Document V3m597kXx8qDLzoajk1EykEkK
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION VI HOUSTON BRANCH SS08 HORN WOOD DRIVE HOUSTON. TEXAS 77074
October 12, 1988 MEMORANDUM
SUBJECT: Laboratory re^ulti for PPG Industries.
FROM: ft
M. Kendall Young Chief Inorganic Section
TO: Diana G. Ayers Chief . Houston Branch
Attached are laboratory results for the subject site. Thirteen (13)
water samples were received on September 1, 1988. Eight (8) of the samples were to be analyzed for metals, cyanide, phenols and total suspended solids.
The laboratory numbers assigned were 8AFEIE7601 through 8AFEIE7613.
This is a final report.
02^353
Date: 10/13/88
US ENUIRQNMENTAL PROTECTION AGENCY ENUIRONtiENTAL SERUICE DIUISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Appendix j
Activity Number: 8AFEIE76 Date Recvd: 09/01/88
Sample Number:
1
Time Recvd: 13:30
Source:
PPG Industries
Site Description: Blank sample
Sample Type:
WATER
Sample Retention:
Param-
Organic: Metals: Inorganic: Biology:
ABN UOA MTL CN OH-
JDue Date: )at Projected:
"Date Completed: Comment: Your Initials:
10/06/88 10/06/88
//
RLR
Date Collected: 03/31/83 Time Collected: 11:15
Tag Number:
SL 023354
pagc 2-or^Y ORGANIC ANALYSIS DATA
Attachment
6ES-HL SAMPLE NO.: 8AFEIE76-01
DATE REPORTED: 9/29/08
SAMPLE TYPE: WATER
ANALYST:MARVELYN HUMPHREY
i-ISL ACID BASE/NEUTRAL COMPOUNDS BY METHOD 625
COMPOUND
ug/L
I
COMPOUND
ug/L
Phenol .......................................................nd dl=4
bis<2-Chloroetnyl) Ether ...nd dl=2
2-Chlorophenol ..................
.nd dl=4
1.3- Dichiorobenzene .................. nd dl=2
1.4- Dich 1 orobenzene ...................nd dl=2
Benzyl Alcohol ...............
nd dl=4
1 >2-Dichlorobenzene .................... nd dl=2
2-Metnylphenol ................................. nd dl=6
bis<2 -chloroisopropyDEther .nd dl=2
4-Methylphenol ................................. nd dl=6
N-Nitroso-Di-n-Propylamine .nd dl=6
Hexacnloroethane ............................ nd dl=2
NitroDenzene .......................................nd dl=2
Isophorone ....................................... ..nd dl=4
2-Nitropheno1 .................................... nd dl = 10
2.4- Dinethylphenol .................... nd dl=6
Benzoic Acid .......................................nd dl=10
bis<2-Chloroethoxy)Methane .nd dl=2 2.4- Dichlorophenol .....................nd dl=6
1.2.4- trich1 orobenzene ......... nd dl=2
Naphthalene ......................................... nd dl=2
4-Chloroaniline ...............................nd dl=4
Hexachlorobutadiene ....................nd dl=2
4-Chloro-3-Methylphenol ....nd d1=0
2-Methylnaphthalene .................... nd dl=2
Hexachlorocyclopentadiene ..nd dl=iO
2,4,6-Trichlorophenol ............. nd dl=6
2.4.5- Trichlorophenol ;.........nd dl=6
2-Ch1 oronaphthalene .................... nd dl=2
2- Nitroaniline ...............................nd dl=0
Dim thylPhthalate ......................... nd dl=2
Acenapnthylene ................................. nd dl=2
3- Nitroaniline ............................... nd dl=8
IAcenaphthene ...................................... nd dl=2
12.4- Dinitrophenol ....................... nd dl=30
l 4-Nitrophenol ................................... nd dl=8
IDibenzofuran ...................................... nd dl=2
12.4- Dinitrotoluene .....................nd dl=6
12.6- Dinitrotoluene .....................nd dl=6
IDiethylphthalate ............................nd dl=2
I4-Chlorophenylphenyl Ether .nd dl=S
IFluorene .................................................nd dl=2
I4-Nitroaniline ................................. nd dl=8
14.6- Dinitro-2-Methylphenol .nd dl=2G
IN-Nitrosodiphenylaciine ...........nd dl=4
I4-BroMophenylpheny1 Ether ..nd dl=8
IHexachlorobenzene ......................... nd dl=2
I Pentachlorophenol ......................... nd dl = 15
I Phenanthrene ...................................... nd dl=2
lAnthracene ............................................nd dl=2
IDi-n-Butylphthalate ....................nd dl=2 I Fluoranthene ...................................... nd dl = 2
I Benzidine .............................................. nd dl = 20
IPyrene ...................................................... nd dl = 2
IButylbenzylphthalate ................. nd dl=4
l3,3'-Dichlorobenzidine ...........nd di = lG
IBenzo<a)Anthracene ...................... nd dl=8
lbis-(2-Ethylhexyl>Phthalate
60
IChrysene ................................................. nd dl=0
IDi-n-Qctyl Phthalate ................. nd dl=4
I Benzo<b)F1uoranthene ................. nd dl=8
IBenzo<k)Fluoranthene ................. nd dl=8
IBenzo(a;Pyrene ................................. nd dl = 8
IIndeno(1,2,3-cd) Pyrene ....nd d1=8
IDibenzo(a,h)Anthracene ...........nd dl=8
IBenzo(g,h,i)Perylene ................. nd dl=8
SL 023355
PAGE 3 OF<V
Attachment
6ES-HL SAMPLE NO
ORGANIC ANALYSIS DATA
BAFEIE76--01
DATE REPORTED: 9/29/88
SAMPLE TYPE:WATER ANALYST: MARVELYN HUMPHREY
TENTATIVE COMPOUNDS BY METHODS 625
EST.CONC SCAN# CAS * (ug/I)
1169
5
COMPOUND NAME UNKNOWN PHTHALATE
1178
UNKNOWN PHTHALATE
1181
8 UNKNOWN PHTHALATE
1196
6 UNKNOWN PHTHALATE
* ANALYSTS NOTE ! - THE COMPOUNDS LISTED ARE TENATIVELY IDENTIFIED BY THE BES1 MATCH WITH THE NIH/EPA/WILEY MASS SPECTRAL DATA BASE OR BY MANUAL MASS SPECTRA INTERPRETATION. STANDARDS WERE NOT AVAILABLE FOR CONFIRMATION OR QUANTITATION. ** Estimated concentration is based on a RF of 1,0 to internal standard !
SL 023356
w ut ui ro oi r j tn ro r j ro tn cn cn ui m cn ro ro to ru to ro oi ro r-j ro ta ro to r j oi loi r j
PAGE 4"0F (/
At t achwent
ORGANIC ANALYSIS DATA
6ES--IiL SAMPLE NO,: BAFEIE7601
DATE REPORTED: 09/30/88
SAMPLE TYPE: Water
ANALYST: R. McMiilin / E. O'Neill
VOLATILE COMPOUNDS BY METHOD 624
PPir
(2V) (3 V) (4V)
(6V) (7V) (10V) (11V) (13V) ( 14V) (15V) (16V) (23V) (29V) (30V) (32V) (33V)
(38V)
(44V) (45V) (46V) (47V) (48V) (51V)
(85V) (86V) (87V)
(88V)
CAS*; 67-64-1 107-02-8 107-13-1 71-43-2 78-93-3 75-15-0 56-23-5 108-90-7 107-06-2 71-55-6
75-34-3 79-00-5 79-34-5 75-00-3 67-66-3 75-35-4 156-60-5
78-87-5 10061-02-6
10061-01-5 100-41-4 519-78-6 108-10-1 75-09-2 74-87-3 74-83-9 75-25-2 75-27-4 124-48-1 100-42-5 127-18-4
108-88-3 79-01-6
108-05-4 75-01-4
95-47-6 108-38-3 1 06-42-3
acetone------------------------------------------------------------------acrolein ----------------------------------------------------------------acrylonitrile ------------------------------------------------------
benzene -------------------------------------------------------------------2-butanone------------------------------------------------------------carbon disulfide -----------------------------------------------carbon tetrachloride --------------------------------------chlorobenzene--------------------------- *------------------- -----1,2~dichloroethane ------------------------------------------1, i,1-trichloroethane ------------------------------------1.1-dichloroethane ------------------------------------------1,1,2-trichloroethane -----------------------------1>l,2,2-tetrachloroethane ---------------------------chloroethane---------------chlorofor-------------------1.1- dichloroethene ------------------------------------------trans-1,2-dichloroethene ------------------------------
1.2- dichloropropane ----------------------------------------trans-l,3-dichloropropene ----------------------------
cis-1,3-dichloropropene -------------------------------ethylbenzene--------------------------------------------------------2-hexanone------------------------------------------------------------4-nethy1-2-pentanone --------------------------------------Methylene chloride ------------------------------------------chloronethane -------------------------------------------------------
broMOMethane --------------------------------------------------------broMoforM---------------------------------------------------------------
broModichloroMethane --------------------------------------chlorodibroMOMethane-------------------------------styrene---------------------------------------------------------------------tetrachloroethene ---------------------------------------------toluene ------------------------------------------------------------------- trichloroethene-------------------------------------------------vinyl acetate -----------------------------------------------------vinyl chloride---------------------------------------------------o-xylene -----------------------------------------------------------------M-xylene and/or p-xylene ------------------------------------------------------------------
(ug/1) ND DL= 5 ND DL=100 ND DL=100 ND DL= ND DL= ND DL= ND DLND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DLND DL= ND DL=
ND DL= ND DL= ND DL = ND DL= ND DL= ND DL= ND DL= ND DL = ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL=
ND DL= 5
==3=a3===33a====33==^3====33=3=333=======S========
023357
PAGE S" dfQ7
Attachment ^
ORGANIC ANALYSIS DATA
6ES--HL SAMPLE NO.: 8AFEIE7601
DATE REPORTED: 09/30/00
SAMPLE TYPE: Water
ANALYST: R. McMillin / E. O'Neill
TENTATIVE COMPOUNDS BY METHOD 624
EST.CONC SCAN* CAS * < ug/1)
COMPOUND NAME
No VOA TIC's detected.
* ANALYSTS NOTE ! - THE COMPOUNDS LISTED ARE TENATIVELY IDENTIFIED BY THE DCS MATCH WITH THE NIH/EPA/WILEY MASS SPECTRAL DATA BASE OR BY MANUAL MASS SPECTRA INTERPRETATION. STANDARDS WERE NOT AVAILABLE FOR CONFIRMATION OR QUANTITATION ** Estimated concentration is based on a Rlr of 1.0 to internal standard !
St 23358
PAGE U OF _(JL_
ATTACHMENTS
US ERA HOUSTON BRANCH
SAMPLE #: SOURCE: TYPE: ANALYSTS:
8AFEIE76-01 PPG INDUSTRIES AQUEOUS CLARK,FELDMAN
DATE RECEIVED: DATE REPORTED:
0l-Sep-88 11-Oct-88
PARAMETER CONCENTRATION
DETECTION LIMIT <=
UNITS
ARSENIC SELENIUM THALLIUM MERCURY SILVER BERYLLIUM CADMIUM CHROMIUM COPPER NICKEL LEAD ZINC ALUMINUM BARIUM COBALT IRON MANGANESE VANADIUM ANTIMONY SODIUM POTASSIUM CALCIUM MAGNESIUM
ND 46 ND 48 ND 38 ND 0.2 ND 10 ND s ND 3 ND 10 ND 20 ND 20 ND 30 36 5 ND 100 ND 10 ND 20 ND 25 ND 3 ND 30 ND 60 ND 500 ND 1000 ND 150 ND 150
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
CYANIDE PHENOLS
ND 0.02 ND 5
MG/L UG/L
ND: NOT DETECTED
M ^Datei 10/13/83
US ENVIRONMENTAL protection agency ENUIRONMENTAL SERUICE DIVISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Append i x
Activity Number: 8AFEIE76 Date Recvd: 09/01/38
Sample Number:
2
Time Recvd: 13:30
Date Collected: 03/31/33 Time Collected: 13:45
Source: Sit Description: Sample Type: Sample Retention:
PPG Industries Canal |3 PH bridge WATER
"toxic
samp"
Tag Number:
Param-
Organic: Metals: Inorganic: Biology:
ABN MTL CN
UOA OH-
Due Date:
ate Pro jected: ate Completed: Comment: Your Initials:
10/06/98 10/06/38
//
RLR
SL 023360
PAGE 2^ OF^ ORGANIC ANALYSIS DATA
Attacnnent 2-^
6ES-HL SAMPLE NO.: 8AFEIE76-02
DATE REPORTED: 9/29/88
SAMPLE TYPE: WATER
ANALYST;MARVELYN HUMPHREY
MSL ACID BASE/NEUTRAL COMPOUNDS BY METHOD 625
COMPOUND
ug/L
Phenol .......................................................nd dl=4 bis(2-ChloroethyI) Ether ...nd dl=2 2-Chlorophenol ................................. nd dl=4 1.3-Dichlorobenzene .................... nd dl=2 1.4-Dichlorooenzene .................... nd dl=2 Benzyl Alcohol ................................. nd dl=4 1,2-Dichlorobenzene .................... nd dl=2 2TMMetnyIphenol ................................. nd dl=6 bis<2-chloroisopropyl)Ether.nd dl=2 4-Methylpheno1 ..................................nd dl~6
N-Nitroso-Di-n-Propylafiine .nd dl=6 Hexacnloroethane ............................ nd dl=2 Nitrob nzene .......................................nd dl=2 Isophorone ............................................ nd dl=4 2-Nitropheno1 .................................... nd dl = 10 2 > 4~Difiethylphenol .......................nd dl=6 Benzoic Acid .......................................nd dl = 10 bis(2-Chloroethoxy)Methane .nd dl=2 2.4-Dichlorophenol .......................nd dl=6
1.2.4-trichlorooenzene ...........nd dl=2 Naphthalene ......................................... nd dl=2 4-ChIoroaniline ...............................nd dl=4 Hexacnlorobutadiene .................... nd dl=2 4-Chloro-3-Methylphenol ,...nd dl=8 2-Methylnaphthalene .................... nd dl=2
Hexacnlorocyclopentadiene ..nd dl=10 2,4,6-Trichlorophenol ...............nd dl=6 2.4.5-Trichlorophenol ..............nd dl=6 2-Ch1 oronaphthalene .................... nd dl=2 2-Nitroaniline ................................. nd ol=0 DinethylPhthalate ......................... nd dl=2 Acenaphthylene ................................. nd dl=2 3-Nitroan11ine ................................. nd dl^S
COMPOUND
ug/L
Acenaphthene ...................................... nd dl=2
2,4~Dinitrophenol ......................... nd dl=30
4-Nitrophenol ....................................nd dl=8
Dibenzofuran ...................................... nd dl=2
2,4-Dinitrotoluene ...................... nd dl-8
2.6-Dinitrotoluene .......................nd dl=6
Diethylphthalate ......................nd d'1-2
4-Chlorophenylphenyl Ether .nd dl=8
Fluorene ................................................. nd d'l=2
4-Nitroaniline ................................. nd dl=8
4.6-Dinitro-2-Methylphenol .nd dl^SO
N-Nitrosoaiphenylanine ...........nd dl-4
4-Bronophenylphenyl Ether ..nd dl-8
Hexach'lor obenzene ......................... nd dl=2
Pentachlorophenol ......................... nd dl = 15
Phenanthrene ....................................... nd dl = 2
Anthracene ............................................nd dl=2
Di-n-Butylphthalate ...................
2
Fluoranthene ...................................... nd dl=2
Benzidine .............................................. nd di=20
Pyrene ...................................................... nd d'l=2
Butylbenzylphthalate ................. nd dli=4
3,3'-Dichlorobenzidine ...........nd d.L = 10
Benzo(a)Anthracene .......................nd dl=8 bis-(2-Ethylhexy 1 )Phthalate nd di3=4
Chrysene ................................................. nd dl=G Di-n-Octyl Phthalate ................. nd dl~4
Benzo<b)Fluoranthene ................. nd dl=8
Benzo<kJFluoranthene ................. nd d1=8
Benzo(a)Pyrene ................................. nd di=0 Indeno<1,2,3-cd) Pyrene ....nd dl=8
Dibenzoia,h)Anthracene ...........nd dl=G
Benzo<g,h,i)Perylene ................. nd dL=8
023361
PAGE 1> OF ^
2Attachment * ,/
ORGANIC ANALYSIS DATA
6ES-HL SAMPLE NO.: 8AFEIE76-02
DATE REPORTED: 9/29/88
SAMPLE TYPE:WATER
ANALYST: MARVELYN HUMPHREY
TENTATIVE COMPOUNDS BY METHODS 625
EST.CONCI SCAN* CAS * (ug/1)
COMPOUND NAME
Q UNKNOWN BROMINATED COMPOUND
528 100
UNKNOWN
400 6 UNKNOWN
405
20
UNKNOWN
548
12
UNKNOWN BROMINATED COMPOUND
590
45
UNKNOUN
* ANALYSTS NOTE ! - THE COMPOUNDS LISTED ARE TENATIVELY IDENTIFIED BY THE BES MATCH WITH THE NIH/EPA/WILEY MASS SPECTRAL DATA BASE OR BY MANUAL MASS SPCCTR^ INTERPRETATION. STANDARDS WERE NOT AVAILABLE FOR CONFIRMATION OR QUANTITATION #* Estimated concentration is based on a RF of 1.0 to internal standard !
SL 023362
PAGE ^TQlfy
At tacnmen t
ORGANIC ANALYSIS DATA
6ES-HL SAMPLE NO.: SArLIC76Q2
DATE REPORTED: Q9/3G/C0
SAMPLE TYPE; Water
ANALYST: R, McMillin / E. O'Neill
VOLATILE COMPOUNDS BY METHOD 624
pp$
(2V) (3V) (4V)
(6V) < 7 V) (10 V) ( 1 IV) (13V) (14V) (13V) (16V) (23V) (29V) (30V) (32V) (33V)
(38V)
(44V) (45V) (46V) (47V) (48V) (51V)
(85V) (86V) (87V)
(88V)
CAS 67-64-1 107-02-8 107-13-1
71-43-2 78-93-3 75-15-0 56-23-5
10C-90-7 107-06-2
71-55-6 75-34-3 79-00-5 79-34-5 75-00-3 67-66-3 75-35-4 156-60-5
78-87-5 10061-02-6
10061-01-5 100-41-4 519-78-6 108-10-1
75-09-2 74-87-3 74-83-9 75-25-2
75-27-4 124-48-1 100-42-5 127-18-4 1Q8-8G-3
79-01-6 108-05-4
75-01-4 95-47-6
108-38-3 106-42-3
acetone -------------------------------------------------------------------
acrylonitrile -----------------------------------------------------benzene ------------------ ------------------------------------------------2~b u tan one------------------------------------------------------------carbon disulfide ------------------- ----------------------------carbon tetrachloride --------------------------------------chlorobenzene -----------------------------------------------------1.2- dich1 or oethane-----------------------------------------1 ,1>1-trich1 oroethane -------- --------------------- ------1,i-dichloroethane ------------------------------------------1.1.2- tricn1 oroethane ----------------------------------1.1.2.2- tetrachloroethane----------- --------------chloroethane ------------------------------------------ -------------chloroform ------------------------------------------------------------1,1 -dichloroethene ------------------------------------------trans-1>2~dichloroethene----------------------- ------1,2~dichlorbpropane------------------- --------------- ------trans-1,3-dichloropropene------------ --------------cis-1,3-dich1 or opropene -------------------------------ethylbenzene--------------------------------------------------------2-hexan one----- -------------------------------------------------------4-methy1-2-pen tan one------------------------*--------------Methylene chloride -------------------------------------------chloromethane ------------------------------------------------------bromometnane -------------------------------------------------------broMoforM --------------------------------------------------------------brOModichloromethane --------------------------------------chlorodibromomethane --------------------------------------st yrene--------------------- ------------------------------------------------tetrachloroethene ---------------------------------------------toluene ----------------------------------------------------- --------------trich1 oroethene ---------------------------------- --------------vinyl acetate ----- ------------------------------------------------vinyl chloride ---------------------------------------------------o-xylene ----------------------------------------------------------------M-xylene and/or p-xylene --:-------------------------------------------------------------
( u g /1)
ND DL = 5
ND DL=:LOO
ND DL = LOO
ND DL = Li
ND DL= 5
ND DL= 5
ND DL" 2
ND DL= 2
96.4
ND DL= 2 ND DL= r>
10.3
ND DL= 2
ND DL= 5
30.0
ND DL= ND DL= ND DL=
oc. r>
ND DL= 2 ND DL = 4O.
ND DL= 5
ND DL = 5
ND DL = 5
ND DL = 5
ND DL = 5
ND DL= 5
937 i*_** o7
Wrir/) * W7l
ND DL= t*_r)
ND DL = il
ND DL = 5
6.7
ND DL = 5
ND DL = 5
ND DL = 5
ND DL= 5
PAGE 3 OF Lt
At tacnwent
ORGANIC ANALYSIS DATA
6ES-HL SAMPLE NO.; BAFEIE76Q2
DATE REPORTED: 09/30/88
SAMPLE TYPE; Water
ANALYST: R. McMillin / E. O'Neill
TENTATIVE COMPOUNDS BY METHOD 624
EST.CONC SCAN#I CAS * (ug/1)
COMPOUND NAME
No VOA TIC's detected.
* ANALYSTS NOTE ` - THE COMPOUNDS LISTED ARE TENATIVELY IDENTIFIED BY THE BEST MATCH WITH THE NIH/EPA/WILEY MASS SPECTRAL DATA BASE OR BY MANUAL MASS SPECTRA INTERPRETATION. STANDARDS WERE NOT AVAILABLE FOR CONFIRMATION OR QUANTITATION. #* Estiwated concentration is based on a RF of 1.0 to internal standard !
02336A
k_0F PAGE
ATTACHMENTS 2^
US EPA HOUSTON BRANCH
SAMPLE #! SOURCE: TYPE: ANALYSTS:
8AFEIE76-02 PPG INDUSTRIES AQUEOUS CLARK,FELDMAN
DATE RECEIVED: DATE REPORTED:
01-Sep-88 1l-0ct-88
PARAMETER CONCENTRATION
DETECTION LIMIT <=
UNITS
ARSENIC SELENIUM
THALLIUM MERCURY SILVER BERYLLIUM CADMIUM CHROMIUM COPPER NICKEL LEAD ZINC ALUMINUM BARIUM COBALT IRON MANGANESE VANADIUM ANTIMONY SODIUM POTASSIUM CALCIUM MAGNESIUM
ND ND ND 0. 35 ND ND ND 28 518 50 ND ND 364 101 ND 1690 168 ND ND 4980000 115000 157000 358000
46
48 38 0.2 10
5 5 10 20 20 30
5 100
10 20 25
5 30 60 500 1000 150 150
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
CYANIDE PHENOLS
ND 0.02 ND 5
MG/L UG/L
ND: NOT DETECTED
023^65
10/13/83
US ENUIRONMENTAL PROTECT ION AGENCY ENUIRONMENTAL SERUICE DIUISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Append l x
Activity Number: 8AFEIE76 Date Recvd: 09/01/88
Sample Number:
3
Time Recvd: 13:30
Source: Site Description: Samp 1e Type: Sample Retention:
PPG Industries Outfall # 401 WATER
Param- Organic: Metals: Inorganic: Biology:
UOA
Due Date: m.ate Projected
ate Comp 1e t ed Commen t: Your In i t la Is :
10/06/83 10/06/88
//
RLR
Date Collected: 08/31/33 Time Collected: 11:15
Tag Number:
St 023366
cn cn cn ro cn r j cn ro fJ tj cn cn cn cn cn cn ro ro ro ro ro cn ro ro ro ro ro ro cn cn ro
PAGE ZoF
A t tacrmen x
ORGANIC ANALYSIS DATA
6ES-HL SAMPLE NO.: 8AFEIE7603
DATE REPORTED: Q9/30/Q8
SAMPLE TYPE: Water
ANALYST: R. McMiUin / . O'Neill
VOLATILE COMPOUNDS BY METHOD 624
pp*
(2V) (3V) (4V)
(6V) <7V) (10V> ( 1 1 V) (13V) (14V) (15V) (16V) (23V) (29V) (30V) (32V) (33V)
(38V)
(44V> (45V) (46V) (47V) ( 48V) (51V)
(85V) (86V) (87V)
(88V)
CAS* 67-64-1
107-02-8 107-13-1
71-43-2 78-93-3
75-15-0 56-23-5
108-90-7 107-06-2
71-55-6 75-34-3 79-00-5 79-34-5 75-00-3 67-66-3 75-35-4
156-60-5 78-87-5
10061-02-6
10061-01-5 100-41-4 519-78-6 108-10-1 75-09-2 74-87-3
74-83-9 75-25-2 75-27-4 124-48-1 100-42-5 127-18-4
108-88-3 79-01-6
108-05-4 75-01-4 95-47-6
108-38-3
106-42-3
acetone -------------------------------------acrolein --------------------- -------------acrylonitrile -----------------------benzene ------------------------------ ---2-butanone -----------------------------carDon disulfide ----------------carbon tetrachloride --------
chlorobenzene -----------------------1,2-dichloroethane ------------1.1.1-tricnloroethane -----1.1- dichloroethane ----------
1.1.2-trich1 oroethane ---------
1.1.2.2-tetrachloroethane
chloroethane -------------------------chi or of oni -----------------------------1 , l-dichloroethene -------------
trans-1,2-dichloroethene 1,2~dichloropropane ----------trans-1,3-dichlor opr opene cis-1,3-dichloropropene -- ethylbenzene -------------------------2-hexanone ------------------------------4-nethyl-2TMpentanone -------Methylene chloride ------------ch1 oronethane-----------------------
brononethane ------------ ------------broMoforn -------------------------------bronodichloronethane -------chlorodibroMowethane -------styrene---------------------------------------tetrachloroethene --------------toluene ------------------------------------trichloroethene ------------------vinyl acetate -----------------------vinyl chloride --------------------o-xylene ----------------------------------n-xylene and/or
p-xylene -------------------------------
( u g /1) ND DL= 5 ND DL=10 0 ND DL=10 0 ND DL = ND DL= ND DL= ND DL = ND DL=
ND DL= ND DL= ND DL= ND DL= ND DL=
ND DL = ND DL= ND DL= ND DL= ND DL= ND DL= ND DL = ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL= ND DL = ND DL= ND DL = ND DL= ND DL= ND DL= ND DL=
SL 023367
ORGANIC ANALYSIS DATA
6S--i{s_ SAMPLE NO.: 8ArEIL7603
DATE REPORTED: 09/30/00
SAMPLE TYPE: Water
ANALYST: R. McMiUin / E. O'Neill
TENTATIVE COMPOUNDS BY METHOD 624
EST.CONC SCAN# CAS * (ug/1)
COMPOUND NAME
No VOA TIC's detected.
* ANALYSTS NOTE ! - T!tE COMPOUNDS LISTED ARE TENATIVELY IDENTIFIED BY THE DCS" MATCH WITH THE NIH/EPA/WILEY MASS SPECTRAL DATA BASE OR BY MANUAL MASS SPECIE INTERPRETATION. STANDARDS WERE NOT AVAILABLE FOR CONFIRMATION OR QUANTITATION ** Estimated concentration is based on a RF of 1,0 to internal standard !
023368 SL
Da t e : 1O/lJ/88
US ENVIRONMENTAL PROTECTION AGENCY ENVIRONMENTAL SERVICE DIVISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Append 1x
Activity Number: 8AFEIE76 Date Recvd: 09/01/38
Sample Number:
4
Time Recvd: 13:30
Source:
PPG Industries
Site Description: Outfall 018 (201)
Sample Type:
WATER
Sample Retention:
Param-
Organic: Metals: Inorganic: Biology:
VOA
Due Date: ate Pro jected: ate Completed:
Comment: You r Initials:
10/16/88 10/16/88
//
RLR
Date Collected: 08/31 Time Collected: 14: 00
Tag Number:
023369 Sb
aCilMen T
ORGANIC analysis data
6ES-HL SAMPLE NO.: GAEEIE76Q4
DATE REPORTED: 09/30/80
SAMi'cL TYPE; Water
ANALYST: R. Mchillin / E. O'Neill
VOLATILE COMPOUNDS BY METHOD 624
PP If
(2V) (3V> ( 4 V)
(6V) < 7V :> < l ov> ( 1 1 V) < 13V) (14V) (15V) (16V) (23V) (29V) (30V) (32V) (33V)
(38 V)
(44V) (45V) (46V) (47V) (48V) (51V)
(35V) (86V) (37V)
(88V)
CAS# 67-64-1
1 07 -0 2-9 107-13-1
71 -43 -2 70 -93-3 75-S5-0 56-23-5
108-90-7 107-06-2
71-55-6 75-34-3 79-00-3 79-34-5 75-00-3 67-66-3 75-35-4 156-60-5 78-87-5 10061-02-6 10061-01-5 100-41-4
519-70-6 108-10-1
75-09-2 74-87-3 74-33-9
/ J u J <_
75-27-4 124-48-1 1 0 0-42-5 127-18-4 108-88-3
77-01-6 108-05-4
75-01-4
95-47-6 108-38-3 10 6-42-3
acetone ------------------------------------
acrolein -----------------------------------
acrylonitrile -----------------------
benzene ----------
--
2 "b u tan one------------------------------
carbon disulfide ----------------carbon tetrachloride -------chlorobenzene -----------------------1 ,.2-dichlor oethane------- *--
1.1.1-trich1 oroethane -----i, i-dichloroethane-----------1.1.2-trichioroethane ------
1.1.2.2-tetrachloroethane chloroethane -------------------- -- chloroforM ------------------------------
1.1-dichloroethene -----------trans-1,2-dich1 oroethene
1.2-dichloropropane ----------trans-1,3-dichlor opr opene cis-l,3-dichloropropene -- ethylbenzene --------------------------
2-hexanone -----------------------------4-nethy1-2-pen tan one--------
wethylene chloride ------------chlor onethane------------------------
browoMethane ---------------------------- ~--
broMO-forM--------------------------------broModichloroMethane --------chlorodibrOMowethane --------
styrene---------------------------------------tetrachloroethene-------------
toluene -------------------------------trichloroethene ------------------vinyl acetate------------------ -- vinyl chloride ----------------------
o-xylene ----------------------------------M-xylene and/or p-xylene -----------------------------------
( ug /1>
202
ND DL = 100
ND DL= 100
ND DL= 2 ND DL = tur
ND DL= ND DL=
tr
o
n
4.
ND DL= -->
1 44 ND DL = r>
ND DL=
14
ND DL= 2
ND DL = 5
321
ND DL =
n
4.
ND DL= ND DL=
t_
r>
i--
ND DL= 2
ND DL = i_
ND DL= 5
ND DL= 5
ND DL= 5
ND DL= 5 ND DL= t*rJ
ND DL= 5
/
ND DL=
_ /
14 5
4.
ND DL = 5
ND DL = ND DL =
ND DL =
5 5 5
ND DL= 5
ATa &
SL 023370
ORGANIC ANALYSIS DATA
6ES-ML SAMPLE NO.: 8AFEIE7604
DATE REPORTED: 09/30/88
SAMPLE TYPE: Water
ANALYST: R. McMillin / E. O'Neill
TENTATIVE COMPOUNDS BY METHOD .24
EST.CONC SCAN* CAS * (ug/1)
COMPOUND NAME
No VOA TIC's detected.
* ANALYSTS NOTE ! - THE COMPOUNDS LISTED ARE TENATIVELY IDENTIFIED BY THE BES'i MATCH WITH THE NIH/EPA/WILEY MASS SPECTRAL DATA BASE OR BY MANUAL MASS SPECTRA INTERPRETATION. STANDARDS WERE NOT AVAILABLE FOR CONFIRMATION OR QUANTITATION. ** Estinated concentration is based on a RF of 1.0 to internal standard !
SL 023371
10/13/88
US ENUIRONMENTAL protection agency ENUIRONMENTAL 5ERUICE DIUISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Appendix
Activity Number: 8AFEIE76 Date Recvd: 09/01/83
Samp 1e Number:
5
T i me Recvd: 13:30
Source: Site Description Sample Type: Sample Retention
PPG Industries Outfall # 118 (201) WATER
Param-
Organic:
Metals: I no rgan i c : Biology:
MTL T33
Due Date: ^^pats Projected: ^P)ate Completed:
Comment: Your In 11 iaIs:
10/16/38 10/16/83
//
RLR
Date Col 1 ec t ed: 09/01/33 T i me Col lected: 06: 00
Tag Number:
023372 SL
ATTACHMENTS ^
US ERA HOUSTON BRANCH
SAMPLE #: SOURCE: TYPE: ANALYSTS:
8AFEIE76-0fT PPG INDUSTRIES AQUEOUS
CLARK,FELDMAN
DATE RECEIVED: DATE REPORTED:
Ol-Sep-88 1l-0ct-88
PARAMETER CONCENTRATION
DETECTION LIMIT <=
UNITS
ARSENIC SELENIUM THALLIUM MERCURY SILVER BERYLLIUM CADMIUM CHROMIUM COPPER NICKEL LEAD ZINC ALUMINUM BARIUM COBALT IRON MANGANESE VANADIUM ANTIMONY SODIUM POTASSIUM CALCIUM MAGNESIUM
TSS
ND ND ND 1. 16 ND ND ND 320 40000 1510 63 231 9450 59 ND 9930 113 ND ND 28800000 27400 8720 10800
510
46 240
38 0. 2
10 5 5
10 20 20 30
5 100
10 20 25
5 30 60 500 1000 150 150
n
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
MG/L
ND: NOT DETECTED
SL 023373
M
Date: 10/13/33
2/
US ENVIRONMENTAL PROTECTION AGENCY ENVIRONMENTAL SERVICE DIVISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Appendix (L7
Activity Number: 8AFEIE76 Date Recvd: 09/01/88
Sample Number:
6
Time Recvd: 13:30
Source: Site Descript ion : Samp 1 Type: Sample Retention:
PPG Industries Outfall # 018 (201) WATER
Param-
Organic:
Metals: Inorganic: Bio logy:
MTL BOD TSS
uDue Date:
m ate Projected
Date Completed Comment:
Your Initials:
10/16/38 10/16/88
//
RLR
Date Collected: 09 -"0 1/88 T i me Col 1 ec t ed: 05 : 40
Tag Number:
SL 023374
PAGE
^ 2^
ATTACHMENTS
US EPA HOUSTON BRANCH
SAMPLE #: SOURCE: TYPE: ANALYSTS:
SAFEIE76-06 PPG INDUSTRIES AQUEOUS CLARK,FELDMAN
DATE RECEIVED: DATE
REPORTED:
Ol-Sep-BS ll-Oct-88
PARAMETER concentration
ARSENIC SELENIUM THALLIUM MERCURY SILVER BERYLLIUM CADMIUM CHROMIUM COPPER NICKEL LEAD ZINC ALUMINUM BARIUM COBALT IRON MANGANESE VANADIUM ANTIMONY SODIUM POTASSIUM CALCIUM MAGNESIUM
ND ND ND 0.36 ND ND ND 69 1000 170 ND B7 411
133 ND
6790 122 ND ND
6120000 15300
142000 4360
TSS BOD
ND: NOT DETECTED
.15 ND
DETECTION LIMIT <=
46 48 38 0.2 10
5 5 10 20 20 30 5 100 10 20 25 5 30 60 500 1000 150 150
o
Am
3
UNITS
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
MG/L MG/L
Sh 023^75
10/13/88
US ENVIRONMENTAL PROTECTION AGENCY ENVIRONMENTAL SERUICE DIUISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Append 1 x
Activity Number: 8AFEIE76 Date Recvd: 09/01/38
Sample Number:
7
Time Rec vd: 13:30
Sourc : Site Description: Sample Type: Sample Retention:
PPG Industries Outfal 1 # 014 C101) WATER
Param-
Organic: Metals: I no rgan i c: Bio logy:
MTL TSS
Oue Date: ate Pro jec t ed: ate Compie ted:
Comm n t: Your In i t i a 1 s :
10/16/88 10/16/88
//
RLR
Date Collected: 09/01/38 Time Collected: 05:30
Tag Number:
SL 023376
^ OF PAGE
ATTACHMENTS
US ERA HOUSTON BRANCH
SAMPLE #: SOURCE: TYPE: ANALYSTS:
8AFEIE76-0'?' PPG INDUSTRIES AQUEOUS CLARK "PELDMAN
DATE RECEIVED: DATE REPORTED:
01-Sep-88
GO
GO
l +J
0u
1
tT--
tH
1 !
PARAMETER CONCENTRATION
DETECTION LIMIT <=
UNITS
ARSENIC SELENIUM THALLIUM MERCURY SILVER BERYLLIUM CADMIUM CHROMIUM COPPER NICKEL LEAD ZINC ALUMINUM BARIUM COBALT IRON MANGANESE VANADIUM ANTIMONY SODIUM POTASSIUM CALCIUM MAGNESIUM
ND
ND ND 1.34 ND ND ND 11 57 25 ND 154
314 193
ND 1630
248 ND ND
3130000 17800 46200 60700
46 48 38 0.2 10
5 5 10 20 20 30 o 100 10 20 25 5 30 60 500 1000 150 150
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
TSS
ND 2
MG/L
ND: NOT DETECTED
SL 023377
Da e 10/13/38
US ENUIRONMENTAL PROTECTION AGENCY ENUIRONMENTAL SERUICE DID IS I ON HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Append lx
Activity Number: 8AFEIE76 Date Recvd: 09/01/88
Sample Number:
8
Time Recvd: 13:30
Source:
Site Description : Sample Type: Sample Retention :
PPG Industries Outfall * 019 (101) WATER
Param-
Organic: Metals: Inorganic : Bio logy:
MTL TSS
Due Date:
|Date Projected: Date Completed: Comment: Your Initials:
10/19/88 10/19/88
//
RLR
Date Collected: 09/01/38 Time Collected: 05:30
Tag Number:
SL 023378
^OF ^ PAGE
ATTACHMENTS
US EPA HOUSTON BRANCH
SAMPLE #: SOURCE: TYPE: ANALYSTS:
8AFEIE76-0S' PPG INDUSTRIES AQUEOUS CLARK,FELDMAN
DATE RECEIVED: DATE REPORTED:
01-Sep-88 11-Oct-88
PARAMETER CONCENTRATION
DETECTION LIMIT <=
UNITS
ARSENIC SELENIUM THALLIUM MERCURY SILVER BERYLLIUM CADMIUM CHROMIUM COPPER NICKEL LEAD ZINC ALUMINUM BARIUM COBALT IRON MANGANESE VANADIUM ANTIMONY SODIUM POTASSIUM CALCIUM MAGNESIUM
ND ND ND 0.28 ND ND ND 19 49 752 105 574 1370 3240 ND 15100 2440 ND ND 80000000 ND 7300000 96000
230 480 190 0.2
10 5 5
10 20 20 30
5 100
10 20 25
5 30 60 500 1000 150 150
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L
TSS
91
MG/L
ND: NOT DETECTED
10/13/88
US ENVIRONMENTAL PROTECTION AGENCY ENVIRONMENTAL SERVICE DIVISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Append 1 x 1
Activity Number: 8AFE IE76 Date Recvd: 09/01/83
Sample Number:
9
Time Recvd: 13:30
Source: Site Description: Sample Type: Sample Retention:
PPG Ind ustrie# Ou t fall # Oil (101) WATER
Param- Organic: Metals: Inorganic: Biology:
M#*
Due Date: late Projected: late Completed: Comment: You r Initials:
10/19/88 10/19/38
//
RLR
Date Collected: 09/01/88 Time Collected: 05:30
Tag Number:
SL 023380
PAGE _2cOF__2^i
ATTACHMENTS ^
US ERA HOUSTON BRANCH
SAMPLE #: SOURCE: TYPE: ANALYSTS:
8AFEIE76-0<? PPG INDUSTRIES AQUEOUS CLARK,FELDMAN
DATE RECEIVED: DATE REPORTED:
Ol-Sep-88 ll-0ct-88
PARAMETER CONCENTRATION
DETECTION LIMIT <=
UNITS
MERCURY
6.2
0
UG/L
Date: 10/13/88
US ENUIRONMENTAL PROTECTION AGENCY ENUIRONMENTAL SERUICE DIUISION HOUSTON LABORATORY SECTION
LAB SAMPLE REPORT
Appendix ^0
Activity Number: 8AFEIE76 Date Recvd: 09/01/88
Samp 1e Number:
10
Time Recvd: 13:30
Source: Site Description:: Sample Type: Sample Retention:
PPG Industries Outfall # 111 (101) WATER
Param-
Organic: Me t a 1s : I no rgan i c: Bio logy:
M#*
^^Due Date: ^HDate Projected:
Date Completed: Commen t: Your Initials:
10/19/88 10/19/88
//
RLR
Date Collected: 09/01/88 Time Collected: 06:00
Tag Number:
SL 023382
PAGE
2-
ATTACHMENTS \D
US EF'A HOUSTON BRANCH
SAMPLE #: SOURCE: TYPE: ANALYSTS:
8AFEIE76-10 PPG INDUSTRIES AQUEOUS CLARK,FELDMAN
DATE RECEIVED: DATE
REPORTED:
01-Sep-88 ll-0ct-88
PARAMETER CONCENTRATION
DETECTION LIMIT O
UNITS
MERCURY
* 0.2
*: UNABLE TO ANALYZE DUE TO ORGANIC INTERFERENCE
UG/L
*