Company 201 North Braddock Avenue Pittsburgh PA 15208 2 National Environmental Instruments Inc. P.O. Box 590 Warwick RI 02888 3 Willson Products Divsiion
ESB Incorporated
P.O. Box 622
Reading PA 19603
B. SOURCE OF CLOTHING SPRING CLIP Catalog number 1140 John F. McGuire Company 120 Bacon Street Pawtucket RI 02860
C. SOURCE OF TUBING MONITOR ADAPTOR
Catalog number LH Bection Dickinson & Company Rutherford NJ
D. SOURCE OF FIELD MONITOR
1 Complete monitor plastic case filter pad and caps catalog number
MAWP 037A0 box 2 Filters and pads only catalog number
AAWP 03700 box
3 Monitors only catalog number M0000
37A0 box from the
Millipore Corporation
:
Ashby Road
Bedford MA 01730
E. SOURCE OF SEALING BANDS Cellulose bands white opaque 41x25
28 minimum order 2500 Walter H. Jelly & Company
2822 Birch Street
Franklin Park IL 80131
It is recognized that equipment and services other than those cited in this report may be available Mention of company or product
names is not to be considered an endorsement
by NIOSH
.
Appendix C
FL
FL
ABOVE
LINE INCREASER LINE INCREASER LINE INCREASER
BRANCH INCREASR HEADER
HEADER
HEADER
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BRANCH 2-2
BRANCH 2-2
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DRINGS pig OF
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REFERENCE
REFERENCE
REFNCE DUST
REFERENCE DUST
REFERENCE MATERIAL
REFRENCE TYP
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