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< DATE ')
(LOT NUMBER)
EST, WT. 2567* LBS, STD/ HRS- _____/ TIME
PREPARATION NOTES:___ ________
C )RT-618-D <U> EWK 12-8^85^
TYPED BY: KLU JQB . NAME : 32RT61 8DMU
4/ mtsji
NON-BLEEDING
EQUIP MENT
PREP 1
I: USE
]J
NAME; WATCHUNG RED Y
1 LBS I |------- --, _
! i j RECORD:____J.___BATCHES SINCE SPARKLER LAST |
I I CLEANED* AFTER 4 BATCHES, CLEAN, DRESS
I
} | SPARKLER & PRE-COAT WITH 15* DICALITE
|.
I L* FILTER AID
I
\J3S\ OBTAIN FOR S11 2-CHL0R0-4-AMIN0T0LUENE-5- |
I SULFONIC ACID r*'- v: *
.
\^S\ OBTAIN FOR S24 3-HYDROXY-2-NAPHTBGIC ACIY j
INSTALL DV 6 CV RECORDER 6 CONTROLLER CHART I
1 NOTE: NOTIFY PRESS ROOM AND ROPE OFF AREA I
UNDER V--922
I
N-CODE
777-A 1I I
740-C I I
2=53-0 ] !
ACCT LBS*
AL
RUN 10 * (1 0G) WATER INTO V~_?jgZ. & ABU .70
-100 DEC F DD IN 1-2 MIN. DRESINA>TTEE)X .
2 MIN 6 RECORD: PHL. j^J^.S-l. 5) STIR 20 MIN OR LONGER FOR S27
II 58 | 530-A | 58
932T2
N 32* <659G> WATER INTO V-922
WEIGH. IN V-926 SODIUM HYDROXIDE 6 R
$.Li23~ -- m.___ 3L_.,,,k2.tS?l-Z
TURN ON AGITATOR 6 STEAM & DUMP IN FROM S2
2-CHLORO-
LOT y
LO0X
%, .
I 1 4-AMINOTOLUENE-
-5-SULFONIC
________ _______________ _______
D ___________ __________ ________
IN ACTIVATED CARBON
45
IN DICALITE FILTER AID
_ tJ
10
&**T HEAT TO 2)2-214 DEG F, RECORD HT^/V_..* F,
I l ^__JM2^d e g w f WAATTCCH FOAM
W^iRECOgJl^W__jLlX + >, IF NECESSARY ADJ TO ~+BY
I '^^SODIUM HYDROXIDE
ASSUME 50%
j--rWtPHT STIR 30 MIN AT 212--22114' DEG F, THEN SHUT *.
I 1 OFF STEAM
WATCH FOAM
/\
I I NOTE: RECORD: SPARKLER PRESSURE __S^__PSI
I OT ZERO, NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNITJILLL Si>UOLL'INN ^.IS LCLLtE-rAirsR; IMirAi INJTLJJAJi *IN*" A" TI 1l/9V0-1*/95 .#F FDRR S19 L` R--E--C--O--R--D- :^HT__^Ju_DEG F~ A**N"D
JUNj.
RECCORDER
DEG F .
~~
RECCOORRDD: START ___^__^_S__^__T_ OTAL MI.N__^P____ ,
CLARlTY__,^!t. NOTE: SAMPLE FROM HOSE -
SHOW TO SUPERVISOR FDR O.K
7-D 740-C
113-B 777-A
7-D
1982
N39230
EQUIP MENT
GE 2 OF 3 CG 32 CODE RT-618-D (U)
N 1* (50G) WATER INTO V-904
WHEN 517 COMPLETE, PUMP IN V-922 THRU
SPARKLER, MAINTAIN V^922 AT 190-195
ORD:
TOTAL MIN_,
USE N-CODE 1 ACCT LBS I LBS
I~----
EIGH IN PT FOR S35 SODIUM NITRITE
cgijj/fi
m___ ________>__
%
MEASURE 5L_^ttNITS IN V-928 FOR S33 rT
HYDROCHLORIC ACID 'M'TM^./_____ tJSjUj L%
% *) < I I
i
I 725-A J
I 28-D |
309 390
.16" (15300 WATER INTO V-___ WEIGH IN V-926 SODIUM HYDROXIDE & RUN IM_
m___i._____ DUMP IN FROM S3 3-HYDR0XY-2NAPHTHOIC ACID
SLiksfl 7-D 253-C
IJKX
i i I 471
mmmm
TO 70-9 DEG F &.STIR TO DISSOLVE STEAM EJECT V-921/931 INTO CV
I |.
WHN SI 9 COMPLETE;--SHUT OFF PUMP & INSERT. I
22 FOOT PLUG
J
RUN IN 10" (2070 WATER & HEAT TO 190-i95 Fj
CIRCULATE 15 MIN THRU SPARKLER, .
I
"PUMP V-922 THRU SPARKLER INTO V-904
|
RUN IN 5" (10.3CF WATER INTO V-922 & HEAT TOf 190^4-95 Fa CIRCULATE 15 MIN THRU SPARKLER |
904 F V-922 THRU SPARKLER INTO V-904
MTY BLOW" OUT SPARKLER INTO V-904
At TO 165-170 F <SMPL` TO SUPVR FOR O.K.)
EU# IN N-28-D FROM S21 IN 12H5 MIN & SJIR
MIN AX-465-170 DEG F
'r .
^ 129*(34090 AT 28-30 DEG F AND .
CORD^TEMP __">__*F,
ICE 40X3301 57-A
N-725-A FROM S20 AFAP (5-1.0 MIN)
& RINSE IN PT
STIR 30 MIN AT 28-35 DEG F MAINTAINING
I I, +CR, +KI FOR S41 AND RECORD:
i r TIME START
yp*TR : 4~ (+) ,KI_JfZZ.(+>
I
I-
NOTE (1) IF CR-, KI-, ADD 200 AS IS IN- .
CREMEN.TS
HYDROCHLORIC ACID ASSUME 32%
r i I 28-A I__-___
RECORD: CR_j;,,__b(+ ) , KI_~-- ( + > :
II
i (2) IF CR+, KI-, ADD 200 AS IS INCREMENTS
1I
SODIUM NITRITE.
ASSUME 33%
_______ I 725-A I- ____
RECORD: CR__._( + ), KI____ ___ ( + >
DUP050047901
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EQUIP I MENT
PAGE 3 OF 3 CG 32 CODE RT-613-D <U>
USE I N-CODE ACCT
LBS i
LBS
ftp INTO CV BARIUM SULFATE
167 I 65-A
167
n
ADJ TO 37* (3496G)/^AT 28~32*F
ICE _ a
32X330 I 57-A
I UftecOt RD TEMP__^s.5__DEG F 6 VOLUME 3/ i3.pTr'^^UGWegilcGH IN FROM DRUM AMMONIUM CHLORIDE
I i 165-A I. 222
<PSTlR 2-3 MIN
.'
IMMEDIATELY COUPLE DV THRU UNDERSURFACE
I i I; I I,'
DISTRIBUTOR INTO CV. IN 45-6 MIN* MAINTAIN I __ I . 57-A I ____
CV AT 28-32 DEG F.: RECORD: STARTjfcjL
Ii
TAL MIN
I I,
STIR 3 MIN & RECORDw BME
+ >,
DIAZD _-5.*_^^>fH^i:LS-*.(9.0-9V8) ,
fjjsm: t e mp gy d e g f
?
I I
i
N^CEE|SA/ RY, ADJ TO PH 9--9*8 AND RECORD
SODIUM HYDROXIDE
ASSUME 5%
HYDROCHLORIC ACID . ASSUME 32%
I 7-D 28-D
HEAT TO
DEG F IN 65-7 MIN AND
RECORD : HTLJ4XDEG F & RECORDER |^C__DEG F
NOTE: AT 174-176 F, OPEN WATER
1 1/4. TURNS ;
902 :j_RWN 24* <618G) WATER INTO V962
12
TURN ON AGITATOR 6 STEAM 6 DUMP IN BARIUM
1506 | I 16-B | 1506
'CHLORIDE
HEAT TO /#H6,F 6 STIR TO DISSOLVE
CV WHEN S44 COMPLETE, IMMEDIATELY STRIKE "V92'
13 1 THRU UNDERSURFACE DISTRIBUTOR INTO CV IN .
i 7-10 MIN* MAINTAIN CV AT
DEG F*
RECORD: START_^^i|fl, TOTAL MIN__/0___
49^0iEAT CV TO 198-202 DEG F IN 10-12 nIN
O^TJXIR 5 MIN AT 198-202 DEG F
l-'t^EOUD T 1S0->90* < +/-18,000G.)
RECORD: PH__V2jf9,-9.4) A STOP AGITATOR
SHUT OFF WATER SPRAYS/
...
OPTR^
I WHEN INSTRUCTED BY PROCESSING AREA HALF WAY!
I THRU PRESSING, DUMP IN, STIR 5 MIN 6 STOP |
I
I
I AGITATOR* RESUME PRESSING. I-OCTANOL * I 1 | 588-A | 1
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