Document VjKwxwD11e7pm666rZmb2mbbw

27-CV-10-28862 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM Hennepin County, MN STATE OF MINNESOTA DISTRICT COURT COUNTY OF HENNEPIN FOURTH JUDICIAL DISTRICT State of Minnesota, by its Attorney General, Lori Swanson, its Commissioner of Pollution Control, John Linc Stine, and its Commissioner of Natural Resources, Tom Landwehr, Case Type: Other Civil Judge Kevin S. Burke Court File No. 27-CV-10-28862 Plaintiff, vs. PLAINTIFF STATE OF MINNESOTA'S SECOND AMENDED EXHIBIT LIST 3M Company, Defendant. Plaintiff State of Minnesota ("State") states that it may offer into evidence in its case-in chief at trial of the above captioned matter: (1) the documents identified on the parties' Joint Exhibit List filed January 19, 2018; and (2) the documents identified on the State's Second Amended Exhibit List attached.1 In addition, the State respectfully reserves the right to use or offer as exhibits (1) all documents identified or referenced on Defendant's exhibit list, (2) any publicly-available materials, including articles, reports, or journal publications, and (3) any documents that may be necessary to respond to undisclosed evidence from Defendant, to rebut Defendant's evidence, to impeach Defendant's evidence, or to clarify or correct the record. In addition, the State respectfully reserves the right to submit an amended or supplemental exhibit list, or to withdraw any of the exhibits on the State's Second Amended Exhibit List, as becomes necessary or1 1Please note that the exhibit numbers in the Second Amended Exhibit List are not consecutive and contain gaps due to exhibits that were removed from the State's Initial and Amended Exhibit Lists filed January 19, 2018 and January 31, 2018. The Second Amended Exhibit List contains 777 entries. 1 27-CV-10-28862 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM Hennepin County, MN appropriate, including in light of (1) ongoing discovery, (2) the Court's rulings on other motions filed by the parties, and (3) Defendant's exhibit list. Finally, the State reserves the right to use demonstrative exhibits not listed on the State's Second Amended Exhibit List. DATED: February 14, 2018 Respectfully submitted, LORI SWANSON Attorney General State of Minnesota /s/ Alethea M. Huyser Alethea M. Huyser (No. 0389270) Assistant Solicitor General 445 Minnesota Street, Suite 1100 St. Paul, Minnesota 55101-2127 (651) 757-1243 (Voice) (651) 282-5832 (Fax) alethea.huyser@ag.state.mn.us John E. Hall Anthony Herman Covington & Burling LLP One CityCenter 850 Tenth Street, N.W. Washington, D.C. 20001 (202) 662-6000 ATTORNEYS FOR PLAINTIFF STATE OF MINNESOTA 2 Plaintiff's Ex. No. 1001 1002 1003 1005 1008 1009 1010 1011 1012 1020 1025 1026 1028 1029 1031 1032 Date 3/28/1999 3/28/1999 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n L ette r from R. P urdy to 3M re: R esignation Em ail from R. Purdy to E. R einer et al. re: Rich P urdy's R e s ig n a tio n 3/29/1999 8/24/1948 Em ail from G. A d a m s to D. S onstegard re: 8e F o llo w up - Fish U.S. P atent O ffice, S im ons, J. H., F luorination o f O rg an ic Com pounds, U.S. Patent No. 2,447,717 9/26/1949 1/10/1950 8/22/1950 00/00/1952 3M Com pany Fluorochem icals Brochure Heptafluorobutyric Acid PFBA LD50 test (3M Toxicology) U.S. P atent O ffice, S im ons, J. H., E le ctrochem ical P rocess o f M aking Fluorine-C ontaining Carbon-C om pounds, U.S. Patent No. 2,519,983 State W ater Pollution Control Board, Report on the Investigation of Leaching of Ash Dumps: 3-87. 00/00/1953 9/26/1958 7/13/1960 8/9/1960 11/3/1960 4/14/1961 12/1/1961 00/00/1961 State W ater Pollution Control Board, Field Investigation of W aste W a te r In R elation to G round W a te r R eclam ation: 3-124. Report on Investigation of W aste Disposal M innesota Mining and M anufacturing Company, Chem olite Plant W ashington County Septem ber 22-26, 1958 M e m orandum from J. Brown to H. W essel re: P roposed Dum p Site Field le tte r o f A. M ille r and R. C o llins For G eo lo g y D e partm ent Use Only 3M Interoffice C orrespondence from J.T. Ling to V arious R ecipients re: C hem olite M onthly W a te r R eport w ith C entral Analytical Laboratory Report No. 3873 3M Life M agazine S cotchgard Ad 3M Interoffice C orrespondence from L.C. H oudek to H.S. Parkinson re: R ebuilding and R elocation o f S ew age Pond C hem olite Plant State W ater Pollution Control Board, Effects of Refuse Dumps On Ground W ater Quality Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00480715 3M_MN01427584 3MA01373218 STATE_07524645 3M_MN03109500 3MA02497530 STATE_07524631 N/A N/A 3MA01933815 3M_MN00000135 3MA00335929 3M_MN00052163 N/A 3MA00456329 N/A 1 Plaintiff's Ex. No. 1033 1035 1042 1043 1044 1046 1052 1053 1054 1058 1062 1064 1065 1068 1070 1079 1083 Date 4/1/1962 5/15/1962 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 3M Interoffice C orrespondence re: C hem olite W aste D isposal Program 3M Report No. 61-22, Supplem ent Pond Sealant Study 6/15/1963 7/10/1963 7/26/1963 12/2/1963 8/16/1966 9/21/1966 10/6/1966 12/2/1966 3/3/1967 Technical Inform ation 3M Brand Fluorochem ical Surfactants FC95, FC-98, FC-128, FC-134, FX-161, FC-170, FX-172 M e m o ra nd u m from M. C. G oldsm ith and K. H. K noblock to J. A. Brown re: the W oodbury T o w n ship D um p Site 3M Interoffice C orrespondence from K.R. Knoblock to J.A. Brown re: W oodbury T o w n ship D um p Site Present O perations (W oodbury Site) Em ail from J. T. Lins to D. R. G uthrie re: P roceed to C o n struct P hase II - W aste W a te r T re a tm e n t F acilities C h e m olite P roject No. 66-1354 AFE No. 8197 Report to M innesota M ining and M anufacturing Com pany Acute Oral Toxicity Studies on Two Materials Results of Residential W ell W ater Sam pling Village of Cottage Grove and W oodbury Township 3M C hronological H istory St. Paul - C hem olite - H utchinson W et Scrap Disposal 3M Interoffice C orrespondence from C.E. Kiester to W.W. W atson re: W et and Dry S crap D isposal at 3M Plants 6/26/1967 Letter from Dr. Ling to J. Leirfallom re: A pplication fo r P erm it to Appropriate W ater, 3M Property W oodbury Village, M innesota 11/30/1967 1/11/1968 2/12/1968 7/22/1969 6/15/1970 3M Interoffice C orrespondence from C.E. K iester re: O pen Field Burning W est Scrap Accum ulation W oodbury Meeting M inutes W oodbury Q uestions by J. Ling and C. Kiester Q uarterly Meeting - Board of Directors (3M) Supplem entary Engineering Report of Sludge Disposal at C hem olite prepared by R.A. Paschke (Environm ental and Civil E n g in e e rin g ) 3M Letter to the E ditor o f Fire Journal re: Lightw ater 2 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00456330 3M_MN00000380 3MA01201629 3MA00335832 3MA00335828 3MA00335802 3MA00456431 3MA01789595 3MA00512637 3MA00512611 3MA00337724 3MA00286355 3MA02603657 3M_MN00050139 3M_MN05374003 3MA00456474 3M_MN02267863 Plaintiff's Ex. No. 1085 1087 1088 1095 1098 1105 1106 1107 1109 1110 1116 1118 1119 1121 1123 1124 27-CV-10-28862 Date 10/23/1970 8/31/1971 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Authority for Expenditure for Sludge Dewatering at the C hem olite Sludge Dewatering Facility 3M Interoffice C o rre sp on d en ce from J.T. Ling to H.G. B ryce re: Ecological A spects of Fluorocarbons 9/13/1971 9/1/1972 4/26/1973 4/24/1974 4/24/1974 3M Interoffice C orrespondence from H.G. Bryce to R.M. Adam s re: E cological A spe cts o f F luorocarbons - y o u r m em o 7/14/71 Bioassay Report: Acute toxicity of Light W ater to bluegill (Lepom is marcochirus) 3M Interoffice C o rre sp on d en ce from C.E. K ie ste r to J.T. Ling re: W oodbury Disposal Site 3M Interoffice C orrespondence from L.F. Krank to D.W. Johnson, H.J. Van N oordw yk, and R.E. E dw ares re: [W ashington County] Landfill Dry Scrap Project Landfill Dry Scrap List. Day 1 4/25/1974 7/8/1974 Log of 3M trucks dum ping w aste at W ashington C ounty Landfill M e m orandum and a tta ch m e nt from D. S iddow ay, R. Rosen, and B. Fong to va rio us recipients: R eport on D isposal o f H yd ro fluo ric Acid 9/17/1974 2/24/1975 3M Perm it for Construction and Operation of Disposal System Disposal of Existing Stockpile of HF Tars 8/20/1975 8/29/1975 10/16/1975 G.H. C raw ford to L.C. Krogh et al., Record of a Telephone C o n versa tio n W ith W illiam G uy O f T he U niversity O f Florida re: Fluorocarbon In Blood S am ples From T e xas A nd N ew Y ork A cute Toxicity to Fish (Bluegill) C o ve r Letter from W arren S. G uy to R. A. M itsch and attached m anuscript 11/6/1975 12/5/1975 Central Analytical Laboratory, Fluorine-19 NMR of ten sam ples 1975 Field Letter re: M eeting w ith D uPont Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00456507 3M_MN03423905 3M_MN03423907 3M_MN01998404 3MA00336067 3MA00276827 3MA00276829 3MA00276832 3MA01201774 3MA00456576 3MA00214086 3MA10034962 3M_MN01658211 3MA00257421 3MA00967400 3MA10024380 3 Plaintiff's Ex. No. 1131 1132 1133 1135 1137 1138 1139 1140 1142 1143 1144 1145 1146 1148 1152 1153 1158 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 8/26/1976 9/16/1976 9/20/1976 11/18/1976 5/4/1977 5/17/1977 6/9/1977 7/1/1977 8/9/1977 8/10/1977 8/26/1977 10/19/1977 11/3/1977 11/30/1977 3M Interoffice C o rre sp on d en ce from B elisle to F re ie r re: Determ ination and Characterization of Trace Fluorochem icals Acute Oral Toxicity - Rats T-1585 from Bioresearch to 3M 3M Interoffice C o rre sp on d en ce from B elisle to Long re: Analytical Request A62781 3M Interoffice C orrespondence from T.E. Shannon to D.D. D w orak re: C hem olite HF T a r D isposal -- Final R eport Technical Report Sum mary, Analysis of Fluorochem icals from Belisle and D.F. Hagen to B.W. Nippoldt T e chn ica l R eport S um m ary: B ioconcentration o f FM 3422 in Bluegill S unfish and in C hannel C atfish Report to 3M Company, 28-day Oral Toxicity Study with FC-143 in A lb ino M ice 3M Interoffice C o rre sp on d en ce from R. C. Johnson to R. L. A hlne ss re: S um m ary O f W o rk A t C hem olite 3M Interoffice C o rre sp on d en ce from B elisle to F re ie r et al. re: F lu o ro che m ica ls in Blood Acute Toxicity to A quatic Invertebrates (Daphnia Magna) 3M C hro no lo g y - F lu o ro che m ica ls in Blood 3M Interoffice C o rre sp on d en ce from L. C. Krogh to J.D. La Zerte, 3M, re: P resentation to C orporate R esponsibility C om m ittee on P rogress - F lu o ro che m ica ls in Blood 3M Interoffice C o rre sp on d en ce from B elisle to F re ie r et al. re: F lu o ro che m ica ls in Blood Technical R eport S um m ary re: 1977 S um m ary 00/00/1978 1/9/1978 2/27/1978 Noordwyk, Hugh et al., M innesota M ining and M anufacturing C om pany's Hazardous W aste Program (1978) T echnical R eport S um m ary, Fate o f F lu o ro che m ica ls in the E nvironm ent, B iodegradation S tud ie s o f F lu o ro carb o ns - II, from E.A. R einer to D.L. Bacon T echnical R eport S um m ary re: A dsorption o f FC 95 and FC 143 on Soil 4 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00967404 3M_MN01688827 3MA00967406 3MA01201767 3MA01107188 3M_MN01640103 3M_MN01690370 3MA10035104 3MA10067223 3M_MN01658221 3MA10035028 3M_MN00000479 3MA00967424 3MA00016495 N/A 3M_MN03424083 3MA10036129 Plaintiff's Ex. No. 1162 1164 1165 1166 1168 1170 1171 1172 1173 1174 1175 1176 1177 1178 1179 1180 27-CV-10-28862 Date 3/22/1978 4/1/1978 4/1/1978 4/6/1978 4/12/1978 5/5/1978 5/8/1978 5/10/1978 5/16/1978 5/17/1978 5/31/1978 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 3M Interoffice C o rre sp on d en ce from H. J. Van N oordw yk re: Incinerator Ash and W astew ater Treatm ent Sludge Disposal Meeting M inutes 3M Light W ater Ad Brochure 3M Light W ater Ad Brochure 3M Interoffice C orrespondence from Belisle to Long re: FM3422 Rat Toxicity study Request A67820 3M Interoffice C orrespondence from Prokop re: M eeting M inutes - Fluorochem icals Technical R eview C om m ittee A cute O ral T o xicity (LD 50) S tudy in Rats FC -143 3M Interoffice C o rre sp on d en ce from J. M. O sbo rn e re: C hem olite Landfill M eeting M inutes and Status Report; File: C hem olite Sludge Disposal 3M Interoffice C orrespondence from Prokop re: R esults of Anim al Studies at I.R.D.C. C entral A na lytica l Laboratory R eport No. 6919 re: FC-143 Analysis of IRDC 137-090 Sam ples 3M Interoffice C orrespondence from Prokop re: M eeting M inutes - Review of Anim al Studies International Research and Developm ent Corporation, Fluorad Fluorochem ical Surfactant FC-95 6/1/1978 C hronic Toxicity to Fish (PFOA, FC-116, FC-169, or FC-143) 6/8/1978 3M Interoffice C orrespondence from Prokop re: M eeting M inutes from M ay 22, 1978 Meeting to R eview Recent Inform ation on F lu o ro che m ica ls in Blood o f W o rke rs and to Determ ine W hether this Poses a Substantial Risk Under TSCA 6/20/1978 7/19/1978 8/1/1978 M e m o ra nd u m re: Blood Levels o f RF/F in S elected E m ployees 3M Technical Report Sum m ary, Biodegradation Studies of F lu o ro carb o ns - III by R e in er to Bacon C entral A na lytica l L aboratory R eport No. 6962 re: FC in Blood by Belisle 5 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00282200 3M_MN01048940 3M_MN05340691 3MA10035579 3MA10067042 3M_MN01688767 3MA00281139 3MA10066961 3M_MN02343997 3M_MN00053074 3MA00404300 3M_MN01655650 3MA02607386 3M_MN01692291 3MA10054929 3MA00967481 Plaintiff's Ex. No. 1181 1184 1185 1191 1192 1193 1195 1196 1198 1199 1200 1204 1205 1208 1210 1211 27-CV-10-28862 Date 8/4/1978 8/16/1978 8/16/1978 12/18/1978 12/19/1978 1/2/1979 2/6/1979 2/14/1979 3/15/1979 3/20/1979 3/23/1979 4/26/1979 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n C entral A na lytica l Laboratory R eport No. 6967 re: IR D C 137 092: FC-95/Monkey Interim Site for Disposal of 3M C hem olite W astes Technical Report Sum m ary, Evaluation of the Bioconcentration Potential of FN 3422 by W elter Ninety-Day Subacute Rhesus M onkey Toxicity Study on Fluorad Fluorochem ical Surfactant FC-95 L ette r from R. S usag to C h a rle s S w anson re: 3M 's p ro cess in obtaining perm its and authorizations to operate landfill on Chem olite property Aborted FC95 Monkey Study 3M Internal C orre sp on d en ce from Belisle to Ubel re: Fluoride A nalysis of China Serum (A71011) 3M Interoffice C orrespondence from J.M. O sborne to D.E. Pederson re: S ources o f C adm ium , C hrom ium , and Lead Technical Report Sum m ary, Final C om prehensive Report: FC 95 by W elter FC-95, FC-143 and FM-3422 - 90 Day Subacute Toxicity Studies C onducted at IRDC - R eview of Final Reports and S um m ary Technical Report Sum m ary, Final C om prehensive Report: FC 143 by W elter 3M Interoffice C orrespondence from Prokop re: M eeting M inutes - Meeting with H.C. Hodges 5/3/1979 5/22/1979 6/7/1979 6/25/1979 An A cute Inhalation T o xicity S tudy o f T -2305 C oC in the Rat Technical Report Sum mary, Bioaccum ulation of F lu o ro che m ica ls in Tenn. R iver Fish by G agnon 3M Interoffice C orrespondence re: M eeting M inutes - M eeting with H.C. Hodge 3M L etter from M. S antoro (3M ) to J. H arthum (M P C A ) re: request for inform ation pertaining to disposal of m aterials at Oakdale dum psite Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN02343995 3MA00456675 3MA10066619 3MA10065004 3MA00280909 3M_MN01663513 3MA00967517 3MA00280139 3MA00176880 3MA00593073 3MA01410327 3MA00967775 3M_MN01688759 3MA01409559 3MA00592803 3M_MN00000353 6 Plaintiff's Ex. No. 1212 1213 1215 1216 1217 1220 1229 1231 1232 1233 1234 1235 1239 1242 1244 1246 1247 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 7/6/1979 7/23/1979 8/1/1979 8/1/1979 8/1/1979 8/27/1979 2/1/1980 3/12/1980 3M R iker Laboratories Interoffice C orrespondence from M. T. C ase to R. A. Nelson re: Fluorochem ical C h ro nic T oxicity D uP ont M em orandum from K usick to French re: D iscussion of Fluorochem icals with 3M Acute Toxicity to A quatic Invertebrates (Grass Shrim p) from PFOS A cute Toxicity to Fish (M um m ichog) from PFOS Acute Toxicity to A quatic Invertebrates (Eastern Oyster) from PFOS 3M Internal C o rre sp on d en ce from R. A. P rokop to S am Boyd et al. re: M eeting M inutes Jack Mandel & Leonard Schum an, An Epidem iologic M ortality Study of Em ployees at the C hem olite Plant O ral R a n ge fin de r S tudy o f T -2 9 9 8 C o C in P regnant Rats 6/5/1980 6/23/1980 7/10/1980 7/28/1980 8/15/1980 10/28/1980 11/25/1980 12/8/1980 12/18/1980 L ette r from M ichael B. A ye rs (M P C A ) to R ussell H. S usag (3M) re: requesting 3M subm it a detailed breakdow n o f w h a t specific 3M w astes w ere or w ere likely disposed at the O akdale dum psite T e chn ica l R eport S um m ary, D etection o f F lu o ro che m ica ls in D ecatur W astew ater by Mandel, Schrandt, and Gagnon 3M Interoffice C orrespondence from R.E. O ber to R.A. Prokop re: Rural C hinese M anuscript 3M Letter from O sborne to Paul Sm ith (M et C ouncil) re: 3M C h e m olite w a ste s form e rly landfilled in the interim h azardous w aste landfill at Chem olite Som e Probable Q uestions on 3M Fluorochem icals with Suggested Answers M PCA Division of Solid W aste Enforcem ent Section Status of Inve stig ative S tudy R elating to an Industrial W aste D um p in O a k d a le M CPA Status Report of O akdale Dump Site D ictation T aken from R uss S usag by Phone re: Points to D escribe 3M Invo lve m e n t w ith T h re e S ites in O akdale O ral T e ra to lo g y S tudy o f F C -95/P F O S in Rats 7 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00593079 3M_MN00053484 3M_MN01656873 3M_MN01656885 3M_MN01656900 3M_MN00000290 3MA00638775 3M_MN02327266 3MA00284881 3MA01406743 3MA10034975 3MA00456729 3MA00472445 3MA02604700 3MA00610634 3MA01248573 3MA00356530 Plaintiff's Ex. No. 1249 1250 1251 1252 1253 1254 1255 1256 1257 1259 1260 1261 1264 1266 1267 1275 Date 1/23/1981 2/12/1981 2/18/1981 2/24/1981 4/15/1981 4/17/1981 5/12/1981 5/29/1981 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n O ral T e ra to lo g y S tudy o f FM -3422 in Rats MPCA C om plaint Report at Cottage Grove 3M -Chem olite Plant re: burial o f fluorocarbons O ral T e ra to lo g y S tudy o f FM -3422 in Rats O ral R a n ge fin de r S tudy o f T -2 9 9 8 C o c in P regnant Rats Third D raft FC -143 D e ca tu r S tan d by P ress S ta te m e n t by L. Ludford re: M oving Fem ale W orkers R ecom m endation Regarding Fluorochem ical Exposure to Fem ales of C hildbearing Potential by Ubel Annual Meeting Board of Directors M innesota Mining and M anufacturing Com pany 3M Letter from Susag to Louis B reim hurst (M PC A ) re: A yers written request for inform ation on alleged disposal of w astes at C hem olite plant 6/16/1981 Belisle et al., C haracterization of Fluorinated M etabolites by a Gas C hrom atographic Helium M icrow ave Plasma D etector The Biotransform ation of 1H, 1H, 2H, 2H Perfluorodecanol to Perfluorooctanoate, Analytical Biochem istry 118, 336-343 9/4/1981 3M Internal C o rre sp on d en ce from J.W . Eberlin to J.R. Krall re: Recovery of Perfluorooctanoic Acid (FC-26) Bottom s (FZ-155) 9/8/1981 10/1/1981 11/18/1981 3M Internal C o rre sp on d en ce from L.F. Ludford to L.C. Krogh re: call w ith a n e w spa p er re p orte r in P ennsylvania abo u t A F F F A cute Toxicity to Fish (Fathead M innow ) from PFOS O ral R a n ge fin de r S tudy o f T -3 1 4 C o C in P regnant R abbits 12/14/1981 12/15/1981 8/12/1982 3M Internal C o rre sp on d en ce from Ubel to G riffith et al. re: Phone C onversation from Dr. M cK usick - D uPont - 12/14/81 O ral T e ra to lo g y S tudy o f T -2 9 9 8 C o C in Rats 3M Internal C o rre sp on d en ce from D.E. Roach to P.F. R iehle re: 1981 C hem olite Health Evaluations Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00011419 3MA00456742 3MA00326722 3M_MN01691720 3MA00047947 3MA00257790 3M_MN05371968 3MA00456743 3MA00509473 3MA00082742 3MA00065421 3M_MN01657269 3M_MN01691770 3MA00257805 3MA01508403 3M_MN01692296 8 Plaintiff's Ex. No. 1278 1279 1281 1282 1283 1284 1287 1290 1291 1292 1295 1298 27-CV-10-28862 Date 3/15/1983 4/8/1983 5/19/1983 5/20/1983 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n L ette r from M ichael T ib b e tts (M P C A ) Fred R obinette (3M ) re: Inspection of the 3M Chem olite Incinerator (SW -9) and Boiler Ash Disposal Site (SW -224) 3M Internal Correspondence from A. Norberg and W. Pearlson re: M inutes of Fluorochem ical Study C om m ittee M eeting March 16, 1983 3M L etter from J. O sbo rn e to M ichael T ib b etts (M P C A ) re: M P C A L etter dated M arch 15, 1983, concerning the M arch 3, 1983, M PCA inspection of C hem olite incinerator of the 3M C hem olite Incinerator (SW -9) and the Boiler Ash Disposal Site (S W -224) Fate o f F lu o ro che m ica ls - Phase II prepared by 3M Environm ental Laboratory, E.A. Reiner, Editor 5/20/1983 5/25/1983 7/13/1983 7/26/1983 8/16/1983 9/1/1983 1/11/1984 Letter from W eston S olutions to J. Pilney (3) re: tw o W eston reports with attachm ents Prelim inary Evaluation of Soil and G round-W ater A nalytical Data and Proposed W ork Plan Prelim inary Evaluation of "New" Drum Site C hem olite Plant 3M Internal C o rre sp on d en ce from R. L. Bohon to J.D. Lazerte re: Fate o f F lu o ro che m ica ls P hase II Questions and Answ ers on the Need for the Fate of F lu o ro che m ica ls Phase II S tudy Adm inistrative O rder by Consent and Response O rder by C onsent signed by Robert Adam s (3M) M inutes of M eeting Fate of Fluorochem icals A ugust 16, 1983 8:00 A.M. by W.H. Pearlson Technical Report Sum mary, Environmental Aspects of POSF by R e in e r L etter from Larry C h ristensen (M P C A ) to Joseph Ling (3M ) re: Notice of Violation, U.S. EPA and M PCA Hazardous W aste V io la tio n s 4/3/1984 L ette r from L. C h ristensen (M P C A ) to J. Ling re: Notice o f Violation, U.S. EPA and M PCA Hazardous W aste V iolations at the 3M C hem olite Facility, Cottage Grove M N D 006172969 9 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00296066 3MA10067173 3MA00296063 3MA10052935 WE10268751 3MA10065596 3M_MN00000204 3MA00283975 3MA10063227 3MA00193738 3MA00282920 3MA00282913 Plaintiff's Ex. No. 1304 1305 1306 1309 1312 1313 1315 1318 1322 1328 1329 1334 1337 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 6/27/1984 7/9/1984 7/13/1984 7/17/1984 3M Internal Correspondence from J.E. G agnon to D.M. S chnobrich re: O akdale Incine ra tor A sh Oil & G rease E xtracts Biodegradation (OECD 301E) of PFOS 3M Internal C orrespondence from L.H. H offm eier to R.C. Libey et al. re: T re a tm en t o f Fluorinated W astes at Chem . Ctr. Incinerator 3M Internal C o rre sp on d en ce from S antoro to H o ffm eier re: C hem olite Boiler Ash Landfill 8/31/1984 8/31/1984 Data Sum m ary Report on the Tests for Acute & Chronic Toxicity o f Fluorochem icals (FC -143) to D aphnia M agna (W ater Flea) 3M Internal C o rre sp on d en ce from D. Roach to P. Riehle re: O rganic Fluorine Levels 10/4/1984 1/3/1985 5/30/1985 11/00/1985 Rem edial Actions to Alleviate G roundw ater Pollution from a Form er Industrial W aste Disposal Site Presentation by Paschke, Santoro, and Allan Gebhard (Barr), for the 57th Annual C onference of the W ater Pollution Control Federation Report on Land A cquisitions for 3M W oodbury Site by Bruce Liesch Response O rder by C onsent for C hem olite Site, Cottage Grove, M innesota signed by Robert Adam s (3M) 3M Fluorad Fluorochem ical Surfactants Product Inform ation Brochure 11/15/1985 10/2/1986 8/29/1987 Letter from T. Kalitowski (M PCA) to M. Forsythe (Honorable C hair of House Appropriations Com m ittee) with M PCA Report on the Use of the Environmental Response, Com pensation and C om pliance Fund During Fiscal Y ear 1985 Industrial C hem icals Products Division Fluorad Brand Fluorochem ical Surfactant FC-143 Two Y ear Oral (Diet) Toxicity/Carcinogenicity Study of F lu o ro che m ica l FC -143 in Rats, V olum e 1 o f 4 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00300324 3M_MN01657233 3MA00067382 3MA00456910 3M_MN01639470 3M_MN03269963 3MA00296731 3M_MN00000222 3MA00840027 STATE_07543929 N/A 3M_MN01059198 3MA00027126 10 Plaintiff's Ex. No. 1338 1342 1343 1345 1346 1348 1349 1351 1353 1356 1357 1358 1359 1360 1362 1365 27-CV-10-28862 Date 9/00/1987 12/9/1987 1/5/1988 4/6/1988 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 3M Fluorad Fluorochem ical Surfactant FC-143 Product Information Brochure 3M Phone C onversation Report of Robert Gail with Roger P erkins re: R eview o f FC -143 final report: Leydig cell tu m o r incidence 3M Internal C o rre sp on d en ce from R. P erkins to F. G riffith re: Sum m ary of the Review of the FC-143 Tw o-Y ear Feeding Study R eport to be presented at the January 7, 1988 m eeting with DuPont Two Y ear Oral (Diet) Toxicity / Carcinogenicity Study of F lu o ro che m ica l FM -3924 in Rats, V olum e 1 o f 5 6/3/1988 8/11/1988 12/28/1988 12/30/1988 00/00/1989 2/23/1989 4/6/1989 4/25/1989 9/1/1989 10/5/1989 12/22/1989 00/00/1991 Letter from Boots & C oots to 3M re: Foam S ystem s Testing 3M Chem olite Hazardous W aste Manifest P art B. R C R A P erm it A pp lica tio n fo r 3M C om pany, M ND006172969, 3M Chem olite Center 3M Internal C orre sp on d en ce from E ric R einer re: FC-129 B io d e g ra d a b ility Jack Mandel & Leonard Schuman, Mortality Study at the 3M C hem olite Plant 3M M aterial Safety Data Sheet: FC-118 Fluorad Fluorochem ical S u rfa c ta n t L etter from J. M andel to L. Zobel (3M ) re: results o f the com parison of cancer incidence between the M innesota population and the U.S. w ith attachm ent Table 5: O bserved and Expected Deaths by Cause, S tandardizes M orality Ratio (SMR), 95 Percent C onfidence Lim its and CHi Square Values, Males, Chem ical Division Hunting Elevator Com pany RFRA 3M Brand Technical Inform ation for A FFF FC-783 M em orandum from R. P erkins to A. S ethre re: A m m onium Perfluorooctanoate TSCA 8(e) Subm ission 3M M aterial Safety Data Sheet: FC-118 Fluorad Fluorochem ical S u rfa c ta n t A Chem ical History of 3M 1933-1990 by M acKay 11 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. STATE_07543929 3MA10014327 3MA00631017 3MA00593233 3M_MN01315290 3M_MPCA00006608 3MA00152550 3MA10035965 3MA00632297 3MA00202500 3MA00632313 N/A 3M_MN02369894 3M_MN02323182 3M_MN01044772 3MA00005401 Plaintiff's Ex. No. 1368 1369 1370 1372 1373 1374 1376 1378 1384 1386 1387 1388 1391 1402 1403 1404 27-CV-10-28862 Date 4/1/1991 5/10/1991 00/00/1992 2/5/1992 2/28/1992 6/5/1992 8/28/1992 9/15/1992 12/16/1992 12/30/1992 9/00/1993 1/18/1993 3/6/1993 8/3/1993 9/1/1993 9/1/1993 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Study Sum m ary of Environm ental Effects of Light W ater Brand A FFF and C om ponents - 1991 3M Internal C o rre sp on d en ce from L. Zobel to G. D am erell et al. re: C hem olite Exam inations, Fall, 1990 The Solution to Y our Problem s 3M Brochure 3M Internal C o rre sp on d en ce from R. How ell to C. O lsen re: F lu o ro che m ica ls in the E nviro nm e n t w ith a ttachm ents L ette r from D. Hall (M P C A ) to R. B rin g er (3M ) w ith A uth o riza tion to Discharge and to Constrict, Install and O perate a W astew ater Disposal System Product Toxicity Sum m ary Sheet Fluorad Brand Fluorochem ical Surfactant FC-95 Letter from J. W allrath (D uP ont H um an R esources) to Y. P ow er (W ashington W orks Polymers) with Interpretation of Epidem iologic Surveillance Data 3M Internal C o rre sp on d en ce from R. How ell to C. B urton re: Environmental Concerns with Fluorochem icals 3M Internal C orrespondence from T. A she n m a che r to R. A. P aschke et al. re: W oodbury U pdate R eport T ra n sm ittal o f M e m orandum from Dale B acon to B ute n ho ff re: Fluorochem icals Gilliland FD and Mandel JS. 1993. Mortality among em ployees of a perfluorooctanoic production plant. Journal of O ccupational Medicine 35:950-954. Environm entally Responsive Functional Fluorochem icals by Tony Manzara R eport on 3M Corp. P rogram s in E nvironm ental T o xico lo g y by John P. G iesy 3M Internal C o rre sp on d en ce from R. M. Flynn to C. A. Burton et al. re: ECM M eeting Notes w ith attachm ents PFOS as Pesticide Frank G illiland & Jack Mandel, M ortality Am ong Em ployees of a Perlfuorooctanoic Acid Production Plant Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN01657097 3M_MN01692315 STATE_07543929 3M_MN00000001 M N.103.0639.000439 3M_MN02252650 N/A 3MA00323897 3M_MN00039613 3M_MN03108995 N/A 3M_MN02470086 3M_MN04734387 3M_MN02470101 3M_MN02470063 3MA00631764 12 Plaintiff's Ex. No. 1408 1409 1413 1415 1418 1420 1421 1431 1445 27-CV-10-28862 Date 11/18/1993 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n PFOS, with sections for Disposition, Toxicity Considerations, Environm ental Consideration, Kinds of Studies for Human PFOS Aspect 12/7/1993 3M Internal C orre sp on d en ce from J. M andel to Fluorochem ical S teering C om m ittee M em bers re: Papers/D r. G illiland w ith a tta ch m e n t "P eripheral Blood Lym phocyte C ount in Men O ccup a tion a lly E xposed to P erfluo ro ctan o ic A cid " by F. G illiland 4/3/1994 4/19/1994 5/13/1994 7/18/1994 9/6/1994 3/13/1995 12/14/1995 3M Interoffice M e m orandum from K. G oebel to I. D enenholz re: List of questions of several fluorochem ical products Fluorine Health/Environm ental Concerns; FC Concentrations Factors Affecting These Concerns; Proposed Program Operational Com m ittee Draft Health Hazard Sum m ary of Perfluorooctane Sulfonic Acid, Potassium Salt as Represented by FC-95 Locations and Data From Avian Blood Plama Sam ples by John P. G iesy Health Hazard Sum m aries and Proposed Testing Program for Several 3M Fluorochem icals 3M M orality S tudy o f E m ployees at 3M P lant in Decatur, Alabam a M ajor Vision Obstacle Num ber 1 1446 1451 V a rio u s 5/20/1996 M aterial Safety Data Sheets. 1984, 1989, 1990, 1995, 1996, 1997, 1998, 2000 3M M aterial Safety Data Sheet: FC-118 Fluorad Fluorochem ical S u rfa c ta n t 13 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA10037365 3M_MN00051484 3M_MN04741126 3M_MN00000367 3MA10064687 3MA01404531 3M_MN02345238 3M_MN01661790 3MA00089191 3MA01543444; 3MA01452579; 3MA00085087; 3MA01622491; 3MA01946892; 3MA10082349; 3MA00087197; 3MA00082405; 3MA00202819; 3M_MPCA00041106 3MA10057753 Plaintiff's Ex. No. 1457 1459 1460 1461 1466 1467 1469 1471 1476 1479 1482 1486 1488 1489 1493 1496 1502 1504 27-CV-10-28862 Date 9/17/1996 10/24/1996 10/25/1996 11/12/1996 12/12/1996 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 3M Internal C o rre sp on d en ce from E. R einer to M. S hiba re: RCRA Em ail from E. R e in er re: D raft F luorochem ical W aste D isposal G u id a n ce 3M Internal Correspondence from Eric R einer to Scott Strand et al. re: M ore Ideas on D raft Fluorochem ical W aste D isposal G u id a n ce Em ail from T ony M anzara to W endling et al. re: V isit to D uP ont 11/12/96 - Technical Im pressions of 3M Fax M essage re: ca rcinogenicity label o f FC -143 / 1996 Fax and M inutes o f Call w ith Dr. Jung Em ail from E. R e in er to S cott S trand, R obert H owell, and Jam es 12/12/1996 Johnson re: D raft Fluorochem ical W aste Disposal G uidance 1/10/1997 V a rio u s 11/5/1997 00/00/1998 1/16/1998 A cute O ral T o xicity S tudy o f T -6 6 69 in Rats (O E C D G uidelines) 3M M aterial Safety Data Sheet: FC-118 Fluorad Fluorochem ical S urfactant fo r February 7 & 19, 1997 3M M aterial Safety Data Sheet: FC-118 Fluorad Fluorochem ical S u rfa c ta n t D raft M e m o ra nd u m re: F lu o ro che m ica ls in H um an Blood Em ail from L. Zobel to J. B ute n ho ff re: F luorochem ical P rojects U n derw ay in the E nvironm ental Laboratory 2/9/1998 2/26/1998 2/28/1998 3/18/1998 3/20/1998 E stim ation o f "S afe" R eference Level (ppb) fo r PFO S in Plasm a FDA C om m unications Plan; EPA C om m unication Plan Toxicology Contribution to W hite Paper by John Butenhoff PO SF/C8 Acid Cell Hour Production W orksheet M em orandum from C. Reich to TSC A 8(e) C om m ittee m em bers re: T S C A S ection 8(e) Decision 5/1/1998 Environm entally Relevant Properties of 3M Fluorochem icals 5/8/1998 S creening o f PFO S levels in E agles and A lb a tro ss - 3M Environm ental Laboratory Fluorine Analytical Chem istry Team 14 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A 3MA10051804 3MA10051796 3M_MN02470157 3M_MN03591099 3MA01410733 3M_MN01688780 STATE_07543958 3MA00203395 3MA10082645 3MA00906295 3MA01366219 3MA10063015 3MA10072182 3M_MN04782935 3MA10064459 3MA10071137 3MA01404534 Plaintiff's Ex. No. 1519 1523 1526 1527 1529 1531 1533 1534 1535 1558 1571 1575 1585 1586 1587 1588 1589 27-CV-10-28862 Date 9/1/1998 10/16/1998 11/4/1998 11/9/1998 11/16/1998 11/25/1998 12/3/1998 12/3/1998 12/10/1998 2/5/1999 4/8/1999 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Em ail from D. S chnobrich to M. Falco et al. re: FC's and Past Disposal Sites O ccurre nce o f P erfluorooctane S ulfo n ate (P FO S ) in W ildlife P art I. E agles and A lb a tro sse s by Rich Purdy 3M M aterial Safety Data Sheet: FC-118 Fluorad Fluorochem ical S u rfa c ta n t B oard o f D irectors P resentations N o ve m b e r 9, 1998, A ugust, 1998, FC Issues 3M Internal C o rre sp on d en ce from D. S an d ers to M. M cK erlie re: A tta c h e d P athology R eview o f R eported T u m o rig e n e sis in a Tw o Y e a r S tudy o f FM -3924 in Rats Email from R. Purdy to G. A da m s re: Risk to the environm ental due to the presence of PFOS with attachm ent Pioneer Food Chain Risk A ssessm ent of PFO P io ne e r R isk A s se ssm e n t o f A d ve rse E ffects in M arine M am m als fro m PFO S in the Food C hain by Rich Purdy Science Publication Strategy The Science of O rganic Fluorochem istry Letter from M. A sh to D. S onstegard re: Purdy return to 3M 4/23/1999 5/20/1999 5/21/1999 5/24/1999 PFO S Environm ental Risk: Potential TS C A 8( e ) S ubstantial risk 3M Internal C o rre sp on d en ce from D. S an d ers to D. Bacon et al. re: M eeting M inutes o f FC C ore Team - M ay 14, 1999 Laboratory R eport: A n a lysis o f FCs in S am ples o f C h ild re n 's Sera 3M - FC Issue C om m unications Plan 5/26/1999 Letter from C. Reich to Office of Pollution Prevention and Toxics of the EPA - TSC A 8(e) Supplem ental Notice on: SulfonateBased Fluorochem icals Docket Nos. 8EHQ-1180-373; 8EHQ1180-374; 8EHQ-0381-0394; 8EHQ-0598-373 5/26/1999 Em ail from D. G raham to T. B altutis re: F-6002 w a ste w a ter Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN00498519 3MA01404529 3M_MN02892806 3MA10081840 3M_MN02980584 3MA10025147 3MA00242688 3MA10031581 3MA00729193 3MA00523419 3M_MN05336314 3MA01238114 3MA01404555 3MA00659721 3M_MN04732222 3M_MN01329658 3M_MN02465688 15 Plaintiff's Ex. No. 1595 1599 1612 1615 1616 1617 1618 1630 1633 1645 1653 1657 1664 1665 1667 1668 1669 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 6/16/1999 7/9/1999 8/31/1999 9/30/1999 9/30/1999 10/1/1999 3M Internal C o rre sp on d en ce from D. S an d ers to T. D iP asquale e t al. re: FC Issues C ore T eam M eeting M inutes - Ju ne 8, 1999 Em ail from R. Purdy to J. W a lk e r re: F-chem 3M Internal Correspondence from G. Adam s to EHS&R W orking G roup re: EH S &R M inutes fo r A u g u st 10, 1999 Products of incom plete com bustion of POSF Based Fluorochem icals Em ail from S anders to Perry Logan et al. re: D ecatur FC E xposure A s se ssm e n t - P resentation at IH C onference Sum m ary PFOS Oral Rat Toxicology Screen 10/1/1999 11/23/1999 12/15/1999 2/2/2000 3/1/2000 3/16/2000 4/10/2000 4/11/2000 4/20/2000 4/21/2000 4/21/2000 Em ail from G. O lsen to P. Logan re: P resentation o f FC Papers Em ail D. M andel on b e h a lf o f Dave S an d ers to J. B ute n ho ff et al. re: S cie ntific P ublication S trategy attaching S cie ntific Publication Strategy, Proposals Draft Inform ation fo r all Dyneon Em ployees 3M W aste Stream Profile Program C over Sheet (w3580) for Cottage Grove S ulfonated P erfluo ro ch em icals in the E nvironm ent: S ources, Dispersion, Fate and Effects report Identification o f F lu o ro che m ica ls in S era o f C hildren in the United States C harlie A uer Telephone Call Handwritten Email from C. A u e r to D. H akes re: Follow -up on Perfluorochem icals Request L etter from L. Zobel to O . H e rnandez re: W riting to C larify Inform ation contained in the tw o -g en e ra tion reproduction Attachm ents to April 2 1 ,2 0 0 0 letter to C. A uer from W. W eppner | (Radiolabel Oral Absorption and Intravenous P ha rm aco kin etics S tud ie s in Rats) Attachm ents to April 2 1 ,2 0 0 0 letter to C. A uer from W. W eppner | (Dermal Absorption and Intravenous P ha rm aco kin etics in R abbits) Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA10082287 3MA00245904 3MA00927118 3MA01412209 3MA01540632 3M_MN02336490 3MA00004617 3MA00467427 3M _M N 01524232 3M_MPCA00033120 3MA00045043 3M_MN01661880 3MA00470824 3M_MN02457016 3MA00517725 3MA00251390 3MA00251391 16 Plaintiff's Ex. No. 1670 1671 1674 1679 1681 1682 1683 1684 1685 1690 1691 1694 1698 1703 1704 1707 1716 1717 1718 1719 1720 27-CV-10-28862 Date 4/21/2000 4/21/2000 4/27/2000 5/3/2000 5/4/2000 5/5/2000 5/8/2000 5/9/2000 5/9/2000 5/16/2000 5/16/2000 5/16/2000 5/16/2000 5/19/2000 5/19/2000 6/5/2000 6/26/2000 6/27/2000 6/27/2000 6/28/2000 6/28/2000 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n A ttachm ents to April 2 1 ,2 0 0 0 letter to C. A uer from W. W e p p n e r | (T e ra tolog y S tudies in Rats and R abbits) A ttachm ents to April 2 1 ,2 0 0 0 Letter to C. A uer from W. W eppner (M edical Surveillance and Epidem iology) L ette r from R. S ussm an (Latham & W atkins) to C. A u e r re: M eeting with 3M April 28, 2000 Letter from J. B utenhoff to J. Seed (EPA) re: S erum M easurem ents for A rgus Studies 418-013 (through Lactation) and 418-015 (during Gestation) Letter from W. W e p p n e r to C. A u e r re: Inform ation on Perfluorooctane Sulfonate with several attachm ents Em ail from C. A u e r to D. H akes et al. re: Follow -up on Perfluorochem icals Meeting on April 28 Handwritten notes 3M Fluorochem ical EHS & R Initiative Chuck Kiester's Board of Directors Presentation Annual Meeting Board of Directors M innesota Mining and M anufacturing Com pany 3M Phasing out Som e of Its S pecialty M aterials Em ail from C. A u e r to B. W e p p n e r re: P ha se -o ut o f PFO S Press Release 3M Phasing out Som e of Its S pecialty M aterials with handwritten notes 3M SEC Form 8-K EPA S ays it Pressured 3M o ve r S cotchgard C hem ical Email from T. S loan to T. B rooks et al. re: The N ew Y ork Tim es A rticle Today about the EPA's V ersion of W hy W e Abandoned O ur FC's... BusinessW eek, 3M 's Big C leanup Sum m ary of W ork Performed for the German G overnm ent A gency fo r M ilitary Technology and Procurem ent on Fire Extinguishing Foam C om pounds from M ultiple Com panies A cute Toxicity to Fish (Bluegill Sunfish) Acute Toxicity to A quatic Invertebrates (Daphnia Magna). Acute Toxicity to Invertebrates (G rass Shrimp) Acute Toxicity to A quatic Invertebrates (Eastern Oyster) 17 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00251392 3MA00251393 3M_MN02457023 3MA00254228 M N.039.0016.000280 3MA01135534 3MA00469749 3M_MN05367080 3M_MN05367814 3M_M N02345284 3M_MN02457072 3MA01169714 N/A 3M_MN03112642 3MA01190648 3M_MN02492758 3M_MN01657796 3M_MN00436402 3M_MN01656831 3M_MN00437323 3M_MN00437343 Plaintiff's Ex. No. 1721 1725 1726 1728 1731 1734 1735 1736 1737 1740 1749 1758 1762 1763 Date 6/30/2000 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n DuPont Haskell Laboratory Visit Meeting M inutes 7/1 1 /20 0 0 O ral D evelopm ental T o xicity (Teratology) in Rats and R abbits 7/11/2000 7/12/2000 7/25/2000 S erum F luorochem ical tre nd s o f o ut-o f-co un ty residents in C LU E I (1974) and C LU E II (1989) e pid e m io lo g ic in ve stiga tio ns Email from D. G raham to S. Kruse et al. re: Draining C8 A cid to Sewer Email from M. E lnabaraw y to M. S antoro re: S creening-Level R isk A sse ssm e n t fo r O rg an o fluo rine S ub sta nce s in P hilippines W ell W ater 8/21/2000 L etter from K. Reed to J. B askerville re: 3M C o m p an y T S C A Section 8(e) Com pliance A udit - Disclosure of Phase One Findings Pursuant to "Incentives For Self-Policing, Discovery, Disclosure and Correction and Prevention of Violations," 65 Fed. Reg. 19618 (A pr.11,2000) 8/21/2000 Current CG FC W aste Status (221272 lbs./yr. as of 8/21/00) 8/21/2000 8/21/2000 9/9/2000 12/26/2000 2/20/2001 3/1/2001 3/2/2001 Letter from K. Reed to J. B askerville w ith a tta ch m e n t re: 3M Com pany TSC A Section 8(e) C om pliance A udit - Disclosure of Phase One Findings Pursuant to "Incentives For Self-Policing, Discovery, Disclosure and C orrection and Prevention of Violations," 65 Fed. Reg. 19618 (Apr. 11,2000) L etter from K. Reed to D ocum ent P rocessing C e n te r (7407) re: TSC A Section 8(e) Supplem ental Subm issions: Docket Nos. 8EHQ-1180-373 and 8EHQ-1180-374 Email from J. G iesy to D. Bacon re: m anuscript [E xcerpt] Em ail from D. Bacon to K. Reed re: S tu ff w ith a tta ch m e nt 3M SEC 10-K for the year ended Decem ber 3 1,2 00 0 3M Internal C orrespondence J. B utenhoff to M. Santoro re: Draft Drinking W ater Health Advisory (DW HA) - PFOS L etter from C u n nin g ha m (T oxicological S ciences) to J. B utenhoff (3M) re: ToxS ci 01-002 18 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00469911 3M_MN01660801 3M_MN01661883 3MA01623209 3M_MN01020427 3M_MN01257572 3MA00043765 3MA01220040 3MA01220047 3MA00198538 3MA00186126 N/A 3MA00812416 3M_MN02337242 Plaintiff's Ex. No. 1764 1780 1781 1782 1783 1784 1785 1787 1793 1798 1799 1806 1812 1814 Date 3/7/2001 5/30/2001 6/1/2001 6/1/2001 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Em ail from M. S antoro to F. P alensky et al. re: C o ttage G rove W ells Email from M illet to G regory et al. re: U.S. News and W orld Report Magazine Reporter Email from M illet to R enner re: D raft Phase O ut S chedule for Reporter Draft - Phase Out Tim eline 6/1/2001 6/13/2001 6/19/2001 7/3/2001 9/5/2001 10/9/2001 TSC A Section 8(e) C om m ittee Meeting - Record of Proceedings L etter from K. Reed (3M ) to A. P ontius (E P A) re: 3M C om pany TSCA Section 8(e) C om pliance A udit -- Disclosure of Phase Two Findings Centre Analytical Laboratories, Analytical Report: Fluorochem ical Characterization of W ater Sam ples - Cottage Grove Potable W ater Evaluation (E01-0812) Em ail from M. S antoro to P alensky et al. re: C ottage G rove W ells Draft FC C om m unications Plan 2001-2002 Letter from C lark (EPA) to H atcher (3M) 10/11/2001 11/9/2001 12/18/2001 1/1/2002 O lsen GW, B urlew MM, Burris JM, and M andel JH. 2001. Final report: Epidem iology, 220-3W -05: A longitudinal analysis of serum perfluorooctanesulfonate (PFOS) and perfluorooctanoate (P FO A ) levels in relation to lipid and hep a tic clinical chem istry test results from m ale em ployee participants of the 1994/95, 1997, and 2000 fluorochem ical medical surveillance program. Em ail from D. S chn o brich to L. Zabel et al. re: C ordova FC W aste M anagem ent Review Thom ford, Peter, Final Report: 26-W eek C apsule Toxicity Study w ith A m m o n iu m P erfluo ro o cta n oa te (A P FO ) in C yn o m olgu s Monkeys Report (Covance 6329-231) P rotocol A m e nd m e n t: C a n ce r Incidence in 3M W o rke rs Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN00000806 3M_MN05342352 3M_MN05342355 3M_MN05367921 3MA02608788 3MA01246311 3MA00853349 3MA00001371 3MA02512798 3MA00383888 3M_M N02482163 3MA00000982 3M_MN02343342 3M_MN02291548 19 Plaintiff's Ex. No. 1818 1822 1823 1824 1831 1833 1836 1845 1848 1855 1864 1872 1881 1883 1887 1889 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 1/11/2002 2/1/2002 2/5/2002 2/18/2002 3/6/2002 3/8/2002 3/11/2002 8/6/2002 9/4/2002 10/17/2002 11/15/2002 1/1/2003 2/10/2003 2/13/2003 3/10/2003 4/7/2003 Thom ford, Peter, Final Report: 26-W eek C apsule Toxicity Study with Perfluorooctane S ulfonic Acid Potassium Salts (PFOS; T6 295) in C yn o m olgu s M o n keys R eport (C ovance 6 32 9-223) 3M Cottage Grove M egaphone February 2002: Volum e 54, Number 2 U.S. Environm ental Protection Agency A pplication for Perm it to Discharge W astew ater Existing M anufacturing, Com m ercial, Mining and Silvicultural O perations Form 2C NPDES, M ND006172969; signed 3M Draft Talking Points Cottage Grove W ells Em ail from D. K riens to D. D ouglas & M. Rys re: 3M -P F O S and related co m p ou n ds in discharge Email from D. S chnobrich to S. E thier et al. re: P F O S /P F O A at Cottage Grove 3M SEC 10-K for the year ended Decem ber 31,2001 O ffice M e m orandum from D. W etzstein to R. M essing and L. G ust (M D H ) re: R equest fo r D evelopm ent o f Industrial Soil HBV for PFOS & PFOA Compounds C ancer Benchm ark Dose Calculation for Fluorochem ical-143 (FC-143): Am m onium Perfluoroctanoate S ubsurface Investigation W ork Plan Neutralized HF T a r (D1) Disposal Area 3M C ottage Grove Facility Report Draft sum m ary of PFOA exposure Chronology, Off-Site W aste Disposal Locations - 3M Cottage Grove, M innesota M e m orandum from D. C om eau and P. B ook (ER G ) to D. D ouglas and M. R hys (M P C A ) re: 3M C ottage G rove; A re a D1 Initial G roundw ater Sam pling Results M e m orandum from D. C om eau and P. B ook (ER G ) to D. D ouglas and M. Rys (M P C A ) re: 3M C ottage G rove; A re a D1 Initial G roundw ater Sam pling Results 3M SEC 10-K for the year ended Decem ber 31,2002 Email from J. G iesy to D. Bacon and W. R eagen re: P aper 20 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN03278834 3MA00064713 3MA00110772 3MA00469948 STATE_02795011 3MA01376827 N/A STATE_02338983 3M_MN02339249 3MA00048084 3M_MN01526194 3MA01243198 3MA00046947 3M_MN01010361 N/A 3MA00194174 Plaintiff's Ex. No. 1897 1898 1907 1908 1910 1912 1918 1920 1925 1926 1927 1928 1930 1932 1933 1937 1938 1939 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 5/7/2003 5/7/2003 8/1/2003 8/5/2003 8/7/2003 9/15/2003 10/27/2003 11/13/2003 12/22/2003 12/22/2003 12/22/2003 12/22/2003 Em ail from M. G ravdahl to D. S chnobrich re: PFO A P roduction Letter from M. S antoro (3M ) to W. P enberthy (EPA) re: Follow up Q uestions Regarding 3M and Dyneon LOI Environm ental M onitoring Com m itm ents Letter from M. S antoro (3M ) to U.S. EPA re: S ubm ission of M onitoring Data Pursuant to the 3M LOI Dated March 13, 2003 and A P F O Users LOI Dated M arch 14, 2003 Em ail from D. D ouglas to B. B rott et al. re: EPA Risk Assessm ent for PFOS/PFOA Draft Talking Points Cottage Grove W ells Em ail from D. D ouglas (M P C A ) to J. Kelly (M D H ) et al. re: M onitoring of PFOA/PFOS Em ail from T. Fasking (3M ) to R. M ark (M P C A ) et al. re: P FO A production in C ottage G rove L ette r from D. D ouglas (M P C A ) to T. Fasking (3M ) re: 3M C hem olite Superfund Site L ette r from V. Y ingling (M D H ) to L. B au e r and N. B auer Letter from V. Y ingling (M D H ) to D. Eilers Letter from V. Y ingling (M D H ) to D. H endrickson L etter from V. Y ingling (M D H ) to J. T schida and P. T schida 1/2/2004 Em ail from D. D ouglas (M P C A ) to B. Brott (M P C A ) et al. re: Prelim inary results for PFOA at W ashington C ounty Landfill 1/26/2004 1/27/2004 2/12/2004 2/13/2004 2/25/2004 L ette r from R. P aschke (3M ) to D. D ouglas (M P C A ) re: C o n sen t O rder Addendum and Facility-wide Fluorochem ical Investigation W ork Plan, 3M C ottage G rove Site Facility-W ide Flourochem ical Investigation W ork Plan 3M Cottage Grove T o xicity T e st Final R eport E vent 1, E 04-0120 Em ail from D. D ouglas (M P C A ) to B. Brott (M P C A ) et al. re: 3M Cottage Grove Toxicity Test Final Report Event 2, E04-0126 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00044477 3MA00888342 3MA00048383 STATE_02468135 3MA02600510 STATE_02468963 3MA00406699 M N.303.0085.000274 STATE_01524662 STATE_01524663 STATE_01524664 STATE_01524665 STATE_02496240 3M_MN00044012 3MA00046844 3M_MN01538387 3M_MN00044031 3M_MN01539152 21 Plaintiff's Ex. No. 1940 1941 1942 1946 1948 1949 1955 1957 1958 1959 1964 1966 1969 1972 1976 1979 1984 1985 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 6/20/2001 New environm ental toxin destroys the liver - translated article 3/1 2 /20 0 4 Em ail from P. B ook to T. Fasking and D. C om eau re: C grove list 4/1/2004 4/26/2004 6/21/2004 6/29/2004 7/20/2004 7/23/2004 7/26/2004 7/29/2004 9/14/2004 9/27/2004 10/12/2004 10/15/2004 11/8/2004 11/21/2004 12/1/2004 12/8/2004 Exygen Research, Fluorochem ical Characterization of Aqueous Sam ples W oodbury Com bined Main FC M onitoring (E04-0241) L etter from B. Brott (M P C A ) to T. Fasking (3M ) re: Reim bursem ent of M innesota Pollution Control A gency Costs for the 3M C hem olite State Superfund Site MDH Environm ental Laboratory, M PCA Closed Lanfill Assessm ent Meeting Between KEMI and 3M: Human Risk Characterization for PFOS MDH Chain of C ustody Form Em ail from D. D ouglas (M P C A ) to D. K riens (M P C A ) re: 3M Cottage Grove/Call from Bob Paschke Letter from T. Fasking (3M ) to M. Rys (M PC A ) re: O akdale Disposal Site Email from R. P aschke to M. S antoro et al. re: Phone conversation with Dave Douglas, M PCA FC Core Team 2004 - 2005 Project / Process Priorities Email from J. B utenhoff to M. Falco re: Notes on Proposal to NTP Em ail from M. Falco (3M ) to L. W e n dling (3M ) et al. M P C A and 3M m eeting re: P erfluorochem icals Em ail from L. Zobel to J. B ute n ho ff re: Files A ssociate d w ith Stockholm University Bruce A lexander, Final R eport: B la dd e r C a n ce r in Perfluorooctanesulfonyl Fluoride M anufacturing W orkers Letter from T. Fasking to M. Rys re: O akdale P um p-out S ystem Discharge Fluorochem ical Sam pling Em ail from I. V erha g en to S. R uotsinoja re: Inte rvie w w ith M P R PFOA tim eline at W ashington C ounty Landfill Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00452308 3MA00048348 3M _M N00719367 3M_MN00721525 STATE_02091948 3M_MN02317718 M N.303.0003.000060 STATE_02803858 3MA00348164 3MA00886748 3M_MN00838661 3MA00955624 3MA01554012 STATE_02328450 3MA00408335 3MA00755705 3MA01932893 STATE_01200544 22 Plaintiff's Ex. No. 1986 1988 1989 1993 1994 1995 2004 2009 2012 2017 2033 2035 2040 2041 2044 2045 2046 2049 2057 27-CV-10-28862 Date 12/10/2004 00/00/2005 00/00/2005 1/24/2005 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Letter from M. Rys to R. Paschke, 3M, re: O akdale P um p-out System Discharge Fluorochem ical Sam pling Letter Dated D ecem ber 1,2 0 04 , O akdale Disposal Site (the Site) 3M Talking Points - Oakdale W ells 3M 's FC C om m ittees Chart MDH. Q uestions About the O akdale Public W ater Supply 1/24/2005 1/25/2005 2/1/2005 2/18/2005 2/23/2005 3/9/2005 5/26/2005 6/8/2005 6/30/2005 7/1/2005 8/2/2005 Pictures of Scotchgard from M innesota Public Radio website, http://news.m innesota.publicradio.org/features/2005/01/25_bens o n l_ o a k d a le / Plastics Europe - Q&A On PFOA Edgerly, Mike et al., T oxic Traces, M innesota Public Radio (2005) Health C onsultation 3M C hem olite Perfluorochem ical Releases at the 3M - C ottage Grove Facility Email from S. E thier to R. P aschke et al. re: Fw: M PR C om m ent from W ebsite SKB Environm ental, SKB Rosem ount Industrial W aste Facility (2005) 3M FC M anufacturing Update W eston Off-Site W aste Disposal Locations Table - 3M Cottage Grove, M innesota M PCA PFC Investigation June 30, 2005 Letter from J. H atcher to D. Ziegel re: A dditional Data and Revised Draft C onsent A greem ent and Final O rder Email from M. G aetz to T. Fasking & T. G allow ay re: Fw: Cottage Grove Sludge Sam ple Results 8/4/2005 8/10/2005 8/26/2005 10/15/2005 Em ail from M. G eetz to G. H ohenstein re. C ottage G rove Sludge Background Inform ation on PFOS and PFOA 3M Fluorochem icals Chronology and Various Tim elines MPCA, Prelim inary results of the M PCA PFC Investigation with 2 attachm ents Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00344317 STATE_02496227 3M_MN00000703 3MA00513900 N/A 3M_MN01525833 3MA01169469 3MA00383006 3MA01242570 WE10336422 3MA01870504 3MA00511276 STATE_01998653 3M_MN00053740 3MA01326865 3MA00866656 3MA00550095 3M_MN04769925 STATE_01998636 23 Plaintiff's Ex. No. 2072 2078 2081 2083 2084 2085 2088 2093 2095 2096 2097 2099 2102 2119 2125 2127 2130 2132 2133 27-CV-10-28862 Date 1/7/2006 2/1/2006 2/12/2006 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n S .B each, S.A., et. al. E cotoxicological E valuation o f Perfluorooctanesulfonate (PFOS). Reviews of Environm ental Contam ination and Toxicology (2006) Letter from G. M illet to R. C heng re: R esponse to em ail dated January 23, 2006 Em ail from J. G iesy to D. Bacon re: E S& T P aper 2/16/2006 2/17/2006 2/21/2006 3/7/2006 3/28/2006 4/1/2006 4/24/2006 4/26/2006 5/25/2006 6/14/2006 10/27/2006 FC C om m unications Michael Santoro 3M Regulatory Affairs M em orandum from J. G iesy to D. Bacon re: Follow up to February 2, 2006 m eeting (revised memo) Em ail from J. G iesy to D. Bacon re: re: chironom id study D R AFT Key Points - C ottage G rove Fish Data MDH, News Release, Revised fish consum ption advice issued fo r bluegill sunfish in Pool 2 o f the M ississippi R iver Fluorochem ical (FC) Data A ssessm ent Report by W eston Settlem ent agreem ent between 3M and the U.S. Environm ental Protection Agency. Em ail from S. S an ch ez to F. P alensky et al. re: N ew s C o verage TSCA Em ail from T. D iP asquale to T. Boardm an et al. re: 3M and EPA Press Release C ost-benefit analysis of repeating the chronic study of the potential effects o f P FO S on reproduction in quail E stim ation o f "S afe" R eference Level o f P FO S in Plasm a 12/11/2006 1/31/2007 2/11/2007 2/26/2007 2/26/2007 Em ail from J. G iesy to W. R eagen & D. Bacon re: C onfidential Em ail from J. Kelly to D. M andy, et al. re: T esting o f co n su m e r GAC filters with attachm ent Email from W. Nelson to D. Bacon et al. re: P ioneer P ress Sunday M em o from H. G oeden to J. S tine re: Health Based V alue s fo r Perfluorooctane Sulfonate (PFOS) Discharge of Perfluorocarbons (PFCs) from 3M C ottage Grove Plant Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN02255189 3M_MN01524242 3MA01320043 3M_MN01524902 3MA01320414 3MA01320495 3M_MN04799651 STATE_02082048 3MA01551778 N/A 3MA01538872 3MA01562347 3MA02513752 3M_MN00042206 3MA01461356 STATE_01201422 3MA01645376 STATE_01488041 STATE_01995465 24 Plaintiff's Ex. No. 2134 2137 2138 2144 2145 2146 2147 2155 2158 2161 2162 2163 2164 2168 2174 2177 Date 2/26/2007 3/7/2007 3/13/2007 4/3/2007 4/4/2007 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n M em o from H. G oeden to J. S tine re: Health Based V alue s fo r Perfluorooctanoic acid (PFOA) Email from W. Nelson to D. Bacon et al. re: P ioneer Press, S tar Tribune and Link to M PR story Email from J. G iesy to D. Bacon and W. R eagen re: Fwd: Avian toxicity reference values Email from J. G iesy to W. R eagen re: Fwd: Looking fo r a post doc candidate M em orandum from J. S tine to T. S che rke n ba ck re: Hazard Determ ination of PFOA and PFOS 4/17/2007 4/24/2007 5/8/2007 5/22/2007 5/30/2007 6/1/2007 Los Angeles Tim es, U.S. fires com pany over apparent conflict MPCA, Presentation, Request for Response Actions, Board Presentation, 3M Perfluorochem ical Disposal Sites Letter from S. S tevenson to M. Fortado re: 3M O akdale Site insurance policy 2007 S ettle m e n t A g re e m e n t and C o n sen t O rder, In the m a tter of Releases and Discharges of Perfluorochem icals A t and From S ites in W a sh in gto n C ounty, M innesota, and C ertain Related M a tters H andw ritten notes re: M DH MTG W eston, Rem edial Investigation Report, Phase 2 Fluorochem ical (FC) Data A ssessm ent Report for the Cottage Grove, MN Site 6/18/2007 7/19/2007 8/22/2007 9/24/2007 10/1/2007 W eston, Rem edial Investigation Report Soil Supplem ental Fluorochem ical Data A ssessm ent - Addendum , O akdale Site Email from J. G iesy to D. Bacon and W. R eagen re: m anuscript FYI Lundin, J. and A lexander, B. Final R eport: M ortality o f em ployees of an am m onium perfluorooctanoate production facility Presentation, Dyneon APFO R eplacem ent Program Email from G. O lsen to W. R eagen re: R equest fo r com m ents with attachm ent 25 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. STATE_02430434 3MA01645741 3M_MN03014876 3M_MN03016361 STATE_02338891 N/A 3MA01839219 3M_MN01313152 3M_MN00568807 3M_MN02324009 3M_MN01483002 3M_MN04969186 3MA02516746 3MA02557439 3M_MN02372412 3MA02540633 Plaintiff's Ex. No. 2191 2192 2194 2204 2206 2207 2209 2219 2222 2231 2232 2233 2295 2297 2300 2301 Date 1/9/2008 1/10/2008 1/28/2008 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Em ail from J. S w eeney to S. B ernatchez re: Q uestion follow ing presentation on 3M PFC facts Em ail from K. A n d re s to G. O lsen re: CG D raft R eport w ith attachm ent Em ail from J. B ute n ho ff to S. A n p ra r and K. Taolin re: R eview Process with attachm ent 3/26/2008 3/29/2008 3/31/2008 4/1/2008 6/13/2008 6/30/2008 Em ail from J. G iesy to W. R eagen et al. re: Entrix C onsulting P resentation, J. Butenhoff, T o xico log ica l R esearch P rogram in Perfluorinated Chem istries Em ail from W. R eagen to M. Nash re: Entrix C onsulting Em ail from W. R eagen to M. Nash re: Entrix C onsulting Em ail from R. C risw ell to W . Keagen et al. re: C o m m e n ts on Foth Environm ental Infrastructure Report (3M Vault) with attachm ent Delta Environm ental C onsultants Inc., Perfluorocarbon (PFC)C o n ta in in g Firefighting Foam s and T h e ir Use in Firefighting T raining in M innesota (2008) 8/27/2008 8/29/2008 10/22/2008 3/8/2010 4/7/2010 6/1/2010 7/2/2010 Draft, Ecotoxicology and Environm ental Fate Testing of Short Chain Perfluoroalkyl C om pounds Related to 3M Chem istries ATSDR, Public Health A ssessm ent for Perfluorochem ical C o n ta m in a tion in Lake Elm o and O akdale, W a sh in gto n C ounty, M innesota Delta Consultants, Addendum to Perfluorocarbon (PFC)C o n ta in in g Firefighting Foam s and T h e ir Use in Firefighting T raining in M innesota, P repared fo r M P C A (2008) MPCA, M ississippi River Pool 2 Intensive Study of P e rfluo ro ch em icals in Fish and W ater: 2009 Letter from G. O lsen re: 3M D ecatur Buidling 2/49 dem olition and disposal project W eston, C onstruction Com pletion Report, Form er Main Disposal Area, W oodbury Site M PCA to 3M, Request for Response Action 26 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN00567710 3MA02543910 3M_MN02295793 3M_MN00110700 3M_MN03589087 3M_MN05334328 3M_MN05334324 STATE_01782725 STATE_02820958 3M _M N 01537089 STATE_01300660 STATE_02826813 STATE_02010400 3M_MN02288255 3M_MN05361976 STATE_02339051 Plaintiff's Ex. No. 2303 2304 2318 2343 2354 2367 2368 2374 2379 2382 2397 2398 2399 2400 2405 27-CV-10-28862 Date 7/23/2010 7/28/2010 1/18/2011 12/5/2011 4/11/2012 7/30/2012 7/30/2012 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n W eston, C o n structio n C o m p le tion R eport D1 and D2 A reas, C ottage Grove Site, C ottage Grove, M innesota Environ, sp re ad sh ee t re: bioaccum ulation m odel to predict the co nce n tratio n o f P FO S in fish tissue, including the quantification o f the proportion of exposure derived from surface sedim ent versus the w ater column W eston, Construction Com pletion Report D9 Area, Cottage Grove Site, C ottage Grove, M innesota Probable Link Evaluation of Pregnancy Induced Hypertension and Preeclam psia (2011) D raft M e m orandum from L. Zobel to FC C ore T eam re: R eview of FC M anuscripts Probable Link Evaluation of Autoim m une Disease (2012) Probable Link Evaluation of Thyroid disease (2012) 10/29/2012 1/3/2013 2/22/2013 Probable Link Evaluation for heart disease (including high blood pressure, high cholesterol, coronary artery disease) (2012) Email from M. Falco to M. Nash re: Fw: A sse ssm e n t o f Long Chain Fluorochem ical Use Newstead, John et al., S patial and Tem poral Trends of P erfluoroalkyl C o m p ou n ds in Fish Fillets C ollected From Pool 2 of the Upper Mississippi River (2013) 11/21/2013 Fish C onsum ption G uidelines for the G eneral Population, Lakes 12/19/2013 1/27/2014 1/27/2014 Fish C onsum ption G uidelines for the G eneral Population, River L etter from Jean B. S w eeney to M P C A C o m m issio n e r John L. S tine re: C om m ents on the 2014 M P C A D raft Im paired W aters List 3M A ppendix A - S um m ary Data R eport - Pool 2 Fall 2013 Fish Data 6/5/2014 Route, W illia m T. e t al, S patial and T e m p oral P atterns in C o n cen tra tion s o f P erfluorinated C o m p ou n ds in Bald Eagle N estlings in the U pper M idw estern United S tates (2014) 27 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN01533753 STATE_00942604 3M_MN00716872 N/A 3M_MN04777930 N/A N/A N/A 3M_MN04836974 3M_MN03205198 N/A N/A 3M_MN03203477 3M_MN04813517 N/A Plaintiff's Ex. No. 2406 2421 2431 2435 2436 2437 2440 2448 2450 2455 2475 2476 2477 2487 2491 27-CV-10-28862 Date 7/22/2014 10/6/2015 4/00/2016 5/15/2016 5/23/2016 5/23/2016 6/10/2016 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n A qua-Pure Plum bing W holesale Update Q2 Falco, Fluorochem ical EHS Background, The M agic Behind the Innovation Anchor, 2013 Data Sum m ary Report, Mississippi River - Pool 2 and A djacent Locations The Madrid Statem ent on Poly- and Perfluoroalkyl Substances (PFASs) EPA Drinking W ater Health Advisory for P erfluorooctanoic Acid (PFOA) EPA Drinking W ater Health Advisory for Perfluorooctane Sulfonate (PFOS) C8: association between prenatal exposure to perfluorinated compounds 7/19/2016 8/11/2016 10/12/2016 MDH, Fish C onsum ption G uidelines fo r W om en W ho Are or M ay Becom e Pregnant, and C hildren U nder A ge 15, Lakes Fish C onsum ption G uidelines for W om en W ho A re or May Becom e Pregnant, and C hildren U nder A ge 15, Rivers 3M Analysis of Mississippi River Pore W ater and Surface W ater Sam ples near the 3M Cottage Grove Facility - S eptem ber 2016 Sam pling 5/3/2017 PFO A_R e-Evaluation_FinalToxR eview W orksheet_M ay2017.pdf 5/3/2017 PFO S_R e-Evaluation_FinalToxR eview W orksheet_M ay2017.pdf 5/17/2017 6/7/2017 00/00/0000 Environmental Surveillance and Assessm ent M em orandum from N ancy Rice (M DH) to Jam es Kelly (M DH) re: H ealth-B ased Values for Perfluorooctane Sulfonate MDH, Notice of Health Risk Advisory for Perfluorochem icals (PFCs), City of C ottage Grove, (2017) APFO summary document Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN05101829 3M_MN03639885 N/A N/A STATE_07081959 STATE_07082062 N/A STATE_04501887 STATE_04513318 3M_MN04844733 STATE_07438004 STATE_07438096 STATE_07457240 N/A 3M_MN01524233 28 Plaintiff's Ex. No. Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 2493 V a rio u s Factory O perating Standards. 1973, 1974, 1976, 1978, 1981, 1988, 1989, 1990, 1991, 1992, 1993, 1996, 1997, 1999, 2000 2496 2498 2499 2513 2515 2516 2517 V a rio u s 3M W aste Inventory Forms - Chemolite 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 Gilland, Frank and Jack Mandel, Peripheral Blood Lym phocyte C ount in Men O ccup a tion a lly E xposed to P erflu o ro o cta n o ic A cid Chart on FC-95 or PFOS P resentation, B asic S tudies in E lectrochem ical F luorination - A 3M Core Technology Handwritten Notes Bullet-Point Notes Regarding Paper for Subm ission Presentation, Representative LCM Flow Chart 29 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00050322 3MA00053311 3MA00053882 3MA00056266 3MA00072899 3MA00072984 3MA00081493 3MA00202292 3MA00204906 3MA00204927 3MA00204957 3MA00206150 3MA01168550 3MA01200731 3MA01201394 3MA01201453 3MA01828643 3MA10064412 3MA01986530 3MA01986529 3MA01986528 3MA01986538 3MA01986532 3MA01986536 3MA01986534 3MA01986531 3MA10016749 3MA10031469 3M_MN00838987 3M_MN02323912 3M_MN02329964 3M_MN02492763 Plaintiff's Ex. No. 2521 2522 2534 2542 2545 2546 2547 2548 2549 2550 2551 2552 2553 2559 2561 2563 2565 2566 2567 27-CV-10-28862 Date 00/00/0000 4/10/0000 00/00/0000 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Business O pportunity Memo Q uestions for C harlie A u e r fo r M onday, April 10 C h ro no lo g y o f PFC s in Blood 00/00/0000 00/00/2017 00/00/2001 10/12/1995 1/13/1997 4/3/1985 7/13/2014 00/00/2001 2/6/1997 12/18/1996 8/25/1954 6/18/1966 2/7/1979 3/8/2010 T o xico log y E ducation F oundation Is It S afe? D ose M akes the Poison Video, available at http://toxedfoundation.org/is-it-safe/ Pictures of 3M products from website, http://docplayer.m e/64695777-Deponisem inaret-pfas-i-sigevannfra-deponier-ase-hoisaeter-ngi.htm l Biegel et al., M echanism s of E xtrahepatic Turner Induction by P eroxisom e P roliferators in M ale C D Rats, T o xico log ica l Sciences 60, 44-55 (2001) Email from P erkins to B utenhoff et al. re: A P M E M eeting Aqua-Pure Video Ad, https://ww w.youtube.com /w atch?v=eer1VSRM m M 4 Email from Loushin to W e p p n e r re: FC -143 M SD S Aqua-Pure Video Ad, https://ww w.youtube.com /w atch?v=B55G 3ix6ShQ Presentation by Perkins entitled FC-143 and APM E Toxicology Related Issues From 1995 to Present Aqua-Pure Video Ad, https://ww w.youtube.com /w atch?v=rU3j_R 8Hbik Email from P ickett to W e p p n e r re: FC -143 Issues Potassium Perfluorooctanoate Routine Toxicity Screening W oodbury E vent H andw ritten T im eline by Dr. Ling "In the long-term hum an health effects m ay be correlated with the presence o f FM -3422 in the a q u a tic e n viro n m e n t." M ississippi River Pool 2 Intensive Study of Perfluorochem icals in Fish and W ater: 2009 2/19/1986 6/27/1979 1986 3M hazardous w aste m anifest indicating that acid bottom s are classified as D002 hazardous-- i.e., corrosive-- w astes 3M docum ent indicating W W TP sludge and incineration ash and sludge are hazardous wastes Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00330478 3MA00470823 3MA10039277 N/A N/A N/A 3MA10024469 N/A 3MA00621672 N/A 3MA00194560 N/A 3MA10066727 3MA01828941 3M_MN00000466 3M_MN00000151 3M_MN03043077 3M_MPCA00006161 3MA00280412 30 Plaintiff's Ex. No. 2568 2569 2570 2571 2572 2573 2574 2575 2576 2577 2579 2580 2581 2582 2583 2584 2585 2586 2589 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 9/13/1960 3/23/1979 12/6/1995 7/18/2006 7/29/2004 5/25/1983 3/9/2006 5/00/2017 5/22/2007 7/3/2001 4/00/2008 1/4/2017 4/15/2012 7/30/2012 12/5/2011 3M docum ent indicating that by 1960, Building 15 discharged 131,000 gallons of effluent to the chem ical sew er per day, which included 206 pounds of HF acid per day March 23, 1979 Technical Report Sum m ary 3M w aste stream profile indicating fluorochem ical inerts contain PFCs L etter from M P C A (E ckberg, w ith copy to Kriens) to 3M in w hich M PCA alleged that 3M violated federal requirem ents pertaining to its 2002 NPDES perm it application July 2004 State emails Fate o f F lu o ro che m ica ls P hase II S tudy 3M-EPA Consent Agreem ent MDH HBV for PFOA and PFOS MPCA Settlem ent Agreem ent and Consent O rder July 2001 Santoro email to Palensky and W alker, copying others, regarding C ottage Grove W ells April 2008 MDH Fish C onsum ption A dvisory for PFOS 2016 Draft Im paired W aters List C-8 Science Panel Probable Link Report: probable link between PFOA exposure and testicular/kidney cancer C-8 Science Panel Probable Link Report: probable link between PFOA exposure and ulcerative colitis C-8 Science Panel Probably Link Report: Probable link between PFC exposure and pregnancy-induced hypertension/pree cla m p sia 10/1/2014 Johnson et al. (2014), The N avigation G uide - E vidence-based m edicine m eets environm ental health: S ystem atic R eview of Human Evidence for PFOA Effects on Fetal Growth 7/30/2012 1/7/1964 8/23/1966 C-8 Science Panel Probable Link Report: Probable link between PFOA exposure and thyroid disease and high cholesterol. 3M C o rre sp on d en ce from C. Diets to H. Jones M eeting M inutes re W oodbury Tow nship M eeting 31 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00456289 3MA01410316 3MA10051876 M N.064.0120.000599 STATE_02795716 3MA10065463 N/A N/A M N .0 6 4 .0 1 0 3 .0 0 0 0 0 2 3MA00348418 STATE_02061740 N/A N/A N/A N/A N/A N/A 3MA00335783 3MA00285494 Plaintiff's Ex. No. 2590 2591 2593 2594 2595 2596 2597 2598 2599 2600 2601 2602 2603 2604 2605 2606 2607 2614 2615 2616 27-CV-10-28862 Date 00/00/1954 7/28/1960 8/14/1975 4/12/1978 8/16/1978 5/22/1979 6/23/1980 10/28/1980 5/4/1981 8/31/1984 12/30/1988 5/15/1998 9/2/1998 11/17/2003 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 3M, Docum entation of the 3M Exposure Guideline for N-M ethylperf/uorobutanesu/fonam idoethanol (N -M cF B S E ) Letter R.C. C ollins and J. Brown re Field Letter M e m o ra nd u m from G.H. C raw ford to C. Krogh et al. re: F lu o ro carb o ns in H um an Blood Plasm a Anim al studies 3M Technical Report Sum m ary, Evaluation of the Bioconcentration Potential of FM 3422 3M Technical Report Sum mary, Bioaccum ulation Studies 3M T echnical R eport S um m ary, D etection o f F lu o ro che m ica ls in Decatur W astew ater M PCA Issue Statem ent L ette r from M. B. A ye rs (M P C A ) to Dr. R. S usag (3M ) re: investigation of a disposal site 3M Internal C orrespondence from D.E. Roach, M.D. to P.F. Riehle (S pecialty Chem ical Division - C hem olite C enter 41-1) re O rganic Fluorine Levels 3M Technical Report Sum m ary, Effect of Potassium P erfluorooctanesulfonate on Survival, etc. Letter from 3M to EPA re: T S C A S ection 8(e) -P erfluorooctane S u lfo n a te 3M lab notebook M e m o ra nd u m from T. D iP asquale to J. R. A lliso n et al. re : FC M eeting - Novem ber 11,2003 2/17/2006 7/18/2006 12/30/2009 5/6/2002 00/00/2017 12/14/1948 M e m o ra nd u m from J. G iesy (E N T R IX Inc.) to D. B acon (3M ) re: Follow up to February 2, 2006 m eeting (revised memo) Letter from MPCA to 3M EPA Report Entitled: "Long-C hain Perfluorinated C hem icals Action Plan" M eeting Minutes W est Virginia DEP & DuPont "CATT" Toxicity Team and Report Excerpts Dourson Emails U.S. Patent 2,456,027 32 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA01628937 3M_MN00000231 3M_MN00000293 3MA100666974 3MA00326803 3M_MN01639837 3MA01409767 3M_MN00001391 3MA00334184 3M_MN01655416 3MA10035953 3M_MN02456909 3M_MN04758351 3M_MN04778452 3MA02513749 3M_MN0492289 N/A N/A N/A N/A Plaintiff's Ex. No. 2617 2621 2632 2639 2640 2649 2651 2660 2662 2667 2673 2679 2682 2683 2684 2685 2686 2687 27-CV-10-28862 Date 00/00/0000 5/14/1962 10/18/1966 12/28/1966 3/24/1967 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Final C om prehensive Report FC-95 MN M ining L etter from J.T. Ling to D. H. C ochran RE W aste Disposal W oodbury Dump Site Interoffice Letter from J.T. Ling to D.R. G uthrie RE R esidence W ell W ater Sam pling W oodbury Tow nship and C ottage Grove V illa g e W a te r P ollution P roblem in W o o db u ry - 1 page sum m ary regarding investigation of Chem olite Meeting M inutes RE W oodbury Ground W ater Problem with Hargraves (MWPC) 8/31/1971 Interoffice M em o from J.T. Ling to H.G. Bryce RE Ecological A spects of Fluorocarbons - com m ents on Bryce's draft report 9/13/1971 1/00/1967 00/00/1980 8/18/2017 9/22/2017 11/7/2017 9/24/1993 4/28/2017 6/30/2011 7/3/2017 4/27/2010 7/12/2017 Interoffice Letter from H.G. Bryce to R.M. Adam s RE Ecological Aspects of Fluorocarbons - your mem o 7/14/1971 H ickok, E. R eport titled "G round W a te r Investigative P rogram at W oodbury" Site No. 8 - 3M Com pany - W oodbury Email from Lucas Martin containing two spreadsheets with East M etro W ater Quality Data.xlsx. Kier Soderberg Field Photos: im g_0940 - img_1081 Davis Expert Report Figure 5-6: Hazard Indices 3M Com bined A ir and Hazardous W aste Perm it Renewal; Perm it No. 23-AI-89-0-6 M P C A Letter from G. K rueger to J. S w eeney RE N ew D rinking W ater Health Advisories for PFOA and PFOS Lim noT ech (2011). T M D L S coping - P FO S in Pool 2 o f the M ississippi River Letter from Brewer to M PCA RE Settlem ent A greem ent and Consent O rder (SACO), dated May 22, 2017 Em ail from Balogh to L. Rogacki RE E stim ated P FO S loads in M etro effluent and the M ississippi River Letter from Brewer to M PCA RE 3M disputes a reim bursem ent request for certain expenditures 33 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A 3M_MN00048247 3M_MN00000728 3MA00285419 3MA00285471 3MA02496585 3M_MN00048386 3MA00286008 3MA01934828 N/A N/A N/A 3MA00288649 N/A STATE_01170462 N/A MET0007023 N/A Plaintiff's Ex. No. 2688 2689 2690 2691 2692 2693 2694 2695 2696 2697 2698 2699 2700 2701 2702 2703 2704 27-CV-10-28862 Date 7/12/2017 00/00/2016 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n MN AG Letter to Brewer RE 2007 Consent O rder and 3M cost reim bursem ent M PC A, 2016. Fish tissu e data provided in spreadsheet. 7/20/2017 12/16/2010 11/21/2017 11/29/2017 00/00/0000 1/1/1998 Letter from B rew er to A. C ohen RE receipt of July 12, 2017 letter Environ, 2010. R eview o f P FO S Im p airm e nt in Pool 2 o f the M ississippi River. Prepared fo r Barnes and Thornburg LLP on behalf of M etropolitan Council Environm ental Services, D ecem ber 16, 2010 Letter from Hogan (MPCA) to G. Hohenstein RE Drinking W ater Health Advisory for Cities of W oodbury and O akdale M unicipal W ells Letter from B rew er to M. Kieley (AG O ) RE Response to N ovem ber 2 1 ,2 0 1 7 letter. Dilks CV 3M Presentation: Environm ental Fate and Effects of F lu o ro che m ica ls by R. H owell 3/5/2005 2/26/1997 00/00/2003 PFOS Case Study by Butenhoff, Olsen and Pfahles-Hutchens Email from M a e nd le r to Howell, et al. RE T ox/E nvt'l Issues DuPont Risk A ssessm ent 2003 Proxy Statem ent 3/9/1981 6/25/1970 M em o from K.J. M iller to C.D. King RE Drum Liner Disposal Letter from 3M to M CPA RE O akdale Dump Site 11/17/1981 10/19/1977 00/00/0000 00/00/0000 Letter and W ork Plan: H ydrogeological Investigation of Disposal A re a s at the 3M C hem olite P lant in C o ttage G rove, MN Interoffice Corr. from L.C. Krogh to Lazerte, Sheukrm an, Ubel RE Nov 7 presentation and co pies o f tra n sp a re n cie s used in last report. O verview of Potential Dredging Areas (2.2 PPB Threshold, Depth 1 ft.) Dredging Volum es by Area (2.2 PPB PFOS Threshold) Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A STATE_07459336 N/A STATE_01178225 N/A N/A N/A 3MA10051826 3MA00762535 3MA00194581 N/A 3MA00150027 3M_MN00049959 3M_MN00001563 3M_MN00000479 N/A N/A 34 Plaintiff's Ex. No. 2705 2706 2707 2708 2709 2710 2711 2712 2713 2714 2715 2716 2717 2718 2719 2720 2721 2722 2723 2724 2725 27-CV-10-28862 Date 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 1/3/2018 11/18/1998 12/00/2009 00/00/1974 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n O ve rvie w o f P otential D redging A re a s (1 PPB Threshold, D epth 1 ft) D redging V olum es by A re a (1 PPB PFO S T h reshold) W etland Bank Service Areas and M ajor W atersheds for County B o u n d a rie s M innesota Pre-Settlem ent W etland Areas Rem aining Estim ated Cost of C redits Required to A ddress PFC W etland Im p acts W etland Bank Price Per C redit from BW SR 2017 RFP L ette r from Bilot to H uyser RE PFC s in M innesota A Review of the Environm ental Fate and Effects of Sulfonyl Based Fluorochem icals DRAFT Frisbee, S., et al., The C8 Health Project: Design, M ethods, and P articipants, 117 E nvironm ental Health Persp. p. 1873 (Dec. 2009) Algicidal Activity Test Substance 12/13/1961 5/29/2007 12/00/1998 4/26/2000 11/2/1998 00/00/0000 5/15/1998 4/26/1979 MN Mining & Manf. Co. G eology D epartm ent Report No. 61-22 Consulting Services Agreem ent FC T o xicity/S a fe ty T esting In P articular PFO S & N -E tF O S E by N abbefeld, et al. CAS No. 2795-39-3 Potassium Perfluorooctanesulfonate EPA Proposed Meeting Draft by C. Reich DeW itt CV Email from Jerry (?) to J.E. G regory and J.R. Lewis RE Accum ulation and Disposal of W aste W ater at Decatur 3M Interoffice C orrespondence from Prokop re: M eeting M inutes - Meeting with J.R. Mitchell 7/26/1979 8/23/1978 7/22/1992 Phone C onversation Report from R.A. Prokop to L.C. Krogn and J.D. Lazerte with Eugene Berman, attorney for DuPont 3M Interoffice C orrespondence RE M inutes of M eeting with H.C. Hodge, held in Portland, M aine M inutes of Fluorochem ical Steering Com m ittee Meeting 35 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A N/A 3M_MN05374965 N/A 3M_MN00436466 3MA00335895 3M_MN00255852 3MA10054016 3MA01657924 3MA10071231 N/A 3MA00905854 3MA10034826 3MA10035034 3MA00967742 3M_MN00000789 Plaintiff's Ex. No. 2726 2727 2728 2729 2730 2731 2732 2733 2734 2735 2736 2737 2738 2739 2740 2741 2742 Date 5/27/1993 1/22/2007 1/9/2007 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n In S earch o f N on-Industrial S ou rce s o f O rg a n ic Fluorine In Normal Human Blood from the G eneral Public Em ail from M.A. S antoro to P. H off RE Fw: C o n sid e ra tio n s fo r conducting PFOA avian repro study Corporate Messages, Environm ental Energy and Safety Issues. Issues: FC - East Metro Drinking W ater 4/6/1989 4/25/2006 11/2/2017 00/00/1993 5/23/1997 2/23/2001 8/21/2017 9/8/2017 3/8/2017 Table 6: Observed and Expected Deaths by Cause, Standardized M ortality Ratios (SMR), 95 Percent Confidence Limits and Chi Square Values, Males, C hem olite Plant 2006 EPA press release on TSCA fine for 3M Rotondo, J.C. et al., Environm ental doses of perfluorooctanoic acid change the expression o f genes in ta rg e t tissu e s o f com m on carp. 3M Update M agazine Battelle Presentation: Ecosystem Fate M odeling A cu te T o xicity R eport in H oney Bee (AR 2 26 -1 0 17 ) Low er and U pper Pool 2 M aps of R ecords of Live Lam psilis higginsii surveyed 1999-2017 Map of R ecords of Live Q uadrula nodulata above Pig's Eye WWTP Y ingling, G. "P e rflu o ro ch e m ica ls (PFCs; aka PFA S) in G rey Cloud Island Tow nship" 12/2/2017 Letter from M. Kieley (AGO) to B rew er RE Response A ctions Related to PFC Releases from 3M PFC Disposal Sites 8/00/2005 00/00/2008 00/00/2008 1/9/2008 W ashington C ounty and W ashington C onservation District, Integrating G roundw ater & Surface W ater M anagem ent Southern W ashington County, Prepared by Barr Engineering Olsen. D ecatur Medical Surveillance Study Olsen. D ecatur Medical Surveillance Study Email advising Jean Sw eeney of inaccuracy of statem ent: "3M no longer m anufactures PFOS, PFOA, or PFBA" 36 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN03112528 3M_MN03436924 3M_MN03521906 3MA00632317 N/A N/A 3MA00044881 3MA01429655 MET 0438364 STATE_07507089 STATE_07543913 N/A N/A N/A 3M_MN05372035 3M_MN05372003 3M_MN00567706 Plaintiff's Ex. No. 2743 2744 2745 2746 2747 2748 2749 2750 2751 2752 2753 2754 2755 2756 2757 2758 27-CV-10-28862 Date 10/30/2007 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Presentation containing statem ent: "3M no longer m anufactures PFOS, PFOA, or PFBA" 00/00/1999 4/2/1979 00/00/2014 8/26/1958 2/17/1976 6/28/1905 2/9/2017 9/1/1999 00/00/2003 Cottage Grove Chemical Monthly Report. 11/1998 and 06/1999 "St. Paul M egaphone" Landsteiner, A., Huset, C., W illiam s, A., Johnson, J. B iom onitoring fo r P erfluo ro ch em icals in a M innesota C o m m u n ity with Known Drinking W ater F.B. Richerson sum m ary RE: Discussion of C hem olite W astes with Mr. Johannes of the SW PCB O rg a n ic Fluorine C o m p ou n ds in Blood C hro no lo g y List of Studies to be Moved to 8(e) Docket 3M SEC 10-K for the year ended Decem ber 3 1,2 01 6 SM M D FC W aste M anagem ent (CY1998) M PCA Annual Report on W ashington C ounty Sanitary Landfill 2003 10/9/2017 5/26/1999 A ffidavit of Charles Kiester ISO 3M 's Response to O pposition to State's Motion to Com pel Discovery, with attachm ent "Fluorochem ical Use, Distribution and Release Overview", Prepared by 3M 00/00/1989 5/19/1992 7/23/2013 V a rio u s Just, W .W ., G orgas, K., Hartl, F-U., H einem ann, P., S alzer, M., S chim assek, H. B iochem ical E ffects and Zonal H eterogeneity of Peroxisome Proliferation Induced by Perfluorocarboxylic Acids in R at Liver. H epatology Vol. 9 (4) 570-581 Term inated Study Final Report (GLP) Titled: PFOS and POAA S tudy in G oats. S tudy No. F A C T -T O X -100 Presentation entitled "Status of the PFC A ssessm e n t/R e m e d ia tio n P rojects in M in n eso ta " Sum m ary of 3M Hazardous W aste M anifests 1980 - 2008 assigning one or more EPA Hazardous W aste codes to waste characterized as containing PFCs; The Sum m ary com prom ising underlying exhibits 2758.0001 - 2758.2325. Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN00566907 3MA01204490; 3MA00229513 3MA00323984 N/A 3MA00456233 3MA10067216 3MA01220049 N/A 3M_MN02792261 3MA00402203 N/A 3M_MN03270260 3MA00632733 3MA01725206 STATE_02942271 N/A 37 Plaintiff's Ex. No. 2759 2760 2761 2762 2763 2764 2765 2766 2767 2768 2769 2770 2771 27-CV-10-28862 Date 11/13/1997 9/00/1996 4/00/2003 10/00/2017 11/9/2017 11/30/2007 11/30/2007 11/30/2007 10/27/1961 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Beach, Susan. Report titled: Results from Analyses of Soil and G roundw ater S am ples from the E.I. D uPont de N em ours and C o m p an y Facility in P arkersburg, W V EPA M onthly Hotline Report MPCA M innesota Environm ent Special Report. FY 2002 Superfund Report to the Legislature. "Use of the M innesota Environmental Response, Com pensation and Com pliance Account (Superfund)." M DH W e b site - C u rre n t A ctivities: P erfluroch e m ica ls (P FC s) in M innesota Handwritten equation by Connolly Report on the m anufacture, Use, and Releases of PFCs at the 3M C ottage G rove Facility - attachm ents 2 - 6 Report on the m anufacture, Use, and Releases of PFCs at the 3M C ottage G rove Facility - attachm ent 7 Report on the m anufacture, Use, and Releases of PFCs at the 3M C o ttage G rove Facility - atta ch m e nts 8 - 11 3M Life M agazine Scotchgard Ad 4/13/2007 12/9/1999 1/19/1999 8/22/1975 L etter from K. S a th e r (M P C A ) to Board M em bers RE R equest for Issuance of a Request for Response Action (RFRA) to the 3M Com pany: For the Release and Threatened Release of Hazardous Substances from the 3M C hem olite Disposal Site, 3M O akdale Disposal Site, and 3M W oodbury Disposal Site 3M /D uPont Meeting Notes for Rem oving PFOA from W astewater 3M Draft Com pany Statem ent Interoffice C orrespondence from J.D. LaZerte to L.C. Krogh RE Telephone Call from Dr. W arren Guy, Uni of Florida RE F lu o ro che m ica ls in H um an Blood Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN00043306 N/A N/A N/A N/A 3MA02527154 3MA02527167 3MA02527243 N/A STATE_07088102 3M_MN05377877 3M_MN05382332 3M_MN05382159 38 Plaintiff's Ex. No. Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 2772 2773 2774 2775 2776 2777 2778 2779 2780 2781 V a rio u s M aterial Safety Data Sheets from February and March 1997, stating that m ultiple PFC-containing products can cause cancer. (2772A - 2772P) Sum m ary of Certain 3M Paym ents for John G iesy W ork; The 00/00/0000 Sum m ary com prising underlying exhibits 2773.0001-2773.0147 2/28/1978 Interoffice C orrespondence from A.N. W elter to R.A. Prokop RE Fate of Fluorochem ical Project, Inform ational Meeting 2/24/1978 5/00/2017 Fish C onsum ption G uidelines for the G eneral Population, Lakes 6/00/2016 5/00/2017 6/00/2016 00/00/2001 Fish C onsum ption G uidelines for the G eneral Population, Rivers Fish C onsum ption G uidelines for W om en w ho A re or May Becom e Pregnant, and C hildren under A ge 15, Lake Fish C onsum ption G uidelines for W om en w ho A re or May Becom e Pregnant, and C hildren under A ge 15, Rivers 2001 Proxy Statem ent 0 0 /0 0/0 0 00 U ndated photograph show ing open burning o f d rum s in landfill 5/00/2000 Project Spring C om m unication Plan Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN05419460 3M_MN05421995 3M_MN05423232 3M_MN05434588 3M_MN05435506 3M_MN05423793 3M_MN05433545 3M_MN05419466 3M_MN05433550 3M_MN05435511 3M_MN05423238 3M_MN05434593 3M_MN05423799 3M_MN05419472 3M_MN05423244 3M_MN05429408 N/A 3MA10066978 N/A N/A N/A N/A N/A 3M_MN00000473 3M_MN05381646 39 Plaintiff's Ex. No. 2782 2783 2784 2785 2786 2787 2788 2789 2790 2791 2792 2793 2794 2795 2796 Date 6/2/1993 2/17/1975 6/18/2008 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Internal Correspondence from T. M anzara R M icroorganism Sources for Degradable F.C. Study Memo to T. Scherkenbach from G. Frazier RE 3M W oodbury Site M PCA Rem edy Decision Docum ent - W ashington County Landfill, Lake Elmo, MN 6/13/2001 5/11/1983 1/25/1991 12/17/2998 9/5/2001 L etter from K. Reed to EPA re T S C A S ection 8(a) S up p le m e nta l Submission: Docket Nos 8EH Q -1180-373 and 8EHQ-1180-374 Pilot Rat Teratology Study T-3352 - Final Report Final Report Titled Prim ary Eye Irritation/C orrosion Study of T5298 in rabbits (O E C D G uidelines) Final Report - Protocol 418-011 Oral (G avage) Developm ental T o xicity S tudy o f N -E tF O S E in Rats, S po n sor's S tudy Num ber: T-6316.7 Letter from G. A da m s (3M ) to U.S. EPA re: T S C A 8(e) Supplem ental Notice on Sulfonate-based Fluorochem icals, A R 2 2 6 -1 0 3 8 5/14/1999 11/3/1995 3M Medical Departm ent, Toxicology Services, Report for Study No. T-6316.9; DT21 F luorochem ical (FC) Levels in N aive Rats Product Safety Labs, W norow ski, G., Prim ary Eye Irritation 5/3 0 /19 9 7 Stum p, D., A D evelopm ental T o xicity S tudy o f 313401 in Rats 11/9/1994 Determ ination of the Partition Coefficient (N-O ctanol/W ater) of T5874 by High Perform ance Liquid C hrom atography (HPLC) 11/9/1994 1/10/1979 2/14/1996 Determ ination of the Partition Coefficient (N-O ctanol/W ater) of T5869.4 by High Perform ance Liquid C hrom atography (HPLC) Technical Report Sum m ary: Distribution C oefficient of FM 3925 in n -O cta n o l/W a te r M.S.I. Report No. 4B223-4B227, Determ ination of Physico chem ical P roperties o f S am ple D-1 by M itsubishi C hem ical S afety Institute Ltd. 40 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN05437251 3M_MN00048377 3MA02645872 MET 0438451 3MA00248286 3M_MN01241251 3MA10083119 MET0438638 3M_MN00428316 3M_MN01062303 3M_MN01062651 3M_MN01532235 3M_MN01639872 3M_MN01640028 3M_MN01640581 Plaintiff's Ex. No. 2797 2798 2799 2800 2801 2802 2803 2804 2805 2806 2807 2808 2809 2810 2811 27-CV-10-28862 Date 2/16/1993 2/25/1980 6/11/1999 4/26/2000 4/12/1979 1/11/1999 5/14/1999 1/11/1999 4/15/1998 5/31/1978 11/29/1995 1/14/1987 9/5/1996 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Twenty-eight-day Repeated Dose Oral Toxicity Study of Sam ple D-1 in Rats T w o -W e e k O ral R ange finding T o xicity S tudy o f T -2 5 0 9 C o C in Rats R eport o f Data fo r E xploratory 2 8-da y O ral T o xicity S tudy in Rats: Telom er Alcohol, Telom er Acrylate, PFBS, PFHS, PFOS, Laboratory Report No. FACT-TO X-120.3 G allagher, S. et al., PFOS: A Dietary LC50 S tudy with the Northern Bobwhite Bio/D ynam ics Inc., Project No. 78-7187, An Acute Inhalation T o xicity S tudy o f T -2 3 08 C oC in the Rat Final Report, Protocol 418-010 Oral (Stom ach Tube) D evelopm ental T o xicity S tudy o f N -E tFO S E in R abbits 3M Medical Departm ent, Toxicology Services, Report for Study No. T-6316.9; DT21 F luorochem ical (FC) Levels in N aive Rats Further Investigation of Rat Chow Final Report, Protocol 418-012 Oral (Stom ach Tube) D evelopm ental T o xicity S tudy o f PFO S in R abbits 104-W eek Dietary C hronic Toxicity and C arcinogenicity Study with Perfluorooctane S ulfonic Acid Potassium Salt (PFOS; T6295) in Rats International research and Developm ent Corporation, Fluorad Fluorochem ical Surfactant FC-95, Acute Oral Toxicity (LD50) S tudy in Rats 3M Final Report - A nalytical Study, Single-dose Intravenous P h a rm aco kin etic S tudy o f T -6 2 46 in R abbits S. G laza (H azelton), P rim ary Eye Irritation S tudy in R abbits Method, Sum m ary Raw Data Appendix S. Glaza (Corning Hazelton), Final Report, Prim ary Eye Irrigation/C orrosion S tudy o f T -6 5 64 in R abbits (O E C D G u id e lin e s) 2/18/1981 1/17/1984 A cu te O cu la r Irritation T e st w ith T -2 9 6 0 C o C in A lb ino R abbits A cu te O ral T o xicity S creen w ith T-3421 in A lb in o Rats 41 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN01649987 3M_MN01695616 3M_MN02336491 3MA00233956 3MA00234875 3MA00239722 3MA00242650 3MA00353213 3MA00395762 3MA00725705 3MA01502168 3MA10001092 3MA10006895 3MA10008130 3MA10019997 Plaintiff's Ex. No. 2812 2813 2814 2815 2816 2817 2818 3008 3013 3017 3020 3021 3022 3023 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 8/11/1999 Final Report - E pidem iology - Fluorochem ical Exposure A ssessm ent of D ecatur C hem ical and Film Plant Em ployees 1/19/1983 00/00/0000 1/5/2003 4/1/2014 3/8/2010 5/00/2013 00/00/1950 8/1/1955 00/00/1961 00/00/1963 00/00/1963 00/00/1964 00/00/1965 Absorption and Biotransform ation of N-Ethyl FOSE and Tissue Distribution and Elim ination of Carbon-14 after A dm inistration of N-Ethyl F O S E -14C in Feed by R iker Laboratories, Inc. Com posite Analytical Laboratory Report on the Q uantitative A n a lysis o f F lu o ro che m ica ls in E nvironm ental S am ples, R eport No. Fact Gen-021, Gen-024, Gen-030, Gen-033, LRN - W 2491, W2845, W 3197, E00-1386. Decatur W orker Com m unication Tim eline Concerning Fluorochem ical Health and Safety Issue M PCA R esponses to the 2014 Impaired W aters List 30-day Public Notice C om m ents MPCA, M ississippi River Pool 2 Intensive Study of P erfluo ro ch em icals in Fish and W ater: 2009 M PC A, P erfluo ro ch em icals in M ississippi R iver Pool 2, 2012 Update S im ons, J. H., 1950. F luo ro carb o ns and T h e ir Production. Fluorine Chem istry, 1(12): 401-422. Nordby, G. L, et al., 1955. P erflu o ro o cta n o ic A cid Interactions W ith Human Serum Album in. Journal of Biological Chem istry, (219): 339-404. A u g u st 1. Saunders, B.C., 1961. The Physiological Action of O rganic C o m p ou n ds C ontaining Fluorine. A d va n ce s in Fluorine Chem istry, 2: 183-210. Ham ilton, J. M., 1963. The O rganic Fluorochem icals Industry. A d va n ce s in F luorine C hem istry, 3: 117-180. Hodge, H. C. et al. 1963. B iological E ffects o f O rg an ic Fluoride. Fluorine C hem istry, 3: 1-55. Bryce, H.G., Industrial and Utilitarian Aspects of Fluorine Chem istry. Taylor, N. F. et al., 1965. S tructural A sp e cts o f M onofluoroS teroids. A d va n ce s in F luorine C hem istry, 4: 113-141. 42 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA10050434 3MA10053186 3M_MN01665997 3M_MN05439756 N/A N/A N/A STATE_07525274 3MA00631310 N/A N/A N/A 3M_MN04855110 N/A Plaintiff's Ex. No. 3028 3029 3043 3048 3054 3092 3098 3145 3162 3180 3184 3200 27-CV-10-28862 Date 00/00/1973 00/00/1973 00/00/1982 00/00/1985 00/00/1986 1/12/1998 00/00/1998 00/00/2003 00/00/2003 00/00/2004 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Clark, Leland et al., Perfluorocarbons Having a S hort Dwell Tim e in the Liver, S cience 181(4100):680-2. Clark, L. C. et al., 1973. PFC s H aving a S ho rt Dwell Tim e in the Liver: Science. 18(4100): 680-682. M PCA Pream ble, Statem ent of Need and Reasonableness (1982) Ikeda T, A ib a K, Fukuda K, T a na ka M: The induction o f peroxisom e proliferation in rat liver by p erfluorinated fatty acids, m etabolically inert derivatives of fatty acids. J Biochem 1985, 98(2):475-482. EPA, National Priorities List Fact Book (1986) lntrasuksri, Urusa et al., M echanism s of Peroxisom e Proliferation by Perfluorooctanoic Acid and Endogenous Fatty Acids, Gen. Pharm ac. (1998) MPCA, Draft G uidelines Rem edy Selection A lexander BH, Olsen GW, Burris JM, Mandel JH, Mandel JS: M ortality of em ployees of a perfluorooctanesulphonyl fluoride m anufacturing facility. O ccup Environ Med 2003, 60(10):722729. Thibodeaux JR, Hanson RG, Rogers JM, Grey BE, Barbee BD, Richards JH, Butenhoff JL, Stevenson LA, and Lau C. 2003. E xposure to p erfluo ro o cta n e su lfon a te during pre gn a ncy in rat and m ouse: I: m aternal and prenatal evaluations. T o xico log ica l Sciences 74:369-381. M PCA G round-W ater Sam pling for PFOA near the W ashington Co. Landfill 00/00/2005 00/00/2006 Kannan, K., Tao, L., S inclair, E., Pastva, S.D., Jude, D.J., G iesy, J.P. 2005. P erfluorinated C o m p ou n ds in A q u a tic O rg an ism s at V a rio u s T ro p h ic Levels in a G re at Lakes Food C hain. A rch ive s of Environmental Contam ination and Toxicology 48:59-566. Lau C, Thibodeaux JR, Hanson RG, Narotsky MG, Rogers JM, Lindstrom AB, S trynar MJ: Effects of perfluorooctanoic acid e xpo su re during p regnancy in the m ouse. T oxicol Sci 2006, 90(2):510-518. 43 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3MA00631101 N/A N/A N/A 3MA00610364 3M_MN04736476 N/A N/A N/A 3MA00511220 N/A N/A Plaintiff's Ex. No. 3203 3207 3210 3217 3223 3234 3245 3246 3269 27-CV-10-28862 Date 00/00/2006 00/00/2006 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n M olina, E.D., Balander, R., Fitzgerald, S.D., G iesy, J.P., Kannan, K., M itchell, R., Bursian, S.J. 2006. E ffects o f A ir Cell Infection of Perfluorooctane Sulfonate Before Incubation on D evelopm ent of the W hite Leghorn Chicken (Gallus dom esticus) Embryo. Environmental Toxicology and Chem istry 25(1):227-232. Science Advisory Board: SAB R eview of EPA's Draft Risk A ssessm ent of Potential Human Health Effects A ssociated with PFO A and Its Salts. In. W ashington, DC: U.S. E nvironm ental Protection Agency; 2006. 00/00/2006 00/00/2006 12/7/2007 00/00/2007 00/00/2007 1/15/2008 00/00/2008 Stevenson, C.N., M acm anus-S pencer, L.A., Luckenbach, T., Luthy, R.G., Epel, D. 2006. N ew P erspectives on Perfluorochem ical Ecotoxicology: Inhibition and Induction of an E fflux T ra n sp o rte r in the M arine M ussel, M ytilus C alifornians. Environmental Science & Technology 40:5580-5585. City of Oakdale. Update: Perfluorochem icals and the City of Oakdale Public W ater Supply. M P C A Investigating PFC s in g ro u n d w a te r n ea r the W a sh in gto n Co. Landfill M innesota C a n ce r S urveilla nce S ystem : C a n ce r incidence in D akota and W a sh in gto n counties. In: M C S S E pidem iology R eport 2007:1. St. Paul, MN: M innesota C ancer S urveillance System; 2007 M PCA 2007. Perfluorochem icals Past, present and future actions. https://w w w .pca.state.m n.us/sites/default/files/gp5-18.pdf M DH: Health R isk Lim its fo r P erfluorochem icals. In: R eport to the M innesota Legislature. St. Paul, MN: MDH; 2008. http://ww w.health.state.m n.us/divs/eh/hazardous/topics/pfcs/final report011508.pdf MDH 2008 Site-Specific Meal Advice for Men and W omen Not Planning on Becom ing Pregnant Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A 3MA01467679 3M_MN01535036 3M_MN04780535 N/A N/A N/A 44 Plaintiff's Ex. No. 3280 3310 3312 3313 3314 3320 3332 3334 3335 3337 3344 3376 3377 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 00/00/2008 00/00/2009 00/00/2009 00/00/2009 00/00/2009 M innesota Pollution C ontrol Agency, "M innesota's Fish C ontam inant M onitoring Program ," Pollution Prevention/Sustainability Fact Sheet, July 2008, https://ww w.pca.state.m n.us/sites/default/files/p-p2s4-05.pdf Lundin JI, A le xan d er BH, Olsen GW, Church TR: A m m onium perfluorooctanoate production and occupational mortality. Epidem iology 2009, 20(6):921-928. MDH, Toxicological sum m ary for perfluorohexane sulfonate (PFHxS) (2009) MDH, Toxicological sum m ary for perfluorooctane sulfonate (PFOS) and salts (2009) MDH, Toxicological sum m ary for perfluorooctanoic acid (PFOA) and salts (2009) 00/00/2009 00/00/2009 2/16/2010 5/1/2010 5/24/2010 00/00/2010 00/00/2011 00/00/2011 Peden-Adam s, M.M., Stuckey, J.E., Gaworecki, K.M., BergerRitchie, J., Bryant, K., Jodice, P.G., Scott, T.R., Berrario, J.B., G uan, B., Vigo, C., Boone, J.S., M cG uinn, W .D ., Dewitt, J.C., Keil, D.E. 2009. D evelopm ental T o xicity in W hite Leghorn C h icke ns Follow ing in ovo E xposure to P erfluorooctane Sulfonate (PFOS). Reproductive Toxicology 27:307-318. MPCA, The Lethality C haracteristic. A M innesota specific Hazardous-waste Characteristic Custer, T hom as et al., Perfluorinated C om pounds and P olybrom inated D iphenyl E thers in G re at Blue Heron Eggs from Three C olonies on the M ississippi River, M innesota, W aterbirds 33(1):86-95. 2010 M innesota Pollution Control A gency (M PCA) (2010). G uidance for Perfluorochem icals Analysis EPA, The Presence and Distribution of Perfluorochem icals (P FC s) in M innesota MPCA, Identifying, Using and M anaging PCBs. W aste/Hazardous W aste #4.48a. MPCA, F List of Hazardous W astes MPCA, Characteristic Hazardous W astes 45 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A STATE_02770359 N/A STATE_00929284 MET0887473 STATE_07240721 STATE_07239974 STATE_07239985 Plaintiff's Ex. No. 3379 3380 3420 3431 3437 3452 3459 3512 27-CV-10-28862 Date 00/00/2011 00/00/2011 00/00/2011 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 2011 Annual G roundw ater Report Perfluorochem ical (PFC) G roundw ater A ssessm ent and Hydraulic Capture Zone Evaluation 3M W oodbury, MN prepared by W eston Solutions, Inc. MPCA, P List of Acute Hazardous W astes & M anaging Acute Hazardous W astes MDH, Toxicological sum m ary for perfluorobutyrate (PFBA) (2011) 00/00/2011 W ang, M., C hen, J., Lin, K., C hen, Y., Hu, W ., Tanguay, R.L., Huang, C., Dong, Q. 2011. C hronic Zebrafish PFO S Exposure A lters S ex Ratio and M aternal R elated E ffects in F1 O ffspring. Environm ental Toxicology and Chem istry. 30(9):2073-2080 3/13/2012 Steenland K and W oskie S. Cohort m ortality study of w orkers exposed to perfluorooctanoic acid, Am J Epidem iol. 2012 Nov 15;176(10):909-17. Epub 2012 O ct 18. 00/00/2012 00/00/2012 00/00/2013 Custer, C.M., Custer, T.W ., Schoenfuss, H.L., Poganski, B.H., Salem , L. 2012. E xposure and E ffects o f P erfluoroalkyl C o m p ou n ds on T ree S w a llo w s N esting at Lake Jo ha n na in East Central M innesota, USA. Reproductive Toxicology 33:556-562. G randjean P, A n d e rse n EW, B udtz-Jorgensen E, N ielsen F, M olbak K, W e ih e P, H eilm ann C: S erum va ccin e a ntibody co nce n tratio n s in children exposed to perfluorinated com pounds. JAM A : the journal of the Am erican Medical Association 2012, 307(4):391-397. Barry V, W in q u ist A, and S teenland K. 2013. P e rfluo ro o cta n oic acid (PFOA) exposures and incident cancers am ong adults living near a chem ical plant. Environm ental Health Perspectives 121:1313-1318. Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. 3M_MN04998484 N/A N/A N/A N/A N/A N/A N/A 46 Plaintiff's Ex. No. 3516 3520 3527 3530 3532 3533 3539 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 00/00/2013 00/00/2013 Fair, A.P., Rom ano, T., Schaefer, A.M ., Reif, J.S., Bossart, G.D., Houde, M., Muir, D., A dam s, J., Rice, C., Hulsey, T.C., Peden-Adam s, M. 2013. A ssociations Between Perfluoroalkyl C o m p ou n ds and Im m une and C linical C h e m istry P aram eters in Highly Exposed Bottlenose Dolphins (Tursiops truncatus). Environmental Toxicology and Chem istry 32(4):736-746. G ranum B, Haug LS, N am ork E, S tole vik SB, T hom sen C, A a b e rg e IS, van Loveren H, Lovik M, N ygaard UC: P re-natal exposure to perfluoroalkyl substances may be associated with altered vaccine antibody levels and im m une-related health o utco m e s in early childhood. J Im m unotoxicol 2013, 10(4):373379. 00/00/2013 Lou, Q.Q., Zhang, Y.F., Zhou, Z., Shi, Y.L., Ge, Y.N., Ren, D.K., Xu, H.M., Zhao, Y.X., W ei, W .J., Qin, Z.F.2013. Effects of Perfluorooctanesulfonate and Perfluorobutanesulfonate on the G rowth and Sexual D evelopm ent of X enopus laevis. Ecotoxicology 22:1133-11440 00/00/2013 00/00/2013 M innesota Registration & Certification, D ocum entation of Death (2013), http://ww w.health.state.m n.us/divs/chs/osr/deathreg/wksheet.pdf Perez F, Nadal M, N a varro-O rtega A, Fabrega F, D om ingo JL, Barcelo D, and Farre M. 2013. A ccum ulatio n o f perfluoroalkyl su bsta nce s in hum an tissues. E nviro nm e n t International. 59:354-362. 00/00/2013 00/00/2013 S teenland K, Zhao L, W in q u ist A, Parks C: U lcerative colitis and p erflu o ro o cta n o ic acid (P FO A ) in a highly exposed population o f co m m u n ity residents and w o rke rs in the m id-O hio valley. Environ Health Perspect 2013, 121(8):900-905. Raleigh, K atherine, D issertation: C a n ce r M ortality in 3M Chemical W orkers (2013) Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A 3M_MN03059185 47 Plaintiff's Ex. No. 3554 3560 3563 3589 3592 3617 3630 3632 3633 27-CV-10-28862 Date 00/00/2014 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Custer, C.M., Custer, T.W ., Dummer, P.M., Etterson, M.A., Thogm artin, W .E ., W u, Q., Kannan, K., T row bridge, A., McKann, P.C. 2014. Exposure and Effects of Perfluoroalkyl S ub sta nce s in Tree S w a llo w s Nesting in M innesota and W isconsin, USA. Archives of Environm ental Contam ination and Toxicology 66:120-138. 00/00/2014 Hardell E, Karrm an A, van Bavel B, Bao J, C arlberg M, Hardell L: C a se -con tro l study on p erfluorinated alkyl acids (P FA A s) and the risk of prostate cancer. Environ Int 2014, 63:35-39. 00/00/2014 Liu, C., Gin, K.Y.H., Chang, V.W .C. 2014. M ulti-biom arker R esponses in G reen M ussels E xposed to PFCs: E ffects at Molecular, Cellular, and Physiological Levels. Environm ental Science and Pollution Research 21:2785-2794. 00/00/2015 00/00/2015 12/29/2015 00/00/2015 5/30/2016 8/23/2016 PFC W ater Treatm ent, Recom m endation on Perfluorinated Com pound Treatm ent Options for Drinking W ater (June 2015). Y ingling, V., K arst Influence in the C reation o f a PFC M egaplum e. 14th Sinkhole Conference M DH: E ast M etro PFC 3 B iom onitoring Project. In. St. Paul, MN: Environm ental Public Health Tracking and Biom onitoring, MDH; 2015. W eston, 2014 Annual Perfluorochem icals (PFCs) Groundwater, Pore W ater and Surface W ater Report for the 3M Cottage Grove Site. (2015) L etter from M organ (E P A) to Johnson (E P A A d m in istra to r) re: SAB Draft Risk A ssessm ent of the Potential Human Health Effects Associated with Exposure to Perfluorooctanoic Acid and its Salts M DH, Health officials m ove to p rotect m ore w ell ow ners in east metro from exposure to PFOS, PFOA http://ww w.health.state.m n.us/new s/pressrel/2016/pfc082316.ht ml Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A N/A STATE_02972445 N/A 3M_MN01595950 3MA01562402 N/A 48 Plaintiff's Ex. No. 3634 3637 3639 3643 3651 3657 3675 3682 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 8/25/2016 12/15/2016 00/00/2016 00/00/2016 D a lsa ge r L, C h ristensen N, H usby S, Kyhl H, Nielsen F, H ost A, G randjean P, Jensen TK: A ssociatio n betw een prenatal exposure to perfluorinated com pounds and sym ptom s of infections at age 1-4 ye a rs am ong 359 children in the O dense Child Cohort. Environ Int 2016, 96:58-64. USDOJ. 2017. Press Release. Public and Environm ent to Benefit from $50 M illion Proposed Settlem ent for Natural Resources Harmed by Virginia DuPont Facility. USDOJ O ffice of Public Affairs. MDH, 3M - O akdale disposal site, http://ww w.health.state.m n.us/divs/eh/hazardous/sites/w ashingto n/oakdale/oakdaledum p.htm l EPA Fact Sheet PFOA & PFOS Drinking W ater Health A d v is o rie s 00/00/2016 00/00/2016 00/00/2016 Colli-Dula, R.C., M artyniuk, C.J., Streets, S., Denslow, N.D., Lehr, R. 2016. M o le cu la r Im pacts o f P erfluorinated C h e m ica ls (P FA S s) in the Liver and T e stis o f M ale Largem outh Bass (M icro pte ru s sa lm o id es) in M innesota Lakes. C o m p arative Biochem istry and Physiology, Part D 19:129-139. IARC. 2016. M onograph 110: Som e chem icals used as solvents and in p o lym e r m anufacture. IAR C m o n og ra p hs on the evaluation of carcinogenic risks to hum ans. W orld Health O rganization Lyon, France. Stein CR, M cG overn KJ, Pajak AM , M aglione PJ, and W olff MS. 2016. Perfluoroalkyl and Polyfluoroalkyl Substances and Indicators o f Im m une Function in C hildren A ged 12 - 19 years: National Health and Nutrition Exam ination Survey. Pediatric Research 79: 348-357. 1/4/2017 M PCA R esponses to the 2016 Draft Im paired W aters List Public N o tic e https://ww w.pca.state.m n.us/sites/default/files/wq-iw 1-55g.pdf Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A STATE_07354701 N/A N/A N/A N/A 49 Plaintiff's Ex. No. 3684 3688 3692 3693 3694 3695 3697 3699 3711 3714 27-CV-10-28862 Date 1/20/2017 5/23/2017 9/7/2017 00/00/2017 00/00/2017 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n Qin, X iao-D i et al., A ssociation of perfluoroalkyl substances e xposure w ith im paired lung function in children (2017) M DH: M DH issues n ew guida n ce on ch em icals in som e private w ells, city w a te r in East M etro, Bem idji. In., vol. 2017. St. Paul, MN: MDH; 2017. A bbott Service Com pany. W ire Forming Services: https://abbottservicecom pany.wordpress.com /wire-form ingservices/. Evaluation of Perfluorochem ical Removal by a Small, In-home F ilte r.p d f MPCA, Harmful Substance Com pensation Program, https://ww w.pca.state.m n.us/sites/default/files/c-s1-01.pdf 00/00/2017 00/00/2017 W eston, 2016 Annual Perfluorochem ical (PFCs) G roundwater Report for the O akdale Site. Oakdale, M innesota. (2017) US Arm y C orps of Engineers, Low er Pool 2 Channel M anagem ent Study: B oulanger Bend to Lock and Dam No. 2, DRAFT 00/00/2017 00/00/2017 00/00/2017 AR-226. 2017. C hem View database on chem ical health and safety data received by EPA and EPA's assessm ents and regulatory actions for specific chem icals under the Toxic Substances Control Act, https://java.epa.gov/chem view . EPA, Per- and polyfluoroalkyl substances (PFASs) under TSCA (2017), https://ww w.epa.gov/assessing-and-m anagingchem icals-under-tsca/and-polyfluoroalkyl-substances-pfassunder-tsca Fire Fighting Foam Coalition (FFFC). Fact S heet on A FFF Fire Fighting Agents, https://docs.w ixstatic.com /ugd/331cad_fa5766eb867b4a5080330 ce96db195fa.pdf Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A STATE_07430527 N/A N/A N/A N/A N/A N/A 50 Plaintiff's Ex. No. 3716 3724 3725 3726 3729 3738 3741 3746 3747 3748 3749 3750 Date 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n 00/00/2017 00/00/2017 00/00/2017 00/00/2017 00/00/2017 00/00/2017 G randjean P, H eilm ann C, W e ih e P, Nielsen F, M ogensen UB, B udtz-Jorgensen E: S erum V accine A n tib o d y C o n ce n tra tio n s in Adolescents Exposed to Perfluorinated Com pounds. Environ Health Perspect 2017, 125(7):077018. 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Environ Health 2017, 16(1):56. 2017_PFBA_Inform ation Sheet.docx 2017_PFBS_Inform ation Sheet.docx 2017_PFHxS_Inform ation Sheet.docx MDH Background document: Toxicokinetic model for perfluorooctane sulfonate (PFOS) and perfluorooctanoic acid (P FO A ) and its use in the derivation o f hum an health-based w ater guidance values (2017) MDH, Background Docum ent Toxicokinetic Model for Perfluorooctane Sulfonate (PFOS) and Perfluorooctanoic Acid (P FO A ) and Its Use in the D erivation o f H um an H ealth-B ased W ater Guidance Values Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A N/A STATE_07429985 STATE_07429981 STATE_07429983 STATE_07436246 STATE_07437954 51 Plaintiff's Ex. No. 3751 3752 3753 3754 3755 3756 3758 3764 3766 3767 3768 3773 3779 27-CV-10-28862 Date 00/00/2017 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n MDH, Response to EPA Health Advisory for 2017 PFOS and PFOA 00/00/2017 MDH, Toxicological Sum m ary for Perfluorooctane Sulfonate 00/00/2017 MDH, Toxicological Sum m ary for Perfluorooctanoic Acid 00/00/2017 00/00/2017 00/00/2017 00/00/2017 10/00/2008 5/2/2013 MPCA, Hazardous Terms - W hat They Mean https://ww w.pca.state.m n.us/sites/default/files/w-hw0-15.pdf PFAS update.docx PFO S_Inform ation Sheet_2017.pdf MPCA, Em ergency Program Spill Cleanup Policy https://w w w .pca.state.m n.us/sites/default/files/c-er4-13.pdf F reshw ater S ociety G uardianship Council, "W ater is Life: Protecting A Critical Resource for Future G enerations" (O ctober 2008). This report is available at http://ww w.freshwater.org/im ages/stories/PD Fs/publications/W at e r-is -L ife -R e p o rt.p d f. Lee I and V iberg H. A single neonatal exposure to perfluorohexane sulfonate (PFHxS) affects the levels of im p o rta nt neuro p ro te in s in the developing m ouse brain. NeuroToxicology. 3 7 :1 9 0 - 196. 1/13/2018 5/20/2016 1/13/2018 7/25/2017 MDH 2017 Site-Specific Meal Advice for Tested Lakes and Rivers, available at http://ww w.health.state.m n.us/divs/eh/fish/eating/sitespecific.htm l MDH. Perfluorochem icals (PFCs) and Health. http://ww w.health.state.m n.us/divs/eh/hazardous/topics/pfcshealt h .h tm l M innesota's Im paired W aters and TM D Ls https://ww w.pca.state.m n.us/water/m innesotas-im paired-waterslist U.S. EPA. "Basic Inform ation about Per- and Polyfluoroalkyl Substances (PFASs)." Accessed August 29, 2017. https://ww w.epa.gov/pfas/basic-inform ation-about-andpolyfluoroalkyl-substances-pfass#tab-1 52 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. STATE_07430221 STATE_07534027 STATE_07533992 N/A STATE_07429780 STATE_07429830 N/A N/A N/A N/A N/A N/A N/A Plaintiff's Ex. No. 3780 3781 Date 1/8/2018 27-CV-10-28862 p|aintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 D e s crip tio n U.S. Fish and W ildlife Service. ECO S Environm ental Conservation Online System , Species Profile for Rusty Patched Bum blebee (Bom bus affinis). w w w .fw s.gov/m idw est/endangered/insects/rpbb. W ashington C ounty D epartm ent of Public Health and 00/00/2013 Environm ent, W ashington C ounty G roundw ater Plan 2003-2013 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February lHpanEpin County, MN Beg. Bates No. N/A N/A 53