Document VJGLydmBpbx9yXvaXQYwegzbp

E. I. d u Po n t d e Ne mo u r s & Co mp a n y INCOIVOMTKD Wil min g t o n . De l a w a r e 19898 CHEMICALS AND PIGMENTS DEPARTMENT CHESTNUT RUN TO: B. H. GARTH C&P, CHESTNUT RUN CC: ELBaenen-C&P, Chicago Sales RRNorton-C&P, Chicago Sales DGray-C&P, Newark REPeavy-C&P, Newark LWPancoast-C&P, Newark WRZonin-C&P, Newark `\j; PAWriede-C&P, Jackson Lab* 51 OALamiet/EWStewart-C&P, C.R. NJKane-C&P, C.R. RHZabel-C&P, C.R. FRHilfiker-C&P, C.R. WORoberts-C&P, C.R. PABosin-C&P, C.R. CUSTOMER FILE February 17, 1982 3M COMPANY CHESTNUT RUN VISIT February 10, 1982 3M PERSONNEL: Richard Pinamonti-St. Paul Cindy Ashton-St. Paul Larry McAnally-Brownwood, TX Garland Bailey-Brownwood, TX DU PONT PERSONNEL: L. W. Pancoast-Newark W. R. Zonin-Newark R. R. Norton-Chicago Sales G. R. Patrick-Chestnut Run PROGRAM OBJECTIVE: To define dispersion tests that will permit 3M to develop color quality parameters for our pigments and permit establishing color specification on our pigments that are acceptable to both 3M and Du Pont. (In many cases, 3M products are a single pigment dispersion and color variability is a major concern. The attached letter states 3M customers' position.) SUMMARY OF DISCUSSIONS: Richard Pinamonti and Cindy Ashton reviewed their 3-roll mill dispersion studies of: Monastral Red Y RT-759-P Lots: $7846 (current shipping lot) 31881 (shipment to. Brownwood Plant) N 26985 TO: B. H. GARTH C&P, CHESTNUT RUN - 2- February 17, 1982 Krolor Yellow KY-781-D Lots: TS-9747.1 ! 806241 (shipment to Brownwood Plant) 817272 (shipment to Brownwood Plant) Krolor Orange K0-789-D Lots: PS-99166 806281 (shipment to Brownwood Plant) Monastral Green B GT-674-D Lots:! St-90999 (TCI Product) PS-89855 973372 (shipment to Brownwood Plant) 829932165 (shipment to Brownwood Plant) 833324 (shipment to Brownwood Plant) The 3-roll mill dispersion method was chosen based on this method being used in production, at the Bro.wnwood, TX Plant. The attached instrumental color data summarizes 3M's studies, While re viewing this data, Roy Pancoast and Bill Zonin presented instrumental color data for the same lots dispersed using the Hoover-Muller equipment. In summary, it appeared that a correlation in color data between HooverMul ler and 3-roll mill dispersion existed for the inorganic pigments (Krolor), while major differences were noted for RT-759-D and GT-674-D. Based on our technical discussions the following was agreed to as a con tinuation of our cooperative program with 3M. This phase is targeted for com pletion and review in late May. Round-Robin Dispersion - Color Measurements. - L. W. Pancoast will supply a lot of RT-759-D to Chestnut Run, St. Paul, and, Brownwood locations of 3M. - R. Pinamonti will supply vehicle and formulation for 3-roll mill dispersing RT-759-D at Newark, Chestnut Run and Brown wood 3M Plant. - Tint color exhibits from St. Paul, Brownwood and Newark will be sent to G. R. Patrick for obtaining DuColor color data (L.a.b. color difference).. Tentative Proposed Specifications for 3M. - This cooperative study is targeted to determine whether the following pigment specifications on our products can be agreed to .for 3M: DUP050146236 TO: B. H. GARTH C&F, CHESTNUT RUN - 3- February 17, 1982 535 on strength. FMC2 Color Difference = 2 units (adjusted for strength). Color measurements will be made at Chestnut Run in order to obtain DuColor data consistent with the Newark plant's procedure. R. R. Norton plans to investigate the position of 3M's Traffic Control Materials Division on GT-674-D. GRP:dm Attachments DU P050146237 3W Coirpany Bid*. 209 - IK 3M Center St. Paul. Minn. Attention: Marlin Seifert Deer Marlin: A* per our conversation, note the anclooed draw down pf 3991 Magenta aide by side, (lot #27 and Lot #26). As you can imagine, this does irake it rather difficult with our FORMULAS. Just thought you might be Interested. Beet Rogarda DU P050146238 N 26985.01 COLOR K Y -781D R M -32138 G T-674D R M -6413 DISPERSION STUDY PASSES DC DL DE 0.0 0.0 0.0 0.3 0.0 0.3 mCM CM 0*0 0*0 0*0 ot 1.5 0*0 a* o CM cr o Cs| K\ Q- <(9ft CO 00 (O K r11 o2 * CL I t [ 0.8 ! O1 0.0 0.8 DUP050146239 N 26985.02 DISPERSION STUDY \ CO h- CC oo UJ o O u> o oo Oo oO m CO UJ CO CM CO < Q. ID O CC o a 0 o--I o> CO to T" K to oi 1 H2 GC CC DUP050146240 L O T # DC D L REPRODUCIBILITY STUDY CO 8cc oo oo CT> <--I o Hi o oD * o io o )o \o o to o o tr> oO ro vo o VO o ho oI Uf> o CM 04 CM CM .... ,TC COLOR 00 CO CM 00 N CO 1I >2 * cc Q * N (O I h O <0 * CO I 0 O) 00 N1 O CO <0 0 00 O) 00 TP-* to r>. 11 2 h- OC OC CO CO T-- to I 2 oc J. DUP050146241 N 26985. 111 i i RG YB DC DL DE RTS 0.0 0.0 1 0*0 0*0 0*0 0*0 0*0 0*0 1.9 -0.1 106 ooH =r cvj 3.6 .CoD .J)* di oo ac-j to sr r-5 2.3 2.7 3.5 -=r H ci' --i t Hsr R S' R 3 0H0 99166 (CONTROL) 806281 97471 ___ (CONTROL)_ 0 Jr 1 *. 2CO ^ l % o 2 '2 is S S <o 7 8 0.1 iL_______ 0.7 1.5 i l LOT# COLOR N 26985.04 11 * **' * DUP050146242 * *- *h w * Ah***. COLOR LOT# RG YB DC DL XR PS-89855 DUP050146244 N 26985.05 PS-89855 DUP050146245 PS-89855 DUP050146246 \ 80.0 PS-88855 / 10.00 DUP050146247 COLOR PURPLE v ^HOOVER MULLER DUPONT s) s CO 3 ROLL MILL BLUE HOOVER MULLER 3 M (ACS) DUPONT rn i r--1 1 cr m =r oo m H in o oo m O cr i RG YB DC DL i '0.3 -0 .1 0 ,1 sr r-v i OO r-i oo o 1 ---------- -- CM ot o o </> o < s CO DUP050146248 3 ROLL MILL 3M (ACS) t i 1 1 1 ! -0 .8 2 .1 N 26985.06