Document Y9jGLRNn5X0eyqv0MpvqO76R8
SEVERN TRENT LABORATORIES ANALYTICAL REPORT
JOB NUMBER: 238585
Prepared For:
Weston Solutions, Inc. 1400 Weston Way Building 5-2
West Chester, PA 19380-1499
Project: Confidential Decatur - FC Investigation
Attention: Jai Kesari
Date: 07/29/2005
Signature Name: Richard C. Wright Title: Project Manager E-Mail: rwright@stl-inc.com
Date
STL Chicago 2417 Bond Street UcSveas iia Park, IL 60466
PHONE: (708) 534 5200 FAX..: (708) 534 5211
This Report Contains (_____) Pages
STL Chicago is part of Severn Trent Laboratories, Inc.
SA M P LE IN F O RM A T ION Date: 07/29/2005
Job Number. 238585 Customer... Weston Solutions, Inc. Attn...... Jai Kesari
Project Number....... 20004891 Customer Project ID.... CONFIDENTIAL DECATUR Project Description.... Confidential Decatur - FC Investigation
Laboratory Sample ID
238585-1 238585-2 238585-3 238585-4 238585-5 238585-6 238585-7 238585-8 238585-9 238585-10 238585-11 238585-12 238585-13 238585-14 238585-15 238585-16 238585-17 238585-18 238585-19 238585-20 238585-21 238585-22 238585-23 238585-24
Customer Sample ID DLS-SW-TRM307-0-050718 DLS-SW-TRM301-0-050718 DLS-SW-TRM295-0-050719 DLS-SW-TRM289-0-050719 DLS-SW-TRM283-0-050719 DLS-SW-TRM277-0-050719 DLS-SW-TRM271-0-050719 DLS-SW-TRM265-0-050719 DLS-SW-TRM261-0-050720 DLS-SW-TRM256-0-050720 DLS-SW-TRM254-0-050720 DXS-SW-T01001-0-050721 DXS-SW-T01002-0-050721 DXS-SW-T01003-0-050721 DXS-SW-T01004-0-050721 DXS-SW-T01005-0-050721 DXS-SW-T01006-0-050721 DXS-SW-T01007-0-050721 DXS-SW-T01008-0-050721 DXS-SW-T01009-0-050721 DXS-SW-T01010-0-050721 DXS-SW-T02001-0-050721 DXS-SW-T02002-0-050721 DXS-SW-T02003-0-050721
Sample Matrix Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water
Date Sampled 07/18/2005 07/18/2005 07/19/2005 07/19/2005 07/19/2005 07/19/2005 07/19/2005 07/19/2005 07/20/2005 07/20/2005 07/20/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005 07/21/2005
Time Sampled
14:50 15:30 08:15 09:00 09:45 10:15 14:40 15:00 10:00 11:55 12:15 08:10 08:25 08:40 08:55 09:10 09:25 09:33 09:45 09:55 10:10 11:00 11:15 11:25
Date Received 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005 07/23/2005
Time Received
09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00 09:00
Page 1
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM307-0-050718 Date Sampled......:07/18/2005 Time Sampled......:14:50 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-1 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 78 4.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1540 jmk
5.0 1
mg/L 155426
07/25/05 0739 jmk
* In Description = Dry Wgt.
Page 2
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM301-0-050718 Date Sampled......:07/18/2005 Time Sampled......:15:30 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-2 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 76 3.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1542 jmk
5.0 1
mg/L 155426
07/25/05 0742 jmk
* In Description = Dry Wgt.
Page 3
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM295-0-050719 Date Sampled......:07/19/2005 Time Sampled......:08:15 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-3 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 68 9.0
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1545 jmk
5.0 1
mg/L 155426
07/25/05 0750 jmk
* In Description = Dry Wgt.
Page 4
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM289-0-050719 Date Sampled......:07/19/2005 Time Sampled......:09:00 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-4 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 94 5.5
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1547 jmk
5.0 1
mg/L 155426
07/25/05 0752 jmk
* In Description = Dry Wgt.
Page 5
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM283-0-050719 Date Sampled......:07/19/2005 Time Sampled......:09:45 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-5 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 68 7.0
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1550 jmk
5.0 1
mg/L 155426
07/25/05 0755 jmk
* In Description = Dry Wgt.
Page 6
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM277-0-050719 Date Sampled......:07/19/2005 Time Sampled......:10:15 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-6 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 62 3.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1552 jmk
5.0 1
mg/L 155426
07/25/05 0757 jmk
* In Description = Dry Wgt.
Page 7
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM271-0-050719 Date Sampled......:07/19/2005 Time Sampled......:14:40 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-7 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 72 6.5
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1555 jmk
5.0 1
mg/L 155426
07/25/05 0800 jmk
* In Description = Dry Wgt.
Page 8
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM265-0-050719 Date Sampled......:07/19/2005 Time Sampled......:15:00 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-8 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 84 6.0
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1557 jmk
5.0 1
mg/L 155473
07/25/05 0806 jmk
* In Description = Dry Wgt.
Page 9
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM261-0-050720 Date Sampled......:07/20/2005 Time Sampled......:10:00 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-9 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 34 3.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155586
07/25/05 1600 jmk
5.0 1
mg/L 155473
07/25/05 0809 jmk
* In Description = Dry Wgt.
Page 10
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM256-0-050720 Date Sampled......:07/20/2005 Time Sampled......:11:55 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-10 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 130 2.5 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155676
07/26/05 1010 jmk
5.0 1
mg/L 155473
07/25/05 0812 jmk
* In Description = Dry Wgt.
Page 11
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DLS-SW-TRM254-0-050720 Date Sampled......:07/20/2005 Time Sampled......:12:15 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-11 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 98 4.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155676
07/26/05 1013 jmk
5.0 1
mg/L 155473
07/25/05 0821 jmk
* In Description = Dry Wgt.
Page 12
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01001-0-050721 Date Sampled......:07/21/2005 Time Sampled......:08:10 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-12 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 110 4.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155676
07/26/05 1017 jmk
5.0 1
mg/L 155473
07/25/05 0824 jmk
* In Description = Dry Wgt.
Page 13
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01002-0-050721 Date Sampled......:07/21/2005 Time Sampled......:08:25 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-13 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 110 5.0
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155676
07/26/05 1020 jmk
5.0 1
mg/L 155473
07/25/05 0827 jmk
* In Description = Dry Wgt.
Page 14
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01003-0-050721 Date Sampled......:07/21/2005 Time Sampled......:08:40 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-14 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 82 2.5 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155801
07/27/05 1449 jmk
5.0 1
mg/L 155473
07/25/05 0830 jmk
* In Description = Dry Wgt.
Page 15
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01004-0-050721 Date Sampled......:07/21/2005 Time Sampled......:08:55 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-15 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 100 3.5 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155801
07/27/05 1452 jmk
5.0 1
mg/L 155473
07/25/05 0833 jmk
* In Description = Dry Wgt.
Page 16
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01005-0-050721 Date Sampled......:07/21/2005 Time Sampled......:09:10 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-16 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 82 3.5 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155801
07/27/05 1455 jmk
5.0 1
mg/L 155473
07/25/05 0836 jmk
* In Description = Dry Wgt.
Page 17
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01006-0-050721 Date Sampled......:07/21/2005 Time Sampled......:09:25 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-17 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 82 3.5 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155801
07/27/05 1458 jmk
5.0 1
mg/L 155473
07/25/05 0839 jmk
* In Description = Dry Wgt.
Page 18
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01007-0-050721 Date Sampled......:07/21/2005 Time Sampled......:09:33 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-18 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 78 4.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155801
07/27/05 1501 jmk
5.0 1
mg/L 155473
07/25/05 0842 jmk
* In Description = Dry Wgt.
Page 19
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01008-0-050721 Date Sampled......:07/21/2005 Time Sampled......:09:45 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-19 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 88 2.5 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155801
07/27/05 1504 jmk
5.0 1
mg/L 155473
07/25/05 0845 jmk
* In Description = Dry Wgt.
Page 20
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01009-0-050721 Date Sampled......:07/21/2005 Time Sampled......:09:55 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-20 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 100 4.5 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155925
07/28/05 1244 jmk
5.0 1
mg/L 155473
07/25/05 0848 jmk
* In Description = Dry Wgt.
Page 21
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T01010-0-050721 Date Sampled......:07/21/2005 Time Sampled......:10:10 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-21 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 100 6.5
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155925
07/28/05 1247 jmk
5.0 1
mg/L 155473
07/25/05 0851 jmk
* In Description = Dry Wgt.
Page 22
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T02001-0-050721 Date Sampled......:07/21/2005 Time Sampled......:11:00 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-22 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 32 4.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155925
07/28/05 1249 jmk
5.0 1
mg/L 155473
07/25/05 0854 jmk
* In Description = Dry Wgt.
Page 23
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T02002-0-050721 Date Sampled......:07/21/2005 Time Sampled......:11:15 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-23 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 110 4.0 B
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155925
07/28/05 1251 jmk
5.0 1
mg/L 155473
07/25/05 0857 jmk
* In Description = Dry Wgt.
Page 24
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
. CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DXS-SW-T02003-0-050721 Date Sampled......:07/21/2005 Time Sampled......:11:25 Sample Matrix.....:Water
TEST METHOD
PARAMETER/TEST DESCRIPTION
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 238585-24 Date Received....... :07/23/2005 Time Received....... :09:00
Date:07/29/2005 ATTN: Jai Kesari
SAMPLE RESULT Q FLAGS 98 6.0
MDL 8.3 1.1
RL DILUTION UNITS BATCH DT DATE/TIME TECH
10 1
mg/L 155925
07/28/05 1253 jmk
5.0 1
mg/L 155473
07/25/05 0900 jmk
* In Description = Dry Wgt.
Page 25
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
LA B ORA T O R Y C HR ON IC LE
Date: 0D7/29/2005
| CUSTOMER: Weston Solutions, Inc.
PROJECT: CONFIDENTIAL DECATUR
ATTN: Jai Kesari
| Lab ID: 238585-1 | METHOD | EDD | 160.1 | 160.2
Client ID: DLS-SW-TRM307-0-050718 DESCRIPTION Electronic Data Deliverable Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-2 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM301-0-050718 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-3 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM295-0-050719 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-4 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM289-0-050719 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-5 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM283-0-050719 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-6 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM277-0-050719 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-7 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM271-0-050719 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-8 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM265-0-050719 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-9 | METHOD | 160.1 | 160.2
Client ID: DLS-SW-TRM261-0-050720 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
| Lab ID: 238585-10 Client ID: DLS-SW-TRM256-0-050720
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-11 Client ID: DLS-SW-TRM254-0-050720
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-12 Client ID: DXS-SW-T01001-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
Date Recvd: 07/23/2005 Sample Date: 07/18/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1
1 155586 155586
07/25/2005 1540
1 155426 155426
07/25/2005 0739
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/18/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1542
1 155426 155426
07/25/2005 0742
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/19/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1545
1 155426 155426
07/25/2005 0750
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/19/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1547
1 155426 155426
07/25/2005 0752
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/19/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1550
1 155426 155426
07/25/2005 0755
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/19/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1552
1 155426 155426
07/25/2005 0757
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/19/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1555
1 155426 155426
07/25/2005 0800
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/19/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1557
1 155473 155473
07/25/2005 0806
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155586 155586
07/25/2005 1600
1 155473 155473
07/25/2005 0809
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155676 155676
07/26/2005 1010
1 155473 155473
07/25/2005 0812
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155676
07/26/2005 1013
1 155473 155473
07/25/2005 0821
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155676 155676
07/26/2005 1017
DILUTION
Page 26
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
LA B ORA T O R Y C HR ON IC LE
Date: 07/29/2005
. CUSTOMER: Weston Solutions, Inc.
PROJECT: CONFIDENTIAL DECATUR
ATTN: Jai Kesari
| Lab ID: 238585-12 Client ID: DXS-SW-T01001-0-050721
| METHOD
DESCRIPTION
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-13 Client ID: DXS-SW-T01002-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-14 Client ID: DXS-SW-T01003-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-15 Client ID: DXS-SW-T01004-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-16 Client ID: DXS-SW-T01005-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-17 Client ID: DXS-SW-T01006-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-18 Client ID: DXS-SW-T01007-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-19 Client ID: DXS-SW-T01008-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-20 Client ID: DXS-SW-T01009-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-21 Client ID: DXS-SW-T01010-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-22 Client ID: DXS-SW-T02001-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
| 160.2
Solids, Total Suspended (TSS)
| Lab ID: 238585-23 Client ID: DXS-SW-T02002-0-050721
| METHOD
DESCRIPTION
| 160.1
Solids, Total Dissolved (TDS)
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155473 i55473
07/25/2005 0824
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 i55676 i55676
07/26/2005 1020
1 i55473 i55473
07/25/2005 0827
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i5580i i5580i
07/27/2005 1449
i i55473 i55473
07/25/2005 0830
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i5580i i5580i
07/27/2005 1452
i i55473 i55473
07/25/2005 0833
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i5580i i5580i
07/27/2005 1455
i i55473 i55473
07/25/2005 0836
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i5580i i5580i
07/27/2005 1458
i i55473 i55473
07/25/2005 0839
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i5580i i5580i
07/27/2005 1501
i i55473 i55473
07/25/2005 0842
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i5580i i5580i
07/27/2005 1504
i i55473 i55473
07/25/2005 0845
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i55925 i55925
07/28/2005 1244
i i55473 i55473
07/25/2005 0848
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i55925 i55925
07/28/2005 1247
i i55473 i55473
07/25/2005 0851
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
i i55925 i55925
07/28/2005 1249
i i55473 i55473
07/25/2005 0854
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155925 i55925
07/28/2005 1251
DILUTION
Page 27
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 238585
LAB ORA TORY CHR ON IC LE
Date: 07/29/2005
CUSTOMER: Weston Solutions , Inc.
PROJECT: CONFIDENTIAL DECATUR
ATTN: Jai Kesari
|
Lab ID: 238585-23 Client ID: DXS-SW-T02002-0-050721
METHOD
DESCRIPTION
160.2
Solids, Total Suspended (TSS)
Lab ID: 238585-24 Client ID: DXS-SW-T02003-0-050721
METHOD
DESCRIPTION
160.1
Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS)
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155473 155473
07/25/2005 0857
DILUTION
Date Recvd: 07/23/2005 Sample Date: 07/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 155925 155925
07/28/2005 1253
1 155473 155473
07/25/2005 0900
DILUTION
Page 28
Job Number.: 238585 CUSTOMER: Weston Solutions , Inc.
QUA L ITY CON TR O L RE SU LTS PROJECT : CONFIDENTIAL DECATUR
Report Date.: 07/29/2005 ATTN: Jai Kesari
Test Method...... 160.1 Method Description. Solids, Total Dissolved (TDS) Parameter........ Solids, Total Dissolved (TDS)
Batch.......... .: 155586 Equipment Code...
Analyst... jmk Test Code. TDS
QC Lab ID
Reagent
Units
MB 155586-001
mg/L
LCS 155586-002 I04LSTTS1 mg/L
QC Result
QC Result
8.30000 U 236.00000
True Value Orig. Value QC Calc. F * Limits
Date Time
250.00000
8.30000 U 94
07/25/2005 1500 % 80-120 07/25/2005 1502
Test Method...... : 160.1 Method Description. Solids, Total Dissolved (TDS) Parameter........ Solids, Total Dissolved (TDS)
Batch.......... .: 155676 Equipment Code...
Analyst... jmk Test Code. TDS
QC Lab ID
Reagent
Units
MB 155676-001
mg/L
LCS 155676-002 I04LSTTS1 mg/L
QC Result
QC Result
8.30000 U 258.00000
True Value Orig. Value QC Calc. F * Limits
Date Time
250.00000
8.30000 U 103
07/26/2005 0900 % 80-120 07/26/2005 0903
Test Method...... : 160.1 Method Description. Solids, Total Dissolved (TDS) Parameter........ Solids, Total Dissolved (TDS)
QC Lab ID
Reagent
Units
MB 155801-001 LCS 155801-002 I04LSTTS1 MD 238585-19 MS 238585-19 I04LSTTS1
mg/L mg/L mg/L mg/L
QC Result
QC Result
8.30000 U 246.00000 108.00000 336.00000
Batch.......... .: 155801 Equipment Code...
Analyst... jmk Test Code. TDS
True Value Orig. Value QC Calc. F * Limits
Date Time
250.00000 250.00000
8.30000 U 88.00000 88.00000
98 20.4 99
% 80-120 * R 20.0
% 75-125
07/27/2005 1400 07/27/2005 1403 07/27/2005 1507 07/27/2005 1510
Test Method...... : 160.1 Method Description. Solids, Total Dissolved (TDS) Parameter........ Solids, Total Dissolved (TDS)
Batch.......... .: 155925 Equipment Code...
Analyst... jmk Test Code. TDS
QC Lab ID
Reagent
Units
MB 155925-001
mg/L
LCS 155925-002 I04LSTTS1 mg/L
QC Result
QC Result
8.30000 U 260.00000
True Value Orig. Value QC Calc. F * Limits
Date Time
250.00000
8.30000 U 104
07/28/2005 1240 % 80-120 07/28/2005 1242
Test Method...... : 160.2 Method Description. Solids, Total Suspended (TSS) Parameter........ Solids, Total Suspended (TSS)
Batch.......... .: 155426 Equipment Code...
Analyst... jmk Test Code. TSS
QC Lab ID
Reagent
Units
MB 155426-001
mg/L
LCS 155426-002 I05GSTSS1C mg/L
MD 238585-2
mg/L
MS 238585-2 I05GSTSS2C mg/L
QC Result
QC Result
0.73700 U 202.50000
3.50000 B 104.00000
True Value Orig. Value QC Calc. F * Limits
Date Time
200.00000 100.00000
1.10000 U 101 3.00000 B 0.50000 3.00000 B 104
% 80-120 A 5.00000 % 75-125
07/25/2005 0700 07/25/2005 0703 07/25/2005 0744 07/25/2005 0747
Page 29
* %=% REC, R=RPD, A=ABS Diff., D=% Diff.
Job Number.: 238585 CUSTOMER: Weston Solutions , Inc.
QUA LITY CON TRO L R ESU LTS PROJECT : CONFIDENTIAL DECATUR
Report Date.: 07/29/2005 ATTN: Jai Kesari
Test Method...... 160.2 Method Description. Solids, Total Suspended (TSS) Parameter........ Solids, Total Suspended (TSS)
Batch.......... .: 155473 Equipment Code...
Analyst... jmk Test Code. TSS
QC Lab ID
Reagent
Units
MB 155473-001
mg/L
LCS 155473-002 I05GSTSS1C mg/L
MD 238585-10
mg/L
MS 238585-10 I05GSTSS2C mg/L
QC Result
QC Result
0.73700 U 206.00000
4.00000 B 106.00000
True Value Orig. Value QC Calc. F * Limits
Date Time
200.00000 100.00000
1.10000 U 103 2.50000 B 1.50000 2.50000 B 106
% 80-120 A 5.00000 % 75-125
07/25/2005 0800 07/25/2005 0803 07/25/2005 0815 07/25/2005 0818
Page 30
REC, R=RPD, A=ABS Diff., D=% Diff.
QUA L ITY A SSU RA N CE M E THO D S
RE FEREN CE S AN D N O TES
Report Date: 07/29/2005
REPORT COMMENTS 1) All pages of this report are integral parts of the analytical data. Therefore, this report should
be reproduced only in its entirety. 2) Soil, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for
landfill disposal or incineration parameters. All other solid matrix samples are reported on an "as received" basis unless noted differently. 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201 5) According to 40CER Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed immediately after aqueous sample collection. When these parameters are not indicated as field (e.g. pH Field) they were not analyzed immediately, but as soon as possible on laboratory receipt.
Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) Inorganic Qualifiers (Q-Column) U Analyte was not detected at or above the stated limit. < Not detected at or above the reporting limit. J Result is less than the RL, but greater than or equal to the method detection limit. B Result is less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is less than the RL, but greater than or equal to the methoddetection limit. Inorganic Flags (Flag Column) A ICV,CCV,ICB,OCB,ISA,ISB,CRI,CRA,MRL: Instrument related QC exceed the upper or lower
control limits. * LCS, LCD, MD: Batch QC exceeds the upper or lower control limits. + MSA correlation coefficient is less than 0.995. 4 MS, MSD: The analyte present in the original sample is 4 times greater
than the matrix spike concentration; therefore, control limits are not applicable. E SD: Serial dilution exceeds the control limits. H MB, EB1, EB2, EB3: Batch QC is greater than reporting limit or had a
negative instrument reading lower than the absolute value of the reporting limit. N MS, MSD: Spike recovery exceeds the upper or lower control limits. Wf AS(GFAA) Post-digestion spike was outside 85-115% control limits. Organic Qualifiers (Q - Column)
Analyte was not detected at or above the stated limit. Compound not detected. Result is an estMiated value below the reporting limit or a tentatively identified compound (TIC). Result was qualitatively confirmed, but not quantified. Pesticide identification was confirmed by GC/MS. The chromatographic response resembles a typical fuel pattern. The chromatographic response does not resemble a typical fuel pattern. Result exceeded calibration range, secondary dilution required. AFCEE:Result is an estMiated value below the reporting limit or a tentatively identified compound (TIC)
B MB: Batch QC is greater than reporting limit. +- LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lower control limits.
EB1, EB2, EB3, M E : Batch QC is greater than reporting Limit A Concentration exceeds the instrument calibration range a Concentration is below the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not
obtained because the extract was diluted for analysis; also compounds analyzed at a dilution will be flagged with a D. H Alternate peak selection upon analytical review I Indicates the presence of an interfence, recovery is not calculated. M Manually integrated compound. P The lower of the two values is reported when the % difference between the results of two GC columns is
Page 31
QUA L ITY A SSU RA N CE M E THOD S RE FEREN CE S AN D N O TES Report Date: 07/29/2005
greater than 25%.
Abbreviations
AS Post Digestion Spike (GFAA Samples - See Note 1 below)
Batch Designation given to identify a specific extraction, digestion, preparation set, or analysis set
CAP Capillary Column CCB Continuing Calibration Blank
CCV Continuing Calibration Verification
CF Confirmation analysis of original
C1 Confirmation analysis of A1 or D1
C2 Confirmation analysis of A2 or D2
C3 Confirmation analysis of A3 or D3
CRA Low Level Standard Check - GFAA; Mercury
CRI Low Level Standard Check - ICP
CV Calilbration Verification Standard
Dil Fac Dilution Factor - Secondary dilution analysis
D1 Dilution 1
D2 Dilution 2
D3 Dilution 3
DLFac Detection Limit Factor
DSH Distilled Standard - High Level
DSL Distilled Standard - Low Level
DSM Distilled Standard - Medium Level
EB1 Extraction Blank 1
EB2 Extraction Blank 2
EB3 DI Blank
ELC Method Extracted LCS
ELD Method Extracted LCD
ICAL
Initial calibration
ICB Initial Calibration Blank
ICV Initial Calibration Verification
IDL Instrument Detection Limit
ISA Interference Check Sample A - ICAP
ISB Interference Check Sample B - ICAP
Job No. The first six digits of the sample ID which refers to a specific client, project and sample group
Lab ID An 8 number unique laboratory identification
LCD Laboratory Control Standard Duplicate
LCS Laboratory Control Standard with reagent grade water or a matrix free from the analyte of interest
MB Method Blank or (PB) Preparation Blank
MD Method Duplicate
MDL Method Detection Limit
MLE Medium Level Extraction Blank
MRL Method Reporting Limit Standard
MSA Method of Standard Additions
MS Matrix Spike
MSD Matrix Spike Duplicate
ND Not Detected
PREPF Preparation factor used by the Laboratory's Information Management System (LIMS)
PDS Post Digestion Spike (ICAP)
RA Re-analysis of original
A1 Re-analysis of D1
A2 Re-analysis of D2
A3 Re-analysis of D3
RD Re-extraction of dilution
RE Re-extraction of original
RC Re-extraction Confirmation
RL Reporting Limit
RPD Relative Percent Difference of duplicate (unrounded) analyses
RRF Relative Response Factor
RT Retention Time
Page 32
QUA L ITY A SSU RA N CE M E THO D S RE FEREN CE S AN D N O TES Report Date: 07/29/2005
RTW Retention Time Window Sample ID A 9 digit number unique for each sample, the first six digits are referred as the job number
SCB Seeded Control Blank SD Serial Dilution (Calculated when sample concentration exceeds 50 times the MDL) UCB Unseeded Control Blank SSV Second Source Verification Standard SLCS Solid Laboratory Control Standard(LCS) PHC pH Calibration Check LCSP pH Laboratory Control Sample LCDP pH Laboratory Control Sample Duplicate MDPH pH Sample Duplicate MDFP Flashpoint Sample Duplicate LCFP Flashpoint LCS G1 Gelex Check Standard Range 0-1 G2 Gelex Check Standard Range 1-10 G3 Gelex Check Standard Range 10-100 G4 Gelex Check Standard Range 100-1000 Note 1: The Post Spike Designation on Batch QC for GFAA is designated with an "S" added to the current abbreviation used. EX. LCS S=LCS Post Spike (GFAA); MSS=MS Post Spike (GFAA) Note 2: The MD calculates an absolute difference (A) when the sample concentration is less than 5 times the reporting limit. The control limit is represented as +/- the RL.
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