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D.V.OOg I (3T5), 31 7, 322,^32
, CG 46 COM YT-820-D PKG___
*JUJI 9 1932
F2J62
T'd at eT!-" ~(LOT^m0mBER>
EST. UT 2563# LBS-
PROCESSES
( ) YT-820-D (D>
( >-
(>
() <)
TYPED BY: JMH
/^STANDARD HRS. . 8.8
APPROVED BY EWK 10/21/81
TINE _____ M
PREPARATION NOTES___ ^
.JfeLJtL'A,
7T7a/~^Iu'5gi^c'
EQUIP MENT ---------
PREP 1
J
J NAME: DALAMAfS YELLOW - R
--L
1 1 | OBTAIN 3-NITR0-4-AMTN0ANIS0LE FOR S6
1 2 | OBTAIN ACETOACET ORTHO ANISIDIDE FOR S22
3 I CLEAN, DRESS, CLOSE '24" CLARIF PRESS -
I 15 FRAMES
/
t USE I LBS
N-CODE I Acer 1 LBS
396-C | I 46-C |
______'_____ - Mil__________________ rl $
]eo_____fa rj>
DV N 777-<595 G>~WATiR"rrNTO vll_ZZZI"
~7~~
snW4 EIGH IN HYDROCHLORIC ACID FROM ., xfSijiXjx.
Uijjs. iI
28-D | 559
DUMP IN FROM SI 3-NI TR0-4-AM I NO ANI SOLE
396-C | 1190
LOT. A
* 1O0%
%^ :____ JJlP--
3I i it.
i__
! ___i
I__
__ 1 ___I ___I
RUN i7j
^Ht s TIr 10 MIN OR LONGER TO WET
i/IT"!
A&J TO 33* (1155G) AT 28-32# F (ICE)
iidX330I
'`SIPHON IN SODIUM NITRITE IN 12-15 MIN
, __%
[R0OMIN AT 28-32 DEG F MAINTAINING
iZfZfe:! |I
I + CR, + KI FOR S 12
.____
11
i RECORD : TIME SlhRlJAAlA, CRj7TZZ<+>,
i
I
| KI + >
iI
1 NDTE>^'
II
} (1-riF CR-, KI-, ADD 20* "AS IS" INCREMENTS!
j
I HYDROCHLORIC ACID
ASSUME 32% |______ |
| - ^^PECORD: CR___ __(+), KI___ __( + >
II
| (ST IF CR+, KI-, ADD 20=5= "AS IS" INCREMENTS!
|
| SODIUM NITRITE
ASSUME 33% i________|
I
RECORD: CR_.____ ( + ), KI______ ( + >
I1
EQUIP MENT I M'.SC
uV A
cv 5
DV 6
CV 7
DATE PRINTED:
1/12/82
I,USE | N-CQDE ! ACCT
AGE 2 OF 3 CG 46 CODE YT-820-D (D> I LBS .|
1 LBS
SLURRY IN 40 GAL WATER IN DRUM & PRECOAT CLARIF PRESS WITH DICALITE, FILTER AID
i! | 77?--A 1
WHEN S 10 STIR COMPLETE, DUMP IN ACTIVATED
fBON
IMP IN DICALITE, FILTER AID
STIR 30 MIN AT 28-32 DEG F MAINTAINING
+ CE, + KT FOR S 20 , ,
i
RECORD: TIME' START_//J^2Y^, CR,,.XTM< + ),
_ ,Ki_rr!r_{+)
NO
(<> IF CR-, KI-, ADD 20* "AS IS1- INCREMENTS
HYDROCHLORIC ACID
ASSUME 32%
^-t?ECORD: CR____ <+) , `KI ---------- <+)
<#TIF CR+, K2-, ADD 20* "AS IS* INCREMENTS
SODIUM NITRITE
ASSUME 33%
RECORD: CR____._< + > , KI_____< + >
15 10
! ..._____1
i
_______} 1
113-B | 15 777-A I 10
1 57-A I______
i
28-D
725- M | ___
RlJbMO* (970 G> WATER INTO V_ZJf_K._ 6
TALL TEMP CHART
^ t/t-ca
IN SODIUM HYDROXIDE M_X_____I
J TO 40* (3880G) AT 66-70 DEG F
SE STACK DAMPER
STIR FOR S 22
,
1
I 3X3301 II I1 11
7-D I 569
57-A X'^SJLt i I I
WHEN l~T4"sflR"cpMPLiTi:"fES:r3.V~i"RicORD""'T
~I
CRJTX-J^->, KI< +) TEMP : Jli__( 28-32 F J [
1
NQTp^
I CfTTF CR-, KI-, ADD 20* "AS IS* INCREMENTS!
i
HYDROCHLORIC ACID
ASSUME 32% |___ I
?CORD : CR___ __< + >, KI_____ < + )
II
(2TIF CR+, KI-, ADD 20* "AS IS" INCREMENTS!
T
SODIUM NITRITE
ASSUME.33% i___ i
RECORD: -^CR______< + >, KI_____ ( + )
1!
L ON V~&(& AGITATOR. CHOP &ADD ICE i !
iEN TURN OFF AGITATOR.
2X330
PUMP DV THRU CLARIF PRESS INTO DV
MAINTAINING TEMP AT 28-22 DEG F
:ORD: TIME START_/Z&$, TOTAL MIN
J---- 57-A [______
28-D 725-A
1
I !____
!
57-A A h&!L~
! .
d u mp ~a c e t 6a c e t _6r t h o -a n is id id e ~in t o ""c v _
FROM S2 . .
-- LOT
*100%
iSin___ --Jd&kr
^
Mb i t . z~n&: WL
iUSL
}______
MIN TO DISSOLVE
N STACK DAMPER
RUN IN ACETIC ACID UNDERSURFACE IN 20-25
M. L Of'
IR 5 MIN & RECORD: PH^fc&2L(5.8-6.3) IF NECESSARY, ADJ TO PH 5.8-6.3 & RECORD
1 I
I I
PH <5.8-6.3) SODIUM HYDROXIDE ASSUME50%!_____ I
ACETIC ACID
ASSUME70% I ___ ._!
46-C I 1547 1 I ! :
I 30-D I 371
7-D 1_____ _ 30-D 1__.___ ,
DUP050047593
BATE PRINTED: 1/12/82 MAKING INSTRUCTIONS:BATCH UNIT
EGUIP I MENT |
I | PGE 3 OF 3
USE | N-CODE
CG 46 CODE YT-820-D <D> I LBS I|
I LBS
kDV* J2. i WHEN S 21 CLARIF COMPLETE, WASH
DV <S 4) 1
1
8I
l LINES, PUMP tx PRESS FOR 20 MIN OR TO A -CR |
1
( f TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT,* I
1
i | WHICHEVER COMES FIRST* COLLECT WASHINGS I
i
| I ILDV <S 21). .
*
I
\2^rrim 5 MIN & RECORD: TEMP3j 2L<28-32*F> & I jbjkGt]
57-A
3 "ijHfr NECESSARY, ADJ TO 28~32*F. RECORD_______ *F!
i
iWEIGH SULFAMIC ACID IN RUBBER BUCKET & WASH I
DV J I 15 | 395-D
5 MIN & RECORD: KIj!+r^__<-)
i!
NECESSARY, ADJ TO -KI (SULFAMICACID) JrND RECORD KI,,rr__-.<-)
i f
10
\
395-D
RECORD: VOL,,&.?__*
I
I
wiiGH"HDluFHYDRDXiDi_lN_DRUMS~F0R~S4j"""T
m___ %___
I DISSOLVE IGEPAL CD-630 IN 20 GAL WATER IN I
I DRUMS FOR S43
i
JlSLl 50 i
7-D 1 337 979-D I 50
cv |36*TWHEJ* S 33 COMPLETE, ADJ CV TO 43" <4197 G)
10
L*ftT''80~84 DEG F
Wja>
13''9TCHECK ACCURACY: HT_2l 3___DEG F 6
RECORDER__DEG F
IMMEDIATELY RUN IN DV THRU~UNDERSURFACE
DISTRIBUTOR IN 60-65 MIN* MAINTAIN CV
AT 80-84*F*
y
ORB: TIME STARTTOTAL MIN___ ___
STIR 10 MIN* DISCONNECT TRANSFER LINE AT CV IMMEDIATELY
RECORD: DIAZO_crr,,,<->, BASE_4:____ < +
PH,,_*jL_<4.3-4.7> NOTE: (1) IF DIAZO +,
BASE
& PH BELOW 4-3:
| (A) ADJ TO PH 4*3-4.7 SDDUIM HYDROXIDE { ASSUME 50%
7-D I ____ _
J <B) RECORD: PH________
{ (2) IF DIAZO *,BASE - 6 PH ABOVE 4*3 ADD 84 I 100% N-7-D SODIUM HYDROXIDE ASSUME 50% 1 TO A 55G DRUM. ADJ WITH WATER TO +/-25G
I ADD 204 100% N-46-C AND STIR TO I DISSOLVE, POUR IN CV AND STIR 10 MIN* | <35 REPEAT ABOVE AS NECESSARY TO - DIAZO,
7-D 46-C
, + BASE
I4><F-0UR IN N-7-D SODIUM HYDROXIDE FROM S34 6
' ""IR 5 MIN*
RECORD PHJaTlffi < 7.1-9.0) 6 IF NECESSARY ADJ
I F-hL-T* 1-9.0 ^ SODIUM HYDROXIDE ASSUME 50% .Z~ RD: PH$Lt HYDROCHLORIC ACID ASSUME 32%
7-D 28-D
IN N-979-D FROM S 35
Tr'HEAT TO 2OO-204 DEG F IN 53-62 MIN
\/t5. 1 STIR 30 MIN AT 200-204 DfG/F ? j RECORD: TIME START,,,,'Jd&/3z:J~
|46 | FLOOD TO 94*H9174 G) AND STOP AGITATOR
START
FIN
OPTR
DUP050 047594
DUP050047595