Document VG2Gy462oaOnLGvEV68Xjqjr4
> C.VS9M
{VG 32 . COPE RT-867-D PKI
0Ct44.J98M'
K?8i5--.
< DATE >
(LOT NUMBER)
EST. WT. 2386* LBS.
' PREPARATION NOTES:_________
90S P.V. 902,904
tf/fl
PROCESSES ( ) RT-867-D <G>
APPROVED BY: EWK 01/21/82
COMTYP JOB NAME: 32RT867DMG
STANDARD HRS. ___________ TIME___ __..M
EQUIP MENT
NAME: WATCHUNG RED B
USE LBS
NOTE: DO NOT START IF PRESS WILL NOT BE
1
AVAILABLE WITHIN 3 HRS AFTER MAKING. MAKING}
SUPVR TO REVIEW WITH P.R. SUPV 6 RECORD:
}
PRESS WILL BE READY______ M__,____PR SUPVR }
START MAKING _____M_____ __MAKING SUPV________ I
NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF I
AREA UNDER V-922
I
NOTE: RUN 15* WATER INTO V-904. PUMP WATER i
FROM V-904 THRU DISTRIBUTOR. IF WATER DOES i
NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH !
FULL FORCE, NOTIFY SUPERVISOR.
-1
PREP 1
i 1 | RECORD:_,____BATCHES SINCE SPARKLER LAST
}
I 1 CLEANED. AFTER 4 BATCHES, CLEAN, DRESS
i
} } SPARKLER 6 PRE-COAT WITH 15* DICALITE,
i
j j *-F1l t e r AID
},
l^ST| OBTAIN FOR S7 2-CHLORO-4-AMINOTOLUENE-5- |
'SULFONIC ACJ.D
I
i 3 LJJBJAIN FOR S23 3-HYDROXY-2 NAPHTHOIC ACID 1
lii^-TINSTALL DV 6 CV RECORDER & CONTROLLER CHART I
-38* <7830> WATER INTO V-922
1
WEIGH SSMUM HYDROXIDE IN V-926 6 RUN IN 1 y ,, .
m_\iL.
f TURN ON AGITATOR 6 STEAM & DUMP IN FROM S2 I
IO. ! 2-CHLORO-
L&T .
10O% . JZ
tJ JJIi4-AMINO TOLUENE j0L._ -----------
f 5-SULFONIC
________ _____________
N-CODE
A OCT LBS
777-A 740-C
81
i____ |
i
' 7-D 740-C
i 226 11157 I I
ACTIVATED CARBON FILTER AID
25
1 1.3-B
25
10
777-A
10
\J^ 2i2-21>*EG F
WATCH FOAM
RECORD: BYMUST BE + SODIUM
lYDROXIDE
ASSUME 50%
STIR 30 MIN AT 212-214 DEG F, THEN SHUT
7-D I;___ _
OFF STEAM
UATCH^FOAM
RECORD: SPARKLER PRESSURE __Q?___PSI. IF
.ZERO, NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNTIL SOI.1N IS CLEAR. M1AAIINN1TAIN. <^T^90~195
FOR SI 6 RECORD: START_fj>
:OTAL. MIN__<gb^L__ CLARITY.'
RECORD: HT /9< DEG F 6 REC
DEG F
I
MAKING INSTRUCTIONS BATCH UNIT
EQUIP WENT
.
! PAGE 2 OF 3 CG 32 CODE RT-867-D < G )
. 904/C 3
It i i lUTI
P1
RUN i * <__,_G) WATER INTO
NOTE:
Uu^^eEr- CI V IF MTY, IF CV IS NOT AVAILABLE USE
-904
WHEN SI 3 COMPLETE', PUMP IN V-922 THRU
SPARKLER MAINTAIN V-922 AT 199-195 DEG F
USE LBS
I N-CODE ! ACCT I I LBS
I----- If
t1
MI SC 4
QS&t*-
WEIGH SODIUM NITRITE IN P M
WEIGH SODIUM NITRITE IN DRUM FOR S40
HEIGH SODIUM NITRITE IN DRUM FOR S41
X
MEASURB$^l|aMITS IN V-92i_F0R\S52~~ ___7.
HYDROCHLORlJiT ACID
M,,
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'V i
''M.
N
1
1 ...... ,,.v. \
1_________-Htl i i{
I______U_ i j|
725-A i 375
725-A
m
725-A
\
1
i i 1
33 33
2S-D i 556
N 66* <1720G> WATER INTO V-902
t,WEIGH IN V-926 RUN IN M_f3___,, ^LQ3 I DUMP IN FROM S3 <~fr 3-HYDROXY-
^f-NAPHTHOlC ACID
i 1 7-D !! 713
I 82-C i1956
I!
ADJ TO 70-90 DEG F f,. STIR 10 MIN OR LONGER i
TO DISSOLVE FOR S41
1
922 O./
i
ri i
WHEN Si 8 COMPLETE, STOP PUMP 6 INSERT
1
^9^2 FOOT PLUG
1
RUN IN 10* <i67G) WATER & HEAT TO 190-195 F|
! CIRCULATE 15 MIN THRU SPARKLER
1
ii
THRU SPARKLER INTO V-904/CV
I
(BOG) WATER ft HEAT TO 190-195 F |
15 MIN THRU SPARKLER
!
1 I 1 i 1
i i |
) 1
*-922 THRU SPARKLER INTO V-904/CV 'WHEN MT BLOW OUT SPARKLER INTO V-904/CV
1 HEAT TO 165-170 DEG F
| I NOTE; IF N-740-C SOL'N (SI 5 f, 16) WAS PUMP-
| i ED DIRECTLY FROM SPARKLER TO CV OMIT S30,31
CV 1,30 r-^UU $N 1* (95G) WATER INTO V-;_____ .
10 i^.,l,,ij.l.ipUi'ir,,V-904 AT 165-170 DEG F THRU UNDERSUR-
FApE DISTRIBUTOR INTO CV AFAP (12-15 MIN)
JMHNTAIN 165-170 DEG F IN CV
'k.RUN
N-28-D HYDROCHLORIC ACID FROM S29
>-15 MIN
( 15 MIN AT 165-170 DEG F
i/d
TO 47* (4442G) AT 32-38 DEG F l
|fe5X330|
IN N-725-A SODIUM NITRITE FROM Si 7 AFAP
57-A
iO MIN) f. RINSE IN PT.
DU P050102168
EQUIP I MEN!
, - j -r----- t------------
MAKING INSTRUCTIONS:BATCH UNIT
E 3 OF 3
-867-D
I USE I N-CODE ! ACCT
(O i LBS |
i LBS
NTAIMING
LZSe>
CRJ^T_____< + > ,
<+>
NOTE: <!> IF CR-,
AS IS*
ASSUME 32%
._< + >
(2> IF .CR+, KI- ADD 205= *AS
INCREMENTS
5JDDIUM NITRITE
A, IME 33%
iECORD CR_______ _(+) KI__________
PIN CALCIUM CHLORIDE
HP IN BARIUM SULFATE
`0 MAINTAIN CV AT 32-38 THRU S44
IN N-725-A SODIUM NITRITE FROM SIS
1)
i{ J j il ri
ii ii ii ii I1 US 55 I j 3$X330|
57-A
28-D
725-A 20-A 65-A 57-A
I
1
I } |
1 i }
i I ! 1
POUR N-725-A SODIUM NITRITE FROM SI 9 INTO
85902 DUMP IN AMMONIUM CHLORIDE 6 STIR 2-3 MIN
I1
i
I 226 | 165-A 1 2,26
IMMEDIATELY COUPLE V-902 THRU UNDERSURFACE
DISTRIBUTOR INTO CV IN 18-22 MIN* MAINTAIN
32-38 DEG P*
*--*'"
RECORD : START^Jy&__TOTAL MlNj^L-
30 MIN
a
ASE__j j fc--<+> DiAzo__rrrri_(-)
_____(9 *0-9 *8) . ,'iC
H 9*0|-F*2 SODIUM HYDROXIDE
I A -
ASSUME 50%
- IPH
YDROCHLORIC ACID
> 'V ASSUME 32%
| | !___ _
Pd
1
57-A
7-D 28-D
*/- 70G AT 135-145*F FROM HOT WATER "XER INTO PT DUMP IN BARIUM CHLORIDE STIR TO DISSOLVE FOR S50
200
16-B
20
mms-srT
S49 c o mp l e t e , r u n p t in t o c v & r in s e i
i ixIn p t
I
5Ji \' MEASURE I OCTANOL IN CALIBRATED CONTAINER |
POUR IN
|
TEAT TO 193-195 Dfit F IN 75-80 'MIN' . I
[CORD: HT..JJ5L4___ DEG F & RBC_J^^2__DEG Fj
MIR 60 MIN AT 193-195 DEG F
20 MIN S54 STIR RECORD:
i3___ <8* 2-8* 6)
WHEN S54 COMPLETE, FLOOD TO 180-190"
<+/- 18,0000' & STOP AGITATOR
38
588-A
38
WHEN INSTRUCTED BY PROCESS AREA HALFWAY THRU PRESSING, DUMP IN I OCTANOL & STIR 5 MIN STOP AGITATOR & RESUME PRESSING
START
QPTR.
10 I 588-A 1 10
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