Document VGbj7xErneZ7zb9R9x37MnEbw
"I1; /fy'4 Pty/Atf'sr*y, 3>fiy 36 rtep <& /#* *K
,.v, (l.05 ) 106
nCSa--*
CQ \ 45 c o d e
YT-85$*D
pko .
c.v.
mit'" 34353
EST, WGT *^LK-
:4&X0. HRS.
TIME
MAKING INSTRUCTIONS: BATCH
d ,v . 300, 315, 317, 322, 323
PROCESSES
APPROVED BV
( ) YT-858-0 (A) EWK 10-18-76
( > ....... ...r ()
( > . .........': TYPED BY emwU8U/78
< ) BCT05^Z2P78 U DCS 05-30-7F ( ) TOT'1)'P3{P78
r
k-*p A<sXrfr++`'f*-" A>
&c u/* A*a * JPo*+
i*A/e To STgsM* Pto**/? *//*
7/*j*/f** a *s To
:
*
S^thfSS/
-yT T'***y ?&-/* $-//*>su, >* /.
So**#* -
BLEEDING
q u ip me n t
NA^E: "DAIiAMAR" YELLOW
.
Prep 1 Obtain For S?
1 2 Obtain For S's 23 a 52 3. Install dust hood
3A Clean, dress, close 24" clarif press - 15 frames
Close ALM - outlet and run in 1900# water AIM J5--*- Zero water meter
2 added to fluid.iz .1e*0.m.ust be m11e.t1er>et d_C sl.u Uliifi* w<L
6 Start agitator 7 Dump & rinse in usinq minimum water
. -
Note; (1) Stir 1 minute after each drum addition (2) Use minimum water to maintain fluid
--fi *
Record:
Drum stencillinq
Lot Dr No Net % #100%
Tfc "73
tkS Hv 9 7
Newark Check-Weigh
Gross
Tare
Net
m '... v#
WB
/iO /Ct.
lift
r/> t.cb
/// if 3
/'9C /fC.
/a- /4S U,t /> /6S 6/,o
/9< 7W
/A9Ss
// 15s
>fD
t6* >*S
f(?S Zto
tHS ft
fiS 2*
.............
...........
*
//0_ /Of /eS //* t/oi?f
i/S --3*n
/*}
Wo / 8i/
/7Ti
/t i7 _/<M
/7
1/<ZS*r5.
(& 3 /6 7 //. 9*
USE LBS. .
>
~-N..-- CODE
N-157-C
46-C
ACCT. LBS,
.f - :J< . 157-C 974
-
7 75 ' . ."%0~ *S,&
372"
' i X.t'r=.M'i:J--' *a--------- -------------------~
. /7C V-- fJ
8 Stir 45 min
Record: Start /{y.Sf&f
Note: Add minirtnim water to fluidize if necessary
9 When S8 stir complete, take 2 - 16 oz samples and deliver to Analytical lab for % . amine analysis
il ^Record: Water meter readinq
// fo #
Stop agitator & record: pH
I3.b - 5.0)
DV 3
3E9 REV,
7* ------------------ '---- '------------- -/
,R^n 2" (50 g) water into V- .r^OQ
14/ ^ujnp ALM without agitation into DV a turn on agitator
iV 2CSd'' 1000# water to ALM & pump in
16/ .Rinse down sides of ALM a basket a pump in
tjss/nbt. proceed with batch until lab analysis available.
'When analysis available, calc total amine
1900# +
#net wt N-157-C + t / \r, # water
From Sll X .,2^43 %----A--m--i-n--e----=---.-..------------9-----^-*--7-----#----a--m--i-n--e--- --
(r....
/ rfjari \ iJL/
' iT * /
EQUIPMENT
PAGE 2 Cg 46. c o d e YT-^^-D^w k ^^s t . WGT. 2313
1ST Calc factor for adjusting^batch = 9*34/# amine from"
irwtin = C
LBS.
c\
20 Scaleup or down ingredients (calculate) 1. N-7-D Step 22 32 Xtf. Ci5Y factor ^
3/ #
2. N-46-C Step 23 88 X
3. N-725-A Step 28 26 X 4. N-30-D Step 30 189 X 5. N-28-D Step 35 458 X 6. N--725--A Step 38 405 X 7, TJ-7-D Step 40 444X 8. N-30-D Step 41 689 X 9. N-979-D Step 51 67 X
ftQ. W--46--C Step 52 1263 X
LI. N-398-C Step 61 10 X L2. Calc Est wt = 23X3 X
factor = H5-H
^ factor = ...7`5 #
^ factor """fm'H yrnsJamssaa #
factor U
tt
factor ? 3$$
factor
4'zzr#
factor mo #
factor
UJL
.-jEactor = /-2/ =0.
'factor * /ys #
factor Q.2 !g #
-7 'NOTE: Proceed with batch" when above calc complete
303 24" (583 g) water into V-303
Welch on Postal Scale S dump in From S2
te: Break up lumps Lot
#100%
-
~T- qsL
45 rain, to dissolvej, ..foorr.,.S 28
jl
DV
S24 Run in 10" 1323
water into V- ^5>F!
& stir 5 min
Pumg/~DV thru clarif press to precoat
303
24 stir complete weigh on postal M
Z5SSX
}y pour in & stir 5 min ip &Q~62gF Record Temp
F
.on in in 4-6 min
*4- V
o 49" (1175 G) at 66-70E
min & record'; p H
(4,1^5)
inecessary, adj to pH'4.1-4.5 S Record; p H
Assume 77% Assume 50%
3 hrs minimum for S58 maintaining at 66-70F
Record:
Start
fV,lATptal miin~
DV
into DV from V-324
_M
7 10 min or longer to wet
aj DV to 37" (1280 q) at 20-22uF
; Siphon in in 12-15 min
uJ "
39 Stir 30 min at 28-32F maintaining -t CR Kx for S42
Record: /Time StartM .. CR NOTE: / ypL-i/'/VyiLr S^lU^ tJ
W KI_
(+)
liL..If, CR-.Kl-. add yfe# as is increments
-CR. iLc_KI_
(L
If CR+,KI-, ad^20# "as is "^increments
Record: CR
<+),KI
(+)
Assume 32% Assume 33%
Misc 8
S39 stir Weigh in drums for S46. M JSl .
dn Buddy for S55
M 3
a*
DV
K 53030 REV 5'. J ' > -
S39 stir complete, dump in
rn 30 min at
28-32nrF maintaining + CR.
+ Kt
4for S49
NOTE:
(1) If CR--. add 20# "as is" increments
Assume 32%
Record:___CB_
i+1 KI...
43-
~pr
at
15 10
7D 4firC
37
SI
777-A 5 |
J25=K
57-A 30--D 57-a
as.
30-D 7-0
57-A 443*
28-D
57-A 725-A
57-A
28-D 7
725-A
4xb 7-D 30-D
113-A _LSs 777-A
57--A ^ 5.J
28-D
DUP050292952
c9ont'd
....
PAGE --3*-- - CG 4-6-----C--O--D--E-- ----T--T- J-8'..5..8...-.D... jg-.'e~Us't<-*. W GT.--7*-2--3--1--3-
If CR+, KI=. Record: CR
"as is" inacsrxesdmfennkt^s'.
(+) , KI
(+)
LBS. Assume 33%
S44 stir, run 10" (970 G) water into V- \oS temp chart ~ tI-7-D from S 40
30" (2928 G) at 66-70F stack damuef
&
,an33Mfc
ACCT
57-A
v
Misc 12
CV 13
4r When S44 so.ituixri. .cv.ovimujjxp<laeutec t .tuecbsLt. DUVV ,&ot RxnSeCcOojrTdQ*
.? .
4* (+). KI "T' (+) , temp *av F' (2a-32Fl
NOTE;
{1} If CR-, KI- add 22j0# "asis" intffements
Assume 32%
Record: CR
W> KI
JL
) If CR+. KI- add /Son "as is" increagnts
As sume 33%
Record:CR
(+), KI
<+)
im Pump DV^thru clarif press into V-
maintaining
28-32F Record: time startV.ltN^W total min. 52
51 D
in 20 gal water in drum for S68
2. 23
725-A
2 x 330 . 57-a
is: ' 979-D
d*
Dump in from S2 Mote: Break u p lumps
lot
min to dissolve
[i4
#ioQ%
m
1SL
SE I
tack, damper
in Ny^SQ-D from S41 undersurface in 20-25 min
min & Record:^ pH %,
(5.8-6.3)
ecessary, adjptjya^pH 5.8-6.3
Assume 50%
Assume 77%
S34 stir complete, run in V-303 on surface AFAR
-4r-C. LklX
Ik
zf _Z=B_
30-D
?henlr/--S50 ..cmro.-r --m,yp--lete, wash DmmV,. li-n* ^esm-* ,f - pJ-rump S ^press. far ^20 fmV| in to a - CR test on a sample of total press effluent/.
.ickeVer comes first collect washings in DV fs50V
' ^in,S_ record: . Temp
. (28-32FlXf if
u,~
adj to 28-32F Record: in rubber bucket & wash into DV
UF,VDt.\:ggr
s record: KI .
(-)
If necessary adjust to - KI & Record: KI
163 complete,, adj CV to 3j3" (3708G) at 80-84F
.ecord: HT
F, REC dY F 1 VflLUMg
^r-
ImmediatelV run in DV thru undersufvace'rii stHhntoriinn ObuU-'`bDoj Tmniinn . MMaai' in#taai*inm CV at f8iHQ.-P84A'U-'UF* , RPoe^cnovri^d; TTiimmae Start ^
Total min
10
X
wr
57-A 395 D 395-D
R
10
iZhefr S65 complete, stir 10 min
Diazo
* (-,) Base
VpJWMfe.
Of
(+1<PH
(1^ If Diazo 4-. Base
and pH below 4.3:
2
IX(4.3-4.~7l
(a.) adi to pH 4.3-4.7
Assume 50%
(bl record: pH
(2) If Diazo +. Base
and pH 4.3 or above
add 8# 100% N-7-D to a 55 g drum
(b) Adj with water to # 25 G
7-P. . 7-D:
DU P0502 92953
x^.fcAWW.AfuWxi-
EQUIPMENT
------ *-- -- --^--*-i --~ -------1---- ------ "*-- '
PAGE 4 CG 46 CODE YT-858-D
EST. WGT. 2313
*-------- -- tBS.
CV (c) add 20# 100% N-46-C
15(cont d
(d'5 stir to dissove
(e) pour into CV
Y''>
(f) stir 10 min 4"3).. Repeat (1) & (2) above as necessary to - Diazo,
9- $n*s
yvl
J3*SfflST in N-979-A from S 51
JKeat to 200-204F in 40-45 min
?kL JSJferr 30 min at 200-204UF
Record: time
ny? ,ut off steam ^
-
$*g? Record pH &, /5 (4.2-4.7)
j) r %f. -?
!>** ``flood to 94" '(91740 & stop aqitator a c c o r d trew? ~QM-.-jZF ..........
+ Base
r USE LBS.
Zs t a r t T
" '
..... n A- *
XJ f
'
RlN r\ / >0 /y & *--/
! SPTK " ! ~ / 2-o
H CODE
46-C
ACCT. LBS.
---1
'I i
. . "' i
1
$ -< ' '
;$ v
' . . >S . _ /
^`
^
* 1
j: ' \s 1
I '
?
J $*
.
'i
\ j.
.
.* . * *- . ' *
. . .] ;1
S*
&**1^4; i * .'
DUP050292954
N 31964.01
DUP050292955
N 31964.02
DU P0502 92956