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AR 226 -- O48 READY BIODEGRADATION (OECD 301E) TEST SUBSTANCE Identity: A mixture containing perfiuorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a componenotf FC-203CE. (1Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot number was 519. The test sample is FC203CE. Current information indicates itis a mixture of 1.84% PFOS, 30% diethylene glycol butyl ether, 60.23% water, 2.56% Sultone foamer, 3.1% sodium octyl sulfate, 2.1% polyoxyethylene monooctylphenyl ether, 0.12% sodium lauryl sulfate, and 0.05% tolyltriazole. cThhaerafcotlelroiwziendg scounmcmeantrryataipopnlsieosftiompaurmiitxiteusr.eDwaittah imnacyomnpoltetaeclcyurately reflect the biodegradability of the fluorochemical componentofthe test `sample. METHOD Method: Modified OECD Screening Test, OECD 301E, with DOC Analysis Test type: Ready biodegradability GYeLaPr:CoNmopleted: 1989 Analytical monitoring: Dissolved organic carbon (DOC), pH, D.0., and tSetamtpiesrtaitcaulremethods: Results were determined by calculation of the % DOC removed as compared to the blank control. TMeetsrtooWragsatneiwsamtesrouTrrceea:tmAecnttivPaltaentd,sSltu.dPgaeuml,ixMeNd l(iPqrueocrocnodlilteicotneedfdrfoormt7hdeays and restored to original volume prior to use as inoculum). Test condition: Dilution water: Milipore Mill-QTM water Mineral Nutrient Medium: Nutrient medium per OECD 301E method. Initial pH 7.0. Reference and test solution preparation: A stock solution was prepared by adding 10 mLof the test substance to one liter of mineral nourtdreirentto mobetdaiiunma (fienqaulitveasltenctontcoe2n2tr0a0timognoTfOC4/0L)m.g DInOitCiIalLp,H107..39.1 mInL of tTheeststvoecsksesollsu:tio1n0w00asmlusEerdlpeenrme6y0e0rsmLcontetsatinvionlgum6e0.0 mi test solution ~~ aInncducbaaptopredCownidthitfiooanms:pluGgasl.ienkamp constant temperature orbital shaker incubator (constant dark conditions) Temperature: 222C Agitation: Shaken continuously at 100 rpm 001062 Number of concentrations: one plus sodium benzoate standard (Irneofceurelnucme csounbdsittainocne)oanntdesbtlainnki,tiaaltliionn:dupTlSicSat2e2.27 mg/L. (TSS in test flask 1.114 mg/L) Element Basis: and initial Decrease pH 5.4. in dissolved organic carbon compared to tTheestblsaunbkss.tance flask conditions: pD.H0:.:DaDyay0-07-.82.1(f(orbobtohthdudpulpilciactaetse)s,),DaDyay262-68-.58.8(bdouthpd,up5l.i7cdatueps2) RESWYS Nominal concentrations: Blank control, sodium benzoate at ~20 mg DOC/L and test substance at ~ 40 mg DOCIL. Element values: 28 Day Degradation -- 93% duplicate 1 and 88% duplicate 2. Mean value 91%. Remarks: Substance Testing was conducted on Remarks field. The values a mixture as described in the Test reported aptpotlhayt mixture and not the fluorochemical component alone. INCLUSIONS The test substance % degradation based on mean DOC removal was 91% after 28 days. The reference substance obtained 98% degradation, therefore the inoculum used was viable. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY RHeolwiaebvielirt,y:saKmiipmliescphurriatynkwiangs 2n.otTpersotpienrglymecehatrsacaltlecrriizteerdiaafnodr tqhuaelisttyudtyesltiancgk.s analytical confirmation of the amount of fluorochemical proportion in the solution. REFERENCES Thisstudy was conducted by the 3M Environmental Laboratory, St. Paul, MN, ~~ Lab Request number G1358-1, 1989. o0 rWER OOO00 Last changed: 6/26/00 001063 BEST COPY AVAILABLE EESE Ready Biodegradabilivy tan roost vo 61365. tr BR Semple Description EnviroLnabm--eWonrktSahelet "20 -------- of ---- Modiled OECD Screening Tut 3015 One: 5-22-89 Fe-2obck Ler 502 vr IExpemental Teagn --=Two. test chemcals, 1Reference Substance. |Blank Coniral coeimein_duplicate 2 Ron unth LQ 61200, Common Cantrels, TeCetox. --DoCAnalyseson Daye 0,1,3,7 14 41, 37.228 IC Jest Condiin one T Towel volume =LoomQin pondClask --Mamtatns 0000000000000 --- pHZa 82 0000 0 --PFmp0 az0 ta0 ee0000000000 Do > 0.5 male - SIE A EIT orJe hanes 2 i bae ilr:E ERRT NRNE GS 1 BARIEe (ans cp 1TRIO RRiv, iL aEkRe CLA go SSRN Ee aaa Bo soni Benz(oan(isBoEIT Beinn Sa A lSES RR RR sEe e EERE TEA a i hBEy a WR A R RCEBASA aemRR irE isSEAbe a.as E Sse aeSe RN i ooto6a | BEST COPY AVAILABLE ranemo Ready Biodgm ability Lab ReNco.Ga6oL1sB3O5tO8 FRAN Steblad wa Soba armaetlioDescription\ Ref: MB2e279: Modified ified a eypnmentslLu -- Work sheet OECD Scree.. na Test 3015 ~ Pog Oate: eof 5-22-89 fass = fen Sn Bt roe bPoy feo gs B mgsopge 22500 CC Gdpaya 34430 D ftha 250 00 ape 0 spyx par oy:Lio 0 Hy Bo; 5 a 0.030 ESR XT 0.057% SEER +\B CpraERGRET ERECT Ta oa See 0 6ESR| cana Coliratinn (oanSAR)Blk E YE OR To BECHER (SMe 7 TH 1) SEN | RRR, AAP SARE ee pS SR EL (FTI TYN o Wai YEE HATEFOU SAT 0SE RS STavAy, ny OOROWb! BEST COPY AVAILABLE Ready Biodegacability emis 4 0wo ` o, bmi Jodi 51 ` Modi $e ronmental Lab -- WorkShst & "1 Screening Test 301 Landfill Stabilized Foam 4 ReS2 MB 8barq: n P c 14vea G6L13Gm 5O8G Page -- ot Owe S-RA-29___ . S4R -- =Ohtauned_detivnied Sludge Aurel Lops Som or pr = ant Sp Ba MAL lb-29 Trisve pis 2.2 oo Somesass ice he od " ie ~ a - : el a . re as Total Va me = }.O 7 der Tnsial plz 2.0. T.8.5. = 2LR7. iQ ' - x. - Le is $7 Lovo, or Ea CER Lo Tnaciabios 50 SEES RT Teep ClETRRR EECOTE nCUlett Se pt edi ERR ERE Wee, de be dei 0 breea FREE Te ER F RER E ey RL ARSE ERR EE SEAN pee BEST COPY AVAILABLE Ready Buodggadabilivy Lan Roques No. G1 3582 : Samo Fe os Oncn Me cs tor s1q di OESnvsirSoxnmveenmtaulgL gTe--a cWhob rSkoSlheset "O2n9e --E----Z R-- A anayer _SA Fe-206c5 Lot 503 Test Solohions.Pepaca- tton -- FC -203cE_Jot BLY romesemisweeemeeestssistatmicej --Tec2330conmale sack Lomb: 220 Tocmg Sch alni IDE[L_Misuol Wreientmaeelivm = droog br] p --_-- h=zs 7 -- ml =22 ToC sn +8 sete ems --Tatese flaskswant HOmaDoc. lt. ee emer Hom ft = TRsO tack fo Ss 2:2 me, [nL = lo. 9 mo Steck Jboam) -- Toc. =E13C0_2pu0nLCE JofarchSosRnl = 1302 ma Toc Stack Soln ? Jo mg Jo Misael Mossent Solin LE TI) ow = Lica ec i ihn cL nL a e0 e Saas a aS EeLS mam S58 miT e l <ie boo pf "DTRCHTEESe SeoerR BENR RA AR ee 3 | EEL SEEreR E iRS BERRAT C B a OLo PR LEG aNcSa SE e bryREAC irc yr t TTe S aES RA i RIERE FRES ER 11PURE rn 001067vr BEST COPY AVAILABLE L__________________________________ Ready Brodagpadabrlity Lab Request No. G21358. S ampleDescription Mod Sie RSi0s3cx ftaersin OEnKviTroSncmteneteanliLnagb -- Work Sheet Test Sol 729 ------ -------- owe 5-23-69 nays Soba -- Bopader Preparation TPeD r TRICE i Ree ALT mECE ASLAeeblA Saa YewlpMieu joal vSuv 03+ 1an5= boo FARE owl sige +or age = boo ACaomriete Cy o_+o 5976--5 + 0.3 + las= boo 2eferena Sib. Z -- " -- too o C 18 A est Solutions Prepared in ol plicate. { he ig "Remy . s AER:goings ie RE TT 5 ls RL STE Eu nla rod bin ARH INANE PING Cilirafen Chg 3 id 5) SN | REE Eh RE gr Ter mmo 001068 Fam i.1.0.0m0 BEST COPY AVAILABLE 61800, Lab Request No GJBSR eaomplevo Description EnviroLnabm--eWnortkSaheelt 298 --L--of oats: 5:23:84 Landfil) Sebilioad Foam s Temperalre | Hey Brg 3 Compan.Temp.Ore aor i ----------ModiCiel OECDSonya Tet Fels Py < 3 loo gem aie Dale $23.80 Toupals Temp 0 ale San 524-24 uBR a 5:25:89 43 a 5:24-89 AR 2 S298 SAR 2 Sam AB ; S318 S48 A &:/-87 SB a 2-89 SHA / L561 EY 3 b-8 SB 21 bred SW < 62-89 SB A b-2 SM A bolA-89 SAR & bolz-gd SHB a) p14 ~ 8 SA A belies SM a SE oat ABR _ 1:8 SB Al bod. SB. AL...| pitia mp C2 _ - rosette eres EE _-- -- I 001069 BEST COPY AVAILABLE mm Ready Brodeataclabilisy Lab Fount to C2 13.52 FSo aenztoozDcasrcption Fe-2ouct V5 MoEdniviCrroencmelnStaelCLeaebni--ngW,oTrektSh-ee3t01% 7o2y0e-- , 5-l 13o-f 6d0e Tesr Flask Conditions aay: SHR fTm eTm Pe EAE SAL iGWfLEER SYA he Tfa E SomfRASR SENAL RS Tuas, saan 45, 3a. 433AL3de Le 70 biSq 5884 558s FeA03I 73 94 4.5, 8.0LA,8A 089 L179 be $1 55 98 513 FC2 730 916 bsT ,816283 GiSa 1370 55d See1 5sss | FeAOLIE 7.3 34 L592 63.83 Le 9 LRSc 559c S537 5559 | T --_-- EE | Shia i eRe Ga Srna Ty LS Te ona TRI THB EU OSE Ae eed | EHR RRRE | BRRLan I ta : Ii RENE nilEE !: SCSI 01070 ENVIRONMENTAL, LABCRATORY MODIFIED OECD SCREENING TEST 301E READY BIODEGRADABILITY oute Analyst Saas - Test Substance_FC~203CF Lot 5 q `Test Concentration 40mg, Doc JL CInocoulunm SocurcoeefMseunsspoetnndetrdisnosaliiedtsTirneiiantoomceunlntumPlantMired Ligpoc SeBaul,my fresh (in mineral medium) k 2 pre-oonditioned (restoredto original vole) 2. 327 a JL a CarbonDeterninations Carbon Analyzer = Dohmmann Xertex 8 Inoculum Used: Fresh/Pre~conditioned 2 edn ElaskAnalyses Time of incubation (days) n/t) ; 2 mak 3 r.n basfasglomadonfoeooso-er] 2> nN Mn JLooosns]|)1easssoosotnfJoosnofnfsoJuomensfooocnecfo[ooonusrssss)] 2 2 By loserJoe [0.005Jo.ceo fo.ovo.coplo. aus]oom | Mean bk B =Ameoanr+B, menanlno{e.-3l5ao0.156 Jo.c0svt0bloo.scaozlno.o01oai]eo.10s3[o]0e-.0c01910|| HET benbooarhnfeocnralfocnos] Chemica a Pa - 2 oy i D, Evaluation of raw data [oso]wes[susfsanlusal2u9a]zsn] 43.33 [1.90|s3oclsann5.53[a1 frr.s lt0.52[3tacts,+1[s5.26 4 elt. H.io)[4.795] toga]#4 457]39 plassult.aula]4.257]1.82] hs i I XY PH TYPP TYEEN io. 0 1 3 9 = Flask 1 = 1- f{C mean _- bo) X 109 Percent Degradation after t days wo ooeminof" |F#eloqlislgs[Blaaal| 001071 EWI ETAL LARORATORY BEST-COPY AVAILABLEJCOTFIED OBCD SCREENTNG TE"ST 301E wn ELH pate Analyst a 35 Test sustance SodiumBenznate. ReQente Svbstane Test Concentration 20meToe/L(34.3mg i) Inoculum Source MeinLunsieTeegsrrentPlantMisal Lignor Qancoe fsun spet ndex dsoa lidt s ini inoo culn um. Biol, av fresh (in mineral medium) pre~conditioned (restored to original volume) A:237 3 IL Gaston Determinations Carbon Analyzer = Dean sartex Inoculum Used: Fresh/Pre-conditioned dodim las Analyses Timeofincuba(tGaiyeo) n tog) 2 2728 ma 2 FOR PS FOP FO A pspp PN loon [1.889 brontbonfoses[neon rors oss] A, mean sel02pempeabonbachelors] 2 By Lo.t01lo.08, 0.008[0.000[o.0t9[o.eow[0-245[0.024 mes Fosops epot] Mean bo B Aumoeaon'n+-B, lo.35a]o-15Jo-0t0[ocas]s-on[o-cazoetp [oo | mean b23lo.ia Joonlo.puleen[ooons[oona ~ Canter 2 a car >2 0, D, Evaluation of raw data afrbob a fon]i9srfoneenslors banfomsot| Bostlin 79[oorolosiowabsotauos.]aoel fi[e9ta0l[2104..58]3Jlooseises btgaifoareso st[o0.2s8o7f10 370J]0o.d3aogc|] [19.2620.50 Jo.0r0|ostafs.c0r[oasslo3gfo.aa| Mask o tos T= f(Cm ,meanm- bk] ) x 104 Percent Degradation aftert days _ [0 7.31 Jyo3 o177 [a04 [44[28 `[3ag2 wn wCdemins : |[37]e0l17]9s8a]s1sa| 001072 0 (RG 138 : [25 Modified Screening Testof Ready Bioclggradabiliyy 3oir FC-203CE ana FC-RobCE Peccent Degradation After t Days (% boc Remova)TM So Drly a DaoN nr Da; DSayw Feasce-y [31 C21 C08 88 83 3 3 FC-208s 2 |b.) 0.3 12 qo 88 90 88 Fe-gocsn| 07 1A 1 89 92 9A 90 Feaouce-3 oA" 0d 15 42 94 q2 a Sot. e-i| 73 geo 97 qe a9 as 13 fm 2 oo loo 37 leo qq 9 98 Ww - . . % Doc Removal = [1 TESirens ar * tog . 001073 06/23/2000 EANRVCIHRIOVNEMDENTFAILNALLABROERPAORTTORY 1 RLEABQUERSETQOURESTNAMNEO:. GM1T7E9/8EAR DPERPOAJRETCMTENNTO:: 90857305013000 DDEASTCE: REFCCE-I2V0E3D:CE0A5N/D23/F1C9-82906 CE BIODEG. DAY 0 ECXOPNTCROAMCPT LAB(S): DATE: 05/31/1989 DPARTOEJECCOTMPLLEEATD:ED:J0S6T/O02C/K1989 P3MHONFEAXNON:O: 665511--777788--66413786 Please run in duplicate. SAMPLE DATE CODE DESCRIPTION RESULT MOL or (95% C.I.) 1 05/23/89 FC-203 1 ronenneeee ooc DISSOLVED ORGANIC CARBON 40 MG/L 2 05/23/89 FC-203 11 TTTTTIoIe ooc DISSOLVED ORGANIC CARBON 41 MG/L ~~ 3 05/23/89 FC-206 I Tonnes 00c DISSOLVED ORGANIC CARBON 37 MG/L 4 05/23/89 FC-206 11 TTTTTTTTIIO Doc DISSOLVED ORGANIC CARBON 36 MG/L 001074 06/23/2000 ENVIRONMENTAL LABORATORY 1 ARCHIVED FINAL REPORT LRAEBQUERSETQOURESTNAMNEO:. 6MT1E7/9E7AR DPERPOAJRETCMTENNTO:: 90693750013000 DATE RECEIVED: 05/23/1989 DESC: LANDFILL STAB FOAM BIODEG. DAY 0 CEOXNPTRCAOCMTP LDAATBE(:S):05/31/1989 DPARTOEJECCTOMPLLEEATDE:D:JH0S6T/O0C2K/1989 PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176 Please run all samples in duplicate. SAMPLE DATE CODE DESCRIPTION RESULT MOL or (95% 0.1.) 1 05/23/89 Ha HO BLANK ooc DISSOLVED ORGANIC CARBON <0.5 MG/L 2 05/23/89 MEDIUM NUTRIENT Doc DISSOLVED ORGANIC CARBON 0.8 MG/L 3 05/23/69 1ST RINSE FOAM SOLIDS Doc DISSOLVED ORGANIC CARBON 2000 MG/L 4 05/23/89 2ND RINSE FOAM SOLIDS oc DISSOLVED ORGANIC CARBON 540 MG/L 5 05/23/89 9RD RINSE FOAM SOLIDS Doc. DISSOLVED ORGANIC CARBON 150 MG/L 6 05/23/89 4TH RINSE FOAM SOLIDS Doc DISSOLVED ORGANIC CARBON 52 MG/L 7 05/23/89 BLANK 1 CONTROL ooc DISSOLVED ORGANIC CARBON <0.5 MG/L 8 05/23/89 BLANK II CONTROL Ld DISSOLVED ORGANIC CARBON <0.5 MG/L 9 05/28/89 LEACHATE I ~=~==""="""" oc DISSOLVED ORGANIC CARBON 42 Ma/L 10 05/23/89 LEACHATE IT ~~"~"===="= - oc DISSOLVED ORGANIC CARBON 41 Ma/L 11 05/23/89 PRE W-SOLIDS TTTTTTTTTT Doc DISSOLVED ORGANIC CARBON 1.3 MG/L 001075 06/23/2000 EANRVCIHRIOVNEMDENFTAILNALLABROERPAOTROTRY 1 LAB REQUEST NO. G1802 DREEPQAURETSMTEONRT:NAM0E5:35MTE/EAR DPRAOTJEECRTECENOI:VED9:9700051/32040/01989 DESC: FC-203CE AND FC-206CE BIODEG. DAY 1 CONTRACT LAB(S): DEAXTPECCOOMMPPLDEATTEED:: 060/60/20/21/1998899 PPRHOOJNEECTNO:LEA6D5:1-J7W78S-T64O3C8K 3M FAX NO: 651-778-6176 aTneasltyssihsa.res controls & ref. substance With LR G1800, See LR G1801 for day 1 SAMPLE DATE CODE DESCRIPTION RESULT MOL or (95% C.I.) 1 oc 2 oc 3 Doc + ooc FC-203 1 ees DISSOLVED ORGANIC CARBON 42 MG/L FC-203 II TTTTTTTTTTT _ DISSOLVED ORGANIC CARBON 44 Mo/L FC-206 1 semmenneneen DISSOLVED ORGANIC CARBON 35 MG/L FC-208 II TTTTTTTTTTT DISSOLVED ORGANIC CARBON 36 MG/L 001076 06/23/2000 ENVIRONMENTAL LABORATORY 1 ARCHIVED FINAL REPORT LAB' REQUEST NO. G1801 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/24/1989 DESC: LANDFILL STAB FOAM BIODEG. DAY 1 CONTRACT LAB(S): EXP COMP DATE: 06/02/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JH STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176 Please run all samples in duplicate. SWPLE OTE | COE DESGRIPTION RESULT MOL or (s5% G.I.) 1 BLANK I CONTROL Doc. DISSOLVED ORGANIC CARBON 1.9 MG/L 2 BLANK II CONTROL Doc DISSOLVED ORGANIC CARBON <0.5 MG/L ~ 3 LEACHATE I ~7"77"""""TM" oC DISSOLVED ORGANIC CARBON 40 MG/L 4 LEACHATE IT ~77""""""""" Doc DISSOLVED ORGANIC CARBON 39 MG/L 5 SOLIDS I WASHED oc. DISSOLVED ORGANIC CARBON 0.7 MG/L 6 SOLIDS IT WASHED Doc DISSOLVED ORGANIC CARBON 1.2 MG/L 7 LEACH & SOLIDS I oc DISSOLVED ORGANIC CARBON 42 MG/L 8 LEACH & SOLIDS IT Doc DISSOLVED ORGANIC CARBON 41 MG/L 9 REF SUB I SODIUM BENZ. oC DISSOLVED ORGANIC CARBON 20 MG/L 10 REF SUB II SODIUM BENZ. es Doc. DISSOLVED ORGANIC CARBON 21 MG/L 001077 08/23/2000 EANRVCIHRIOVNEMDENTFAILNALLABROERPOARTTORY 1 LRAEBQUREESQTUOERSTNAMNEO:. GM1T8E2/0EAR OEPARTHENT: 0535 CEXOPNTRCAOCWTP DLAATB(ES:):06/05/1989 DATE COMPLETED: 06/02/1969 PDARTOEJECRTECEHIO:VED9:9700051/32060/01989 DESC: FC-203CE AND FC-206CE BIODEG. DAY 3 PPHROONJEECTNO:LEA6D5:1-J7W76S-T6O4C3K8 an FAX NO: 651-778-6176 Test shares controls & ref. sub With LR G1800; See LR G1819 for day 3 analyses SAMPLE DATE CODE DESCRIPTION RESULT MOL or (95% C.1.) 1 Foaar cern oo DISSOLVED ORGANIC CARBON 41 MG/L 2 Fear Treen 00 DISSOLVED ORGANIC CARBON 40 MG/L a Foe ree DOC DISSOLVED ORGANIC CARBON 32 MG/L 4 Foa0e Tr TTT ooo DISSOLVED ORGANIC CARBON 33 MG/L 001078 96/23/2000 EANRVCIHRIOVNEMDENTFAILNALLABROERPAOTROTRY y LAB REQUEST NO. G1819 REQUESTOR NAME: MTE/EAR PDERPOAJRETCMTENNTO:: 90957305013000 DDEASTCE: RELCAENIDVFEIDL:L S0T5A/B2.6/1F9O8A9M BIODEG. DAY 3 CONTRACT LABS): EXP COMP DATE: 06/05/1989 DPARTOEJECCTOMPLLEEATD:ED:JH0S6T/O0C2/K1989 P3MHONFEAXNON:O: 66551-17-7787-86-4631876 Please analyze in duplicate. Sable DATE GOOF | DESGRIPTION RESULT MOL or(95% 0.1.) 1 noc 2 Doc 3 Doc 4 Doc 5 Doc 6 ooc 7 o0c oo 9 DOC 10 Doc. BLANK I CONTROL DISSOLVED ORGANIC CARBON <0. MG/L BLANK IT CONTROL DISSOLVED ORGANIC CARBON <0.5 MG/L - LeAcH 1 LEACHATE DISSOLVED ORGANIC CARBON 31 MG/L LEAH II LEAGHATE DISSOLVED ORGANIC CARBON SOLIS I PRE-WASHED 33 MG/L DISSOLVED ORGANIC CARBON SOLIDS IT PRE-WASHED DISSOLVED ORGANIC CARBON <0.5 MG/L <0.5 MG/L LEACH & SOLIDS I DISSOLVED ORGANIC CARBON LEACH & SOLIDS IT DISSOLVED ORGANIC CARBON 30 MG/L 33 MG/L REF SUB 1 `SODIUM BENZ. DISSOLVED ORGANIC CARBON <0.5 MG/L REF SUB II SODIUM BENZ. DISSOLVED ORGANIC CARBON <0.5 MG/L ! -- 001079 06/23/2000 E"NAVRICRHIOVNEMDE.NTFAILNALLABROERPOARTTORY LAB REQUEST NO. G1797 seis oe eve CONTINUED oescamerion | RESULT 12 os/za/ee PRE-H sous 1 Doc DISSOLVED ORGANIC CARBON 1.1 MG/L 13 05/23/89 LEACH & SOLIDS I oo DISSOLVED ORGANIC CARBON 43 MG/L 14 05/23/89 LEACH & SOLIDS 1 DOC DISSOLVED ORGANIC CARBON 43 MG/L 15 05/23/89 DOC LEACHATE AS-IS DISSOLVED ORGANIC CARBON 2000 MG/L 16 05/23/89 REF SUB I `SODIUM BENZ. oo DISSOLVED ORGANIC CARBON 21 MG/L 17 05/23/89 REF SUB II SODIUM BENZ. DOC DISSOLVED ORGANIC CARBON 20 MG/L 2 MOL or (95%G.I.) ! 001080 06/23/2000 EANRVCIHRIOVNEMDENFTAILNALLABROERPAORTTORY 1 LAB REQUEST NO. REQUESTOR NAME: G1834 MTE/EAR DPERPOAJRETCMTENNTO:: 90957305013000 DDEASTCE: RFECCE-I2V0E3DC:E A0N5D/30F/C1-928096CE BIODEG. DAY 7 CONTRACT EXP COMP LAB(S): DATE: 06/09/1989 PDARTOEJECCOTMPLLEEATD:ED:JW0S6T/O02C/K1989 PaMHONFEAXNON:O: 665511--777788--66413786 Test shares controls & ref sub. With LR G1800; see LR G1833 for day 7 analyses SAMPLE DATE cope DESCRIPTION RESULT MOL or (95% C.I.) 1 oc 2 Doc 3 Doc a 0oC FC 208 T sasseseseses DISSOLVED ORGANIC CARBON 33 Ma/L FO 208 11 CTTTTTTTIOC DISSOLVED ORGANIC CARBON ~~ 35 MG/L ~ FC 206 1 seen DISSOLVED ORGANIC CARBON 30 MG/L FC 206 II TTTTTTTTTTTT DISSOLVED ORGANIC CARBON 30 MG/L 001081 06/23/2000 EANRVCIHIRVOENDMIFEAINLNALLABRUEHPAOIRUTKY ' LAB REQUEST NO. G1833 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DDAETSCE:RELCAENIDVFEIDL:L S0T5A/B3.0/1F9O8A9M BIODEG. Please run in duplicate. DAY 7 CONTRACT LAB(S): EXP COMP DATE: 06/09/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JW STOCK 3PHMONFEAXNON:O: 65615-17-7787-86-4631876 Supls DATE | GOOF | DESCRIPTION RESULT MOL or(96% G.I.) 1 BLANK T CONTROL Doc DISSOLVED ORGANIC CARBON <0.5 MG/L 2 Doc BLANK IT Troms DISSOLVED ORGANIC CARBON <0.5 MG/L ~~ 3 ooo 4 o0c 5 DOC. 5 LEACH I Treen DISSOLVED ORGANIC CARBON LAH TT een DISSOLVED ORGANIC CARBON sos 1 Treen DISSOLVED ORGANIC CARBON sows Ir Tenens 29 MG/L 29 MG/L <0.5 MG/L Doc. DISSOLVED ORGANIC CARBON <0.5 MG/L 7 LEACH + SOLID I Doc DISSOLVED ORGANIC CARBON 32 MG/L 8 LEACH + SOLID IT Doc. 9 DISSOLVED ORGANIC CARBON 27 MG/L REF 1 SODIUM BENZ. DOC DISSOLVED ORGANIC CARBON 0.5 MG/L 10 REF 11 SODIUM BENZ. -- oo DISSOLVED ORGANIC CARBON 0.6 MG/L 001082 06/23/2000 ENVIRONMENTAL LABORATORY 1 ARCHIVED FINAL REPORT LAB REQUEST NO. G1874 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0222 PROJECT NO: 9970013000 DATE RECEIVED: 06/06/1989 DESC: FC-203CE & FC-206CE BIODEG DAY 14. CONTRACT LAB(S:) EXP COMP DATE: 06/16/1989 DATE COMPLETED: 06/12/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176 Test shares controls and ref. substance with LR G1800; See LR 61873 for day 14 analyses. SAMPLE DATE CODE DESCRIPTION RESULT MDL or (95% C.1.) 1 oc 2 oc 3 oc 4 oc. FC 203 I Tomes DISSOLVED ORGANIC CARBON 5.0 MG/L FC 203 IT Rt - DISSOLVED ORGANIC CARBON 4.3 MG/L FC 206 I sommes DISSOLVED ORGANIC CARBON 4.2 MG/L FC 206 II Trommemenes DISSOLVED ORGANIC CARBON 2.9 MG/L 001083 6/23/2000 ENVIRONMENTAL LABORATORY 4 ARCHIVED FINAL REPORT LAB REQUEST NO. G1873 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0222 PROJECT NO: 9970013000 DATE RECEIVED: 06/06/1989 DESC: LANDFILL STAB. FOAM BIODEG. DAY 14 CONTRACT LAB(S): EXP_COMP DATE: 06/16/1989 DATE COMPLETED: 06/12/1989 PROJECT LEAD: JH STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176 SABLE DATE | CODE DESCRIPTION RESULT MDL or(65% G.I.) 1 ooc 2 0c 3 Doc 4 oc 5 00C 6 oc 7 00c 8 oc 9 oc 10 oc BALNK T CONTROL DISSOLVED ORGANIC CARBON <0.5 MG/L BLANK IT CONTROL DISSOLVED ORGANIC CARBON <0.5 MG/L LEACH 1 srmmmeeeeees ~ DISSOLVED ORGANIC CARBON 1.9 MG/L LEACH IT srernneeee DISSOLVED ORGANIC CARBON 3.2 MG/L SOLIDS T srmmmneeeen DISSOLVED ORGANIC CARBON <0.5 MG/L sous Ir TTTTtToTeee DISSOLVED ORGANIC CARBON <0.5 MG/L LEACH + SOLIDS I DISSOLVED ORGANIC CARBON 3.8 MG/L LEACH + SOLIDS IT DISSOLVED ORGANIC CARBON 3.1 MG/L REF SUB I SODIUM BENZ DISSOLVED ORGANIC CARBON 0.8 MG/L REF SUB II SODIUM BENZ DISSOLVED ORGANIC CARBON <0.5 MG/L 001084 vs/23/2000 EANRVCIHIHVUENDMIFEAINNLALLABRUENPAOIRUTRT ' LAB REQUEST NO. G1907 RDEEPQAURETSMTEONRT:NAM0E5:35MTE/EAR PROJECT NO: 9970013000 DDAESTCE: REFCGE-I2V0E3DC:E A0N6D/13F/C1-290869CE BIODEG. DAY 21 CONTRACT LAB(S): DEXAPTECOCMOPMPLDEATTEED:: 060/62/01/61/9189989 PROJECT LEAD: JH STOCK P3HMONFEAXNON:O: 65615-17-7787-86-4631876 Test shares controls & ref. substance With LR G1800, see LR G1906 for day 21 analyses. SAMPLE DATE cooE DESCRIPTION RESULT MOL or (95% C.1.) 1 FC 203 T =egsorecases oc DISSOLVED ORGANIC CARBON 4.7 MG/L . 2 FC 208 IT TTTTTTTTTT oc DISSOLVED ORGANIC CARBON 4.7 MG/L 3 FC 206 T semenenneees Ld DISSOLVED ORGANIC CARBON 3.1 MG/L 4 FC 206 II TTTTTTTTTOOC Doc DISSOLVED ORGANIC CARBON 2.0 MG/L 001085 06/23/2000 EANRVCIHRIONVMEEDNTFAILNALLABROERPAOTROTRY 1 LRAEBQURESETQOURESTNAMNEO:. GHT1E9/0E6AR DEPARTMENT: 0535 PDRAOTJEECRTECENOI:VED9:9700061/81030/01989 DESC: LANDFILL STAB FOAM BIODEG. DAY 21 SAWPLE DATE | CODE | DESCRIPTION CONTRACT LAB(S): DEAXPTECCOOMMPPLDEATTEED:: 060/62/01/61/9189989 PPHROONJEECTNO:LEA6D5:1-J7H78-S6T4O3C8K 3M FAX NO: 651-778-6176 RESULT DLor(95% G.I.) 1 oc 2 oc 3 boc 4 oc 5 00C 6 Doc. 7 0c 8 Ld oc 10 oc BLANK 1 CONTROL DISSOLVED ORGANIC CARBON <0.5 MG/L BLANK II CONTROL DISSOLVED ORGANIC CARBON <0.5 MG/L LEACH T LEACHATE ~ DISSOLVED ORGANIC CARBON 2.3 MG/L LEACH IT LEACHATE DISSOLVED ORGANIC CARBON 3.1 MG/L SOLIDS 1 sreeeeeeaes DISSOLVED ORGANIC CARBON <0.5 MG/L soLIos 11 TTTTTTTTTOT DISSOLVED ORGANIC CARBON <0.5 MG/L LEACH + SOLIDS 1 DISSOLVED ORGANIC CARBON 2.4 MG/L LEACH + SOLIDS II DISSOLVED ORGANIC CARBON 1.5 MG/L REF SUB I SODIUM BENZ. DISSOLVED ORGANIC CARBON <0.5 MG/L REF SUB II SODIUM BENZ. DISSOLVED ORGANIC CARBON <0.5 MG/L 001086 06/23/2000 ENVIRONMENTAL LABORATORY 1 ARCHIVED FINAL REPORT RLAEBQUERSETQOURESTNAMNEO:. MGT1E9/3E6AR PDERPOAJRETCMTENNTO:: 90957305013000 DDEASTCE: REFCCE-I2V0E3DC:E &06/F1C9-/210968C9E BIODEG. DAY 27 CONTRACT LAB(S): EXP COMP DATE: 06/26/1989 PDARTOEJECCOTMPLLEEATD:ED:JW0S6T/O2C3/K1989 3PMHONFEAXNON:O: 665511--77787-86-4631876 2T7estanaslhyasreess.controls& ref. substance with LR G1800, see LR G1935 for day SAMPLE DATE CODE DESCRIPTION RESULT MOL or (95% C.I.) 1 oo 2 oc 3 boc 4 oc FC-208 1 rrrsannees DISSOLVED ORGANIC CARBON 3.0 MG/L FC-208 IT TTTTTTTTC ~ DISSOLVED ORGANIC CARBON 4.2 MG/L FC-208 eeeeeeees DISSOLVED ORGANIC CARBON 3.1 MG/L FC-206 IT TTTTTTTTC DISSOLVED ORGANIC CARBON 2.9 MG/L 001087 UB 23/2000 EANRVCIHIRVUENDMIFEAINLNALLARBEOPHOA|RUTKY 1 LAB REQUEST NO. G1935 RDEEPQAURETSHTEONRT:NAM0E5:35MTE/EAR PDARTOEJECRTECNEOI:VED9:9700061/31090/01989 DESC: LANDFILL STAB. FOAM BIODEG. DAY 27 SWPLE DATE GOE DESCRIPTION CONTRACT LAB(S): EDXAPTECOCMOPMPLDEATTEED:: 0066/2/62/31/9189989 PPRHOOJNEECTNO:LEA6D5:1-J7H78-S6T4O3C8K 3M FAX NO: 651-778-6176 RESULT MDLor (95%0.1.) 1 ooc 2 oc. 3 Ld 4 oo 5 ooc. 6 00C 7 Doc 8 Doc 9 ooc 10 oc BLANK 1 CONTROL DISSOLVED ORGANIC CARBON <0.5 MG/L BLANK IT CONTROL DISSOLVED ORGANIC CARBON <0.5 MG/L LEACH LEACHATE ~ DISSOLVED ORGANIC CARBON 1.8 MG/L LEACH II LEACHATE DISSOLVED ORGANIC CARBON 2.0 MG/L soLIoS 1 tt DISSOLVED ORGANIC CARBON <0.5 MG/L soLIos 11 TTTTTTeees DISSOLVED ORGANIC CARBON <0.5 MG/L LEACH + LIDS DISSOLVED ORGANIC CARBON 2.8 MG/L LEACH + S0LIOS. DISSOLVED ORGANIC CARBON 1.9 MG/L REF SUB I SODIUM BENZ DISSOLVED ORGANIC CARBON <0.5 MG/L REF SUB II SODIUM BENZ DISSOLVED ORGANIC CARBON <0.5 MG/L 001088 vo 2312000 ENVIHUNMEN IAL LABURA|URT 1 ARCHIVED FINAL REPORT LRAEBQUERSETQOURESTNAMNEO:. GM1T9E4/1EAR PDERPOAJRETCMTENNTO:: 90957305013000 DDEASTCE: REFCCE-I2V0E3DC:E &06F/C2200/619C8E9BIODEG DAY 28 ECXOPNTCROAMCPT LDAATBE(:S):06/27/1989 DPARTOEJECCOTMPLLEEATD:ED:JW0S6T/O2C3K/1989 P3HMONFEAXNON:O: 65615-17-7787-86-4631786 TDAEYST2S8HAARNAELSYSCEOSN.TROLS + REF SUBSTANCE W/ LRG1800, SEE LRG1940 FOR SAMPLE DATE CODE DESCRIPTION RESULT MDL or (95% C.I.) 1 Doc 2 Doc 3 ooc 4 oc FC 203 1 meemeseoeees DISSOLVED ORGANIC CARBON ER tid DISSOLVED ORGANIC CARBON Foa0eT Cte DISSOLVED ORGANIC CARBON Fo208 11 Coeeeeneees DISSOLVED ORGANIC CARBON 3.0 MG/L 4.8 MA/L 3.7 MG/L 3.3 MG/L 001089 vera; cvuy EANRVCHAIKVUENDMIFEAINLNALLABRUEKPAOROTRY 1 LAB REQUEST KO. G1940 DREEPQAURETSMTEONRT:NAM0E5:35MTE/EAR PROJECT NO: 9970013000 DDEASTCE:RELCAENIDVFEIDL:L S0T6A/B20/F1O9R8M9BIODEG DAY 26 SAWPLE DATE CODE DESCRIPTION CONTRACT LAB(S:) DEAXTPECOCMOPMPLDEATTEED:: 060/62/72/31/1998899 PROJECT LEAD: JW STOCK SPHHONFEAXNON:O: 65615-17-7787-86-4631876 RESULT OL or(95% 6.1.) 1 BLANK 1 coNTRoL Doc 2 DISSOLVED ORGANIC CARBON BLWK IT CoNTROL <0.5 MG/L Doc 3 Doc ` DISSOLVED ORGANIC CARBON Leach 1 LEACHATE DISSOLVED ORGANIC CARBON LEAGH IT LEAGHATE <0.5 MG/L : 4.1 MG/L ooc 5 DISSOLVED ORGANIC CARBON SOLIDS I PRE-WASHED 4.4 MG/L Doc 6 oo DISSOLVED ORGANIC CARBON SOLOS IT PRE-ASHED DISSOLVED ORGANIC CARBON <0.5 MG/L <0.5 MG/L 7 LEA.#SOLID I ~""""=====" o0c DISSOLVED ORGANIC CARBON 3.7 MG/L 8 LEAssOLID IT "TTT Doc DISSOLVED ORGANIC CARBON 3.9 MG/L s REF SUB T Na BENZOATE 000 DISSOLVED ORGANIC CARBON <0. MG/L 10 REF SUB IT Na BENZOATE boc DISSOLVED ORGANIC CARBON <0.5 MG/L 001090