Document XRZQa0zr5ZkK37XOY1DXG2nOG

ANALYTICAL REPORT FROATFOSAnsys [rp---- LS ANN) nT proedmiO cts i STL ---- IT-- 3N1DeACeanrac8g0LW7ao5net SeverTetLaboratoriSeTsL, Denver PGooeltDeMkaunzazgoer Vay, 3007 IE Ten DEp2soWe.au0sss CasDe NDarSraItive "MTahneuarles.ultAsllinrcelsuudltesdhianvtehibsereenpofrotuhnadvteobmeeeentraelvireewqeudirfeomrenctosmoplfiNanEcLeAwiCthantdheaLnaybeoxrcaetpotriyonQusaslirtynoted below. "sTphoinssorre.porDtislhatlolnnoatcbteorrseparnoddfuocoemdoetxecsephtavien efucllh, wpirtohvoiudtetdhaenwriatcthendaatpapsrhoeveatlo1ftahsesilsatnbortahteory or interpretation ofthe results `SampleArcival ndReceipt "The five water samples presented in this report was received at the STL Denver laboratory ata temperature of 46C on April 18, 2007. Standaras Analytical standards were prepared using the acid form ofthe compound perucrooctanoic acid (PFOA). PFOS i acommercial prepared and certified solution Ausdedicaascabnonien1t3emlaalbeslteadndpaerrdflourorqouoacnttaintoaiteiosncoif,P{F1,O2A-ia-n/dC]PwFOaSs,introduced at the extraction scp and was `Sample Extraction and Aualvsis LThceo0sanmzples presented n this report were analyzed fr th target nalyes by STL Denver's SOP DENFexotrrawcatteedr ussaimnpglseosld2p5h0asmeLexatlriaqcutoitoonfteecxhhnisqaum:pwliet:imaectihdaifnioeld cwointdhit| imonLedofC168N cHarCkrsdogleust.ioEnaacnhdstamsple hfsespainkaeldytweistshrcthceuitnetdemwailthst4anmdLa.rdo,fmpertihorantoole.xtrTachteionf.inaAvoflutmhee issabmrpoluegihstptaos5semdLthursoiungghmheethcaanroclidagned, the extrac is analyzed by LOMS/MS. MetOChSaompldes "sTahmepMleestohfotdheBlsaanmkeismpartoace.ssTedheremaegtehntodwaltaenkspwiaksednwoint-hdtseuerrtogatattehearnedpporrteipnagreldimwititfhoretahcehtbaartgceth f20 analytes. Ewaecrh bwiatchhiniessptraebplairsehdedwciotnhtrLoalbolrimaittos.ryDCuoenttroolliSmaimtepdlessam(pLlCeS)v.oTlhee,LnCoSmaretcroivxesrpiieksefsowebroethpeerfvorsmed. Because the LCS daa were in contol,noComective action wa necessary. A"TnhaelystuimcoalgaCtomremceonvetrsy for 1304 PFOS was below the ower control limit in th low level LCS in QC bach 7114515. Because the LCS recoveries are in control an the contol limits ace deft iis only, 20 comective action was necessary. No other anomalies were noted. STL Denver 2 DEP2.SDWB-000335 EXECUTIVE SUMMARY - Detection Highlights Dims0saz ehmaETER sur BIRCH CREEK BOB 04/17/07 08:25 001 vreoosn. cC0o0s6z7 `BIRCH CREEK WELL 6 04/17/07 08:20 002 pPrFoOsA. Cc0o0e2 a BIRCH CREEK WELL 4 04/17/07 08:45 003 PoFrOosA 00.00208213 DRRNT INLET 04/17/07 13:05 004 Pprroosn 00..0000564533 DREN? PE 04/17/07 13:05 005 eerroos 00.001008373 RLEaPOrRTING wuts o0.i00s0 uueg//LL o0.i01s0 vwaelnu 0o.l0s0 uugg//LL 00..00050 uugg//LL o0.l00s0 uugg//LL AwNeAmLeYoTnICAL DDEBN --1LLcc--00001122 DDEENN --11Lcc--00001122 DDEENN --LLcc--00001122 DDEENN --1Lcc--00001122 DDEENN --11Lcc--00001122 STL Denver 3 DEP2.SDWB-000336 METHODS SUMMARY Dpr6a3az enRETER AMNEATLHYOTDICAL Le/us/us, PFOA DBN -1c-0012 References: Den Severn Trent Laboratores, Denver, Facility Standard Operating Procedure. MPERTEHPOADRATION STL Denver 4 DEP2-SDWB-000337 METHOD / ANALYST SUMMARY Dimeesez AMNERTLHYOTDICAL munyST DEN -1c-0012 Mark Dymerski References: oe Severn Trent Laboratores, Denver, Facility Standard Operating Procedure. noasT n__ 0426 STL Denver 5 DEP2-SDWB-000338 SAMPLE SUMMARY Dmis03ez HO # SAMPLEM CLIENT SAMPLE ID JJTT66VVOL 000012 BBIIRRCCHH CCRREEEEKK WPEOELL 6 JJTTevv2s 000034 BDRIRRWCTHPCRDELEKTWELL 4 76s 005 DRRNTE PE HTooem(s): fo gsi oe ers 0OE A ossetedeeesgicl c en. Rtenttsot NOpweeeat e,td sieeehnalkesprof sy. uaenrrpee.vpiueyrers,er,expFroeeld,yw9gabi,ol, coar,ys, .syl,y.pinn,PeY.csk. g aSAtMePLED STAuMeE 0044//1177//0077 0088::2250 04/17/07 04/11/07 08:45 13:05 04/17/07 13:05 STL Denver, 6 DEP2.SDWB-000339 mexican Water Company Client Sample ID: BIRCH CREEK POR mic DLaotte-SaSmapmlpeled#......:: D0I4D/I1870/03742-0080:125 WDoartke ORredceeirve4d.....:: J0T4G/V1O8/L0A7A PPrreeppDBaattech..#....:: 0741/12415/1057 AAonaallyyssiiss DTaitne.e.:.: 0004:/5266/07 Dilution Factor: 1 Method.........: DEN -LC-0012 Matrix.........: WATER e=nETER Pron R0e.s0o0u6T7 5 0.062 RLEPrORTING mrts wn 0o.0s10 wwaasnt 00..00002301 `TsaucmsRoGpArToEn 130s eros PREECROCVEENRTY 700 RLaeucrorvsERY ((5500 -- 220000)) B1 SoTaEs(Se)n otmn STL Denver DEP2-SDWB-000340 American water Company Client Sample I: BIRCH CREEK WELL 6 pie LDaotte-SaSmapmplleed#......:: D0I4D/I1870/03742-0080:220 Work Date Order ...: Received..: JTEVILAA 04/18/07 PPrreepp DBaattcheB......:: 0741/12415/2057 Phaoaallyyssiiss DTaitmee....:: 0014:/0296/07 Dilution Factor: 1 Method.........: DEN -LG-0012 Matrix.........: WATER E=ARIAMETER ron R0e.s0o07r27 0.061 LREPrORTING mus er 0o.i01s0 uwgg//uL 00..0000301 `S1U3RaROGPAOTRE 134 2eOS REPCEROCVEENRTY 7n RLoEuCrOTVsERY ((5500 -- 2200001) noTE(S) SIL Denver 8 DEP2-SDWB-000341 mexican Water Company Client Sample I: BIRCH CREEK WELL 4 pic LDaotte-SaSammpplleed#....:: D073D/11070/30472-0080:345 WDoartke ORercdeeirve.d....:: JTEVZLAA 04/18/07 PPrreepp DBaattcheB......:: 0741/12415/1057 a`haalaylyssiissDaTitmee.. .:: 0014:/2226/07 Dilution Factor: 1 Method.........:DEN -LC-0012 Matrix.........: WATER P=RR3AETER eon. R0e.s0u0T2 3 0.029 RuEwPrOrRTING rts on 0o.l0o1t0s uugg//LL 00..00002301 `1s3ucmaRoGPaFTOEA 1304 PROS `sREERCCOEVNETRY 76s RLEoCwOeVsERY ((5500 -- 2200001) HoTR(S) + STL Denver s DEP2.SDWB-000342 American Water Company Clieat Sample ID: DRRWIP INLET ie LDoatt-eSaSmapmlepl4e..d.:.: D0I4D/I1870/30472-1030:405 WDoartke ORercdeeirve#d.....:: JTEVIIAA 04/18/07 PPrreepp DBaattcheA.....:. 0741/12415/1057 AAnnaallyyssiissDaTtien.e.:.: 0014:/3256/07 Dilution Factor: 1 Method.........: DEN -LC-0012 Mateix.........: WATER Prorsm.ETER Pron. R0E.S0U0L4T53 0.0054 3 RuEcPOtRTING oats wen vv.o01s0 wuaat 00..00002301 suTRacRsoaPaOTEA 1303 Pros PREECROCVEENRYT. 7os RLEicmoivtsERY ((5500 -- 2200007) BoTR(S) --- STL Denver 10 DEP2.SDWB-000343 mexican Water Company Client sample I: DRRWTP PE Hic LDoatt-eSaSammpplleed......:: D0I4D/I1670/30472-1030:505 WDaotrek ORredceeriv.e.d...:: JTGVALAA 03/18/07 PPrreepp DBaattec.h..B......:: 0741/12815/1057 a`haolaylyssiisaDaTtieme....:: 0041/:2467/07 Dilution Factor: 1 Mothod.........: DEN -LC-0012 Natrix.........: WATER =hR3AETER eon s0s.s0u0r473 0.0103 RuEPrORTING pnts wen 0o.l0s0 uwga//Lu 00..00002301 `TSaUcRsROGPAOTAE 1301 pr0S RpERCOCVEENRTY. oas RLEoCOrVeERY ((5500 -- 2200007) BoTR(S) WE STL Denver 1 DEP2.SDWB-000344 SAMPLES o01 002 003 008 00s QC DATA ASSOCIATION SUMMARY Dp1603az Sample Preparation and Analysis Control Numbers WATRIX AVMREATLHYOTDICAL WATER DEN -1C-0012 WATER DEN -1C-0012 WATER DEN -1C-0012 WATER DEN -LC-0012 WATER DEN -Lc-0012 BLAeTnCcHi 4 eBATdCH E 7110515 esis msis sis sis Ms ROME SIL Denver 12 DEP2.SDWB-000345 MCBlieLnott-SLaotmpl#.e..:#: Analysis Date..: Dilution Factor: PrornETER Pros sTaucRsRocParToen 130s eros oCTR(nS) pret io METHOD BLANK REPORT DRI7DD120400304020-515 04/26/07 1 mic Work Order #...: JVIEKIAA PPrreepp DBaattec.h..H......:: 07141/42511/507 Mateix.........: WATER Analysis Time..: 00:17 RweDsuT w wREPrORTING pers b0.o0r0s0 vwaaltt Dweenmo1o6-0012 oe -1c-0012 `PREERCCOEVNETRY 0& RLEiCmOrVsERY ((5500 -- 2200001) mie i olrs ld -- SIL Denver 13 DEP2.SDWB-000346 LABORNTORY CONTROL. SAPLE EVALUTION REPORT neice CIlCiSenLtotT-oSatmp#l.e.f.:: DRI7DD128400304020-515 Work Order ...: JVKEKIAC PPrreepp BDaattec.h........:: 0741/12415/1057 BAonaallyyssiiss DTaitme.e.:.: 0004:/3206/07 Dilution Factor: 1 Matrix.........: WATER PpreoEnTER Pros. PREECROCVEENRTY 1%200 RLEmCMOrVTEsRY ((09 -- 113200)0 DweETNHo-DLo-0017 DEN -Lc-00z `suRsocaTE T1a3c0s4 PPFROOSA REeRcoEvNeTry 2as RLEmCmOtVsERY ((5500 -+ 220000)) CwolroB(ss) :pera to enn 898 7 ed ens pmdrsompn STL Denver 14 DEP2.SDWB-000347 "LABORATORY CONTROL, SAMPLE DATA REBORT mic C1l0iSenLtot-LSoatmpl.e.h.:: RDI7DD126400304020-515 Work Order ...: JVKBKIAC PPrreepp DBaattec.h..#......:: 0741/12415/1057 AAnnaallyyssiiss DTaitme.e.:.: 0004:/3206/07 Dilution Factor: 1 Matrix.........: WATER PrRoRnANETER pros smpiokew MwEAoSnUtRED wits RPeEcRoCvEeNRTy MEmOD 00..220000 00..220800 uuga/lLL 15200 RDioNn --11.cC--00001122 `TsaucRsRoGpARTOEA. 1304 eF0S RpezcRCoEvNeTry 2cse RLEmCaOTVsERY 5(500 -- 2200000) CBhoToB(nS) :erred for od 0 9 pmdroscepress 70 ed en SIL Denver 15 DEP2.SDWB-000348 "LABORATORY CONTROL, SAMPLE EVALUATION REPORT pie C1l6iSeaLtot-LSoatmpfl.e..d:: DRI7DDI2S400304020-515 Work Order ...: JVKEKIAD PPrreeppDBaattec.h..#......:: 7041/12415/1057 AAnnaallyyssiiss TDaitre.e.:.: 0004:/4236/07 Dilution Factor: 1 Matrix.........: WATER PhemETER erroons RPEECROCVEENRTY E10a2 RLEiCIOTVsERY 0(39 -- 31200)) DeTEHNOD-.ro-00z DEN -nc-0012 `Ts3ucmasocparToEn 1304 PFOS PREERCCOEVNETRY 3are RLEICMOIVTESRY ((5500 -+ 220000)) NCooTbEo(5s) +perti re vt of rschide +kStaproteeaeevsecrymtspreossdce ws. STL Denver 16 DEP2.SDWB-000349 LABORATORY CONTROL. SAMPLE DATA REPORT pic LClCiSenLtot-lSoatmp#l.e.s.:: RDI7DD128400304020-515 Work Order #...: JVKEKLD PPrreepp DBaattec.h........:: 0741/12415/1057 ABnnaallyyssiiss DTaitme.e.:.: 0004:/4236/07 Dilution Factor: 1 Mateix.........: WATER PermonnETER Pros. mspoicweT - `MmEAoSwUTRED 00.00220000 o0.l0o2s035 Guts ReBERCCOEVNETRY METHOD aallit 1"02 DDEwN --1LCc--00001122 s1u3m0msooparToen 134 PrOS pERERCCOEVNETRY a56e BLcmowvzesRY ((5s0o -- 2200000) NCooTEn(S+)pres i odin 704ref ed o+Stpiireeaevecproy mstsctco es. SIL Denver 1 DEP2-SDWB-000350 411 dE Mi: eee HERS bE jl @L TES ell | Lx i si ! Lf ep | Jae 8) Ch! iE HI Rs Pl I `EB a FUE] | BF Alls bet LLTTTTRERRET [= ; et HHH # 3 83 | ER ed A re I en [TIT TT EEE [ee]| DOE pllox 5= Bi Ohii?e | 11] BBE EY NEE HHA i NHR | rJ FO gg NNb i FEE EE--9 i 3 + J ia EEE | 4 te 7 a mm ml Bad |b gf 82 Fl iF Li lobTey] | i zl 8 b r ORR . LC/MS Supporting Documentation Sample Sequence, Chromatograms/Mass Spectra Lot ID: DIn!v034L Client Poesican. Wakes Cougs Method: PFOA [PFos Associated Samples: [a Batch #(s): Tests sonionn_ QD bust 5.407 Irceeprrteisfeyntthsata,tcoompthleebteesatnodfamcycukrnaotwelecdogpey,otfhtehaettoarcighiendapladcaktaa.ge STL Denver 1 DEPZ.SDWB-000352 LC/MS SEMIVOLATILE ORGANIC EXTRACTION LOG SHEETS ppp afiho s 2 2 ss ze 2 ox EI x 5 vr i E i pik = = 3 =z =z =z =f sos os oz oz oa og | Fi i E FER FFFFPA E, OB Y s1 Pros torororop oy cede BEE i i 5s 5 5 5 5 5 8f F ii EF FEE i fr Eb trot 4 : SB: EiSiSi5 iiiTEei Co tub Bl a god 2 LE BIE : bg iE ui Ei Bl EERE iH Fool HlEfB &iBd te 4 : : Hl] foons By Ty pspf iiik Bi ge 8 LER LC/MS SEMIVOLATILE STANDARD DATA L mh fpssvevesei riea ev. eee. e . HFEHETHOF RHEEYRE 5gs gliiss2t 80 or | i: |g :: Hpeleg3 [30gSy . i a88% g22i s[EeEit : 5s3f iBR [iFf { 2g i| 2 3 ocr somamoss {3 gisE vsveE iraezeeeze H27IegNy (H2i62e38 i fHaEs H| p :: fBmi lg ix zz z izHg [HaEtY : iy |i 3 \ B. EY oersomone 3 Eo: AT) i: =5 : :: . : 3 ---- RRERRAE ; FE wa| JE By82 2% 38 & Bijee3e HEL |zz0 lg HH i (NR% vo iifi i \ | STLDe yer *x x 26 : errsonanss PPoo : iieees:eTTieces5 esSHeRisgD ETEe(RfH i.EB FHE h di730d i 2: |g Bl Be 3 2 |g 2 Po & :EN oliyer i J vg SR : i Eos i :: i # 8 3 :s ee $88 Lo.iEa paps g380l83 aigii Bt 8HN8%38 i (mee He |3x2%% 3E Eee [5zaal 2% sai Hi 5 =32 & : DESOWE.0003%1 3 2; 0 :R2IE : 3 : z zs 3 &: : : : : STL Denver 0%. s 3 Fer |nEER g =". *: i ie = 1 mB ELE = d=: S phHnGid F8R eI A % E8 |i 2 EI eo Cs # 83 =a 1h ml 5: of 888& Ty sae 3inoEEd ; 388 Ie 8 g 8 gs gc i. oF fH 253 = 2% i s: Er= "33. 13 883 FE i EH | 3E a8 3 5 3 zc 8 = 23 5il oy --8 % 3 4s & uy Tops =h =;3 =, Eg Pas or 3 ihe & 2 ers sows aosiz i CFEL C.os 3 B|;ieEdRR i: rssryal EB i,$ 1Bo1lakn' i] 11333 i: . io [iE g Eoggt 3 2] i3 P3 lasgz TciiEiig0 1 HSHpin 3 ssssel S:E3 H3 D 82 og3 g3 [aBRdE l2a3 i i 83 : EEE. ooo RC 3H.8E.0E 2 _ GEEEEE irl 3 8 dl ] 8 .3 woo Esi il i i5 at i | | ---- 0gi r-- bo i 3 e 3%. 8 3F [IER 5 0% EF FI 5 4 82 3 5 gE : J3 8 BEEsS e By, o! 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Dep2Sow s0nses FEO s 3F |3mERE i fry ii : a 3 [hE $ s35330 | Bolapee : Sas ich c [88 2 : BEM. 2 ig | 2e 88% Ef BEE EH taigof | HH | soo gl 5iisadg RES io: i Bc LE [|iEt $5 [sf FI 5eE[8 HH fide o.e.enfHlB 2 i= Lo BC LEEER 2 11 5#.8 {: i i25 Epizzfl STLDenver Z nZ 8 vep2soWBanssT ;) :3 3g = Bil*e i 3 BS Wood 2 sBi CL 8a gBeE 3 [i Lx8 "a 5 s .: o id e = jo 2B. aadsoa 3 1HdH 3 i :3 a] 5 Sit s 1 3 |3EE32 3gE |U 1xk 0% g LH fi 8 fe3%Flais 3 PPogooBds He (ak . 3 & [28% $5 [EE |i | m: oli s ofi i Hd s 3% 3 . g 3 stu enver ior ifd 8 5 Lo o8 EH gad i oe 3 ii f3 8 Dep2sowsauoses nl Holm , Es i Sa PEO gz 3 ii i5 F (13E33E0 - | S2 E(E17:0% : EOE8. Bo[ ona i f= =i oy [Brg 553338 } i 3 i8e HiI{ sss ! B2 EaaE Fos s r.... 35I |i 3s [28 32 |g2 e Ef g |i ooo3 i 2i3is: PcaEsBia+"Fs HI od a. al 282880 3 ii seine | |i 8 oepsomeamss 3 5 : 3 fF (meee | a : BoC Boy i : : Pid z y | 2 gg : I : PE g . a 382 3 1 3 i : Wt : tH Ha a . 3 & [22% d . iE : 5 i EH . i. 33 : HI PR i] i g ong 2 3 io 8% & & : ge 5Fr55 8y = *3 1 8 iE of gi i H gf 1 fit 3 _-- wg 2 DEP2.soWe.a0as7o ewe : 3F |3ERe i MEE 11H : Pg Be 5 pin s 3 ir : YE 3g 3 BEE Bl i ig i 2 g8 8 [332 % | Bf [3 i 2 2. 3233 JP 30% jadi i. fof EHiHiLLcH vse ol] LR E HE t B A sr a 2 [IER fgg Hf BE 5fo 152 woul 2 H iLo.iE.f Hoe ol Besssfl : tase A) i 32d i 8g 3 i: it Hd 12% Somer i DEP2.SoWe.a0es71 i et 33 5 3a F [3EEN = . 4 ER ET z |az0%2 g{ s s oa 1 |EEdf2 8 fg Hor 1 Ty fg t Gi . f 53 qi i |i Lb |B $s [EE a3 5 1 1% : aif gi : 3 Hol i#1 a3 33 & s & : STL Denver =1 s - HIbod 8 2 iwl | ; | *3 DEP2sowsaues72 I> ee mn am gs 3 F |33938 5 a IB 3 ii: : aso EF [220% i ii - HE 2 EE W ie F 5 3 | gf {| EE Eg Boas 8 BIaOil.l 825330 ss55sfy Foy iflogi To 3s (888% g|82R3 g (iE |B i 1H IB Ls :a 2EB EE.6E ..8 is S20i2z0ioli Eisiig ii Bf = 3 2 8% 2 i3 istBiaf Foi | i DEP2.soWe.a00s7s i 2 z isdo % : 33% 1(HEER 8 ii; E |an't 00 : 8 : @ Pe k3i 8 LI i 8% Py Bg Bsf o3l(eE888 iF I % s : : g |88 3 [22 i HH COBH | z i8 2 z 5 ': iLI S iEssid : HIE 3 v | z: : $ 3 #15 Demver B5.y z Ie iof g iho H3o : 4fn hi 2 nd2 8 Jr---- , TWT EE... If [EE : as BLE ox on 08 70 3 i iit B : Eg sail HU i Ef : F [HL a JE HEIL FE Be : ECEoiiif 2 w38f = (23[s%eg 3% E355a 55C55 5B 8 HE ii8 IB Cogs |IB2 tf 338% [jiE 2iES oooofl 8 5d 3 Ll 3E.3H,T| S REEZEH 2 rieiify al --_ 1 i i | STL Denver i 2s8 oepsomeams ;i ; 3g : sRy [TEgY : 3 5 : EB olooo's o |BEz 2 i : in ga HE 2; 33 ST 38 [5388%% VOR g if 8 Ls sg Ba af 3 , p& 3 3s 388% [H [28 s .s :. Biode. z i sp g od 8 3 i3 i3 ii B8 od i3 oii i hi i3 z 3: ia : 8 i L308 oii i pl i i1i 7 DEP2.sowe.aues7s ii EaiE . 3 381% L|Ei 5 se iE g: F RasdTsl & 2BofUeixet2 ii :8. Bf A crea Hs Pon380 d= HHHi L 5550 af) fd Ltaaagne B5f ii HE eessl] Ga2iagl 1 SHE 5 Tog2 ERR8 gz i 23[IFEH i F is8 al 8:7 SE i | 3 8 DEPz.SOWB.000377 i3 i i 0:% - 3::% H|3EdE3 gi x 2Ey RK 3= E olaaggtt zi .3 = 2 3. =2 g |uEFff TE fe ef ly CE iCy3 Ee : , gfio [BER & & B #2 3 =1 A 3 gh HH | i oF " 2 STL Denver 2 e3 .: =: i %o: i 2;i 3! 3 = : LowE = i 3 ; "3 Dep2Sow .s00s7s ia 3 i STL Denver mE PRR ProI i33d3l33e8 .si 22 3 E| . Si 3 3F $i 730! 3 3 58 z 1 720 2= 8 iBo. 5 i3 FfF 1380 zs > B 8 HEoz HM i ez se : | & 5 |8g 3 iL l 2 E seo z |i x# 3 s |i gf |g 8 Xie ould 2 cb 5 IEE Bla -- :& 3 | iif itf < td 22 g | |i { I a DEP SOWB-000375 : > Ly ; . J y (Tg 5 5 33 3i ;5 oo+] HPEHEI] BC ki | EH z = 5 FEY : LE. Ls $ 3 y s +1 | gor = : *i#d5 2 : HI. Boz [228 . 30 [EER * gs |B (88 iE g3 =F8:3 :i 5E go: 2 s 1: STL Denver E:3 e pool, HE 3 oz iHoo : i 8 3 if i3 . & a3 8 oersowB000380 i 3 mmm.. : : 3F #1 35232 ih ig H53@ 3E138E H 2Boi Etf R&B. ~ i 23f 1 gd : ss . _-- Pg Hg iin esses 3 Hi gz [13 8 :& EHIIE a EERE 3 siziz pl 7! |88 Esio! iil | STL Denver i 3 8 DEP2.SOWB 000381 i $y ge 3 [EE : x : i 3 ie Jz 3 if ict |a00%2 sits ; [882 3 i om Pt { : a gl 1d 330 Thy EEF lass HE ice Poy is a3 3 aie 3 3 [333 jot no = +3L3i > He ot o|2z3 +3 35g |i55% 7% : aff : 1. 3g iE a # al iL z il FEE tf B38 : Is gt Is 5 58% ol H33y :' i3 ii} $ 2 LB3 OoeR a8rd 3 i ve HH | 7 8 veresownonsez i |RHE p 3 ITF [|3EESp32 2 Frege 3 [5h B mod i a pai $ TI3F3E . 2 l3pe : SE ? i3 i 82 8% a HERE EHi IB BseidizcihEl pl: 81 4 |3gB g3e 3%& Lo oe iJERt . 22gsf El gfHERR a8 Ping. fe1. lg |i B3olg 13 siiiff|: qil g fies 8 3 i; 3: 8: : : Ho. 33 : s3 Byoc Pe I .% 3iE H[EiEN PH sPolEHE: fr I HY a Bed 8 gy 3i : Bod md sf i gi" 1 3 : al iL, # 3 i it fil 33 83 2 z ji t $0 Denes 253 e : iz i iL Boe 3%33 i @ dir : EE 8 oepasomos : -- Ls 37 [EIR 3 ; es |E "33 p|icge : YTE Blaze' ii 233330 tid. g ff ty & i 2 . Bos 3 siii.ieg g LiqoPfE o(3 iB82d5 gSrEiipieilgl Ho fl Lg (BRR 5555508 xt. F388 i PapI [iEEE.IN 85 hs CLFEEE ooo fl 2] i: BHiEM| b----5Ji | 1 8 - ul FEES 3 3 asi i I 7% oer?owe000385 i; 53 Lk 5 F3i [HEEeE EN si 5 | Bgt : .: cBrGe gByorEF oRjasa ld ia I bg ee : #2 if E i 3. s 35 ji : Bo: a! rT it ol 4 z i2 z i Fe gi i3 3} 5 Sift : mC ii g i& i gs erasonmonts > z g s 3F |3EERE i Hie SERN i= if i HE El : EE8R [EL 8:3 : sit Mo---- 8 [B88 f EEaExElE Ao [Ra3 5 (E3g83 3 GSirEi8sgel , WoULpE ot 55558 i$ 88 [8% 33 ! EE. nea 2 |i 5W3oodz iSEERR.E --__* i3 g3 i- aiey i13l Eesisp | StL Denver |i DEp2sows.aucse? i o i 33 3 33FEhiR s z : o iy 3 |S rt 2g 1 jE i 5$ d=; I] : : ;:, o : a,3 oggif [and a BPTOL : oda o 33 38 _ 3 3 [88& 3 =T=e4 ahfe o foEmnEis i . 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RB EsEEa.bEHle GEREER : 3iziEf flfe al gif 3g = ---- 3: & 8 JE "22 nerrsowRaomes { i IRE i 3 : i if ii :: Ee: LH 3 ; ul! : Ie by Bg : i go 1 |3 # Ho1 1s pit ' 3 . is i gy s s 3 |i 2 ] i 2: is i z 1= i3 : al si 3 5Ho} fiiyt #5 zener : BoC s: =} : z 5 3 1&1 3 Hl i i i5 7 odi i oh PELE x EEE 5 3F |3mE3R i BI ig sisalHo Bg ol2 t35 3 Gasish 3 [38s 2 2 L3E%E I3 83 1[35258 % EERE I 1 fg ul Bs 3 HEB 25k3af 555558 HE CLE |B x8 ge i s3 BsafEflE.= 5i i|E h3ag. EK SPEIER : 2rzzsl 8 1%: jl iH #0 toner i of a nerzsowaconin Po 1 1H 5 s . i 2 < 8 a 4 8 33 8: fa i iz & :3 H 1 fi 3 of [358 SF 3 388% i 3 Hi] ; Bs PE 5 : H if : Wo. fi 1 8 i3 ig i2 il t 14 3 i 1 omy B : oi f33 8 = i8 i : Loe od 8: I 3 i1 0 7 Jrp---- :i irer] | EEFR 1: HPiEdE. wi :ob [(aH:E fo - [CE EE | 1} |g a al 1 fi HisiElel0 =ii3 i[22% sss sf is : fl: 8 EEQ folie i BB oof 2 3 23:i8s.i:i0f Se i F0i30s8EEfE | iis a zesiEl | J wki oepsomeannios LC/MS SEMIVOLATILE SAMPLE DATA DEP2-SOWE-000404 `SampleListReport Masslyn4s.1 `LSaasmtpMloedLiiisedt: CF:rMidaays,sALpyrrX27P,F2O0A07PR1O0S:a20m0p8lMeoDuBn\taaiTndD2ay5i(g)htSPTLime Printed: Friday, Apr 27, 2007 10:24:00 MountainDayightTimo. Page tof2 Page positon (1,1) FlloName SampleID FileText SampleType PFOAVgILorky APFOpglorkg Botte 12 ppEaIraassn $$33770912 B0a2nskt BSluanrdkard 002 00208 1i14sA 34 ppaTreaassees 2233779943 0T5poekl SSaunnddaarrd 01 5 o1s08210 11110 57 ppprnaanarasszsoe0rss 25s22333777999567 2SO4up0gks SSStauannndddaaarrrdd 2510 25120040m151 TH2EE8 89130 pppaavserzss0oes 2523337779991870 2B2a0nppkekicv aSBlucannkdar 2020 2020080221 11122A88 i1t2 ppRsIRiSH 8S2233779035 20uS9ykgLCROLVY aacc 02 s 02502802 1HgE 1143 PPAISEIS NNKKEEKKIIAAGA RRITDDZ2AOO00000SS115S LNCBS QBlCank 010 ofart 778A 1185 p PIAE NNKOEVKOIVAAD DR7IDD2I4B000N0Z00501]8 LCS QACnaie 010 010411 117780 1178 PpOIIGSSM SJTOOVV2IIAAAA DDIIDDIIS0OMMZZ0OG023 AAmmaabiiee OO 00 7 7E 2100 p p7T0 JSTOOVVAIIAAAA DDIIDDIISSOOMAZZO00085 AAnvaaiise 00 oo 188A8 22213 pppvoRarIzseGesSs 9$22333777000142 0BTau2ngykonCOV Boalccark 0012 00120018 a T1A0 225 ppre5ss5e 2233779934 OTpSokL aacc 01 s 0150210 1+115 2227 ppprrr2assseesr 955222333777999875 S21wb0ooykke aaaccc 52 1 522005 TjerEd 041 124 20 porases 23798 hon ac Ed 20821 128 STL Denver 72 DEP2-SDWB-000405. `SampleListReport Masslyn4x1 L`aSsamtpMloedLiifsetd.: CFrMidaasy,sALpyrn27P,F2O0A07P1R0O2S0a0m8pMloeunDtBa7in4D2a5y(ig)htSPTLime Printed: FaAdora27,y20,07 1024:00Mountain Daysght Time Extactml 11000000000000 11000000000000 1000000000000 7000000000000000000 01100000000000000000 555000000000000000000 55000000000000 5S5000000000000000000 111..000000000000000000 11000000000000 11000000000000 11.000000000000 SamplemLorg 010.00000000000 11.000000000000 11..000000000000 111..000000000000000000 111.000000000000000000 222555000000000000000000000 224506000000000000 2225503100000000000000000 111...000000000000000000 11..000000000000 11..000000000000 11..000000000000 Dilution InjectVolumeMS Tune Flle Inlet Fle 01000000000000 2200000000000000 PPFFOOAA pPrFoOsA 11000000000000 2200000000000000 PPFFOOAA PPFFOOAA 11000000000000 2200000000000000 PPFFOOAA PPFFOOAA 111000000000000000000 222000000000000000000000 PPPFFFOOOAAA PPPFFFOOOAAA 1T10O0000000000000000 222000000000000000000000 PPPFFFOOOAAA PPPFFFOOOAAA 111000000000000000000 20200000000000000000000 PPPFFFOOOAAA PPPFFFOOOAAA 11000000000000 2200000000000000 PPFFOOAA PPFFOOAA 111000000000000000000 2Z2000000000000000000000 PPPFFFOOOAAA PPPFFFOOOAAA 17100000000000000000 222000000000000000000000 PPPFFFOOOAAA PPPFFFOOOAAA 11000000000000 2200000000000000 PPFFOOAA PPFFOOAA 11000000000000 2200000000000000 PPFFOOAA PPFFOOAA 11000000000000 2200000000000000 PPFFOOAA PPFFOOAA MS Filo PPrFoOAASS PPFFOOAASS PPFFOOAASS PPPFFFOOOAAASSS PPFPFOFOAOA'ASSS PPPFFFOOOAAASSS PPFFOOAASS PPPFFFOOOAAASSS PPPFFFOOOAAASSS PPFFOOAA'SS PPFFOOAAZSS PPFFOOARTSS Page20r2 Page Postion 2, 1) STL Denver 73 DEP2-SDWB-000406. H ER z E"HIG H= eHEmAR marramr5 rnnrmne RB32i32 8s fRSiEpSminEasmEaiiiianciiiniaigtaaEdsiatniiinittiinigny 8e3ni8f3l3 is3f glEEEEcEga aRR eA gT gE eRERsRtg see 3 | iii; 38g5 2t Hi 2 5H 8 EEH EE THES5H 8S 8 H HsEel 5F2R8C, habia 31 21111 Abd bbb 85Sx%ig 15i3PTi333993IREEEILEREEEM gi PERS TR geEgsiTzrti gHiie PHEPTTTOIHIR Ed 5888887 5773888EF8Fs8E8R7g 255 Bo, 3L%E 58% 2 i=sf 383533 2% 8oo [u0c% g Eggies 88 88s EN EETIEEETT.EEREI Bftagy grgpiisiabsd 383358 EE39EIo2ESR 8888583 83%38TTEERES gsgsssy f EE:REREEEEEE| BNERnuuy ERIE3AILH ssEEEs EER 5EiEe 3REIEISEiRE: BEEIRil J 523333 2333833332838 3283553 Bf sRRiRfiiBagegsRiiRRaiEtEe EgliiiaisIiiiincibiisizef EH i | | | E5533 EieanEiseis Egsanesy SHNEHHEE EHH] TN N IRIE ITI gf 3 "iSs nerzsowasonr t3 iA REACT 0 z SyBusEyEssIsSHsBssHysHsHssNasNsNsvHNaNsIengas yp |zEEse | BE bf 2 | 2 EL nl NEE EEE EE 3 BE z86z2 = 552 3 2 i| i oT8 | 1 3 | if 2 1 : i vee sowa.conute  Rng oH ; OB c s7ess i Hii g Bin 3i SGiEsIsTsRsEsBssEsIsRsNsIaasanapsnaTaogLgsRsRnngn8i3y aFhER |7ER3E ii 2 gf t8o% 2 sE m s88S88885s EE 53H%EHEcssE g sE ssE nsssHsaEsLh oB38E nk E ist ad PS TTTTITTIIIT III Et Sp si anngdBiC a= BzEEsdfirse PHETHIE 888888888 3238898888 | i5o2:3 y EN 858 Ig= 2 gg = 88 ii Eispegs : HEHE THIN | S53ESuE Bistigy 282558 5555555 sEuEsIEsvsld frpptisdefzd BRREsiiiaii: 555555555885 RIVES Bi28isy gigze3eg 885 ETg E 33385%E IRTIFiFEENE: BEEsEal 3333333 3333535383833 5533333 ERS BRE RSRIS IRa IE8 EEa RE] SEES REEEERIEiE sey geEEEIE SEREEREREIED fRERREEH on odie 83 si fziiiei 7 | ot erssows 00s 3 em. 5 |agE3e {HHH| i EEEEEE EEEEE ERELEE EE z * i i 3 EF 2 S |&E5 =R% 5 2 ' nLnEdE 2 BB 50338.2 EF5H82 3 FH | STL Denver nii DEP2.SDWB.000410 i]EERSTEBl 07370 (TEER i pRruytiaauariIaNnteBisisiiasisiiiifseiiisieiefsieisisieonlll f30oi0i0Sr2 118ig nndo iEO H [REERERRRTEH RGERREECCIH EERRNEEEY [R EH E EEE E EE E EI SSESESS8853533 ssssssssssssl sue RLRNEEEEE hE ss mECE anpe 28 2 & [and 2 233 3 333 SegseflEsyIzIa: sor Essa n IN SAU HHA Hgeeggieatn: e i| rE & HHH BBBRBRRRERIFIIERRERLRTLLLILLLER iitEe = 515585 2 Bg = if SHH CR PP PP TT ITEP EE TILE | EiiyasisniioipiiEEbiiiacy 5882858838939 5835558855588889 Eiifcgiiiiiizaninaiiinaniiil EENIBSBERZBSaBEINIBIERREEENH onoigpsizfanzeyasesenireissaiins g seresomBmtt Ti = EE s |mpEae |3Eggt 2: 2 nid Selis ey 3i |[4RE8E 3 3 SERNSENNSSNNNNNNANNANNNIIaNatl CEEEEETETILIIEERIqIIIIIs l2ig: |qoe t 3 BS 558 338383%2 7 ggegd z 22 f 52 3 gg 2 57 S70 Dever | I| | we DEPZ.SDWB-000412 i EE [ep se 02000 2732 z : BW fisic |TITEe 2 $ SPU3S33E33R33O30N3ET aIR EiiIiaESieiIfss5 vfaiE nisfE einsE flll B00] GofER 23 zao'f i2 [RRiRiEiRSGfRiAsRiRiRsOiRgEsRaEnRdAiGaAgRsEaRgEaNgNcNaNcLlY os3gsigy i|33ff PITTEIINEER5EARNIANANAsNsA5A8IsA, p53n PUSRRERgpERRar turaRrinETg|rR=eapvs FERRI RR a 3sReErZ -I ccpR-gCgg0gRgC SzIz0 EaRr0 eRr0 REsoss5oer 2158;8 BREE BEE ig 0888% 22 g15e5"3 Ji5805g HgHee PHU 888888808) FasEsesprerery ep 35 8 ` ii 3B35o5n5-8o8o 8= B2z8 wEeFn sBB338o8m8u8o8o | S3E5S5% BEESIEEN SE% ERIE Exiigey frusunaf igd B933922.f i2gfs t2352k25 548 38383%4 $8%558F 5553888F 88% FEES TEM SES3REE SREGERNI BEE EIRINEG 5353533 3isiizss 533 5583333 CLR Ey BSorcmE-0cgc:0 EocEoFcoEo3cEoogee0 Bi sown FBeUaIwEnR-EoGoIoMl STL Das @EgR3E 8 38 s8 BpEigsd 3 80 3 DEP2-SOWB-000413  SREee Eros [20030 i 33333053 33S3SSSSSSNONILIM 8 1 ERE 38% & :| s88aS d2 E 588828 = 22i8 532 Bo: 3 HH | DEp2soWe.au0sts :rE dE asR e 2it7a379 |2EE3P Bie i |BREGROERRRUNRRERERIIRRALNIELIL i sf sPEsIsEIsIsEsIsEsIa1 InaaEaE pLEL5E3nIA AnA AtAA NsAslsB pf52 & g 0[S83% 82 Bef 2 g2 PPEiEigRfresIIIAAnIERILLSNSIIIg 8HH] BEERESSE 25% x BH 8888888E8 rrg y 3388FR3%83Fsgsseee 55 = iF8 HHH HHL | S583 SEBECESNESERECEEEREREES Ergifiiiizaannpepifiptifgiigy | iisiigeiscuifsgiEcssccsszbig 5858558558855 855355585888888% fiat iit 833d 28828 8B E382 EREERERAY sm oapRisitrarsssiyssenteazeisnisy wg oepsomeannis z REE THi EEiHThES :F sySriyssasstgssssssssL ssssisaol 32 C2RESH i LERRERSRRREEERRAEERRRREIRIREY B) ii i HE uae53: lz H[5H52 l|ie82 3 # IE i oer2sonsoomis Poppet z o 8 5i SiEg eH pet 1 : of 28 :3 38 3 2 )1& PpitE .3 Sx sti. Denver 17% Bos LE .i 3 . 3 daB : yd : Bot gj Ea) 2: 2 wif 823 3 HI =F i a 3 LC i i 5= 28 23 1: Hd :3 Jd 05 goat 2 5i S43 8h 2 %: z SF L.F 8 OLE aif i-- =H : 1: [iBtEF |i: 7 wd DeSOWP0002417 i HER =f } BE 0 ERI 3 CASE . s 3F 238 i eon E 7 [ET = BEE PA cd HEhl FI : see Lol. THE Hof PI1 308 8 FEE & 3 2 3:-ii. agd.8 = 3 333m 2 HE 5 fg: 58 3 ; i 8 oersomone }i eo 8 ;Foe% E30 T[EEER iE 3 | 3: : Eggst : aoc Bop ih :: ailed : FI MPEgN fg F53E2 [889 3 85: }3 x8; 3F8 |i(35 5 g. i s &z 3 3 EF i es i uf si : i S o$v l 3 . 5 3 & & | :: H_-- Fy Bs :PooBotf wf [ST : i 3 ii :g 3E33E3E30 HB IolT3ae0'3 Ee d. NBodfosld {| 8 i 88 = bsaiil o Eos dd iil HE Hi He NH 5555s] Bl . 3% |B 2 g i ji % fd E asf K ERsLa sl 8 5i 57 5: 2: Beg| + iHnid rrEddh : STL Denver 03 a nerrsowaaoni i: Se RSIS SN3PIOUIE BONyh+ $ SFR ab Bolaet : JdFi moJhue wo:PiE i BES gIoaA Ii g |iEE aLPO -| : fio E et : : i 3. R2 IE % BI is 8 35 |i 3 29 :3 o [33 : 2J : ta3 f 58 838 g i |: I: af FL i| : i3 z --% 8Ig 7 : 3 2 . gs 3 3 s sh . 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