Document YrOvNoEbvQL7yRD6bwyn3GXN8

TR I - T X SOP - ggjr-'ii'g SOPS: c SOP TITLE: ADD ITT O'.T OF CATtLYIT "0 -M OPERATING vjr FPjr"'! OPERATOR: %!3 'rritcen :v: S3 .lets Ssb r e v i e e d r. v Frank Miller Ton" Curtis l ' /,: q "ONTEOT "00M 3ATE : rroroved nv: Art Reinhardt date: '>'>/ p/Q2 CHECK ACTION STEPS AS THEY ARE COMPLETED THE CATALYST ADDITION SCHEDULE FOLLOWS: (BASIS: 12HR SHIFT. 1/9/1989 MONDAY TUESDAY WEDNESDAY THURSDAY FRIDAY SATURDAY SUNDAY 2 DRUMS 2 DRUMS 2 DRUMS 1 DRUM 2 DRUMS 2 DRUMS i DRUM INSTRUCTIONS REVIEWED. WATCH FOR PINCH POINTS. 2. ENSURE THAT YOU ARE WEARING PROPER SAFETY EQUIPMENT. A. SAFETY GLASSES. B. HARDHAT. C. GOGGLES. D. RUBBER GLOVES. SL 0 E. DUST MASK. PRESSURE THE CATALYST POT UP TO BETWEEN 10 AND 30 PSIG WITH N2 IN ORDER TO MAKE SURE THAT THE POT IS CLEAR AND AT THI SAME TIME MAKE SURE THE PRESSURE GAUGE IS WORKING. DEPRESSURIZE IT TO THE ATMOSPHERE (IF ANY VAPORS APPEAR * DEPRESSURIZE IT TO THE REACTOR). 'CONFIDENTIAL: Subject to Protective Order ^ of 14th Judicial District Cour No. 91-1145 SL 006734 AFTER ALL THE ?) ESSURE RELIEVED AND OPEN THE HATCH _N HE CAT&L7 -ETI "HE HATCH MOLTS C'm 5. 'USING -THE CHAIM HOIST. MOVE A HULL OAT TO BE DUMPED INTO THE CATALYST POT. -''EUM IN POSITTCH DC- NOT GET DIRECTLY -ENEA7H "HE DRUM "N CASE THE CHAIN SLIPS. ONCE THE CATALYST ADDITION POT CHARGING ~?C\\ IS ASCENDED CONNECT THE CHAIN ACROSS THE OPENING TO PREVENT A FALL . POSITION THE FUNNEL IN THE HATCH OF THE CHARGE POT. D. REMOVE THE DRUM LID AND RING AND POSITION THE LINER BAG TO FEE? THE BAG PROM ENTERING THE CATALYST POT. DUMP THE CATALYST IN "HIE POT AND MOVE THE EMPTY DRUM OUT OF 'CHE WAY. b. MAKE SURE THE C-RING IS IN POSITION. TIGHTEN THE BOLTS SECURELY. CLC THE LID AND 7. PRESSURIZE THE CATALYST cOT WITH ME TC APPFC.HTMATELY 20 PSI ABOVE THE REACTOR PRESSURE AND BLOCK THE N2 TO THE CATALYST POT. 3. FULLY OPEN THE CATALYST ADDITION RAM VALVE. LEAKS. BE AWARE OF 9 . OPEN THE CATALYST ADDITION BLOCK VALVE . CNR LOG KING THE M2 A.c NEEDED TO MAINTAIN A POT PRESSURE ABOVE THE REACTOR PRESSURE AND KEEP CATALYST MOVING INTO THE REACTOR. 10. WHEN THE POT IS CLEAR (A LARGE PRESSURE DROP CAN BE SEEN AT THE CATALYST POT AND A HISSING SOUND OF N2 ENTERING THE REACTOR CAN BE HEARD) CLOSE THE CATALYST -OT BLOCK VALVE AND BLOCK THE N2. 11. 12. CLOSE THE CATALYST ADDITION RAM VALVE. (JUST BEFORE COMPLETELY CLOSING THE RAM VALVE, PUT A N2 SWEEP THROUGH THE POT TO KEEP ANY PEACTOR VAPORS FROM BEING TRAPPED BETWEEN THE ELOCK VALVE AND THE RAM VALVE. FINISH CLOSING THE RAM VALVE. ALONG WITH THE 12 'ND ADDITION PO" BLOCK VALVES.) CONFIDENTIAL: Subject to Protective Order of I4th Judicial District Coin No. 91-1145 DEPRESSURIZE THE CATALYST ADDITION POT AND STORE THE EMPTY CATALYST DRUMS IN THE PROPER PLACE. FTER ALL 'F THE CATALYST HAP TEEM AT.EEL . "-"'T op AMY TRASH ON THE DECK THAT HAY HAVE ACCUMULATED AS A RESULT OF THE CATALYST ADDITION. TIE-MRAFS. : LAST'D:-. !"V . HAY RE PLACED IN AN EMPTY DRUM FOR DISPOSAL. SL 006735 CONFIDENTIAL: Subject to Protective Order of 14th Judicial District Cour