Document YjQE2vQnpkByO9nmqarjVN06k
n waste analysis report Environmental Laboratory
PPG Industries, Inc.. Lake Charles. La
mpie : Location of Sample: -nmole collector: Sample -lethod/Device: Date/Time of Sampling :
YC-II Dopp Kettle Bottoms. Drums at TSCA-LS. G. Prejean Random grab - coiawasi 8-1-90 3:U5 am
Late Ail Analyses Completed 8-20-90
i.ALYSIS RESULTS
Test Parameters An.i labuitv 1 y ) N/A
Corrosivity -/) N/A
pH .nch/yr
,:eac t ivifv /) N/A
TCLP 'oxicitv
( mg/L)
As Ba Cd Cr Pb
N/A
Htf Se
AS
Standard 140 F 2-12.5 0,250 max
5.0 max 100.0 max 1.0 max 5.0 max 5.0 max 0,2 max 1.0 max 5.0 max
Report Submitted By Date
Gary Prejean 9-24-90
Lab Log Sample No 1940 1
ND ND ND 0.10 ND ND ND ND
i
ither ammeters (if needed) i S) ,`/a
n/iidiie detected
CHLORINATED'HYDROCARBONS (% 1
chloroethene
(VC)
Chloroetfoane
(EC)
Dichlormethane
(MeC12)
1,1-Dichloroethene
(VDC)
1.1-Dichloroethane
(DCE)
I,2-Dichloroethene
(cis/trans)
Tr ichloromethane
(CHCILI
1,2-pj.chloroethane
( EDC )
1.1,1-Trichioroethane
(MC)
Tetrachloromethane
(CC14)
Trichloroethene
(Trichlor)
1 . 1,2-r-Trichloroethane
( TCE )
Tetrachlorethene
(Perchlor1
1i1i1.2-Tetrachloroethane (unsvm)
1 .1,2.2-Tetrachioroethane !svm)
/entacnloroethane
( Penta )
para-Dichlorobenzene
(p-DCB)
Hexachioroethane
(HEXA )
Hexacnlorobutadiene
(HCED)
Unknown C1HC
Total ClHC
(%)
Disposal Method__________________ __________ Ensco
Profile No
1 PCBs
Heat Value
t'
i 11
i ppmi
BTU/lb
Chlorine
%
Water Densitv
wt%
-
g/ml
Ash Sodium
i
i
wt% wtX
SL 02I396 WMDS - 114701
SOS*SOS*SOS*SOS*S9S*SDSSDSSOS*SOSSDSSDS*SOSS3SSOS*SOS*SOS*SOS*SOS*SOS*SDS*SOS*SDSSOSSDSSDS*SOS*SOSSOS*SOSS9S*
SGS*SQS*SQS*SGS*SGS*SGSSGSSGS*SGS*SGS*SGSSGSSQSSGS*SGS*SGS*SGSSQS*SOS*SQSSOS*SGS
(A
Coea/) o
# SGS Environmental Lab rat ries 9008-038
CA
iOn
Y RESULTS - Sample ID* 1340 VC-II Dopp Kettle Bottoms
O
SGS ID*
9008-38-10
in
in
<in3 in
TCLP Metals
O
in
Date Extracted* 8/13/90
Concentration in ppm (mg/L) in TCLP Extract
in Oiinn
Date Analyzed* 8/20/90
O
Method
(A EPA HW
TCLP Metals
Result
Blank
Detection Limit
<A
O in D004
(A
O
D005
(A
D006
CA
iCmn3
D007 D008
in <iinn3 O
D009 D010 D011
CA
Arsenic Barium Cadmium Chromium Lead Mercury Selenium Silver
ND ND
HD 0.1
ND ND ND ND
ND ND ND ND ND ND ND ND
0.2 0.02 0.03 0.04 0.1 0.0002 0.2 0.02
t CA O CA CA O CA CA O CA CA O CA CA O CA CA O CA CA a CA CA ain in O CA CA ain i*n a in
T tal Metals
Date Analyzed* 8/14/90
Concentration in ppm (mg/Kg) in sample
Result
Blank
Method Detection Limit
Antimony Arsenic Barium Beryllium Cadmium Chromium Lead Mercury Nickel Silver Thallium
ND ND ND ND
0.5 14
0.9 Not Able to Analyze
ND ND ND
ND ND ND ND ND ND ND --
ND ND ND
1.0 1.0 0.3 0.3 0.3 0.3 0.5
--
0.5 0.3 1.5
ND denotes Not Detected at a level above the method detection limit.
o
CA CA
O
CA
(3 Member Of the SGS Group (Socum Gn*rle d Survaillanca)
8Q8 Environmental Laboratories
C9008-038
RESULTS - TCLP TOXICITY VOLATILES S08 IDi 19008-038-10 PPG IDi 1340 VC-II EDC Dopp Kettle Bottoms Dato Extracted! 8/15/90 Data Analyzed! 8/16/90
Concentration In ppb (uq/L) in TCLP Extract
1340 VC-II
Method
BCD Dopp
Detection
Kettle Bottoms
Liait
Benzene
ND 500
Carbon Tetrachloride
ND 500
Chlorobenzene
VD 500
chloroform
24,800
500
1,4-Dlohlorobenzene
BD 500
1,2-Diohloroethane
15,228
500
1,1-Dichloroethylane
18,897
500
Methylethylketone
BD 1000
Tetraohloroethylene
BD 500
Trichloroethylene
2,364
500
Vinyl Chloride
BD 1000
TCLP Blank
BD BD BD BD BD BD BD BD BD BD BD
Blank Detection
Limit 5.0 5.0 5.0 5.0 5.0 5.0 5.0
10.0 5.0 5.0
10.0
S
t I I
surrogate standard Parcant *aooarv_{at 0.050. ao/L)
1340 VC-II BCD Dopp
aim*
1,2-Dlohloroethane-d4 T luena-d8 4-Broeofluorobenzene
118 % 94 % 90 %
99 % 98 % 101 %
021398
ED dan tas Mot Detected at a level above the method detection Halt.
Member of the 008 Group
aaerf * lumwaMM
.
0Cl8eaQ8eaaaeSa0e8aa0Q00O8*0O8*8aaeBO0*aaae8<kSe8a8*8a8*8a0*8aa*0O88OSe0aS*8OS80Sl
8GS EnvtronmontmJ Laborttortoo
E90Q8-938
RESULTS - TCLP TOXICITY 3HMIV0LATILES SOS ID I E9008-838-18 FPO IDi 1340 VC-II EDC Dopp Kettle Bottoms
Not able to run dus to sample matrix.
ft o
S
i
*
SL 021399
Member of tn* sas Group (momm ommm m tuMMi
vm
Iasas*sas*sas*aftsos*8a*safta$*sQ8*tos*sQsos*so4asMQt tas*ftas*sas*$as*sastas
k?.Z7 PROCEDURE
LAB cOG NO. 1340
AAMETER
. iil C* VJ X X J* ^ '
^ \T / \
Cup Tester ASTM Standard D-93-79
METHOD L'SED
J C u Cl L X 'J. S 11 w k W.I O v wt Cup Tester ASTM Standard D-3278-78
i Spec l f )
or rosivitv I pH ; v/A
.SW-846 Method 0040 pH measurement
.Other (Speci f y
Corrosivity 'inch/vr ^ M/A
.National Association of Corrosion Engineers Standard TM-U1-G9
.Other
|
(Spec 11y) |
Reaclivitv
1. Normally unstable without detonating'.'
I
2. Reacts violently with water?
j
WN/A
3. Forms potentially explosive mixture with water?
j
4. Cyanide or sulfide bearing waste which can generate toxic !
< tme
gases, vapor or fumes ;nder pH conditions between 2 and
i r f : rma t i ve
12.5 ?
answer will
5. Capable of detonation or explosive reaction if subjected to:
:iassi f '
strong initiating source or if heated under confinement?
j
was t e
(j. Readily capable of detonation or explosive decomposition or
ic t ive )
reaction at standard temperature und pressure?
7. Forbidden Class A, or Class B explosive as defined in
> 49CFR 173.51, 173.53, and/or 173.88?
TCL?*
Parameter As
SW 846'
1 SW 846
Method Parameter' Method
6010
As
6010
IParameter PCB
SW 846 Method
1
|LD-2571
Y/A
Ba
6010
C1HC
5030
C1HC
ILD-25G2A
Cd
6010
Sodium 3050.6010 Heat ValuelLD-2562E
Cr
6010
dH
'*04 5
chlorine !LD-2362D
Pb 6010
Water
1LD-2566
Hg 7 4 70
Ash
1LD-2 5 6 1
Se 6010 *Toxicitv Characteristic Leaching Procedure
1
LABORATORY IDENTIFICATION Laboratorv; PPG Lake Charles Anaivst(s): SGS Labs
Test Parameters Analysed
rotal metals
8-14-yO
TCLP metals
8-20-90
TCLP volatiles. -
and Date 3-16-90
Rile 503.4.39 Mary Pre.jean
Si lUoo