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A R B fc -0 5 6 ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, FC116, FC-126, FC-169, orFC-143. (Octanoic acid, pentadecafluoro-, ammonium salt, CAS # 3825-26-1) Remarks: 3M production lot number 390. The test sample is FC-126, a white powdery solid. It's purity was not sufficiently characterized, though current information indicates it is a mixture of 78 - 93% test substance and 7 - 22% C5, C6, and C7perfluoro analogue compounds. METHOD: Method: Not stated Type: Static acute GLP: No Year com pleted: 1987 Species: Pimephales promelas Supplier: Dale Fattig of Brady, Nebraska. A nalytical m onitoring: Temperature, pH and DO Exposure period: 96-hours S tatistical methods: Probit analysis Test fis h age: Not noted. Length and weight: Average length = 3.5 cm Average weight = 0.30 g Pretreatm ent: None. Test conditions: D ilution water: Carbon-filtered well water. D ilution water chem istry (initial): Temperature: 21 C Dissolved Oxygen: 9.3 ppm pH: 7.9 Stock and test solution preparation: Test solutions were created by direct weights addition. Concentrations dosing rate: Once S tability o f the test chemical solutions: Not noted Exposure vessels: 4 liter Pyrex glass beakers containing 3 liters test solution. Number o f replicates: two Number o f fish per replicate: 6 Loading rate: 0.60 g/L Number o f concentrations: five plus a blank control 003869 W ater chem istry during the study: Dissolved oxygen range (24 - 96 hours): 6.6 - 7.4 mg/L (control exposure) 5.6 - 6.6 mg/L (320 mg/L exposure)* pH range (24 - 96 hours): 7.7 - 7.9 (control exposure) 7.7 - 8.0 (320 mg/L exposure)* * 320 mg/L test group (third highest concentration) data given because total mortality occurred in the two higher test concentrations by 24 hours. Test tem perature (24 - 96 hours): 20C RESULTS Nominal concentrations: Bk control, 100, 180, 320, 560, and 1000 mg/L Element value: 96-hour LC50 = 301 (244 - 370) mg/L Element value based on nominal concentrations CONCLUSIONS The test sample 96-hour LC50for fathead minnow was determined to be 300 mg/L with a 95% Confidence Interval of 240 to 370 mg/L. Subm itter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY Reliability: Klimisch ranking 2. Testing meets the criteria for quality testing. However, sample purity was not properly characterized and it lacks analytical confirmation of test substance concentrations. REFERENCES This study was conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, Lab Request Number E1282-1, completed on May 1, 1987. OTHER Last changed: 5/24/00 003870 ENVIRONMENTAL LABORATORY FISH TO XIC ITY DATA SHEET DEFINITIVE (FULL-SCALE TEST) LRfr/S P S t-/ % T Y P E T E S T . ^ U ^ A > m P . ^ ^ ( L M A T F R I A I J - g T ^ ^ / r' - l g ^ ___________________ _ L 0 T J 9 % 3 TEST ORGANISH.E3i4Mrt*i H-/*1 f PMS O U R C E D A T E REC' D _ BATCH N O .V - f l V AfTlAOfjAVG. MT. orams AVG. S I Z E c m NO. ORGANISMS PER DOSE ? L OADING FACTQR/l,//i/0o/1 FISH DISEASE TREATMENT. ________________________________________________ ________ TEST SOLUTION V O L U M E ^ L IT E R S / A L L -G L A S S TANK TANK DIMENSIONS: 4 LITER PYREX&GLASS BEAKER TIME STARTED I Z / .m p v W DATE STARTED DATE COMPLETED, 2 AP I L U I I O N - V I A T E R C ^ R B O N - R L T E R E D VjELy^W ATER ( T E M P ____ C . , D . O . ^ - P p m , PH, f r 9 ) J Cto*v>l.so cok><0d 3Q\&M*-310)m^lL>IN V E S T IG A Iflg ^ ^ ^ ^ f e f ^ S ^ j ^ L C ^ t D S X CONFIDENCE L I M I T S ) ^ q f l f t Y l - ^ X W Tank I n i t i a l Total 24 Hours 48 Hou 'S _______72 Hom*s ______ 96 Houi'S N o . C o n e . Am ount T o t a l No. PH D . O . T o t a l N o . pH D . O . T o t a l N o . pH D . O . T o t a l Mo. pH D . O . mg/1 Added Dead ppm Dead ppm Dead ppm Dead ppm r CONTROL * * . * 3 1-1 I T ) P D| - f KAO 1 - 5 K ? n QlnCi ^1 - 4 p o | / p n o n a h /7 7.9 7.V 7,9 V ,/ 7ft ft. o kfi Iff o ... 7,ft 1 iff &. r> 1,1 ((h?i 1,1 left 6 o 1,1 fftf) 11 fa i oo 11 1 1 fa<0 4 h i (e,() / / 7 ) <P> (* '(<? \DD i 1 - 5 O , 5 n o o ? .o t2< o /<? is Test Temp. C I n it ia ls & Date*" ^ Co mme n t s : M .Q . ZD m &1* 1 a k j>U U iq Ia ^ z o z o ... . ft u v H f r s i f i i S f S A ^ ^ i i l ^ 'CTS ( O T H E R THAN M O R T A L I T Y ) Tank No. Symptoms o r Reactions 2 4 -H r. CONTROL r l-l 1-2) "Z1-*) 1 -4 - t'SCl iiSth --------------------- / \y i E C 5Q____________________________ T o t a l Numb e r A f f e c t e d 4 8 -H r. 72-Hr. , 9 6 -H r. y kj _ y ^\ 4 _ Ij Is J kA ^i l -- 1 ----------- -- ENVIRONMENTAL LABORATORY FISH TOXICITY DATA SHEET DEFINITIVE (FULL-SCALE TEST) LR_J=A?P i2 s-I * 0 - ( 2 inTYPE T E S T ^ n f r i f - M A T F rt A I^F S T ^n^ I _________________LOT, < 30 TEST ORG ANISM &LU^ SOURCE _ 3 V .$ I, DATE REC' D_ ^ / V / f f / BATCH AVG. WT./ 7 i > y j grams AVG. SIZE cm NO. ORGANISMS PER DOSE^ Z / LOADING FACTOR7,/^? a /I A p M F .FISH DISEASE TREATMENT,. ________________________________________ ____ TEST SOLUTION VOLUME.&J-ITERS/ALL-GLASS TANK TANK DIMENSIONS: 4 LITER PYREXGLASS BEAKER t ^ 9 hTIME STARTED I Z i m ^ D A T E STARTED. 4 -- DATE COMPLETED, . * y - ( - R ^ f DILUT^fllLJJAJER CARBON-FILTERED WELL WATEH (TEMP. C.. D.0._q,g> pom. pH * i. q ) INV E S T I G A I O f ^ i i ^ ^ ^ ^ ^ ^ i t 50(95% CONFIDENCE LIMITSL^L? Cc^cA^edkCso 3o| *q /u Tank I n i t i a l Total 24 Hours 1 48 Hours _______7 2 Horn" S ______ 96 Houi N o . C o n e . Amount T o t a l N o . pH D . O . T o t a l N o . pH D . O . T o t a l N o . pH D .O . T o t a l N o . pH D . O . mg/1 Added Dead ppm Dead ppm Dead ppm Dead ppm T r CONTROL .-1 1n n 7^>0 2 .- Z . . I S O , - ^ 4 0 Z r v ^ X 2 D QlnCi ^ - 4 KloT) \ldPf) l o o n risono o o n & (/) L> in Y,g, w i,L 1133 13 /PtS ,5 MX ^0 o o / W MO 11%,1 w (e l / Zj w Is 1s -- -- n i n (#{((? a o in fa,/ O / 73 faZt ! 1 7 Hite & > 1/ -- -- & in t f t*.z 77 H 5t(& -- -- --- iTest Temp. C ^-- I n i t i a l s & Dii t e 2 9 -fitZ A 1________ I I ~J -----. B T V -- Z _y m S O ___ I________ _______ < r r .'_ _ _ _g . y se M S ^ jr-z-S V l 3 ECTS (OTHER THAN M O RTALITY) Tank No. Symptoms o r Reactions S'I XLCONTROL Jb -Z SrxptrlciK^i Zs-'x*!rVl ' ^ScrptrtCfkvri , /2 4 - H r . A ,2 --5 T o t a l Numb e r A f f e c t e d /4 8 - H r . Aj 72-H r. I 96-Hr. V# \ 1 _____ cnrtH-7
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