Document VjbwYxqBG65jxOaZ1LrgzGZbK

MONSANTO TERPHENYLS - M o n sa n to T e c h n ic a l B u l l e t i n N o. P -1 0 6 N ovem ber6, 1950 V Monsanto Chemicals- Plastics _ _ _ _ K./4 PLASTICIZER APPLICATION GROUP i MONSANTO TERPHENYLS \'(ft Monsanto Technical Bulletin No. P-106 November 6, 1950 Monsanto Chemical Company Phosphate Division St. Louis, Missouri MONSANTO TRADE LITERATURE PERMANENT Fll F *202 INTRODUCTION The Monsanto TERPHENYLS are a series of hydro carbon solids ranging in melting point from a little above room temperature to as high as 210C. (4lOF.). Monsanto TERPHENYLS have found use as plasticizers, softening agents, wax additives and extenders, and in paper coatings. Various properties of the TER PHENYLS are presented in this bulletin to facilitate the selection of the proper one for specific appli cations . . lor. ronlelned In this bulletin we made without guarantee, 'lftlme any liability incurred in nothing conlilned herein she M* revering any material or ill to our beet knowledge. true and accurate, but all recommendation* or the "condition* of u*e are beyond our control. The Montanlo C htmical neclion with the uee of three date or suggestion*. roiiRtrut'J s\ recommendation to uee sny product in conflict with 0627407 | TOWOLDMON0039974 WATER_PCB-00024443 Formula; PHYSICAL PROPERTIES Ortho Meta Para 1 Color - NPA: <1.5 Penalty - k./cc.: 1.14 Melting Point: Completely liquid 55C. (131F.) Solidification Temp .; First crystals -- <3-5 1.164 90C. (194F.) -> <90c. (<194F.) - Hold point , 53-55g. x (127-131 P-) Plstillation Range: 330-3 50C. D-20 corrected (626-662F.) Flash Points 171C. (340F.) Flame Point: 193C. ' (390F.) . 83-85C. (I8l-185F. 368-378C. (694-712F. 207C. (405F.) 229?C. (445F.) Viscosity S.U.S. ------------ al~2T0OF.s 40.6 (See Graph No. I) 39-3 . Solubility: See Graphs Nos. II, III and : <2.0 1.236 213C. (4l5F.) 209-213C. (40-4l5F.) 38l-388c. (71&-730F.) 207C. (405F.) 238C. (460F.) . 28.8 (at 225C.) -1- 0627408 TOWOLDMON0039975 WATER_PCB-00024444 Vapor Pressure (mm. of Mercury); TC. 90 100 110 120 130 140 150 160 170 l6o 190 200 ' 210 220 230 240 25Q 260 270 280 290 300 310 320 330 340 350 360 37 380 _ Ortho 0.17 0.3 0.5 0.9 1-5 2.4 3-7 1.2 12.0 18.0 25.0 35.0 46.0 62.0 82.0 110.0 140,0 180.0 230.0 290.0 . .36O.O 450.0 550.0 670,0 810.0 990.0 1160.0 1390.0 1600.0 Meta - 0.15 0-3 0.5 0.8 1.3 2.0 3*0 4.6 6.8 <3.8 14.0 19.0 26.0 36.0 48.0 .0 83.0 110.0 140.0 180.0 220.0 270.0 340.0 410.0 500.0 610.0 730.0 870.0 Para _ O.15 0-3 0.6 1.0 1.9 3-2 5*5 , 9.1 14.0 19.0 26.0 35-0 46.0 61.0 80.0 101.0 130.0 165.0 210.0 260.0 320.0 390.0 470.0 570.0 680.0 Solid Terphenyl Ortho Meta Para ELECTRICAL PROPERTIES Dielectric Constant 2.54 2.62 Resistivity - ohm-cm. l66C. . 23013C. 82TOTTT09 ------- 2600 X 109 - - 30 X 10* STABILITY No deteotible effect on boiling Terphenyls in 10$ Sulfuric Acid or Caustic Soda. -2- 0627409 j| TOWOLDMON0039976 WATER PCB-00024445 COMPATIBILITY Ortho Terphenyl frftier Component j, Ortho Terphenvl in Mixture 1U 55 50 75--------- 'go Paraffin (120/125F.) Barnsdall (l60/l65F.) Beeswax Opal Wax Stearic Acid "N" Wood Rosin CCo CCo C CC cI I I I iI X c CII ' Meta Terphenvl Other Component % Meta Terphenyl in Mixture 10 12 25 90 Paraffin (l20/l25F.) Incompatible with 2# or more Meta Terphenyl Barnsdall Wax (160U/165UP.) cBII Ceresin II I Carnauba Wax Candelllla Wax c CCI ccI I Montan Wax III Beeswax III Japan Wax c ,,I I Opal Wax ccI I I. G. Wax 0 III Stroba Wax Acra Wax III c CB Stearic Acid III Shellac c I I. Manila Resin (Loba B) G, I I Ester Qum C' I I "N" Wood Rosin (Hercules) CcI I Piccolite Resin (85) "" C I I Staybellite Resin BI I Para Terphenyl Other 'Component Paraffin (120/l25F.) Paradene No. 1 Paradene No. 2 "N" Wood Rosin j> Para Terphenyl in Mixture 0-5 1-2 ----- 5 10-75 I CI CI I Note: C Compatible , I Incompatible B Almost Compatible -3- ObZl'ilO ,| TOWOLDMON0039977 WATER_PCB-00024446 COMPARATIVE HARDNESS (Smaller values denote greater hardness) Average Penetration In om. x 10-2 in 60 seconds at 25C. under load Indicated (ASTM D-5-25) Material . 50 Grams 150 Grams 250 Grams Meta Terphenyl 0 0 2.3 Para Terphenyl 0 0 3.3 Carnauba Wax 0 2.3 4.7 Candelllla Wax 0 3.3 4.7 Ortho Terphenyl 1.3 4.0 10.7 50$6 Paraffin & 50$ Meta Terphenyl 3-7 12.3 18.0 75$ Paraffin & 25$ Meta Terphenyl 7-3 18.0 25-3 Ceresin Wax ~ . 9--3 15.7 26.0 95$ Paraffin & 5$, Meta Terphenyl 10.7 21.0 29.7 98$ Paraffin & 2$ Meta Terphenyl 11.7 26.0 32.7 Paraffin Wax 14.3 23-3 31-3 Montan Wax 15-0 28.7 .... 37-3 Mixed Isomeric Terphenyl No aging Aged 24 hours 60.0 28.7 - - AVAILABILITY ' The Terphenyls are available in limited quantities. I sctwa-m-1150 rev. -4- 0627*11 Q Prlnted In U.S.A. TOWOLDMON0039978 WATER_PCB-00024447 VISCOSITY* SAYBOLT UNIVERSAL SECONDS TEMPERATURE. DEGREES FAHRENHEIT TOWOLDMON0039979 WATER_PCB-00024448 Graph II SOLUBILITY OP ORTHO TERPHEHYL Temp TOWOLDMON0039980 WATER_PCB-00024449 JU9AIOS jo -oo ooi i9<^^uaii<l.i9,L B^aw jo sure.10 Temp. Graph IV - . SOLUBILITY CP PARA TERPHEHYL Temp \yr ; Monsanto ChEMICAI.S"'PLASTICS ------- _________ For further information about Monsanto TERPHENYLS contact the nearest Monsanto office. MONSANTO CHEMICAL COMPANY St. Louis Birmingham Boston .Charlotte Chicago Cincinnati Cleveland Detroit Los Angeles New York Philadelphia Portland (Ore.) San Francisco Seattle Monsanto (Canada) Ltd. Montreal Toronto Representatives In the Principal Cities of the World o 0627416 -----------^ TOWOLDMON0039983 WATER_PCB-00024452