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T-870-D
A2J40
(l .6t "n u mb e r )
EST. WT. 1818 LBS,
PREPARATION,NOTES:
1 ij .1 * ..I
C ) P7-- 870-D (F)
lllit
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FWK 1/7/02
1 PED *1 i Jill I STANDARD I IKS. ...................
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EQUIP ME-NT
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NAME: WA7CHUNG RED B
:!
MOTE; DO NOT START IF PRESS WILL NOT BE
I........ -|
AVAILABLE WITHIN 3 HRS AFTER MAKING. SUPV i
TO. REVIEW WITH P.R. SUPV & RECORD:
f
PRESS WILL BE READY_...___ M__....... 'PR SUPV i
START 1iAi< I NG_______ M.,,,_____ /_____ ____HAK ING SUPV I
NOXE^-NOTiFY PRESS ROOM BEFORE ROPING OFF 1
EA UNDER V-85.2
!
RUN 15s WATER. INTO V-904. PUMP WATER |
FROM V-904 THRU DISTRIBUTOR. IF WATER DOES ! NOT COKE OUT OF ALL DISTRIBUTOR HOLES WITH |
FULL. FORCE, NOTIFY SUPERVISOR,
|
92/
RE 0 0 R D ;__/____BAT CHES SINCE SPARKLER LAST CLEANED. AFTER 4 BATCHES, CLEAN, DRESS SPARKLER & PRE-COAT WITH 15* DICALITE,
R AID OJQJCMti FOR S11 2-CHLORO-4-AMINOTOLUENE-5-
LFPNIC ACID. .1 J!; TAIN FOR S27 3-HYDROXY-2-NAPKTHQIC ACID \^<THNSTALL DV t, 'DV RECORDER & CONTROLLER CHART
RUN 10" (1 GOG) w a t e r in t o V- m:St ADJ TO i IJ&8-100 DEG F ! 6#TADD IN 2-3 MIN DRESINATE X , 1 7^S7m 5 MIN & RECORD PH_.iQj.JL....<9,5-10,5)
O^^ST IR^, 20 MIN OR LONGER TO DISSOLVE FOR S-49
75
922 (502G) WATER INTO V-922 3D..IUM HYDROXIDE^I^ V-926^F^ IN
TURN ON AGITATOR & STEAM "&^D.UHp""lN~FRO.H S2
2~CHLDEQ-
4-AMiN0T.0LUENE 5-SUJ-F8NIC
JLSW-.
.ACTIVATED CARBON
CtLTER'AIp
212-314 DEG F WATCH FOAM!1 BY.T^TT-') IF NECESSARY ADJ TO +BY
SODIUM HYDROXIDE
ASSUME 30%.
30. MIN AT 212-214 DEG F, THEN SHUT OFT
STEAM WATCH FOAM: NOTE' RECORD SPARKLER
PRESSURE
,,,,,PSI, IF Nl T ZERO NOT7"
SUPERVISOR.
iS
MOK-BLEEDIMG
N-CDDE I ACCT lllllllill'llfllli;
U:.-
777-A
740-0 82-C
i
i | |
J 53G-A i
75
7-D 740- C
IS } iM
'1 50 766
113-B i 777-A 1
! I 7-D
2m ,1 0
r
, EgU lP HE NT
E 2 OF 4
DATE PRINTS
CG 32 CODE RT--870-1; (FT
fjr.cocc
922 3
CONT
1^1 i i 4 i
CIRCULATE i !5 MIN OR LONGER THRU SPARKLER
UNTIL SOL'N IS OeCAR* HAINTAI.N AT J.?0- f 95
DEG F FOR SJ-^HRECORT) STARTJ
TOTAL
___ ..CLARITY-?!:
iCT'
F & REC
F
fiCCT
NTSC 4
' MEASURE-^EF_,, UNITS IN V-923, FOR
&0
wrm o c h t. ORte:ifi/311
WEIGH SODIUM NITRITE IN FT FOR SA2
_%
WEIGH SODIUM NITRITE. IN4 DRUM FOR 550
%
J/CV 2<r
2"' c s b g ) w a t e r in t o v-^rfPA/cv
i. WHEN SI 7 IS COMPLETE, PUMP IN V--922 THRU
I SPARKLER, MAIN/AIr-L7-922 AT 1 90-i^LT/OE;: F,
i RECORD: START.fe]|>0ti TOTAL MIN.
30
' '22 1 WHEN S22 COMPLETE, SHUT'OFF PUMP AND INSERT
6 J^Sf-922 FOOT PLUG T'tfAi' RUN IN 10" (209G) WATER * HEAT TO 190-! 90 r J CIRCULATE 15 MIN THRU SPARKLER
ArlD PUMP V-922 THRU SPARKLER INTO V-fl#*/CV
(12050 w a t er in t o -7-902 2J0^MEIfiB-- SODIUM HVDRCXICE ^N V-97^.N IN
DUMP IN FROM S3 3--HYDR0XY2-NAPMTHGIC ACID
ADJ TO 70-90"DEG F & STIR TO DISSOLVE
f 7-fi^L
7-D. 82-C
201 700
RUN IN 5* (KHC) WATER & HEAT TO 190- 17b
cjRCUi a t f is Min t h r u s p a r k l e r
liliiii
}J I (A - '22 THRU SPARKLER.. I.N^O V~***/CV
F' < BLOW OUT SPARKLER INTO V-HP4/CV
SSOLUE ALXANOL XC IN 20G WATER AT ( 50-160 : u: -inr w a t e r mix e r t n d r u m ?< f o u r t h ,
T TO 165-170 r FOR SCO
23 y.
|,3 HBl
............ .......................-..........
-T& t.....................................:
T T- 1 (FONG) WATER n'-'TO V
nDJ TO
DUP050110520
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MEN! 1
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PAGE 3
OF A
DATE PRINTED: 1/08/32-
7 - 7"n -c o d E"T~ac g t
CG 32 CODE RT--870-D <r) I LI'S I
| Lj l iS
NOTE; IF N-740-C SOL*. WAS PUMPED DIRECTLY ! FROM/SPARKLER TO CV S21,24B,'29 OMIT 537 &38 j
DISTRIBUTOR INTO CV AFAP (12-15 MIN) N-23-DHYDROCHLORIC ACID'FROM .510 INf
,, MIN. MAINTAIN `165-17S*F IN CV*
15 MIN AT 165-170 DEG F
*
, L.rt !*t
TO 33* (3107&) AT 32-38 DEG F ~
jW330J
RECORD: TEMP_^ftu_DEG F, VOLUME"
i
RUN IN N-725-A SODIUM NITRITE FROM SIP AFAP
(5-10 MIN) & RINSE IN PT
TE: PROCESS HAS A VERY- LOU N-28-D EXCESS
CHECK CR VERY CAREFULLY
STIR 20 MIN AT 32-38 DEG F MAINTAINING,
+CR, +KI FOR S44* RECORDV TIME STARTiS?
CR,,_.JSfe^^_* Kr_j5tr____ NOTE:
1) -IF CPi-, Klr^ADD 204* J>AS IS" INCREMENTS
RECORD CRI: >1<+.) KI VFL_( + )'
*
i I
HYDROCHLORIC^ ACID r \
F" CR+, KI^ADD 20* RD CR_.^T_< + )
ASSUME 32%
IS" INCREMENTS +)
IUM NITRITE
ASSUME 33%
IN CALCIUM CHLORIDE'
ADD FOR MAINTAINING 32-38 DEG F THRU 255
f il iT.Pt a p p r o x ima t e l y 1/2 f u l l w it h 90-110*1 WATER FROM H8T WATER MIXER
UMP IN STRONTIUM NITRATE 5I2R- 30 MIN OR LONGER WITH LIGHTNIN MIXER
fION FOR S58 '
J^SisA COMPLETE; STEAM EJECT V-921 /WH
SB INTO V-9G2
y
'OUPr^fl N-725--A SODIUM NITRITE FROM S20
"' '' AMMONIUM CHLORIDE
__ _____ ______ /__ _
IMMEDIATELY COUPLE V-902 THRU UNDERSURFACE DISTRIBUTOR |INiQ CV'IN 18-22 TUN. RECORD:
RING SS2 WEIGH SODIUM HYDROXIDE IN PT,, 1
LUTE TO MAXIMUM VOLUME (+/-10OG) FOR S56
N S52 COMPLETE, STIR 30 MIN & RECORD:"
Azdcrfcrf+J>
rrr BASE__j!<fe__;_<+>
5 * 0-r6 * 0 >
imr.^3L. t32-38 f > 1
SODIUM HYDROXIDE IN PT FROM S54 THRU
UNDERSURFACE LINE, . RINSE .IN PT & STIR'15 MM j
KDRD.,: DIAZQ,,^!!%.._<-). BASE__J!fc*.^_<'+-)
^ __(9 *0-9'* 8)
H STRONTIUM NITRATE N~2.4.6-~B, E SOL ' N
M S48 i, RINSE IN PT * " STEAM EJECT IN V-93# FROM. S36 STIR 5 MIN & RECORD ; PH_5itl_<9 * 0-9 * 8>
j
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RlNTED' I
OF 4 C5
OflDF Rf-Gw; D C-j
s>?3EL0U 7.0 ADJ TO
ONLY. RECORD PH__
. 0--9 .fc5 WITH
HYDROXIDE
ASSUME ro%
IN I OCTANOL
im:
_BEG F AND REC
DEG F
MIN AT *93-195 DEG F.
'RECORD: START&^L.J&.V\
,
AFTSR' 20 MIN S6A STIR
RECORD:
PH,,_3LCk__(8.0-9.3)
BELOW 8.8, ADJ TO PHyB'. 8-9.3 WITH
ONLY. RECORD PH..ASSUME 50%
:S64 STIR. FLOOD TO- i 80--1 9*
9.000G) AND STOP AGITATOR
'
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U *CODL "T
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5&2-A i
7-D
ACcf 23
i WHEN INSTRUCTED BY PROCESSING AREA HALFWAY -1
I 1 .THRU PRESSING, DUMP IN,., STIR 5 MIN 4. STOP I;
! ! AGITATOR. RESUME PRESSING.
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