Document V3gXNXX92NeJp9Vjm49BojD1K
?i W
C.V'^0j^9O3
TE PRINTED: 7/19Z
CG 32 CODE RT-870--D PKG____
JE^.3/1982 ( DATE )
_G2JH1
2579*
< LOT)
<UEST WGT-)
PROCESSES
APPROVED BY
< >RT-87~D <H) EWK 1-11-82
COMTYP JOB NAME: 32RT870DMH
TYPED BY: JMH
/TW G,*ry?irPJiK?.PREPARATION NOTES:
TIME /JLA M
EQUIP 1 MENT I
----------------- j.
I i I I i I !. I I 1 t
i I USE
i NAME: WATCHUNG RED B
1-LBS
s --r---------------------------------- -r~---------------------------------------[---------
i NOTE: DO NOT START IF PRESS WILL NOT BE
I
] AVAILABLE WITHIN 3 HRS AFTER MAKING. SUPV |
i TO REVIEW WITH P.R. SUPV & RECORD:
f
f PRESS WILL BE READY_____M______/PR SUPV.l
] START MAKINGM______ JMAKING SUPV.!
f NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF |
t AREA UNDER V-922
!
i NOTE: RUN 15* WATER INTO V-9S4. PUMP WATER t
j f r o m V-904 THRU DISTRIBUTOR. IF WATER DOES |
I NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH i
i FULL FORCE, NOTIFY SUPERVISOR.
[
NON-BLEEDING
ass sr ts ssss ss ss ssssssssssss ss
I N-COBE l ACCT ! I LBS j----------------,-------__ i\ l1 li
fi I!
PREP i jr\ RECORD: _J_.____'BATCHES SINCE SPARKLER LAST
-1 - ! !
I CLEANED. AFTER 4 BATCHES, CLEAN, DRESS I SPARKLER & PRE-COAT WITH 15* DICALITE,
I
'| L FILTER AID.
i T\ OBTAIN FOR S11 2-CHL0RO-4-AMINOTOLUENE-5- I 2-j T
I -^SULFONIC ACID.
!
i-3 I OBTAIN FOR S27 3-HYDR0XY-2-NAPHTH0IC ACID 1
\ 14^riNSTALL DV & DV- RECORDER & CONTROLLER CHART i
f?f ! 2. '
777--A */*?
740--C 8^~~C
i |_AL_ r7
i ]
921/ 931
3
RUN 11" (1 OG) WATER-INTO V
& ADJ TO i
I 8&-10 DEG F
ADD IN 2-3 MIN DRESINATE X ,
i i08 | 530-A
IR 5 MIN & RECORD PH__/5L'J__(9.5-i 0.5) J
!
STIR ?20 MIN OR LONGER TO DISSOLVE FOR S49 j
108
RUN 35" C722G) WATER INTO V-922 WEIGH SODIUM HYDROXIDE IN V-92
IN 1^41\
.X
7--D i
~ik,
n
212
TURN ON AGITATOR & STEAM & DUMP IN FROM S2
740-C I 1086
2-CHLGRO4-AM I NOTOLUENE
LOT .
A r*~ ^7QhSj 7
5--SULFONIC '
__J$dr
ACID
___ ;_____ __Z____
___
i
DUMP IN ACTIVATED CARBON
25 i 113-B i 25
DUMP IN FILTER AID
1 1 777-A I 10
HEAT TO 212-214 DEG F WATCH FOAM!!
RECORD: BY_jrqri< + > IF NECESSARY ADJ TO +BY
SODIUM HYDROXIDE
ASSUME 50%
STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF
STEAM WATCH FOAM! NOTE: RECORD SPARKLER
I I 7-B r.
I
PRESSURE _?>___ PS I. IF NOT ZERO NOTIFY SUPERVISOR.
JU( 26198^1
N32894
DUP050464623
LQT= ________ COMTYP JOB NAME 32RT870DMH PAGE 02
DATE PRINTED: 7/19/82
EQUIP I MENT
PAGE 2 OF 4 CG 32 CODE RT-8-70-D (H)
V^IRCULATE 15 MIN OR .LONGER THRU SPARKLER-
I UNTIL SOL 1 N IS CLEAR* MAINTAIN. AT 19%-1 95
I DEG F FOR S22^RECORD: STbRT^Jfo.JmTM
1 TOTAL
CLARITY___
{ . I HT_/2l _ F 6 RFC
F'
MISC. Tlj^'^T'^MEASURE ^i^j^PuNITS IN V-92.8 FOR..
4 I ' J^HYDROCHLDRIC ACID ' \jsr\ WWEEIGH SODIUM NITRITE IN PPTTyJOfORR_JS42
M_~J____ ,
WEIGH. SODIUM NITRITE IN DDRR^Tf o
M
EM._%
I USE ! N-CODE I ACCT
I LBS I
LBS
l/^^l
28-D I 438
! 725-A 1 39t
i ZZi_,, 1 725-A i 43
9Q&/CV 15W'"] RUN 2* (58G)'WATER INTO V-58Bt/CV .
5 a^T't WHEN SI 7 IS COMPLETE, PUMP IN V-922 THRU
T I SPARKLER, MAINTA ! i RECORD: START Jll
-922 AT 190-195 DEG F* TOTAL MIN__&P____
1I
| .[
922 \yPZ | WHEN S22 COMPLETE, SHUT OFF PUMP 'AND INSERT)
6 I | V-922. FOOT PLUG
'
I
U24AI RUN IN 10` (209G) WATER & HEAT TO 190-195 F|
' I i CIRCULATE 15 MIN THRU SPARKLER -
i
\i 1
I
9$./Cwi4B ? AND PUMP V-922 THRU SPARKLER INTO V-904/CV I
71
902 8
LKON 65" < 1696G> WATER INTO V-902
\pr\ WEIGH SODIUM HYDROXIDE
T 'M
I DUMP IN FROM S3 I 3-HYDROXY-
I -J 2-NAPHTHOIC ACID
LOT*lllf
IN
1r 1 "l !
7-D 82-C
399 994
j^strT'ADj TO 70-90 DEG F & STIR TO DISSOLVE
I '{
922 9
SB | RUN IN 5" <1040 WATER & HEAT TO 190-195 F | .
I | CIRCULATE 15 MIN THRU SPARKLER'
V
l_ I
_
_ l-
CVU^rT PUMP V-922 THRU SPARKLER' INTO V-904/CV
I
10- I WHEN MTY BLOW OUT SPARKLER INm,V-904/CV |
H<31 1 DISSOLVE ALKANOL XC IN' 20G WATER AT 150-1601
F FROM HOT WATER MIXER IN DRUM & POURIN.
I
2 i HEAT TO 165-170 F FOR S38
"
f
I' f
' :f,,~.....
I
32 |
! I
133-B*
%
32
.;<t~V '
932. \ i1
\'
\\
H*33 T l \
55 I ^36 I
RUN 16" (3280 WATER INTO V-932 & ADJ TO -l./'
|
80-100 DEG' Fl
- ' ',>
: l -V I
ADD IN, 6-7 MIN DRESINATE X '
$ 373 |
STIR 5 MIN 6 RECORD PHji$___<9*5-10.5)
1
|
STIR 20 MIN OR LONGER TO DISSOLVE FOR S59 J
I
530-A
378
DUP050464624
LOT=_________ COMTYP
________________________________
e q u ip t T"T"T
~~
WENT * I
I PACE-3
JOB NAME = 32RT870DMH PAGE G3
. . /.
. .......................... .............. ^
~~ ~ !~~T
OF 4 CG 32 CODE RT-B70-D <H>
DATE PRINTED: 7/19/82
i USE ! N-CODE I ACCT
LBS i
| LBS
,CV 12
Hi
N-TBO-C OL* IJAS r-UMPBD DIRECT!
SPARKLES TO QV Si, 24 t,29 DM 11 S3?
1 *.. A?5G) IWATEra I NTS Vr V-94 ATI 165-170 BEG ~t h r | u Ae r s
DISIRIBUTOR IftTQvG A iP. (12-15 MINI
N N-28-D HYDROCHLORIC ACID FROM SIS
12-15 MIN.' MAINTAIN' 165-170k F IN CV*
STIR 15 MIN AT 165-170 DEG F
ADJ TO 46* (4347G) AT "32-33 DEG F. V
^'^<3301
RECORD: TEMP_3S_JDEG .F, VOLUME_H.__`
RUN IN N-725-A SODIUM NITRITEFROM Si 9 AFAPi
|
(5-10 MIN) & RINSE IN PT
1 |[
NOTE: PROCESS HAS A VERY LOU N-28-D EXCESS |
|
CHECK CR VERY CAREFULLY
1I
STIR 20'MIN AT 32-38 DEG F MAINTAINING
!
+CR, +KI FOR S44 'RECORD: TIME START_2l \A*i | _____ I
CR___4r___, KI___T___ ' NOTE:
I
1 )' IF CR-, KI-- ADD 20* *AS TS* INCREMENTS RECORD OR( + ) KI< + >
HYDROCHLORIC ACID .
ASSUME 32%
2) IF CR+, KI- ADD 20# *AS IS* INCREMENTS'
RECORD CR______< + ) KI( + >
SODIUM NITRITE
ASSUME 33% |1
DUMP IN CALCIUM CHLORIDE
i 1026 I
ADD FOR MAINTAINING 32-38 DEG F THRU S55 4o\5SX33|
57-A
1
57-A i_
28-D
725--A i
20-A i 1026 57-A
FILL PT APPROXIMATELY 1/2 FULL WITH 90-1i.*|
F WATER FROM HOT WATER MIXER
|
DUMP IN STRONTIUM NITRATE
[
IR 30'MIN OR LONGER WITH LIGHTNIN MIXER I
TO SOLUTION FOR S58
,
|
1
68 1 '246-B, E !
68
WHEN S23A COMPLETE, 'STEAM EJECT V-921/931 i
FROM S8 INTO -V-902 .
|
POUR IN N-725-A SODIUM NITRITE FROM S20
i
ADD AMMONIUM CHLORIDE,
i >13
165-A
213
CV [02 I IMMEDIATELY COUPLE V-902 THRU UNDERSURFACE
15 !
! DISTRIBUTOR INTO CV IN 18-22 MIN/ RECORD:
i i START_ji/liKL___ TOTAL MIN___ jgljr._____
PT 'U5TI DURING S52 WEIGH SODIUM HYDR^IDE
1
16 i, i
--*------------------ --*--------------- .
X05A | DILUTE TO MAXIMUM VOLUME (+/-100G) FOR S56 |
ii
,
CV t+55 t WHEN S52 COMPLETE, STIR 30 MIN & RECORD:
17 1
I DIAZ0_3t_-._( + )
BASE__.j P < + )
PH__Sj '5L__.<5.0-6,)
TEMP. '>__( 32-38 F)
\J^i \ RUN SODIUM HYDROXIDE IN PT FROM S54 THRU
t]^7 | UNDERSURFACE LINE, RINSE IN PT 6 STIR 15 MNI RECORD: DIA20_-r:_<-) BASE__-fcr_____ ( + >
!
RUN
IN
PH_^.___ <9*0-9.8) STRONTIUM NITRATE N-246~B,E SOL1N
i . 1 FROM S48 & RINSE IN PT UP59 i STEAM EJECT IN V-932 FROM S36
tt&O 1 STIR 5'MIN & RECORD: PH^i___(9.0~9*8)
7-D 140
J
DUP050464625
l u i=__________ uunirt-' jutt rmnt = j z k i a .'9L>nH pout 04
EQUIP f | MENT | | PAGE 4 OF 4
CG 32 CODE RT-B70-D <H>
uftit. i-'KiNiLD; ,vi y/32
| USE 1 N-CODE i ACCT
1 LBS I
I LBS
17 CONT
iJX' | IF PH BELOW 9.0 ADJ.TO PH 9.0-9.8 WITH I 1 N-7-D ONLY.'RECORD PH
I t
1 I SODIUM.HYDROXIDE
ASSUME 50% |
LL4-2J, POUR IN I OCTANOL
I
U^T\ HEAT TO 193-195 DEG F IN 70-75 MIN & RECORD!
1 -^HT_./JQ__DEG F AND REC__/f^_DEG F
'!
| SJIR 60 MIN AT 193-195 DEG F.
!
I ^HSe CORP: START^**1
I AFTER 20 MIN S64 STIR
RECORD:
|
II
PH_5zS___ (8.8-9.3) |
1 .1 IF PH BELOW 8.8, ADJ TO PH. 8.8-9.3 WITH
i
1 L-N=7~D ONLY. RECORD PH
ASSUME 50% 1
J>Tj AFTER S64 STIR, FLOOD TOISO-190*
|
1 ! (+/-18,OOOG) AND STOPAGITATOR
1
i1 II'
i 1
! i
38 ! ! ! 1
.1 1 1 1
_____1 1 i 1 1
` 7-D 5S8-A
7-D
I 1
1 __ I 38 i 1 T 1 r i i i i i r i
i f WHEN INSTRUCTED BY PROCESSING AREA HALFWAY 1
1 I THRU PRESSING, DUMP IN, STIR 5 MIN & STOP (
] | AGITATOR. RESUME PRESSING.
|
T! 10 |. 538-A i
S' |
10
DUP050464626
N32894.01
DUP050464627
N32894.02
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