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BIODEGRADATION (BOD/COD/TOC) TEST SUBSTANCE Identity:Perfluorooctanoiaccid,ammonium salt;may alsobe referredto as PFOA ammonium salt,Ammonium perfluorooctanoateP,FO, FC116, FC-126, FC-1 69,or FC-143. (Octanoicacid,pentadecafluoro,ammonium salt,CAS # 3825-26-1) Remarks: The testsample isFC-143. The referencedstudyisonlya summary. CurrentinformationindicatesFC-143 isa mixtureof96.5 - 100% testsubstance and 0 - 3.5% C6, C7, and Cg perfluoroanalogue compounds. The 3M productionlotnumber was 261. METHOD: Method: Not noted. Type: Aerobic (BOD). Unknown GLP: No Year completed: 1977 Contact time:14 days lnnoculum: Not noted forGOD and TOC. RESULTS Total Organic Carbon (TOC)*: Chemical Oxygen Demand (COD)*: Biochemical Oxygen Demand (BOD): 5-Day: 14-Day: Duplicatedstudies. 186,000 mg/kg 238,000 <4000 mg/kg <1800 mg/kg Nil <10,200 mg/kg CONCLUSIONS No reliablceonclusionscan be derivedfrom thisstudy. Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA QUALITY ReliabilityK:limischranking4. Summary was createdusingonlya listinogf testvalues.The originasltudyprocedureand raw data were notfound. REFERENCES The data summary sheetwas createdby the 3M Company, Environmental Laboratory,St.Paul,MN, Lab Request number 3844, July14, 1977. OTHER Last changed: 5/24/00 ,2 0 0222 - ENG-ri Ref: ENVIR.3. AASMSSESZSSESS.%S. PRODUCT: PRODUCT ECOLOGICAL ASSESSMENT REQUEST FOR LABORATORY WORK DIVISION LAB REQUEST NO. Name: Request Date: ProjectNo.: Code No.: Sample Date: Description: Purpose of Tests-. REQUESTER /-27 O-PI'LC 6-V Phone No. Prob.No. Date Needed: LABORATORY Date Received Sample: Analyst: Date Completed: Hours Spent: y B-P PleaseCallRequester IfDelaysAre Encounte -d. PHYSICAL & CHEMICAL PROPERTIES HeatotCombustionCal/G(STU/Lb.) Density Ash Other a Iis torul (C ZD'7 P 6430 A42L 24 WATER POLLUTION pH COD BOD 5 BOD,Ultimate TOC GC ii d@, Oxygen Uptake Dehydrogenase Activity(TTC) Other < 'I< 6&10 x )C )r z-o @(/"I I?C 00 0 4@A V zoo 000 _V_ @Z40g.WiD' w )C $r 4/ 2- 0. LTC BIOASSAY Specify Organism and Method: E>&O 4x q6 LEACHATE PH COD BOD FROM LEACHING BOD, Ultimate TOC GC Bioassay Other TEST OTHER Bioaccumulation Persistence Degradat ion Products Rec@clability Burnability Weathering -1 --F @,v IV IZ@-