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BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity:A mixturecontainingperiulorooctanesulfonatew,hich may alsobe referredtoas PFOS, FC-95, or as a component ofFC-206A. (1Octanesulfoniaccid)(CAS # 2795-39-3). Remarks: The 3M productionlotnumber was notnoted. The testsample isFC-206A. Currentinformationindicatesitisa mixtureof0.92% PFOS, 18.75% diethyleneglycolbutylether,75.44% water,1.83% Hydroxy foamer, 1.75% sodium octylsulfate1,.2% poloxyethylenemonooctylphenylether, 0.06% sodium laurylsulfatea,nd 0.05% benzotriazole. The followingsummary appliesto a mixture with incompletely characterizedconcentrations of impurities.Data may not accurately reflectthe toxicityof the t7uorochemkat component of the testsample. METHOD: Method: Standard Methods, 14th Edition Type: Aerobic GLP: No Year completed: 1978 Contact time: 20 days lnoculum: Source notgiven. RESULTS TotalOrganicCarbon (TOC): 114,000 mg/L 120,000 mg/L (duplicate) Chemical Oxygen Demand (COD): BiochemicalOxygen Demand (BOD): 5-Day: 1O-Day: 15-Day: 20-Day: 451,000 mg/L 453,000 mg/L (duplicate) 200,000 rng/L 330,000 mg/L 370,000 mg/L 330,000 mg/L CONCLUSIONS No conclusionsgiven. Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA QUALITY ReliabilitKyJ:imischranking3. Study lacksdescdptionand recordsofthe method followed.The inoculum isnot properlycharacterizedT.here isno characterizatioonfthetestsubstance purityand the studylacksanalytical confirmationofthefluorochemicalproportioninthe solution. REFERENCES The studieswere conducted by the3M Company, EnvironmentalLaboratory, St.Paul,MN, Lab Request number 4462, 1978. OTHER Lastchanged: 6/26/00 Forrn 10620.5-PWO cc: LAB PECIUEST BOOK - 42-5W Ref: ENVIR. ASSESS. INQ. PRODUCT: PRODUCT REQUEST DIVISION 4 ECOLOGICAL ASSESSMENT FOR LABORATORY WORK LAB REQUEST NO. REQUESTF:R Name: Al. 0,/o Request Date: 7,117"-@2;7e@? Phone No, Project No.: Code No.: Sample Date: 70 1 1, 6 J cl / Prob. No. Date Needed: Description: .2 Purpose of Tests: LABORATORY Date Received Sample: Analyst: Date Completed- ._iz@ Hours Spent: -2L6k y B_P I K-,- AM /Itloi-7@, Please Call Requester If Delays Are Encountered. PHYSICAL& CHEMICAL PROPERTIES Heatof Combustion Cal/G (BTU/Lb.) Density Ash Other E)UPL ICA-,Es WATER POLLUT ION rp-HD COD BOD SOD, Ultimate TOC GC Oxygen Uptake Dehydrogenase Activity(TTC) Other C? 5 14.,rT @E-OCP DATA 114.000 SAE4 @@T BIOASSAY Specify Organism and Method: z LEACHATE FROM LEACHING pH COD BOD 5 BOD, k-'!iimate TOC GC_ Li2a;s.lv TEST 1-3 OTHER Bioaccumulation Persistence Degradation Products *turn to R equestw canary Environmental Engrg. Office File Pink - i:nvironrnentaEtngrg. Lob Goldenrod - Return to Roquftter 6r@ -7 co ITtn I-T 10 FILE Em G. DATE SHEET co 0 17 too ID ------Ti I!.!-I T-1 IT- 0- C0 @y tA ci c ci o C 'lid 6 40 v Zia