Document YbL4pnvazqBzR6na1NLYqr80

Emission Unit Enclosure D Inspection Observations 5/28-29/2024 Control Device Parameter Monitor Permit Limit Amodel Process (Down During the Inspection) Observations Hot Oil Heater KB-901 (0A17) Boiler UB-1210 (0A21) None None Flare KB-807 (0A15) None Extruder KM-601 (0A6D) None Visible Emissions (%) Visible Emissions (%) Steam Flowrate (lb/hr) Steam Pressure (psig) Visible Emissions (%) Pilot Flame Indicator <20% <20% <40% Visible Emissions (%) <40% Scrubber KD-633 (0A6B) Pressure Drop (in H2O) Flowrate <5 in H2O >1 gpm Seal Drum (KF613) Exit Temperature (F) <220F Vacuum (C603) Pump Exit Temperature (F) <220F Mix Tank KD-260 (0A2B) None Visible Emissions (%) <40% Mix Tank KD-260 (0A2B) Surge Tank KD-266 (0A2C) Concentrator KD-301 (CONC) Scrubber KT-1001 (A10A) Pressure Drop (in H2O) <6 in H2O Flowrate >20,000 lb/hr Distillation Still KD-806 (0A9A) Condenser C-803 (0A8C) Exit Temperature (F) <350F Hot Oil Heater #1 (00H1) Hot Oil Heater #2 (00H2) None None Sulfone Process Visible Emissions (%) Visible Emissions (%) <20% <20% Process Down Process Down Process Down Process Down Process Down Process Down Process Down Process Down Process Down Process Down 0 0 Waste Heat Boiler LM-731 (00B8) None Visible Emissions (%) Temperature <20% >1500F Railcar Unloading Station (RCU) Tank LD-101 (0C1E) None None Visible Emissions (%) Visible Emissions (%) <20% <40% Reactor LR-201 (0C4D) None Visible Emissions (%) <40% Waste Heat Boiler LM-731 (00B8) Mist Eliminator (0C7L) Pressure Drop (in H2O) Storage Tank LF-111 (0C2B) Storage Tank LF-115 (0C2X) Condenser (0C2A) Exit Temperature (C) >9 in H2O <12.8C Reactor LR-201 (0C4D) Condenser (0C2G) Exit Temperature (C) <12.8C Reactor Cooler LE-202 (0C2E) Tower LT-302 (0C3C) Reactor LR-380 (R380) Condenser (0C2L) Exit Temperature (C) <12.8C Condenser (0C5A) Exit Temperature (C) <12.8C Process Down 0 0 0 Process Down 3.45 0.62 0.98 3.01 Emission Unit Feed Tank LD-458 (0C4I) Feed Tank LD-401 (0C6F) Control Device Condenser (0C6A) Tower LT-460 (0C6G) Condenser (0C6C) Feed Tank LD-501 (0C5F) Tank LD-325 (0C5G) Tank LD-601 (0C6J) Feed Tank LD-621 (0C6K) Tank LD-651 (0C6L) Tank LD-701 (0C7D) Storage Drum LD-751 (0C7E) Tank LD-814 (0C8C) Tank LD-852 (0C8F) Drum LD-1201 (C10H) Drum LD-712 (0C7F) Tank LD-645 (0C64) Condenser (0C7A) Storage Tank LD-310 (0C5D) Storage Tank LD-314 (0C5E) Condenser (0C5B) Parameter Monitor Exit Temperature (C) Exit Temperature (C) Exit Temperature (C) Exit Temperature (C) Permit Limit <12.8C <12.8C <12.8C <12.8C Observations 1.97 2.40 2.88 1.91 Extraction Tower LT-445 (0C7G) Acid Extraction Column LT485 (T485) Acid Extraction Column II Bottoms Cleaner LH-487 (H487) Sulfone Neutralization and Wash Column II LT-495 (T495) Sulfone Neutralization and Wash Column II Bottoms Coalescer LH-497 (H497) II Condenser (0C7B) LD505 Crude Crystallizer Feed Drum (D505) LD531 Crude Crystallizer (D531) LM542 Crude Centrifuge (M542) LD551 Crude Reslurry Tank (D551) Condenser (D576) Tank LD-101 (0C1E) Scrubber (0C1A) Waste Heat Boiler LM-731 (00B8) Scrubber (0C8A) Scrubber (0C8B) Exit Temperature (C) <12.8C 0.74 Exit Temperature (C) <12.8C 3.90 Pressure Drop (in H2O) Pressure Drop (in H2O) Pressure Drop (in H2O) Flowrate pH <20 in H2O 0.2 <10 in H2O Process Down <10 in H2O >27,850 lb/hr >7 Process Down Hot Oil Heater H-601 (00P1) Xydar Process (Down During Inspection) None Visible Emissions (%) <20% Process Down Hot Oil Heater H-603 (00P2) None Visible Emissions (%) <20% Process Down Boiler H-602 (00P3) Boiler H-604 (00P4) None None Visible Emissions (%) Visible Emissions (%) <20% <20% Removed Removed Emission Unit Control Device Reactors R-201 A/B/C (RX01) None Parameter Monitor Visible Emissions (%) Permit Limit <40% Observations Process Down Mixer R-202A (0X2G) None Visible Emissions (%) <40% Process Down Mixer R-202B (0X2H) None Visible Emissions (%) <40% Process Down Mixer R-202C (0X2I) None Visible Emissions (%) <40% Process Down Reactors R-201 A/B/C (RX01) Mixer R-202A (0X2G) Mixer R-202B (0X2H) Mixer R-202C (0X2I) Scrubber (0X2T) Udel Thermal Oxidizer (00C2) None Reactor PR-401 (0U4D) None Pressure Drop (in H2O) Flowrate pH Udel Process Visible Emissions (%) Temperature (F) Visible Emissions (%) <15 in H2O >120 gpm >9 Process Down <40% >1600F Not Built <40% Not Built- Tank PD-411 (0U4A) Tank PD-412 (0U4B) Tank PD-603 (0U6A) Tank PD-604 (0U6B) Udel Thermal Oxidizer (00C2) Reactor PR-401 (0U4D) Column PT-715 (0U7I) Drum PD-425 (0U4E) Tank PD-202 (0U2A) Tank PD-503 (0U5C) Tank PD-730 (0U7G) Scrubber (00C3) Pressure Drop (in H2O) Flowrate pH Hot Oil Heater (BE-01) None KetaSpire/NovaSpire (also known as Jupiter (PEEK) Process) Visible Emissions (%) >5 in H2O >10 gpm >7 <20% Not Built- Boiler (BE-02) None Visible Emissions (%) Steam Flowrate (lb/hr) Steam Pressure (psig) <20% Emission Unit Group HE-2 Process Reactor (PR-200) Emission Unit Group HE-1 HCL Storage Tank (PF-800) Scrubber (SC1) Scrubber (SC2) Unit FD-1210: 2,5-DCBP Mix Tank (FD02) Scrubber (FT01) Unit FR-200: Digestion Tank(FD08) Scrubber (FT02) Carbon Drum Membrane (FA03) Unit FR-400 through Unit FR805 and Unit FF-705 through Unit FF-800 Scrubber (FT03) Pressure Drop (in H2O) <15 in H2O 0.1 Pressure Drop (in H2O) Push Process (Not Built) Pressure Drop (in H2O) pH Pressure Drop (in H2O) pH <15 in H2O <15 in H2O >7 <15 in H2O >7 0.8 Not Built Not Built Pressure Drop (in H2O) <90 psia Not Built Pressure Drop (in H2O) <15 in H2O Not Built