Document YjLpZjMoL3M4pxn7x4vqqv8eE
S-V.
CC 46 CODE YC-13-A PKG
^8 #fIrlMIh MNMS
< DATE )
"<C6t ~NUMBERT~
%y
r. f ur. z^?** l d s .
I REFACTION NOTES _
PROCESSES <6> YC-13-A < )
AFPF.0VED HY i-u i <>/:m rr
TiFE-D BY JMH STANDARD HRS. 8.S
TIME
-----yp------
=. szsz s= a:r= ;s ,ssr= ss ts as s: ss 5:as
EQUIP I
KENT I
NAME DAL.AMAR YELLOW
-- I --- f ~-*"A---------- - ---- ----------------------------------- --
FREP I 1 ! OBTAIN 3-NITR0-4-AI1IN0ANTS0LE F`OR S6
1 1 2 | OBTAIN ACETOACET ORTHO AN1SIDIDE FOR S22
| 3 I CLEAN/ DRESS, CLOSE 24* CLARIS PRESS -
I ( 15 FRAMES
DV 'j^J^T~RUN~?7*~<5?5_G)~WAflR"'iNT0'"vZI]3jfi>r
2 vKS | WEIGH IN HYDROCHLORIC ACID FROM V-324
j|
M 5>
i % // %
A^Jsr i DUMP IN FROM SI 3-NITR0-4=AM^N0ANISbLE''*,'
|| Ii
LOT
#10O% ___
%
purSim
usr N--CODE | ACCT
LBS
r;
46-C
(Vi
28-D 396-C
559 119
!i II
i STIR 10 MIN OR LONGER TO WET
ADJ Tp 33* <11550 AT 20-32* F (ICE)
SIPHON IN SODIUM NlfRlTE IN 12-15 MIN
. . . ft Q __ j
_ _%
STIR 30 MIN AT 28-32~SG^F"MAiNTAINING
s+ c r > + k i f o r
J. n
RECORD: TIME STARTmI_, CR_C:_(+>,
KIJzL.__( + )
NOTE:
<1) IF CR~, KI-, ADD 20# *AS IS* INCREMENTS
HYDROCHLORIC ACID
ASSUME 32%
RECORD: CR______ < + >, KI_______< + ) (2) IF CR+, KI~, ADD 20# "AS IS* INCREMENTS
SODIUM NITRITE
ASSUME 33%
RECORD : CR______ < O , KJ._______( +)
330 LdtJi
57-A 'li>
725-A
495
28-D 725-A
DATE PFJf ( MAKING INSTRUCT 10I\ PATCH
1 | TAG 2 >-*!- ' CG 46 CODE YC~13~A <B)
ciJtfl' I SLURRY Tl' 40 GAL WATER IN DRUM 6 PRECOAT " t I CLAfJr MESS WITH DICALITE, FILTER AID
USE LBS
WHEN S IB STIR COMPLETE, DUMP IN ACTIVATED
CARBON
DUMP IN DICALITE, FILTER AID STIR 30 MIN AT 23-32 DEG F MAINTAINING
^ CR, + RECORD:
KI FDR TIME
SSTA2R0T..,&..,.;.._,,..i..........
c r _:i <-o ,
Kirzl___ < + )
NOTE:
(1) IF CR-, KI-/ ADD 20* 'AS IS" INCREMENTS
HYDROCHLORIC ACID
ASSUME32%
RECORD: CR( + >, KI( + >
<2> IF CR+, KI-, ADD 20* *AS IS" INCREMENTS
SjODIUM NITRITE
ASSUME33%
RECORD: ;CR__`< + >, KI________ ^< + >
%
15 10
N-CODE i
--'--f iilliiifcii
777- A I .
: *3-B !
777-n ,
MU 57-A j
|
^
'
20-D J_. 725-A |_.
U<5 | !1
UK6 1
| UK8 | 1^9 .vl
RUN 10* 1970 G) WATER INTO V^JOiL__ 6
INSTALL TEMP' CHART
-
POUR IN SODIUM HYDROXIDE M_, Jfr3JL?.
ADJ TO 40" (3880' G) AT 66-70 DEG F
CLOSE STACK DAMPER
STIR FOR S 22
3X330
7-D I 5 7'A I ..
DV "J^T'WHiN Ml S 14 STIRjCOMPLETE, TEST! By 6 RECORD
6
I CR
.< + >, Kfll_,,_( + > TEMP
28-32 F)
I NOTE:
I <1) IF CR-, KI-, ADD 20* "AS IS* INCREMENTS
i HYDROCHLORIC ACID
ASSUME 32%
I RECORD: CR_< + >,
)
i (2) IF CRf, KI-, ADD ZOi "AS IS" INCREMENTS
I ..SODIUM NITRITE
ASSUME 33%
RECORD: CR,,___( + >, KI_..,,( + )
ON V-3j^ AGITATOR* CHOP & ADD ICE
THEN TURN OFF AGITATOR*
2X33
PUMP DV THRU CLARIF PRESS INTO DV
J MAINTAINING TEMP AT 28-32? DEG F
> .
I RECORD: TIME SJARTTUSM TOT*AL MIN_rZ?l__
37-A
20-D t
725-A | ;
V |M2 | DUMP ACETOACET ORTHO ANISIDIDE INTO CV
? I I FROM S2
LOT
*100%
%
I .f
S.LU7-- ~J.f*2-- Ji*s
js7.
LV2& ! STIR 10 MIN TO DISSOLVE
l . ' '.0*34^1 OPEN STACK DAMPER
U5 1 RUN IN ACETIC ACID UNDERSiUUKRhFAAUCEb IJLNN 20-25
MINS*
M._/J____
SKMs STIR 5 MIN 6 RECORD:
_S_-__7___,,_.(5 J3-e.3>
1 IF NECESSARY, ADJ TO PH 5.3-623 & RECURS
" . --.I FH_.&.,,<5.8-6*3> SODIUM H'fPRQXTDE ASSUM1-5 ...................................
DATE F RINTLD : 1/13/C2
map [ ,l in * rF.ui 1 lrir.y r *i'i 'i u n ii
L'UUIP" MEMT
I PACE 3 OF 3 CG 46 CODE YC-13-A <B>
ACCT LBS
DV T IH> II 2 21 C'rlFiF COntLLiE UmSH l<* %f 4; 8 i LINES, PUMP PRESS FOF 20 HLN OR TO A -CR I TFST ON A SAMPLE OF TOTAL PRESS EFFLUENT,' I WHICHEVER COMES FIF<ST. COLLECT WASHINGS U-1N DV (S 21 ) 2JPt STIR 5 MIN & RECORD: TEMPj2TjC_<28-32itF> A
I IF NECESSARY, ADJ TO 28-32<F. RECORD*F 30*H WEIGH SULFAMIC ACID IN RUDDER DUCKET & WASH
L^I-NTO DV 3t^p-STIR 5 MIN & RECORD: 1(1 ___Tl__(-)
. i, tIFr-^NuEpCrESSARY, ADJ TO -KI (SULFAMIC ACID) JPfwD RECORD KI_~ _,,<--)
3T I RECORD: VOL_^J?J^-,,
.ir
MISC 9
34w-4*^5JtriGH SODIUM HYDROXIDE IN DRUMS FOR S41 k _j *1___ ,
35*<OlSSOLVE IGEPAL CO-630 IN-2 GAL WATER IN I DRUMS FOR S43
|| i 22-- i
| 50 II
7"D 979-0
337 .50
WHEN S 33 COMPLETE, ADJ CV TO 43" (4197 G)
UAT"80- 84 DEG F
0.
3**"'*^ CHECK ACCURACY: HT_^_ll__DEG F {,
RECORDER___ ife--. DEG F
| I /O 6
i
I ?***
kA-f~
*A-f. STWtTI +A
I:
IMMEDIATELY RUN IN DV THRU UNDERSURFACE
J
DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV
I
AT^S0^S4*F.
r|
CORD: TIME STARTj^Mj^, TOTAL MIN
_.. i
39^1 STIR 10 MIN. DISCONNECT TRANSFER LINE AT [
LJ3V"T MMEDI AT ELY `
.|
4>n RECORD': DI AZ0_.Z^1_<-), BASE.jfc-- < + >, I
! PHL.J^_<4.3~4.7) NOTE: (1) IF DIA20 +,
]
BASE
I, PH BELOW 4.3;
.I
(A) ADJ TO PH4.3-4.7SODUIMHYDROXIDE
|
ASSUME 50%|
7-D |
<B) RECORD: PH
_
!
(2) IF DIAZO +,BASE - & PH ABOVE 4-.3 ADD 8*1
100% N-7-D SODIUM HYDROXIDE ASSUME 50%I
7-D |___
TO A 55G DRUM. ADJ WITH WATER TO +/-25GI
ADD 20* 100%N-46-C ANDSTIR TO
| ________I 46-C ).
DISSOLVE, POUR IN CV AND STIR 10 MIN. |
(3) REPEAT ABOVE AS NECESSARY TO - DIAZO, |
+ BASE
!
POUR IN N-7-D SODIUM HYDROXIDE FROM S34 & {
(STIR 5 MINv '
"
t
RECORD PH_Oj0(7.1-9.0) & IF NECESSARY ADJ I PH^7.i-9.0 SODIUM HYDROXIDE ASSUME 50%1
34 a
7-D 1.1?
Re c o r d : p h ^L*: h y d r o c h l o r ic a c id a s s u me 32%)
28-D
IN N-979-D FROM S 35 EAT TO 200-2O4 DEG F IN 58-62 MIN
STIR 30 MIN AT 200-204 ,DEG J; UNCORD: TIME START___ LlL0JlL____
I MpCi I
<t*v
if S'
je `pint
$h
A4T\ FLOOD TO 94" (9174 G) AND STOP AGITATOR
-v
I START
FIN
OPTR
: t .;
. 1 -JU&ftfe.-- Jimk.................. .-JftJWk.--...
DUP050110611
DUP050110612
DUP050110613
