Document XR6rxvqaLVMdqmb99OJY5oYGK

COMPANY/MYTON LABORATORY/MYTON# 0HI04MOT ESC/DAYTON (Department/Sactlon I ANALYTICAL (Type of Report) REPORT NO.: MDA-47C RECEIVED JOB'PROJECT NO.: 484.4090 DATE: 4 May 1984 PERIOD COVERED: MAY 9 botfO0M#S*A*.MTO COWri*- * j T ,,OU* TITLE: ANALYSIS OP DELAWARE RIVER PLANT SAMPLES AUTHORS: J. A. Giuft' F. D. Hilemanw B. M. Hughe ABSTRACT: Water and sludge samples from the Delaware River plant were analyzed (or specified chemical compounds. The research of these analyses are shown in this repor^. TECHNICAL APPROVAL: Broo br Resea Croup Leader APPROVED BY: A t~ * 4" -- R. r. Ivory Environmental Sci.nc. C.ntar Service Project Manager ( < S: ii I* I APPROVAL DATE: RESTRICTED DISTRIBUTION! (aee over) COMPANY CONFIDENTIAL Tfcla NacHHitt ia tfca at Naeaaata fnafiiny aa4 tk rKlpint ia rtapanalblt far ita aafakaepiaf aad Niapaaltiael It aattalaa caNflMMial ' nPORKlTIOM .hick act act bt rykinf. revealed t. eneetkeriied pereone ar ant eeteld. TT-fTT'-'.'-;'''-- m HONS 022916 TMLS 2. CMKMtntlH a# Aractar 1242 POA-Wall aa.laa m tn. AMamta ad OC Prajact Nat M4.4MII Data! March 7.1784 Araclar 1248 Canaanar NuiMr IS 1* 17 IB It 20 21 22 22 24 29 IM 27 2S AvirtM AI248 Cancantratlan (ua/a) ESC Extraetlai* Hathad Saarla Aat axtract.d It) iNtnel Dilution ESC Extract Na. Pracaaa Flit Naa. TABLE PILE NOI C40F1B SAMPLE IDENTIFICATION FOA-Nall Cantrlfuaad Art A1248 Cane. - 1087 1109 - - - - - - - " .030 .036 - - .043 PDA-Woll Not Area A1248 Cane. (ua/a) 82104 170902 202477 28899 149696 110224 90384 42474 71616 44083 108029 39087 89343 .76 7.76 6.61 11.77 7.98 8.49 8.99 11.67 12.42 10.89 11.69 11.09 16.84 19.67 10.88 ArtcUf 1248 STD <lu*/l> Ar#* 10494 21977 30634 2496 19212 13071 9629 9641 9768 4070 7288 2777 9306 4171 PCEX02 10 Itl PCB992 BP227 PCEX02 10 Itl FCB991 BP226 PCEX02 - Ml 81248 IP228 13 HONS 022932 DETAILED EXPLANATION OF t M effort ta (IrtUllM MNfti HMrM kr (DC m PCS* NM*t l l KIN varlatv *f MttrUli. utlna nUt nrlitr af tackntuua*. Extraction MIMO ISENsI m< NMrl DmItiIi MIlltN (DAN*I hava Nn Nvllml Ktileti can ha llr l>lrfad vlth MCh ether. An iMrivltM far* af the*a SEN* an* SAN* kava kaan iltrtd an tha Hawlatt-Packarf 3337-LAS lakaratorv autanatlan *v*tan wa* kr ESC. In a affarl ca*wiilca(a thaaa fatal!* aalth cuatanar* af ESC. thl* infornatlan la *urrllaf with aach PCS nalvtl*. Hawavar. nanv rraJact* Invalva a vary taall nunkar af malai which ara net MHiurlW tha aaata natrlx. Tharafara. naJar infarnatlan an tha technical fatal I* af an analvcl* ara rraiantaf In tabular farn within tka aana takla which rarart* tha fata. Each takla Inclufe* a aanaral tltla. ESC Project Nunkar anf Data an which tha takla wa* aanarataf. Tha *aarla ifant IfIcatlan I* tha cu*tanar Ifantlflcatian which wat an tha *aar1a battla. Tha naxt (action af tha takla alva* racwlta far tha aartlcwlar analvta llataf. Far Araclar farnolatlan*. tha famlatlan 1* Ifantlflaf althyr vlauallv ar fran ESC favalaraf fata analrtl* araaran*. Tha cancantratlan af tha (emulation 1* calculate* Iran tha avaraaa valua af tha Araclar farnulatlan. bataf warn tha analral* f a nwnkar af ACS art. Tha nunkar af liwari utaf in thl* calculation I* aIvan *No. of Valua** anf tha rana# af Araclar cancantratlan* for thl* nunbor of PCS l*oaor* I* olvan kr Thl of Valua**. Tha (tanfarf faviatlan *nf X ralatlva *tanfarf favlatlan far thl* nunkar af fatarnlnatlon* of tha Araclar farnulatlan ara Ivan In tha fallawln* two Una* af tha takla*. Tha naxt *actlan af tha takla faal* with oualltv control u*af In aach aarla analral*. Tha *urro*ata orlhln* canrounf which I* affaf to tho *aorlo kaforo extraction anf analv*i* I* ll*taf. alano with It* Mount anf X Aacavarv uraf far aach *nrla. In ca*a* whara PCS cancantratlan* ara vary hl*h anf thu* ranulra extract fllutlon. no effort I* nafa ta nuanttfr thl* canpaunf. Thl* caulf ba fan* If ESC know* that thl* fata 1* Inrortant. but tvAlcallv 30 ua/* I* tha Inrortant Iaval ta nuantlfv accuratalv that turraaata fata far cancantratlan* lamer than thl* valua. fran a raoulatarv tanfraint. ara not Inrortant. Tha naxt *actian facunant* haw aach oanrla wa* axtractaf anf analrsaf. Tha ESC Extraction Natkof. anaunt af *Mrla axtractaf. extract final valuna. extract fllutlan factor. ESC extract nunkar anf tka canrutar fata file in kick tha rraca**af fata I* ttoraf are olvan in thl* (action. Tha lat action *lvo* a brief faocrlrtlan of abbreviation* ar alva* anv faatnata* that *lvo affitlanal Infarnatlan about oraclflc anrla*. Thl* takla farnat I* bath canract anf rractaa. It wa* favalaraf in an ttaart ta awlcklv anf accuratalv aanarata fata which tha ewatanar can nulcklv anf accuratalv avaluata. If tkara are anv *uaoa*tlan* cancarnlna thl* farnat. rlaa*a c*ntact no at axtantlan 396. DESCRIPTION STORED IN TDEXOIIIW If HONS 022933 Th fal I Mint m<i foocrlko Itu4v< Extraction Mothofs an ltaMar< Analysis Hsthofs usof far this nraJact. 17 HONS 022934 (SC Ilw4tr4 Extraction Method (SOI) TITtSi PCSe In Varlaaa Natrtcaa maim t x i. ices u Still lattaaai I1. bead tat. latl iara> holt ailk. bead decee (SC Standard Extraction Method Nat PCSXOI TYPICAL SMTLC SUE <a> TYPICAL EXTINCT VOLUtC (all 0.9 -9.0 I - 10 TYPICAL ANNLVTESI Aroclera 1232. 1242. 124S. 1294. 1240. 1242. trlchloro- biphenyl laanere throuah ectachlorofetahonvl laoawra ESC Standard Analvala Method Naal ECANOt. ECAN02. HSAN03 INTERFERENCES' Any alactran carturina oracle* In the ratantlan tlna ration ad trlcktereblPhenvt 1tenort throuah actachlaraklahanvl laanora dor ECANOI and ECAN02. Any dPoclaf In tho appropriate ratantlon tlna raalon hick alva tho tana ralatlva ehoractarlatlc aaa raaoonaai at PCS Itonart dor HSNN02. TYPICAL SURROGATES TYPICAL RECOVERIES (XI rantachlorobanzana 2.4.4-trlehloro- blahanvl 90-120 90-120 APPARATUS AND NATERIALSi Bvrdtck and Jackaon haxana. bantana and nothvlono chlorlda dor aanrle axtraction. Cancontratad awldurlc acid dor tanrlo dlaattlon or tanrlo eloan-ur. Silica act calunna inrroenatod allh rotaaalun roraanoanata. tulfurlc acid. and aataaalim hvdraxlda. Actlvatad kaalc alunlna. Dlaaaaahla elaaamre. LIMITATIONS' Hathad anallot only to natrlcaa uhlch do not contain nen-hydroIliable alactran caatarlno Oracle* In tho trichlarablrhanvl throuah actachlarablrhonyl laanar ratantlan tlna roalon dor EC dotoctlon nothoda. SAFETY PRECAUTIONS! Saa PCS handline rrotocola in laboratory aadoty annual. SATIS OF ICTMOO CREATION AND UPDATES' 10/29/83. 2/3/84 IS MONS 022933 ue otaaoarA Analysis Mattes (wi> TITLE! Arttltr rirmlttlmi in Oelventa nc Itnr4 Mnii IkttM Mel ANALYTICAL INOTAUCNT AND HOK OF OPERATION! ID 3--0 Cent I Urv OC/CC InterNcil te an IF'JWHM UI*rlirT DtU Ivitm tyfical ANALYTC typical INSTRUMENT LEVEL OF DETECTION (LODI </! I Araclar (trwUUiM 1292. 1242. 1248. 1294. 1240. M< 1242 0.1 TYPICAL PRECISION I OX LOO <X> 30 TYPICAL ACCURACY 101 LOO IX) 30 INTERFERENCES AND LIMITATIONS' Anr electren canturina ihcIn In tka retentlen tine reelen af trlchtereblnhenvl thrauah ectackterablrkenvl Ihmm r* retentla) IxtirfirnMi. Exact retentlen tines ef Mil llfcalv PCS litwri can 4 ebtaineA fren tka analysis af Araclar 1240. Acecler 1294 ar Araclar 1240 ferautatlens. CHHHATOORAPHIC COLUWi 30-aeter futeA tlllca J4M 00-3 (0.29 uMI with wi4a kere I0.92aa>. COLUMN TEMPERATURE PROGRAM! 130(11/4/300 INJECTION TYPE! Onlitlaaa CALIDRATION AND OTAfSMRDIZATIONl Ufa Internal atan4ar4 uuantitatien teckaluwe an4 calibrate Instruaent raananaa facters frn authentic Araclar feraulatlen staaAarAs. Use a at Maun af 10 PCS laaaars far tka Aatarnlnatlan af fncaulattan lAantltr anA nuaatltv. CALCULATIONS! Feraalatien cancantratIan (leaner areaI/Maaaar AMP) Mkarai ARP la tka ralattva raananaa factar far tka annranrlata PCI leaner la a alvan faraalatlan. Faraulatlaa cancentrattaa is aktalaaA frao tka avaraaa af at laaat 10 suck calculatlana. SAFETY PRECAUTIONS! Oaa PCD kaaAllna nratacala In labaratarv safety aaaaal. DATES OP KTMOO CREATION AMD ICTMOO UPDATES! 10/29/03. 2/3/04 IS HONS 02293A TM felt*wlnt HMI iHcrlkt iMlrtlul Rttwttt Inforatlltn ttntrttt* lir IMt nrtJtct. 20 HONS 022937 me wiimhnwi sciences center ANALYSIS REQUEST mtii February 2*. 1*04 loo no* t-o4-oa-a*-oi mmmi delaiiaac river/ivoryasa.aopis project noi man kulti toi files/ices. ivory. mocks analysis requests sent toi files.tv^.oiwT.MiLcimTHuncsTmooKS MU PICKUP SVI D. MCKENZIE mi LOCATION) MIPLE DESCRIPTION FOR 4 SAMPLES SAMPLE I08NTIPICAT10N NUMBER OF BOTTLES <S> PM - HATER SLANK - WELL FOR ICAP METALS EXCEPT HO SLUDOE FOR I CAP METALS EXCEPT HO 9 PCS324 4 (cleerl PCS33S (MIlMDt) PCB324 (centrlfuted) PCB332 (net centrluee4> PCS331 1 I RECORDED SVI P. HUPP REQUIRED ANALYSES) PCB.OISOUOFURAMS,METALS (EXCEPT HO> ANALYTICAL TECHNIQUES) X OC/EC (IS) DATE COTLETED 3/24/04 X 1CP ( ) X 0C/H3 (341 DATE COVLETED ----------------- OUALITATIVE* YES SEHIQUANTlTATIVEi OUMNTITATIVCi YES AESU1RED OA/OCi COWLETION DATE REQUESTED) KneAUtetv. COM ENTS) PCD rtnlti eheneA end tent to E4 KWr Plnt. BAWLS DISPOSITION) X HOLD FOR 90 MV9 ANALYSIS REQUEST FILE NAICl AA4090ILI 21 02*38 M0*S COPY NUMBER 1 E. Jamro 12)0 2 R. F. Ivory 1250 3 Cmtril rilaa 1250 4 Technical Raporta Library R2C ABSTRACT ONLY H. A. Woltaraann NOTE: Distribution of this report is restricted. Requests for additional copies should be made through the principal contact at the Monsanto location involved or the Manager, Environmental Sciences Center, Dayton Laboratory, Dayton, Oh : o. ACKNOWLEDGEMENT Contributions of the following Dayton Laboratory personnel to this project are gratefully acknowledged: Analyses J. A. Giust F. D. Hileman B. M. Hughes D. McKenzie G. Thomas C. Trang COMPANY C O N r I D f NT I A; HONS 022917 1M WOWCTIOW Two watar napln war* received frca tla Delaware Mm plant for analyala of thalr poaslble Aroclor (KB) and 2,3,7,1-tetrachlorodlhanaofuran (2,3,7,1-TCDF) eoncantrationa. Two additional am pin*, ona watar and ona aludpa tiara racaivad for the analyala of thalr poaalbla aatal eoncantrationa by Ion coupled plaaaui (1CP) apactroaonie analyaaa. Tit* analytical raaulta ara ahown in thia raport. faction one daacribaa tha TCDF analyaaa, aaction 2 tha KB analyaaa and aaction 3 tha natal analyaaa. 1 HONS 022918 uewai l - wfffrwic**- w *.*.1.9 tear Mttwii Mtat iMpiM frea the Mmn lim Plant war* received (or the analysis of 2,3,7,I-tetrachlorodlbenxofuran (2,3,7,4-TCorj. Tha sasplaa were labeled *(M Nall* and 'PDA Blank Plaid Natar'. Tha saaplaa wara assigned lot nuaber 1-14-02-25-01. angles wara praparad by eaptying tha one litar bottla of watar Into a aaparatory funnal. Tha bottla la rlnaad with (0 aL of aathylana ehlorlda (CBa Cla) and thla la addad to tha aaparatory funnal which is than ahakan to extract tha TCDF's into tha CNaCla. Tha CMaCla is raaoved and savad and two additional CHaCla extractiona ara nada of tha watar and contained with tha original CBaCla axtract. This axtract containad a considarabla aaount of banxyl alcohol and bantaldohyda. Thasa coapounda wara removed by solvant exchanging tha CHaCla to IS at aethanol. Tha aethanol was ex tracted three tines with 10 aL portions of haxana and thasa hexane fractions wars combined and partionad against 50 nl of watar followed by 100 nL of concentrated sulfuric acid. Tha hexane layer was dried over anyhydrous sodiua sulfate and concentrated to 2 aL. The concentrate was applied to tha top of a nultiphasa colixan containing (top to botten) 2 g of silica, 4 g of silica plus 404 sulfuric acid, 1 g of silica, 2 g of silica plus 344 potassiun hydroxide and finally 1 g of silica. The coluan was eluted with 50 aL of hexane with tha eluant going directly onto a coluan con taining 2.5 graas of Moela basic aluadna. This coluan was first olutad with 10 aL of 24 CHaCla/hexane to raaova PCb's and this fraction was discarded. Tha coluan was than eluted with 15 aL of 504 CBaCla/hoxane and this fraction was saved and concantratad to 10 tl in a keeper of dodecane and subaittad for GC/ns analysis. The OC/MS analysis was carried out on a Hewlett Packard S5ISB GC/MB systaa with tha gas chrcastorgraphlc separations on a 50 aster SP-2330 capillary colwn. Tha anas spactroaeter was operated in 2 HONS 022919 the hIuM ion Monitoring node following Ions characterlatic of tho tcor'a and the aurrog-ttea that vara uaad. Ouantltatlon waa achieved by ratiolng tha aaount of 21TI-TC0P In tho aanple to tha aaount of "c-237l-TCDr which had boon addad to tha watar at tha vary outaat of tha extraction procedure. Thia laotopically labeled aurrogate provldaa for accurata quantitation even though tha actual recovery of tha TCor'a can be quite variable. Tha raaulta of tho analyaaa are ahown in Table 1. Included in tha table are tha raaulta from tha apiking atudiaa in which native (non-iaotopleally labeled) TCDF waa addad to the aaaiplee. 3 HONS 022920 analysis or nm uwui rOR 2, 3, 7,S-TKTRACRL0II00IRX1Z0 rURAN Sample PM Well PM Well (Rep) PDA Well (Spike) PDA Blank Fiald Water PM elank Field Water (Spike) D a J Water Lab Blank Method Detection Limit ppt 2371-TCDF found 92 100 12S ND* 2.3 ND i ppt 2370-TCDF added - 25 2.5 - ND non* detected at the Method Detection Limit 4 HONS 0229*1 BSCTIOH 1 TXTUl ICT-UI ANALYSIS Of DKUMAAE RIVEN SAMPLES DATE! 9 MARCH S4 RECORD NUMBER* I-B4-02-29-C1 PROJECT NUMBERI 4S4. 40911 NOT EPOC*.' REFERENCE! MONSANTO 2443927 TITLE! ICP-AES ANALYSIS OF DELAWARE RIVER MATER SAMPLES BACKGROUND TWO WATER SAMPLES WERE RECEIVED FROM DELAWARE RIVER FOR A TRACE METAL SCAN BY 1 CP-AES. THE TWO SAMPLES RECEIVED WERE LADLED! PDA WELL AND PDA SLLOGE. PROCEDURE! 100ML OF EACH SAMPLE HAS DIGESTED WITH HOT HN03 AS OUTLINED INI EPA METHODS FOR CHEMICAL ANALYSIS OF WATER AND WASTES PART 4.1.3 TOTAL RECOVERABLE METALS AFTER DIGESTION. THE TREATED SAMPLE WAS RETLMCD TO ITS ORIGINAL VOLUME. INSTRUMENTAL METHOD: THE DIGESTS AND BLANK HERE ANALYSED BY ICP-AES USING DIRECT ASPIRATION. 5 HONS 022922 ANALYTICAL RESULTS! TABLE 01 (VALUED IN mi) PDA NELL AL 52 <0.5 BA 0.5 K <0.5 CA 40 CD <0.5 CO <0.5 CA <0.5 cu <0.5 FC 410 no 49 m 30 NO <0.5 N] 0.9 PB <0.5 SN 1.1 T1 <0.5 V 0.5 IN 4.4 PDA SLUDGE 39. <0.5 1.0 <0.5 87 <0.3 0.9 <0.3 <0.3 2230 133 71 <0.5 4.0 <0.3 2.1 <0.3 1.9 7.2 TAKE 92 RESULTS OF STANDARD REFERENCE MATERIAL ANALYSIS ELEMENT! X OF TRUE VALUE AS DETERMINED SV ANALYSIS) ALII04XI CD( 107X1 FEI9SX) .(105X1 0(115X1 C0(102X1 PVM90X1 TIC 121X1 BA(93X1 CJH94X1 HOI 133X1 VI102X1 SEI93X) CUI9SX) NKI02X) INI103XI DISCUSSION OF KSU.TS SOIN SAWLESIPDA NELL AMI PDA SLUDOE) CONTAIICD S10NIF1CAHTLY HIGH CONCCNTRATIONS OP INON. HA0CSIUH. IWNGWSK AND ZINC. DUE TO THE SPCCTNAL INTEAFEACNCtS OENENATED *V T>C HIOH CONCEN- S HONS 022923 TRRTtONS OF TTCSE ELOCNTS THE VALUE* FOR ALL OTWR CLMNTO HILL m IIHR EM4RNCSD OR SUPACSSCD DEPENDING UPON TIC NATURE OF TIC OFCCTRRL INTERFERENCE. TICAEFORE. THE VALUES REPORTED FOR ALL CLEMENTS WITH TIC EXCEPTION OF PI. HO. fM. AND IN CAN K CONSIDERED At OEMI-OUANTITRTIVC ONLY. AA/QC INFORMATION DUE TO TIC FACT THAT TIC REQUESTER I ED JAfWO) AT DELAWARE RIVER ASKED THAT THE SJWCLES SE TURNED AROIMt A$ QUICKLY AS FOSSISLE . THE FULL SET OF OA/OC SAMPLES! it... SPLITS ANO SPIKES) MERC NOT GENERATED OUR INO THE ANALYSIS IN AN EFFORT TO SATISFY ED JAHRO'S REQUIREMENTS FOR THE QUICKEST TURN AROUND POSSIPLE. 7 HONS 02292* C1CTX0N 2 mum nron TOR MOOM 1241 mm Rarer 2*> ! im mini 1-04-02-29-01 project m.mu TOi tanM imI via PeCeral Euptmi tei Hr. EC Jur Reftsente Dtlwart River Plant Rt 120 OMCeerert. N. J. 00014 Envtrenaentel Science* Center Heneante Cerranv/Davten laberaterv ISIS Htcheta* Real Davten. OMe 4S4I0 Phene Nei (313) 3*4-3411 Title) Rnalvel* eP Tve Uater Saar lee Per Rrecler 1240 StanSarS Sardine Hethes Helen n/a StenCsrC ExtractIen RetheC Ne< > PCEE02 Stan4ar4 Aealvtlt RetheC Helen ECAN02 Plaal Revert Pile Helen A40PI0 Takle Pile Helen 040910. C4O9I0 Tve eater tsarlet were analvie* Per Arecler 1240. He Arecter 1240 nae CetecteC la the PDA Mater Olanh Searle with a level ee Cetectten ee I wa. Twe alienate eP the eaowte labelleC pm Hell were analvaeC. One centalaeS eellnent arc tha seceaC ceatalneP ne vleahle aneunte el eellwent. The reewlta el analvele Per Rrecler 1240 In theee twe eanrle* are ehewn In Table 1. Chrmatteram al tha Arecler 1240 etaaOarc (1 ve/aLI an4 tha twe extracts Prea tha POA Hell eanrle are ehewn In Plavre 1. Since there te a SIPParanca In cencentratlan aP arrrexlratelv ena erSer eP naenltePa between tha eaarlee thle ene well eanrle wae centrlPveeP an4 reanalvseC In an ePPert te ebtaln accerate valwee Par Rrecler 1240 In a eanrle which has ne seCinent. The re eel te aP analvele *P a eanrle centatnlne eeSIwent aaC a eanrle which has been centrIPweeP are shewn In Table 2. Pleura 2 thaws cenrarltea chrenataerane aP these twe eaarlee arc an Rrecler 1240 etanCarC. Re car ha aaan. the Rrecler cancantmtlan In tha centrlPaeaC water eanrle Is arrrexlaatelv live tines I ewer than tha dear eanrle results ehewn In Table 1. TherePere the cencentratlan Par the dear eanrle rrebablv shews that sene seCiaent was alee in this latter saarle. HONS 022925 It wnim tfcnt nUr hwIii ikMlOi utlnH m Nt m*> IrlfMH in r<r t rtUU accwat* nlMi far ftraclar (MtHtratlm aktcfe rt w*M*t MihImI fCI Id Ntiri < atlck mmr k mint u Kk UikM m 4lMnt Nklck mv t< ninMiI In mtir hwUi. ' cKffltlfi CM Trim 9 HONS 02292* C(/bc Z HONS 022927 HONS 022928 IIHI HONS 022929 p*y~* ifoJ'-O- HONS 022930 TMLI 1. CiMMlritlM *f Araclar 124* NmiwH In tut fpa w*n at nc FraJact Nat 484.40918 Datai (larch 4.1984 Araclar 1248 Canaan*r Nwaaar 19 14 17 ia l 20 21 22 22 24 29 24 27 29 </> ESC Extraction HatKatf tMFla Mat *xtract4 (a) Extract Dilutian nc Extract No. Fracaaa Ft I a Naaa TABLE FILE NOl 840918 swru identification F0A-W.1I Ctaar PDA-Wol1 S4iont Area 2399 4297 7099 - 9420 3974 1329 1733 2904 1070 3092 1107 2432 1401 A1240 Ar* Cone* (wa/al A1248 Cone. </> 18 .24 .20 - .22 .24 .20 .39 .33 .21 .33 .28 .23 .22 30683 70992 83427 0406 41970 48927 21147 17484 28900 19942 37908 13443 37037 24414 2.36 2.49 2.33 3.04 2.94 3.20 3.11 3.99 3.71 3.09 3.44 3.44 3.90 3.44 .29 3.12 Araclar 1248 STD llva/.ll Area 13002 24212 39909 2768 24231 19179 6801 4866 7780 9197 11941 3948 10980 4747 PCEX02 10 1110 PC8329 Kil PCCX02 10 IU0 FC832* mis PCEX02 - tu AI248 *9204 14 HONS 022931