Document XRaqMGyrrpRj7BQ10Z6RbxDQG
CG 0,1 CODE YE^98-D
to/?3J?82 < BATE )
_KS03 ( LOT )
552? LBS. ( EST UT >
PROCESSES < > YE-698-D (T)
APPROVED^ BYT FUP 10/15/82
CDMTYP JOB NAME: 01YE698DMT
EQUIP
MENT
NAME: MOLYBDATE ORANGE
1 USE 1
i ACCT
i LBS I N-CODE 1 LBS
l^H><6BTAIN SODIUM SULFATE FOR S-13 ! /I CALCULATE 6 SET ON BADGER METER FOR S-16 1 c 1 (NITRIC ACID WEAK) U-3"l OBTAIN SODIUM CHLORIDE FOR S~33 i JP'T OBTAIN SODA ASH FOR S-37 IX OBTAIN SODIUM SILICATE FOR S-39 [ in OE TA IN SODA ASH FOR S-43 Q'f l OBJ.ATN ANTIMONY TRIOXIBE FDR S-46
i S^TWEIGH SODIUM CHROMATE INTO V-351.
i 84 | 1 08-A
1 i 734 i 146 1 237 1 350 1 70
I 33-D | 4-A | 3~A 1 32-D | 3-A | 71 1 -B
\Sh I\ 10-D
i 84 i 1 60 ! 734 1 146 I 237 ! 350 1 70
I 1885
OPTP
WEIGH IN SODIUM MOLYBDATE
OPTR
M.K
OPTR
MK
MK _
LUIS^ T T~
zJ, 423-D
3.03-
RUN 10* (5QA 0) WATER INTO V--358
11^ RUN V-359 INTO V-351 & PUMP IN V-351
i1(2J--ADJ TO 55 V (2600 G)
| 4^>rSIFT IN M-108~A FROM, S
A
i^U-STIR 5 MIN & RECORD: PH_i_L_ (9.10.0)
!
i \*T\ ADJ TO PH 9.8-9.9 6 RECORD: PH,,_ifL
!
! | (CAUSTIC SODA SOLUTION)
ASSUME 50% | ___
|J
ASSUME 66%!__
ADD N-33-D FROM S` 2 USING BADGER METER
I
il/l ADJ TO 66 * (3125 G) AT v?-69*F *
[
t V- RECORD: V0L_.44_' &____J?'J*F
I
)18n STIR 5 MIN & RECORD: PBj3L4<7.4~7,.6> & I I G/ML i-Jtli.'krd .08G-1.083)
| I
I 1 NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK i
1 LIST & ATTACH. TAKE 1 QT SAMPLE
]
7~D 33-D
SV 1 RUN 20* (996 G> WATER INTO V~.j
!
5 | | RECORD N--41 -D STORAGE TANK TO FJJi3f FROM.
I L^CIRCLE ONE : 402 410 411 420 (A2A) 425
|20*T CHECK WITH CU SUPV;
i I STORAGE TANK MUST CONTAIN AT LEAST 2376
I GAL: 402-49' , 410-25*, 411-48*, 420=25*,
I i 424--25", 425--31 * ^STORAGE'TANK MUST HAVE STIRRED AT LEAST
[ i 20 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK' MUST BE ISOLATED UNTIL ALL "PUMPING FOR THIS BATCH IS COMPLETE
SET METER 'FOR 300 G '6 PUMP TO SV
OCT 28198?
|
,, DUP050103069
LOT; _ EQUIP I
MEMTI I
COtITYP JOB NAME: 01 YE698BMT PAGE &2
DATE PRINTEB:i0/15/32 I USE i N- IACCT I LBS | CODE | LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP-,
CHECK PH i, DENSITY* 'RECORD BELOW* IF NOT
IN RANGEjXSTQP PUMPING & SEE SUPV* * PH Jhj,, <2.2-4.?)
DENSITY:
G/ML <1.270-1*323)
IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD
DENSITY _4?Jt2rO/ML ON TRAPPED SAMPLE
M END OF S-21 PUMPING* '
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW* NOTE; TABLE
ACCOUNTS FORi300 G ALREADY PUMPED IN S-21*
CIRCLE DENSITY & SETTING IN TABLE BELOW.
##** TABLE ***
! 1 ----
-- -- -- -A _ ,, ...
M^ ^
^ ^ 7__. .
A
1 ! G/ML SETTING ( G/ML SETTING 1 G/ML SETTING I
1 i 1 * 270 1673
! 1 .291
1534
1 1*312 1410 |
! I 1*271
1670
1 1 .292 1527
! 1*313 1404 |
J ! 1 * 272 1663
1 1.293 1521
1 1*314 1399 i
1 1 1-273 1656 ! 1 .294 1515 1 1 .315 1394 |
! f 1.274
1649
! 1 *295
1509
! 1-316 1388 !
! f 1.275 1641
! 1 *296 1:503 ! 1 .317 1383 !
! ! 1-276 1634
i 1 *297
1 497
i 1*313 1378 1
1 1 1 * 277 1627
i 1*298 1490
! 1.319 1372 |
! ! 1*278 1620 1 1 .299 1 484 ! 1*320 1367 1
1 ! 1 * 279
1614
! 1 -300 1473
f 1.321
1362 {
1 f 1 * 280 1607
i 1 .301
1473
1 1*322 1357 |
1 1 1*281
1600
1 1 .302 1467 * ! 1*323 1351 f
i ! 1*282
1593
! ^*304?
11 1.324 1346 |
! f 1*283 1586
! TT334 I455T 1 1*325 1341 }
f 1 1*284
1580
f 1 *305 1449
( 1*326 1336 |
1 I 1 * 285 1573
1 1*306 1444
[ 1*327 1331 |
1 I 1*286 1566
( 1 * 307 1438
i 1 * 328 1326 1
I 1 1*286 1566
1 1 .307 1433
1 1*328 1326 j
1 ! 1*287
1559
1 1 .303
1 432
! 1*329
1543 |
! 1 1.283
1553
1 1 *309
1-427
! 1.330 1537 |
i f 1*289 1546
1 1 .310 1421
} 1.331
1532 1
f l
1 1^290
1540
1. 1*311
1415
! 1 * 332 1526 1
!
!1 ! 1
f I ! [ 1 ! 1 i 1 1 1 ! I 1 I 1 ! ! "1
f
1 1 l | 1 ! j 1 j ! i [
i
1 .1
) 1
f J
I i j f
!
I I FLUSH LINE WITH WATER INTO SV. FOR--APPROX IMATELY
! \S&rSEC 0 NDS
jvr'ay
126TADJ LEAD NITRATE TO 76**7O<J3662255-J-0I)? AT 67-69*F*
I r^SCORD: _
F ns"^>^iA7]
! 1
*1 \27Ts&K 5 MIN & RECORD TPHH; ZBiETte. 2-3*7)
! 2&*r EF NECESSARY ADJ-T PH 3*0-3.1
ASSUME 66"
{ 6 RECORD PH:
ASSUME SOX\
, ^ fH MfOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING!
..d 1291 RECORD:
_ G/ML <1 *143-1 * 144) IF OUT OF SPEC!
FILL OUT CHECK LIST & ATTACH*
j
STIR AT 67~6?*F FOR S-31 * TAKE 1 QT SAMPLE*
!
i i 41-D i 5110
57-A
\ DU P050103070
EftUlP MENT i
COMTYP JOB NAME: TYE698DMT PAGE 3
DATE PRINTED:10/j5/02
I USE | N~- IACCT
i LBS i CODE: I LBS,
-I________ i____
OBTAIN 1 ST SAMPLES OF S-18 & S~3 SOLUTIONS
6 TITRATE TWICE NOTIFY SUPV IF ML N-1-B IS NOT IN RANGE
I
!1
<r
7, 1-7*4 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN 0.1 ML N-1 -D (l'F YES, FLUSH ALL
I
EQUIPMENT G REPEAT TITRATIONS), DO NOT
1!
PROCEED IF N-10-D TITRATION IS OUT OF RANGE |
ADJUST V-358 FOR A TITRATION F'H OF ^,4.-T0 2,-2|
33-D
FROM flft&L IN-LINE TITRATIONTM RECORD LOWEST
|________i
1PH
6 ML N-iO-D
_v_Z* /,gp - /ffO
7-D
WHEN S-31 TITRATION OK , STRIKE V-358 THRU BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
16-18 MIN
t JCJ&
j 0"'
RECORD: START tl-P-lShX TOTAL MIN___ /_L_
NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
G BUBBLES APPEAR IN SIGHT GLASSES IMMEDIATELY DUMP IN N-4-A FROM S 3 6 SET TIMER
FOR 15 MINUTES DURING S 33, WASH IN V-358 & STIR 2 Mlfe & RECORD PPHH.____j_iJL{ 1 ,8-2,5)
^vf__4TT^t mu s t be + )
3><T STIR iOTAL OF 15 MIN FROM S~33 & RECORD- TEHP_._7J._sF (67-73F)
DUMP N-3-A FROM S-4
STIR 3 MIN POUR IN N-32-D FROM S-5
STIR 2 MIN RUN IN LIQUID ALUM USING BADGER METER STIR 3 MIN & FLUSH ALUM LINE WITH WATER
DUMP IN N-3 FROM S-6 St ir 4 MIN FOR S-4S
i I
734 ) 115-Di I' i
367
RUN IN HYDROCHLORIC ACID USING WEIGHTl, FLOW
[- _ i
.CONTROL PANEL
MK m_______ _________ %}_________ i
DURING S-44 SIFT N-7l 1 -B FROM S-7INTO V~39
|
|
i y WITH AGITATOR ON IN 1-2 MIN
I1
\vr S STIR 1-2 MIN TO MILKY SOLUTION
28-D 28-D
i-4S^<WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B SV
8 I t SOLUTION GRADUALLY OVER 5. MIN PERIOD INTO SV
| } WATCH FOAM'!! IF FOAMING IS EXCESSIVE, STOP
! 4- UNTIL FOAM SUBSIDES,
F*t O<DUMP ih BLANC FIXE N
4HEN/SCHEDjUkED, P|P IN /g\END
LIS/f&D O^X i
TOP OF f /a g X. 1
L vRE/CORF>JcODEV____ JSrf LOT
I5SXT*0j STIR 2 MIN
*
i 5SgTT^>R- ERECCOORRDD: PPHH_,,LA^.j__LJJlL_. << 55.,8-66,,)
15*'" LU*ITFF"'N^NNEEECCCEEESSSSSSAAARRYYY', AADJ TTOO-PPHH 5,*w88--6o,
ASSUME 5%
Ii y
& RECOORRDD:: PH-______ hZZZ.
ASSUME 66%
154 | FLOOD TO 153" (7298 G> 6 STOP AGITATOR
Ii !!
START
- FINISH^?
OPTR
__JEfC*________
! 128-AI 33
7-D] 33-D I
DUP050103071