Document Rp5qyonB3X9GG5v37mgn59Don

3M Specialty Materials June 28, 2000 c f yr - - 13M Center S65t.1P7a3u3l, M11N0055144-1000 0300 M 22.6- 062% r&(-5s>, m-o ---aonmmo ---F3aCo coom VIA EXPRESS MAIL Dr. Charles Auer Director Chemical Control Division FYI-00-001378 Office Of Pollution Prevention And Toxics United States Environmental Protection Agency 401 M Street, Southwest FYI-00-001378 Room 403 East Tower (Mail Code 7405) Washington, D. C. 20460 Re: Information On PerfluorooctaneSulfonates Mixtures Dear Charlie: mnreC^S9j c 033 ~v 3 ) m r o ~--uiron 3M has provided studies previously to the Agency on perfluorooctane 72 m sulfonates -- including CAS numbers 1763-23-1 (acid); 29081-56-9 (ammonium salt); g o O 70225-14-8 (DEA salt); 2795-39-3 (potassium-salt); 29457-72-5 (lithium salt) - as well gs on aqueous and/or solvent solutions of these materials. Pursuant to our recent ro communications, 3M is now enclosing information on products in which perfluorooctane sulfonates are deliberately added as an ingredient, i.e., perfluorooctane sulfonates mixtures. We are providing this information on a voluntary basis as part of our continuing discussions with EPA regarding fluorochemistry. As indicated in my letter to you dated May 11,2000, potassium perfluorooctane sulfonate is deliberately added to 3M's aqueous fire fighting foam ("AFFF") products. The amount of PFOS in both current and historical formulations of these products has been quite low - generally around 1 percent. Moreover, 3M customers dilute AFFF products significantly during end use, and thus, the level of potassium perfluorooctane sulfonate in the final applied product would be even lower. As these circumstances indicate, studies and other information on AFFF products have limited relevance, if any, to the potential hazard profile of perfluorooctane sulfonates. 3M is providing the Agency, therefore, with basic health and environmental laboratory studies on these AFFF products. With respect to toxicology studies, 3M is providing copies of all laboratory studies, except that we are listing acute studies in a bibliography. For environmental studies, we are providing copies of all laboratory studies and a bibliography of published literature. 3M is continuing its file review and will supplement the enclosed studies as appropriate. 85000000033 000001 85000000033 Charles Auer June 28, 2000 Page 2 As you review studies, we ask that you bear in mind a point that we have made previously with regard to test substance identity and composition. Many of the studies refer to the test substance only by a 3M product identification number with a "T", "L", "FM", "FC" or other prefix. Although analysis of the test sample has been included, where available, it is often not possible to determine from the study report itself the identity of the test substance or composition of the test sample. To assist in interpreting the studies, we have used 3M's product number records to provide test substance identity and composition information (e.g., composition percentages; solvent content; purity grade, etc.) next to each study name on the index and/or on the study summary. In some cases, the formulation information comes from historical records around the same period as the study was conducted; in other cases, only current product formulation information is available. Thus, the formulation information provided may not reflect the precise formulation of the specific test sample. Moreover, it should be recognized that product formulations have evolved over the years, and thus, some of the test substances do not constitute current products. 3M looks forward to discussing the enclosed information with you and other EPA staff. In the meantime, please do not hesitate to contact me with any questions. Very truly yours Enclosures William A. Weppner, Ph.D Director of Environmental, Health, Safety And Regulatory Affairs Specialty Materials Markets 3M Bldg 236-1B-10 3M Center St. Paul, MN 55144 (651)733-6374 (phone) (E6-5m1a)i7l:33w-a1w9e5p8pn(fearx@) mmm.com 000002 AttachTmoexnictIosnlftooogriLmceaatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 PFOS Mixtures Acute Toxicity Post 1976 Studies (Bibliography only) 1) BFiinosaelaRrecpho,rItn,cP.,riOmcatr.y1E8,y1e9I7r6ri.tation Study - Rabbits, 3M Reference No. T-1328, 2) FBiinoaselaRrecpho,rItn,cP.,riJmuanrey2S5k, i1n9I7r6r.itation Study - Rabbits, 3M Reference No. T-1516, 3) FBiinoaselaRrecpho,rItn,cP.,riJmuanrey2E5,ye19I7rr6i.tation Study - Rabbits, 3M Reference No. T -l516, 4) Final Report, Acute Oral Toxicity - Rats, 3M Reference No. T-1516, Biosearch, Inc., June 25, 1976. 5) Final Report, Primary Skin Irritation Study - Rabbits, 3M Reference No. T-1639, Biosearch, Inc., Nov. 22, 1976. 6) Final Report, Primary Eye Irritation Study - Rabbits, 3M Reference No. T-1639, Biosearch, Inc., Nov. 22,1976. 7) FIninc.a,lNRoevp.o2rt2,,A1c9u7t6e. Oral Toxicity - Rats, 3M Reference No. T-1639, Biosearch, 8) Final Report, Primary Skin Irritation Study - Rabbits, 3M Reference No. T-1943, Biosearch, Inc., Sept. 27,1977. 9) FBiinoaselaRrecpho,rItn,cP.,riSmeaprt.y2E7y,e19Ir7r7it.ation Study - Rabbits, 3M Reference No. T-1943, 10) FIninc.a,lSReeppt.or2t7,,A19cu7t7e. Oral Toxicity in Rats, 3M Reference No. T-1943, Biosearch, 11) BFiinoaselaRrecpho,rItn,cP.,riMmaarr.y2S,k1i9n7I8r.ritation Study - Rabbits, 3M Reference No. T-2080, 12) BFiinoaselaRrecpho,rItn,cP.,riMmaarr.y2E,1y9e7I8rr.itation Study - Rabbits, 3M Reference No. T-2080, 000003 AttachTmoexnictIosnlftooogriLmcaeatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 13) Final Report, Acute Oral Toxicity - Rats, 3M Reference No. T-2080, Biosearch, Inc., Mar. 2, 1978. 14) FIninc.a,lARuegp.o7rt,,1A9c7u8t.e Oral Toxicity - Rats, 3M Reference No. T-2226, Biosearch, 15) Final Report, Primary Skin Irritation Study - Rabbits, 3M Reference No. T-2226, Biosearch, Inc., Aug. 7, 1978. 16) BFiinoaselaRrecpho,rItn,cP.,riAmuagr.y7E,y1e9I7r8r.itation Study - Rabbits, 3M Reference No. T-2226, 17) Final Report, Primary Eye Irritation Study (Wash-out) - Rabbits, 3M Reference No. T-2226, Biosearch, Inc., Aug. 7, 1978. 18) Final Report, Primary Eye Irritation Study - Rabbits, 3M Reference No. T-2226, Biosearch, Inc., Sept. 19, 1978. 19) Final Report, Acute Ocular Irritation Test with T-2278CoC in Albino Rabbits, Riker Laboratories, Inc., Study No. 478E0272, Oct. 11,1978. 20) Final Report, Primary Skin Irritation Test with T-2278CoC in Albino Rabbits, Riker Laboratories, Inc., Study No. 478E0271, Sept. 29, 1978. 21) Final Report, Acute Oral Toxicity - Rats, 3M Reference No. T-2278, Biosearch, Inc., Sept. 25, 1978. 22) Final Report, Acute Ocular Irritation Test with T-2871CoC in Albino Rabbits, Riker Laboratories, Inc., StudyNo. 0880EB0279, June 24, 1980. 23) Final Report, Primary Skin Irritation Test with T-2871CoC in Albino Rabbits, Riker Laboratories, Inc., Study No. 0880EB0280, June 24, 1980. 24) Final Report, Primary Skin Irritation Test with T-2871CoC in Albino Rabbits, Riker Laboratories, Inc., Study No. 0880EB0505, Nov. 12, 1980. 25) RFiinkaelrRLeapboorrta,tPorriimesa, rIyncS.,kiSntuIrdryitNatoio.n08T8e0stEwBi0th71T7-,2M87a1r.C3o,C19in81A. lbino Rabbits, 000004 AttachTmoexnictIosnlftooogriLmceaatlttSeiortnutdooineCsP.aAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 26) FN1i9on8.a1Tl.R-2e9p4o3rCt,oFCH,SInAteArncauttieonInalhRaleasteioanrcThoaxnicditDyeEvvealolupamtieonnt iCnoRrpatosr,a3tiMon,RJeafne.re2n1c,e 27) FSienravlicReesp, oInrtc,.,ASctuutdeyONroa.l T83o6x7ic3i1ty,,M3aMr.R1e0f,e1re9n81ce. No. T-3025, Raltech Scientific 28) FSicnieanl tRifeipcoSret,rPvirciems,arIyncD.,erSmtuadlyINrroit.at8io3n6,7331M, MReafre.r1e0n,c1e9N81o.. T-3025, Raltech 29) Final Report, Primary Eye Irritation, 3M Reference No. T-3025, Raltech Scientific Services, Inc., Study No. 836731, Mar. 10, 1981. 30) RFiinkaelrRLeapboorrta,tAorciuest,eIOncc.u,laSrtuIdrryitNatoio. n08T8e1sEt wBi0t2h2T7-,3A0u97g.C3o,C19in81A. lbino Rabbits, 31) FRiinkaelrRLeapboorrta,tPorriimesa, rIyncS.,kiSntuIrdryitNatoio.n08T8e1stEwBi0th22T6-,3S0e9p7tC. 4o,C1i9n81A.lbino Rabbits, 32) Final Report, Acute Oral Toxicity Screen with T-3097CoC in Albino Rats, Riker Laboratories, Inc., Study No. 0981AR0228, June 22, 1981. 33) Final Report, Acute Ocular Irritation Test with T-3098CoC in Albino Rabbits, Riker Laboratories, Inc., Study No. 0881EB0230, Oct. 26, 1981. 34) RFiinkaelrRLeapboorrta,tPorriimesa, rIyncS.,kiSntuIrdryitNatoio.n08T8e1stEwBi0th22T9-,3A0u98gC. 2o8C, i1n98A1l.bino Rabbits, 35) FLianbaolrRateoproierst,, AInccu.,teStOurdayl NToox. i0c9it8y1SAcRre0e2n31w,itJhulTy-1300,981C98o1C. in Albino Rats, Riker 36) RFiinkaelrRLeapboorrta,tAorciuest,eIOncc.u,laSrtuIdrryitNatoio. n08T8e1sEt wBi0t3h7T4-,3D1e5c4C7,oC19i8n1.Albino Rabbits, 37) RFiinkaelrRLeapboorrta,tPorriiems,arIyncS.,kiSntuIrdryitNatoio. n08T8e1sEt wBi0t3h7T5-,3N1o5v4.C1o6C, i1n98A1l.bino Rabbits, 38) FLianbaolrRateoproierst,, IAnccu.,teStOurdayl NToox. i0c4it8y1SAcRre0e3n7w6,itDheTc.-311,5149C81o.C in Abino Rats, Riker 000005 AttachTmoexnictIosnlftooogriLmcaeatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvean28t ,2000 39) FRiinkaelrRLeapboorrta,tAorciueste, IOnccu.,laSrtuIdrryitNatoio. n08T8e1sEt wBi0t5h6T4-,3S1e9p4tC. 1o8C, i1n98A2l.bino Rabbits, 40) Final Report, Acute Oral Toxicity, Primary Dermal Irritation, Primary Eye MIrrairta. t3io0n, ,139M82.Reference No. T-3215, Hazleton Raltech, Inc., Study No. 924891, 41) LFianbaolrRateoproierst,, IAnccu.,teStOurdayl NToox. i0c8it8y2AScRre0e6n11w,itAhpTr.-353,15948i3n.Abino Rats, Riker 42) Final Report, Acute Oral Toxicity Study, 3M Reference No. T-3558, Hazleton Laboratories America, Inc., Study No. 856443, May 31, 1984. 43) FLianbaolrRateoproierst,APmrimeraicray,EInyce.,IrSrtituadtyioNn,o3.M85R64e4fe3r,eMncaeyN3o1., T1-938545.8, Hazleton 44) FLianbaolrRateoproierst,APmrimeraicray,DInercm., aSltuIrdryitNatoio.n8,536M44R3,efMeraeync3e1,N1o9.8T4.-3558, Hazleton 45) FLianbaolrRateoproierst,, AInccu.,teStOurdayl NToox. i0c9it8y4SAcRre0e3n6w6,itAhuTg.-33600,11i9n84A.bino Rats, Riker 46) Final Report, Acute Ocular Irritation Test with T-3601 in Abino Rabbits, Riker Laboratories, Inc., Study No. 0984EB0364, Study No. Aug. 30, 1984. 47) Final Report, Primary Skin Irritation Test with T-3601 in Abino Rabbits, Riker Laboratories, Inc., Study No. 0984EB0365, Aug. 8,1984. 48) Final Report, Acute Dermal Toxicity Study with T-3601 in Abino Rabbits, Riker Laboratories, Inc., Study No. 0984AB0433, Oct. 23, 1984. 49) LFianbaolrRateoproierst,AAmcuerteicOa,rIanl cT.,oxSitcuidtyy,N3oM. 5R0e1fe0r8e1n5c0e, NFeob..T2-53,711948, 5H. azleton 50) Final Report, Primary Eye Irritation, 3M Reference No. T-3714, Hazleton Laboratories America, Inc., Study No. 50108150, Feb. 25, 1985. 51) Final Report, Primary Dermal Irritation, 3M Reference No. T-3714, Hazleton Laboratories America, Inc., Study No. 50108150, Feb. 25, 1985. I 000006 AttachTmoexnictIosnlftooogriLmcaeatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 52) Final Report, Acute Oral Toxicity, 3M Reference No. T-3715, Hazleton Laboratories America, Inc., Study No. 50108151, Feb. 27, 1985. 53) Final Report, Primary Eye Irritation, 3M Reference No. T-3715, Hazleton Laboratories America, Inc., Study No. 50108151, Feb. 27, 1985 54) Final Report, Primary Dermal Irritation, 3M Reference No. T-3715, Hazleton Laboratories America, Inc., Study No. 50108151, Feb. 27, 1985 55) Final Report, Acute Oral Toxicity Study in Rats, 3M Reference No. T-3910, Hazleton Laboratories America, Inc., Study No. 60501972, Aug. 8, 1986. 56) Final Report, Primary Eye Irritation Study in Rabbits, 3M Reference No. T-3910, Hazleton Laboratories America, Inc., Study No. 60501974, Aug. 6, 1986. 57) Final Report, Primary Dermal Irritation/Corrosion Study in Rabbits, 3M R60e5fe0r1e9n7c3e,NJuol.yT1-13,91109,86H.azleton Laboratories America, Inc., Study No. 58) HFianzalletRoenpLoratb,oArcautotreieOsrAalmTeorxicicai,tyInSct.,uSdtyuidnyRNaots.,630M70R28e1fe5r,eOnccet.N1o0., T19-3896.40, 59) Final Report, Primary Eye Irritation Study in Rabbits, 3M Reference No. T-3940, Hazleton Laboratories America, Inc., Study No. 60702817, Sept. 12, 1986. 60) Final Report, Primary Dermal Irritation/Corrosion Study in Rabbits, 3M Reference No. T-3940, Hazleton Laboratories America, Inc., Study No. 60702816, Aug. 21, 1986. 61) Final Report, Acute Oral Toxicity Study in Rats (OECD Guidelines), 3M R80e3fe0r0e6n6c4e,NMoa. yT3-411, 5129,8H8.azleton Laboratories America, Inc., Study No. 62) Final Report, Primary Eye Irritation/Corrosion Study in Rabbits (OECD Guidelines), 3M Reference No. T-4152, Hazleton Laboratories America, Inc., Study No. 80300666, June 1, 1988. 63) Final Report, Primary Dermal Irritation/Corrosion Study in Rabbits (OECD GStuuiddyelNinoe.s)8,033M00R66e5fe,rMenacye2N6o, .1T98-481. 52, Hazleton Laboratories America, Inc., AttachTmoexnictIosnlftooogriLmcaeatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 64) FR9i0en3fae0lr0eR7ne4cp7eo,NrJtuo, n.AeTcu1-46te3, 1O109r,8aH9l.TazolxeticointyLSabtuodryationriResatAsm(OerEicCaD, IGncu.,idSetluindeysN), o3.M 65) FGiuniadleRlienpeosr),t,3PMrimRaefreyrEenyceeINrroit.aTti-o4n3/C10o,rrHoasizolnetoSntuLdaybionrRataobrbieistsA(OmEerCicDa, Inc., Study No. 90300749, June 21, 1989. 66) Final Report, Primary Dermal Irritation/Corrosion Study in Rabbits (OECD GStuuiddyelNinoe.s)9,033M00R74e8fe,rJeunncee2N7o, .1T98-493. 10, Hazleton Laboratories America, Inc., 67) FRienfaelrRenecpeoNrto, .ATcu-4te31O1r,aHl aTzolxeticointyLSabtuodryationriResatAsm(OerEiCcaD, IGncu.,idSetluindeys)N, o3.M 90300750, June 27, 1989. 68) FGiuniadleRlienpeosr),t,3PMrimRaefreyrEenyceeINrroit.aTtio-4n3/C11o,rrHoasizolnetoSntuLdaybionrRataobrbieistsA(mOEerCicDa, Inc., Study No. 90300752, June 21, 1989. 69) Final Report, Primary Dermal Irritation/Corrosion Study in Rabbits (OECD GStuuiddyelNinoe.s)9,033M00R75e1fe,rJeunncee2N7o, .1T98-49.311, Hazleton Laboratories America, Inc., 70) Final Report, Acute Oral Toxicity Study in Rats (OECD Guidelines), 3M R00e4fe0r1e9n3c0e,NMoa. yT3-501, 7179,9H0.azleton Laboratories America, Inc., Study No. 71) Final Report, Primary Eye Irritation/Corrosion Study in Rabbits (OECD Guidelines), 3M Reference No. T-5177, Hazleton Laboratories America, Inc., Study No. 00401932, May 31, 1990. 72) FGSitunuiaddlyeRlNienope.osr)0,t0,34PM0r1imR93ae1rfey,rMDeneacryem3Na1lo,I.1rTr9i9-t50a1.ti7o7n,/CHoarzrloestioonnLSatbuodryaitnorRieasbAbimtse(rOicEa,CIDnc., 73) FHianzalleRtoenpWorti,scAocnustine,OSrtauldTyoNxioc.it0y1S1t0u2d2y98o,fJTa-n5.249,21i9n9R1.ats (OECD Guidelines), 74) Final Report, Primary Eye Irritation/Corrosion Study of T-5292 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 01102301, Jan. 17, 1991. 000008 AttachTmoexnictIosnlftooogriLmcaeatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 75) Final Report, Primary Dermal Irritation/Corrosion Study of T-5292 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 01102300, Dec. 27, 1990. 76) FGiuniadleRlienpeosr),t,HAaczuetlteoDneWrmisacloTnsoixni,ciSttyuSdtyuNdyo.o0f1T1-052229929i,nJRana.b1b4it,s1(9O9E1.CD 77) Final Report, Acute Oral Toxicity Study of T-5293 in Rats (OECD Guidelines), Hazleton Wisconsin, Study No. 01102302, Jan. 4, 1991. 78) F(OinEaCl RDepGouritd,ePlirnimesa)r,yHEayzeleItorrnitWatiioscno/Cnsoirnr,osSitoundSytNudoy. 0o1f1T0-25320953, iJnanR.a2b5b,it1s991. 79) F(OinEaCl RDeGpouritd,ePlrinimesa)r,yHDaezrlemtoanl IWrriistcaotinosni/nC,oSrtruodsiyoNn oS.tu0d1y10o2f3T0-45,2D93eci.n2R7a,b1b9i9ts0. 80) FGiuniadleRlienpeosr),t,HAaczuetlteoDneWrmisacloTnsoixni,ciStytuSdtyuNdyo.o0f1T1-052239033i,nJRana.b1b4it,s1(9O9E1.CD 81) Final Report, Acute Oral Toxicity Study of T-5454 in Rats (OECD Guidelines), Hazleton Wisconsin, Study No. 11103011, Jan. 15, 1992. 82) F(OinEaCl RDeGpouritd,ePlrinimesa)r,yHEayzleeItorrnitWatiioscno/Cnsoirnr,osSitoundSytNudoy. 1o1f1T0-35041534, iJnanR.a1b0b,it1s992. 83) Final Report, Primary Dermal Irritation/Corrosion Study of T-5454 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 11103012, Jan. 10, 1992. 84) Final Report, Acute Oral Toxicity Study of T-5508 in Rats (OECD Guidelines), Hazleton Wisconsin, Study No. 20203021, Apr. 16, 1992. 85) Final Report, Primary Eye Irritation/Corrosion Study of T-5508 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 20203023, May 21, 1992. 86) F(OinEaCl RDepGouritd,ePlrinimesa)r,yHDaezrlemtoanl IWrriistcaotinosni/nC,oSrtruodsiyoNn oS.tu2d0y20o3f0T2-25,5A08pri.n2R2a, b1b9i9ts2. 87) FHianzalleRtoenpWorti,scAocnustine,OSrtauldTyoNxioc.it4y0S1t0u2d0y83o,fATp-5r.59153,i1n9R9a4t.s (OECD Guidelines), 000009 AttachTmoexnictIosnlftooogriLmcaeatlttSeiortnutdooineCsP.aAFnOudeSrOMdthaiextertduRrJeeulsenvean28t ,2000 88) F(OinEaCl RDepGouritd,ePlrinimesa)r,yHEayzleetIorrnitWatiioscno/Cnsoirnr,osSitoundyStNudoy. 4o0f1T0-25058965, iAnpRr.ab7b, i1ts994. 89) Final Report, Primary Dermal Irritation/Corrosion Study of T-5595 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 40102085, Mar. 23, 1994. 90) Final Report, Acute Dermal Toxicity Study of T-5595 in Rabbits (OECD Guidelines), Hazelton Wisconsin, Study No. 40102084, Apr. 22, 1994. 91) HFianzalleRtoenpWorti,scAocnustine,OSrtauldTyoNxioc.it3y0S1t0u2d5y36o,fATp-5r.6778, 1in99R3a. ts (OECD Guidelines), 92) F(OinEaCl RDepGouritd,ePlrinimesa)r,yHEayzleetIorrnitWatiioscno/Cnsoirnr,osSitoundSytNudoy. 3o0f1T0-25563788, iMn aRra.b1b6i,ts1993. 93) F(OinEaCl RDeGpouritd,ePlrinimesa)r,yHDaezrlemtoanl IWrriistcaotinosni/nC,oSrtruodsiyoNn oS.tu3d0y10o2f5T3-75,6M78arin. 1R6a,b1b9i9ts3. 94) FHianzalleRtoenpWorti,scAocnustien,OSrtauldTyoNxioc.it3y1S2t0u2d7y78o,fMT-a5r7. 3184,in19R9a4t.s (OECD Guidelines), 95) F(OinEaCl RDepGouritd,ePlrinimesa)r,yHEayzleetIorrnitWatiioscno/Cnsoirnr,osSitoundSytNudoy. 3o1f2T0-25778308, iAnpRr.ab1b, i1ts994. 96) Final Report, Primary Dermal Irritation/Corrosion Study of T-5738 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 31202779, Mar. 21, 1994. 97) Final Report, Acute Oral Toxicity Study of T-5739 in Rats (OECD Guidelines), Hazleton Wisconsin, Study No. 31202781, Mar. 11, 1994. 98) F(OinEaCl RDeGpouritd,ePlirnimesa)r,yHEayzleetIorrnitWatiioscno/Cnsoirnr,oSsitoundyStNudoy. 3o1f2T0-25778339, iAnpRr.ab1b3i,ts1994. 99) Final Report, Primary Dermal Irritation/Corrosion Study of T-5739 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 31202782, Mar. 23, 1994. 100) FHianzalleRtoenpWorti,scAocnustine,OSrtauldTyoNxioc.it3y1S2t0u2d7y84o,fMT-a5r8.0114,in19R9a4t.s (OECD Guidelines), 000010 AttachTmoexnictIosnlftooogriLmceaatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 101) Final Report, Primary Eye Irritation/Corrosion Study of T-5801 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 31202786, Apr. 8, 1994. 102) Final Report, Primary Dermal Irritation/Corrosion Study of T-5801 in Rabbits (OECD Guidelines), Hazleton Wisconsin, Study No. 31202785, Mar. 23, 1994. 103) Final Report, Primary Eye Irritation/Corrosion Study of T-6016 in Rabbits (1O99E4C. D Guidelines), Hazleton Wisconsin, Study No. HWI40901956, Dec. 2, 104) F60in7a6l,RSetpilolmrte, aAdcouwteIDnce.r,mStauldTyoNxioc.it1y6S3t5u-d9y4 iJnanR.a5b,b1it9s9,53.M Reference No. T105) FSitnilalml Reaepdoorwt,IPnrci.m, SartuydEyyNeoI.rr1it6a3ti6o-n94S,tuJadny. i3n,R1a9b9b5.its, 3M Reference No. T-6076, 106) . F60in7a6l,RSetpilolmrte, aPdroimwaIrnycD.,eSrtmudalyINrroi.ta1ti6o3n7S-9tu4d, yJainn.R5a, b1b9i9t5s,. 3M Reference No. T107) FSitnilalml Reeapdoorwt,IAncc.u,tSetOudryalNToo.x1ic6i3ty4-i9n4R, Datesc, .32M1,R1e9f9e4re. nce No. T-6076, 108) NFiOnaTlORXep,oPrrto, jAecstseNsosm. 1en80t8o1f1A, cSuetpet.O1r4a,l 1T9o9x6i.city with T-6587 in the Rat, 109) NFiOnaTlORXep,oPrrto, jAecctuNteoE. y1e80Ir8r3i3ta,tSioenp/tC. o1r4r,o1si9o9n6.Study with T-6587 in the Rabbit, 110) F(4in-haoluRreSpoemrt,i-POrcimclaursyivSekAinpIprlricitaattiioonn)/,CNoOrrTosOioXn,SPtruodjyecwtiNtho.T1-685088722in, SthepetR. a1b4,bit 1996. 111) F(OinEaCl RDepGouritd,ePlrinimesa)r,yCEoyveanIcreriLtaatbioonr/aCtoorrrieossiIonnc.S, tPurdoyjeocftTN-o6.675004i0n5R31a3b,bJitusne 19, 1997. 112) F(OinEaCl RDeGpouritd,ePlrinimesa)r,yCDoevramncael LIrarbitoartaiotonr/CieosrIrnocs.i,oPnrSotjuedctyNoof.T7-064605503i1n2R, aJbubneits19, 1997. O O O O ll AttachTmoexnictIosnlftooogriLmceaatlttSeiortnutdooineCs.PaAFnuOdeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 113) MF70ina4ax0li5mR3ie1zp4ao,triJotu,nlDyTe2ers4mt, a(1El9CS9e7Gn. suitiidzealtiinoens)S, tCuodvyaonfcTe -L6a6b5o0raintoGriuesinIenac.P, iPgrso-ject No. 114) FCionmalinRgepHoarzt,leAtocnutIenOc.r,aPlrTojoexcitcNityo.SCtuHdWy o6f0T9-063615200i,nDReact.s1(7O, E1C99D6.Guidelines), 115) F(OinEaCl RDeGpouritd,ePlirnimesa)r,yCEoyvaenIcreriLtaatbioonr/aCtoorrrieossiIonnc.S, tPurdoyjeocft TN-o7.193003.100in10R6a,bMbiatsy 11, 1999. 116) Final Report, Primary Eye Irritation/Corrosion Study of T-7131.1 in Rabbits (OECD Guidelines), Covance Laboratories Inc., Project No. 90300107, Apr. 29, 1999. 117) Final Report, Dermal Sensitization Study of T-5679 in Guinea Pigs Maximization Test (EC Guidelines), Hazelton Wisconsin, Project No. 212022562, Mar. 29, 1993. 118) Final Report, Dermal Sensitization Study of T-5680 in Guinea Pigs Maximization Test (EC Guidelines), Hazelton Wisconsin, Project No. 212022563, Mar. 29,1993. 119) MMFinaarax.lim2R9iez,pa1ot9rio9t,n3D.Teersmt a(El CSeGnsuitiidzealtiinoens)S, tHuadzyeoltfoTn-W56i8s1coinnsiGnu, iPnreoajePcitgNs -o. 212022564, 120) Final Report, Acute Oral Toxicity, Acute Dermal Toxicity, Primary Dermal Toxicity, Primary Eye Irritation, 3M Reference No. T-3651, Hazelton Laboratories America, Inc., Dec. 3, 1984. 121) FHianzaellRtoenpLoratb, oPrraimtoarireysEAymeeIrrirciata,tIionnc.,SMtuadry. i2n, R1a9b87b.its, 3M Reference No. T-4026, 122) Final Report, Primary Dermal Irritation Study in Rabbits, 3M Reference No. T4026, Hazelton Laboratories America, Inc., Mar. 6,1987. 123) Final Report, Primary Oral Toxicity Study in Rats, 3M Reference No. T-4026, Hazelton Laboratories America, Inc., Mar. 24, 1987. 000012 AttachTmoexnictIosnlftooogriLmcaeatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 124) FRiinkaelrRLeapboorrta,tAorciuest,eIOncc.u,laSrtuIdrryitNatoio. n08T8e0sEt wBi0t1h6T5-,2A8p4r9.C7o,1C9i8n0A. lbino Rabbits, 125) FRiinkaelrRLeapboorrta,tPorriimesa, rIyncS.,kiSntuIrdryitNatoio. n08T8e0stEwBi0th16T6-,2A8p4r9.C1o6C, 1in98A0l.bino Rabbits, 126) FLianbaolrRateoproierst,, IAnccu.,teStOurdayl NToox. i0c8it8y0SEcBr0ee1n67w,iMthaTy-21,84199C80o.C in Albino Rats, Riker Pre-1976 Studies (bibliography onlvl 127) R-SteAupdlobireitnstooonRMaFbiCnbn-i1tes9s,4oE,taLyMeotIirn3r,iintAagtciaounntdeTMOersaatnl-uTfAoalxcbtiiucnirtoiynRg-aCAboblbmitisnp,oa3nRMya, tRAs,ecfEuetyreeenTIcroerxiNtiacoitti.oynT-Test 4933, Industrial Bio-Test Laboratories, Inc., Feb. 14, 1966. 128) RA4S9telub3pd6ioni,reotFsRtCooan-Mb1L9bi-5int2,sn2,Le6Ssi5foke,tsianAtrMcIeruairtnmietianOLtgiaroabanlnoSTdrtaoMutxodiarycinie-tusy,fAa-PclrbtAouinjlrbeiocnintRgoNaCRboob.amit1tsps2,,a6E3n4yMy,e,JAuRIrlceyrufit7etar,etei1Ton9noc6exS9iN.tcuiotdy.yT-129) Report to Minnesota Mining and Manufacturing Company, Acute Toxicity Studies on L-2542, Lot 2, Acute Oral Toxicity - Albino Rats, Eye Irritation Study -49A3l9b,iFnoCR-1a9b6b,iLtsi,feSsktrineaImrriLtaatbioonraSttourdieys,-PArolbjeicntoNRoa.b1b3it6s9, ,3JManR. 2ef7e,r1e9n7c0e.No. T130) Report to Minnesota Mining and Manufacturing Company, Acute Toxicity Studies on L-1872, Acute Oral Toxicity - Albino Rats, Eye Irritation Study A50lb2i2n,oLRifaesbtbrietas,mSLkianboIrrraittoartiioens, SPtruodjeyc-t NAolb. i7n6o3R, aAbpbri.ts1,, 31M96R8.eference No. T131) FIninc.a,lFReebp. o2r4t,, A19c7u1t.e Oral Toxicity - Rats, 3M Reference No. T-289, Biosearch, 132) Final Report, Primary Skin Irritation Study - Rabbits, 3M Reference No. T-36.1, Biosearch, Inc., Study No. Dec. 9, 1971. 133) BFiinoaselaRrecpho,rItn,cP.,riDmeacr.y9E, y1e97I1rr.itation Study - Rabbits, 3M Reference No. T-361, 000013 AttachTmoexnictIosnlftooogriLmceaatlttSeiortnutdooineCs.FaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 134) Final Report, Acute Oral Toxicity - Rats, 3M Reference No. T-361, Biosearch, Inc., Study No. Dec. 9,1971. 135) Final Report, Primary Skin Irritation Study - Rabbits, 3M Reference No. T-567, Biosearch, Inc., Feb. 18, 1974. 136) Final Report, Primary Eye Irritation Study - Rabbits, 3M Reference No. T-567, Biosearch, Inc., Study No. Feb. 18, 1974. 137) Final Report, Acute Oral Toxicity - Rats, 3M Reference No. T-567, Biosearch, Inc., Feb. 18, 1974. .138) Report, Oral LDj0, 3M Reference No. T-676, WARF Institute Inc., Project No. 3070098, July 2, 1973. 139) Report, Eye Irritation Study, 3M Reference No. T-676, WARF Institute Inc., Project No. 3070098, July 2, 1973. 140) PRreopjoerctt,NSok.in3I0r7r0it0a9ti8o,nJSutluyd2y,, 139M73R. eference No. T-676, WARF Institute Inc., 141) Report, Oral LD50, 3M Reference No. T-1049, WARF Institute Inc., Project No. 4071932, Aug. 1, 1974. 142) RPreopjoerctt,NEoy.e4Ir0r7i1ta9t3io2n, AStuugd.y,1,3M197R4e. ference No. T-1049, WARF Institute Inc., 143) Report, Skin Irritation Study, 3M Reference No. T-1049, WARF Institute Inc., Project No. 4071932, Aug. 1, 1974. 144) Report, Project NAoc.u4te10O2r8a7l2L,DN5o0,v3. M20,R1ef9e7r4e.nce No. T -1118, WARF Institute Inc., 145) PRreopjoerctt,NEoy.e4I1rr0i2ta8t7io2n, NStouvd.y2, 03,M19R7e4f.erence No.T-1118, WARF Institute Inc., 146) Report, Skin Irritation Study, 3M Reference No. T-l 118, WARF Institute Inc., Project No. 4102872, Nov. 20, 1974. 000014 AttachTmoexnictIosnlftooogriLmceaatlttSeiortuntdooineCs.PaAFnOudeSrOMdthaietxertduRrJeeulsenvea2n8t ,2000 147) RInesptiotrutt,eAIncuc.t,ePOrorajelcLtDN5o0.(5m0a3l0e8&00f,eAmparl.e)1,13,M19R75e.ference No. T-1207, WARF 148) Report, Eye Irritation Study, 3M Reference No. T-1207, WARF Institute Inc., Project No. 5030800, Apr. 11,1975. 149) Report, Skin Irritation Study, 3M Reference No. T-1207, WARF Institute Inc., Project No. 5030800, Apr. 11,1975. 150) BFiinoaselaRrecpho,rItn,cP.,riOmcatr.y6,S1k9in75I.rritation Study - Rabbits, 3M Reference No. T-1328, 151) Final Report, Primary Eye Irritation Study - Rabbits, 3M Reference No. T-1328, Biosearch, Inc., Study No. Oct. 6, 1975. 152) FSitnuadlyRNeop.orOt,ctA. c6u,1te97O5ral Toxicity - Rats, Reference No. T-1328, Biosearch, Inc., 153) Final Report, Primary Skin Irritation Study, 3M Reference No. T-269, Biosearch, Inc., Oct. 1,1970. 154) Final Report, Primary Eye Irritation Study, 3M Reference No. T-269, Biosearch, Inc., Oct. 1,1970. OOOOl AttachTmoexnictIosnlftooogriLmceaatlttSeiortnutdooineCs.PaAFnOudeSrOMdthaiextertduRrJeeulsenvea2n8t ,2000 Genotoxicitv 1) Final Report, In Vitro Microbiological Mutagenicity Assays of Three 3M Company Compounds, 3M Reference Nos. T-2136 [FC-206], T-2138, T-2140, SRI International, Project No. LSC 4442-16, Apr. 1978. 2) Final Report, In Vitro Microbiological Mutagenicity Assays of 3M Company's Compound T-3651, SRI International, Project No. LSC-3145, Feb. 1985. 000016 PFOS Mixtures FC-185F Acronyms: cc817-19, Lab Request Number: 7544 Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability of FC-185F (BOD/COD) Laboratory or Author 3M Env. Lab Completion Date 2/24/82 Type Robust summary, laboratory data summary Ecotoxicity Elements Title Aquatic Toxicity Testing: FC-185F (cc817-19) L 1-2303 LR 7544 (Fathead Minnow) Laboratory or Author 3M Env. Lab Acute toxicity of FC-185F to activated sludge mixed liquor 3M Env. Lab Completion Date 2/1/82 1/28/82 Type Robust summary, technical report summary Robust summary, copies of data sheets FC-200 Summary Reports Title Laboratory or Completion Author Date Type Summary fos work performed for the German Government Agency for Military Technology and Procurement on fire extinguishing foam compounds from multiple companies Dr. H. Hellmann, D. Muller 10/12/77, 3/7/80 Robust summary, Technical Awareness Report, final report FC-201 Acronyms: Lab Request Number: 2563 Physical/Chemical Properties Title None available Environmental Fate and Transport Title Ready biodegradability of FC-201 (BOD/COD) Ecotoxicity Elements Title Laboratory or Completion Author Date Type Laboratory or Author 3M Env. Lab Completion Date 1/28/75 Type Robust summary, copies of data summary sheets Laboratory or Completion Author Date Type 1 000017 Acute static toxicity of FC-201 to fathead minnow 3M Env.Lab 1/11/75 Robust summary, copies of data sheets FC-201AF Acronyms: Lab Request Numbers: N2964, N3281, N3747, L-13652 Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability of FC-201 AF (BOD/COD) Ready biodegradability of FC-201AF (BOD/COD) Laboratory or Author MDS Environmental Services Limited, London, Ontario, Canada Pace Analytical Services, Golden Valley, MN Completion Date Type 5/24/95 2/6/96 Robust summary, summary report Robust summary, laboratory summary report, copies of data sheets Ecotoxicity Elements Laboratory or Title Acute static renewal toxicity of FC-201 AF to fathead minnow Acute toxicity of FC-201 AF to green algae, Selenastrum capricomutum Author 3M Env. Lab 3M Env. Lab Growth inhibition Test with the Marine Alga Skeletonema costatum - FC-201 AF Light Water Brand AFFF RF Rogaland Research, Stavanger, Norway RF Rogaland Acute Toxicity Test with the Marine Copepod Acartia tonsa Research, FC-201 AF Light Water Brand AFFF Stavanger, Norway Acute Toxicity Sediment Test with the Marine Amphipod Corophium volutator - FC-201 AF Light Water Brand AFFF RF Rogaland Research, Stavanger, Norway Acute static toxicity of FC-201 AF to Daphnia magna 3M Env. Lab Acute toxicity of FC-201 AF to Microtox 3M Env. Lab Acute toxicity of FC-201AF to activated sludge mixed liquor 3M Env. Lab Completion Date 10/20/95 1/7/96 1/5/00 1/5/00 1/5/00 8/31/95 12/2/95 9/14/95 Type Robust summary, copies of data sheets Robust summary, copies of data ` sheets Robust summary, final report Robust summary, final report Robust summary, final report Robust summary, copy of data sheet Robust summary, laboratory report, copies of data sheets Robust summary, copies of data' sheets FC-201F Acronyms: Lab Request Number: K1792 Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type 1 I j ' 2 000018 Environmental Fate and Transport Title Ready biodegradability of FC-201F (BOD/COD) Laboratory or Completion Author Date Hygiene Institute for the Ruhr District, Gelsenkirchen, Germany 9/13/93 Type I Robust summary, English language summary, German language report Ecotoxicity Elements Title Acute Toxicity of FC-201F to Fathead Minnow (Pimephales promelas) Further Investigation on the Acute Toxicity of FC-201F to Fathead Minnow (Pimephales promelas) Acute Toxicity of FC-201 F to Daphnia magna Laboratory or Author AscI Corporation, Duluth, MN AscI Corporation, Duluth, MN AscI Corporation, Duluth, MN Completion Date 8/24/92 10/5/92 8/21/92 Type Robust summary, final report Robust summary, final report Robust summary, final report Microbial inhibition (dehydrogenase activity) of FC-201 F Hygiene Institute for the Ruhr District, Gelsenkirchen,' Germany 9/13/93 Robust summary, English language summary, German language report Acute toxicity to fish (Leuciscus idus) Hygiene Institute for the Ruhr District, Gelsenkirchen, Germany 9/13/93 Robust summary, English language summary, German language report FC-201F-X Acronyms: Lab Request Number: K1126 Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability of FC-201 F-X (BOD/COD) Laboratory or Author Pace Incorporated, Minneapolis, MN Completion Date 2/17/92 Type Robust summary, laboratory summary report Ecotoxicity Elements Title Laboratory or Author Acute toxicity of FC-201 F-X to Microtox 3M Env. Lab Acute toxicity of FC-201 F-X to activated sludge mixed liquor 3M Env. Lab Completion Date 4/17/92 3/23/92 Type Robust summary, copies of data sheets Robust summary, copies of data sheets ! 3 000019 FC-203 Acronyms: VW 160390, Sample #5729, Sample 7902, 3M Sample B, Lab Request Numbers 1940, 2002, 2009, 2034, 2036, 2093, 2103, 4971, 4 9 7 1S, 5360A, 5541S, 8483, 9611, H2864-9, J1608-8, J2176-5 Physical/Chemical Properties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Summary of biodegradability tests of FC-203 (BOD/COD) Laboratory or Author 3M Env. Lab Completion Date 1973-1980 Type Robust summary, copies of data sheets OECD Biodegradation Testing on FC-600 and FC-203 3M Env. Lab Repeat OECD Biodegradation Test on FC-600 and FC-203 3M Env. Lab Modified OECD Screening Test on FC-203, FC-203A, and FC-600 Ready biodegradability of FC-203 (BOD/COD) 3M Env. Lab Pace Incorporated, Minneapolis, MN 4/18/83 6/16/83 7/9/84 8/13/91 Robust summary, Technical Report Summary Robust summary. Technical Report Summary. Robust summary, Technical Report Summary, selected copies of data sheets Robust summary, final report Ecotoxicity Elements Title Acute toxicity of FC-203 to rainbow trout Acute toxicity of Liqht Water" to blueaill fLeoomis mscrochirus) Summary o f acute static toxicity tests of FC-203 to bluegill Acute Toxicity of 3M Samples (A and B) to the Water Flea (Daphnia magnal and Scud (Gammarus fasciatus) - robust summary for Daphnia magna Acute Toxicity of 3M Samples (A and B) to the Water Flea (Daphnia maanal and Scud (Gammarus fasciatus) - robust summary for Gammarus fasciatus summary of microbial inhibition (dehydrogenase activity) tests on FC-203 Algicidal Activity of Two Samples Labeled "A" and "B" Acute static toxicity of FC-203 to rainbow trout i Laboratory or Author 3M Env. Lab Bionomics, Inc. Wareham, MA 3M Env. Lab Completion Date Unknown September, 1972 1973-1974 Type Robust summary, copy of data ' sheet Robust summary, final report Robust summary, copies of data sheets Bionomics, Inc. Wareham, MA December, 1973 Robust summary, final report Bionomics, Inc. Wareham, MA 3M Env. Lab Industrial Bio-Test Laboratories, Northbrook, 1L 3M Env. Lab December, 1973 1973-1974 1/23/74 2/23/74 Robust summary, final report Robust summary, copies of data sheets Robust summary, final report Robust summary, copies of data sheets 4 ooopzo Acute toxicity of 3M Company's sample 7902 to grass EG&G Bionomics Marine Research Laboratory, Pensacola, FL Acute Toxicity of 7902 to the Common Mummichog (Fundulus heteroclitus) EG&G Bionomics Marine Research Laboratory, Pensacola, FL Acute Toxicity of 3M Company's Sample 7902 to embryoslarvae of eastern oysters (Crassostrea virginica) EG&G Bionomics Marine Research Laboratory, Pensacola, FL Acute toxicity of Sample #5729 to embryo-larvae of eastern EG&G Bionomics Marine Research Laboratory, Pensacola, FL Static Acute Toxicity of FC 203 to the Alga, Seienastrum capricomutum Acute toxicity of FC-203 without Tolytirazole (VW160390) to Microtox EnviroSystems Division Resource Analysts, Inc., Hampton, NH 3M Env. Lab Static Acute Toxicity of FC 203 to the Daphnid. Daphnia maana EnviroSystems Division Resource Analysts, Inc., Hampton, NH Acute Toxicity Sediment Test with the Marine Amphipod Corophium volutator RF Rogaland Research, Stavanger, Norway Acute Toxicity Test with the Marine Copepod Acartia tonsa RF Rogaland Research, Stavanger, Norway Growth Inhibition Test with the Marine Alga Skeletonema costaturn RF Rogaland Research, Stavanger, Norway I August, 1979 August, 1979 Robust summary, final report -t Robust summary, final report August, 1979 Robust summary, final report July, 1980 Robust summary, final report June, 1991 7/19/91 Robust summary, final report Robust summary, summary sheet, copies of data sheets ; 8/9/91 1/6/00 1/6/00 1/6/00 Robust summary, final report Robust summary, final report Robust summary, final report Robust summary, final report Summary Reports Title Laboratory or Completion Author Date Investigations of toxic effects and biological degradability of foam extinguishing agents in the waste water Environmental Effects of LIGHT WATER Brand AFFF and Components - Robust summary for FC-203 Environmental Effects of LIGHT WATER Brand AFFF and Components - Robust summary for VW160390 (FC-203 without tolyltriazole) Ekkehard Ising 3M Env. Lab 3M Env. Lab 3/29/90 4/1/91 4/1/91 Type Abbreviated robust summary, summary report from German Army Robust summary, Technical Report Summary , Robust summary, Technical Report Summary FC-203A Acronyms: FC-203 NF, Lab Request Numbers: 2543, 2563,9611, Physical/Chemical Properties j 5 000|)2i 1 Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradablllty of FC-203A (BOD/COD) Biodegradation of "Light Water" Products In OECD Test 6/80 Effect of Biodegradation on Foaming of "Light Water" Products. Modified OECD Screening Test of FC-203, FC-203A, and FC-600 Laboratory or Author 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab Completion Date 1/28/75 6/30/80 8/6/80 7/9/84 Type Robust summary, data summary pages Robust summary, Technical Report Summary Robust summary, letter report, copies of data sheets Robust summary, Technical Report Summary Ecotoxicity Elements Title Acute toxicity of FC-203A to fathead minnow Laboratory or Completion Author Date 3M Env. Lab 1/11/75 Type Robust summary, copy of raw data FC-203C Acronyms: L-5440, 81-1/8 Lab Request Numbers; 6 8 1 1S, 7038, 7736, 7737, 7738, 7903, 7625 Physical/Chemical Properties Title None available Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-203C Laboratory or Completion Author Date Type l ! Laboratory or Completion Author Date Numerous 1981-1982 Type Robust summary of several studies, copies of data sheets . Ecotoxicity Elements Title Acute Toxicity of 81-1/8 to Fathead Minnow fPimephales Promelasl Acute Toxicity of a Surfactant Solution (81-1/8) to the Mummichog Fundulus heteroclitus in a Flow-through System. Laboratory or Author EG&G Bionomics, Wareham, MA EG&G Bionomics Marine research Laboratory, Pensacola, FL Completion Date October, 1981 October, 1981 Algal Assay: Bottle Test (AA:BT), Toxicity Testing FC-203C 3M Env. Lab 6/12/81 Type Robust summary, final report Robust summary, final report Robust summary, Technical Report Summary Acute toxicity of FC-203C to Daphnia magna 3M Env. Lab 7/6/81 Robust summary, data summary t 6 000022 Acute toxicity of FC-203C to activated sludge mixed liquor 3M Env. Lab 7/1/81 Robust summary, copies of data , sheets FC-203CE Acronyms: Lab Request Numbers: G1358-1, H 1480-1, H1480-3, J 1884-1 Physlcal/Chemical Properties Title None available Laboratory or Completion Author Date Type i Environmental Fate and Transport Title L ab o rato ry o r Completion Author Date Type Pace Laboratories, Ready blodegradabllity (BOD/COD) & TOC of FC-203CE Inc,. Minneapolis, MN Ready biodegradability (OECD 301E) of FC-203CE 3M Env. Lab 5/12/89 6/23/89 Robust summary, final report Robust summary, copies of data sheets Ecotoxicity Elements Title Laboratory or Author Acute static toxicity of FC-203CE to Daphnia magna' Acute static-renewal toxicity of FC-203CE to fathead minnow Acute toxicity of FC-203CE to green algae, Selenastrum capricomutum Toxicity of FC-203CE to activated sludge mixed liquor 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab Toxicity of FC-203CE to Microtox 3M Env. Lab Toxicity of FC-203CE to activated sludge mixed liquor Toxicity of FC-203CE + antifoamerto activated sludge mixed liquor Static Acute Toxicity of FC-203CE to the Daphnid, Daphnia magna Static Acute Toxicity of FC-203CE to the Alga, Selenastrum capricomutum 3M Env. Lab 3M Env. Lab EnviroSystems Division Resource Analysts, Inc., Hampton, NH EnviroSystems Division Resource Analysts, Inc., Hampton, NH Completion Date 5/13/89 5/15/89 5/28/89 Type Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets 6/16/89 3/19/90 3/19/90 Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets June, 1991 Robust summary, final report July, 1991 Robust summary, final report Summary Reports Title Environmental Effects of LIGHT WATER Brand AFFF and components - Robust summary for FC-203CE Laboratory or Author 3M Env. Lab Completion Date 4/1/91 Type Robust summary, Technical Report Summary | j 000023 FC-203CF Acronyms: FC-203CF-X, Lab Request Numbers: J1884-3, J1885-1, K1905-1, N2977, W1127, Physical/Chemical Properties_____________________ Title None available Laboratory or Author Completion Date Environmental Fate and Transport Title Ready biodegradability of FC-203CF (BOD/COD) Laboratory or Author Pace Incorporated, Minneapolis, MN Completion Date 7/2/91 Type ! i ( Type Robust summary, final report Ecotoxicity Elements Title Static Acute Toxicity of FC-203CF to the Fathead Minnow, Pimephales promelas Static Acute Toxicity of FC-203CF to the Daphnid, Daphnia magna Laboratory or Author EnviroSystems Division Resource Analysts, Inc. Hampton, NH EnviroSystems Division Resource Analysts, Inc. Hampton, NH Acute toxicity of FC-203CF to Microtox Static Acute Toxicity of FC-203CF to the Alga, Selenastrum capricomutum Acute toxicity of FC-203CF-X to activated sludge mixed liquor Acute toxicity of FC-203CF-X to nitrifying bacteria (ISO/DIS Method 9509) Acute toxicity of FC-203CF-X to nitrifying bacteria (NitroseedTM Method) Acute Toxicity of FC-203CF to Fathead Minnow (iPimephales promelas) 3M Env. Lab EnviroSystems Division Resource Analysts, Inc. Hampton, NH 3M Env. Lab 3M Env. Lab 3M Env. Lab ASci Corporation, Duluth, MN Completion Date Type June, 1991 Robust summary, final report July, 1991 7/19/91 Robust summary, final report Robust summary, copies of data sheets August, 1991 6/26/92 8/24/95 8/24/95 Robust summary, final report Robust summary, copies of data ' sheets Robust summary, copies of data sheets Robust summary, copies of data sheets 2/22/99 Robust summary, final report FC-203FC Acronyms: Lab Request Number: R1335 Physical/Chemlcal Properties Title None available Laboratory or Completion Author Date ... i( Type Environmental Fate and Transport Title Laboratory or Completion Author Date Type ' 000024 R1335 BOD Report for 3M Company AScI Corporation, Duluth, Mn September, 1997 Robust summary, final report Ecotoxicity Elements Title Toxicity of FC-203FC to Microtox Toxicity of FC-203FC to activated sludge mixed liquor Acute Toxicity of R1335 to Daphnia magna Growth inhibition of R1335 for Green Alga (Selenastrum capricomutum) Acute static toxicity of FC-203FC to fathead minnow Acute Toxicity of R1335 to Fathead Minnow (Pimephales promelas) Laboratory or Author 3M Env. Lab 3M Env. Lab AScI Corporation, Duluth, MN AScI Corporation, Duluth, MN 3M Env. Lab AScI Corporation, Duluth, MN Completion Date 3/17/97 3/24/97 Type 1 Robust summary, copies of data J sheets < Robust summary, copies o f data sheets 4/1/97 Robust summary, final report 4/7/97 4/18/97 Robust summary, final report Robust summary, copies of data sheets 6/26/97 Robust summary, final report ' FC-203S Acronyms: Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title None available Laboratory or Completion Author Date Type Ecotoxicity Elements Title Acute toxicity of FC-203S to Rainbow Trout Laboratory or Completion Author Date Type ABC Laboratories, Columbia, MO 12/2/88 Robust summary, summary letter, final report missing first 5 pages. FC-206 Acronyms: L3243, Sample C Lab Request Number: 2577 Physical/Chemical Properties Title None available Environmental Fate and Transport Title Laboratory or Completion Author Date Laboratory or Completion Author Date Type .T . < --i Type 9 000025 Ready biodegradability of FC-206 (BOD/COD) Ready biodegradability of FC-206 (BOD/COD) Biodegradation of "LIGHT WATER" Products in OECD Test 6/80 Effect of degradation on foaming of FC-206 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 1/16/75 6/30/76 6/30/80 8/6/80 Robust summary, results summary Robust summary, results summary Robust summary, Technical Report Summary Robust summary, letter report Ecotoxicity Elements Title Summary of microbial inhibition (dehydrogenase activity) tests on FC-206 Acute static toxicity of FC-206 to fathead minnow Acute static toxicity of FC-206 to rainbow trout Acute Toxicity of Sample C to Mummichoa fFundulus heteroclitusL Grass ShrimD (Palaemonetes vulaarisl and Fiddler Crab iUca puailatorl - Robust summary for mummichog Acute Toxicity of Sample C to Mummichoa fFundulus heteroclitusL Grass Shrimp fPalaemonetes vulaarisl and Fiddler Crab fUca puailatorl - Robust summary for grass shrimp Acute Toxicitv of Sample C to Mummichoa fFundulus Laboratory or Author 3M Env. Lab 3M Env. Lab 3M Env. Lab Completion Date 1973-1974 2/15/74 4/5/74 Type Robust summary, copy of data sheet Robust summary, copies of data sheets Robust summary, copy of data sheet Bionomics EG&G, Wareham, MA May, 1974 Robust summary, final report Bionomics EG&G, Wareham, MA May, 1974 Robust summary, final report Fiddler Crab fUca puailatorl - Robust summary for fiddler crab Acute Toxicity of Sample C to Atlantic Ovster fCrassostrea vlrainical Acute Toxicity of Sample C to Water Flea fDaphnia maana) and Scud (Gammarus fasciatusL - Robust summary for Daphnia magna Acute Toxicity of Sample C to Water Flea fDaphnia maana) and Scud fGammarus fasciatusL - Robust summary for Scud Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Acute static toxicity of FC-206 to fathead minnow Acute static toxicity of FC-206 amended to soil to fathead minnow 3M Env. Lab 3M Env. Lab Acute flow-through toxicity of FC-206 to bluegill sunfish 3M Env. Lab Summary Reports Title Laboratory or Author Investigations of toxic effects and biological degradability of foam extinguishing agents in the waste water Ekkehard Ising May, 1974 July, 1974 August, 1974 August, 1974 6/19/76 11/6/76 11/11/78 Completion Date 3/29/90 Robust summary, final report Robust summary, final report Robust summary, final report Robust summary, final report Robust summary, copy of data sheet Robust summary, copies o f data sheets Robust summary, copy of data sheet I Type Abbreviated robust summary, summary report from German Army Summary for work performed for the German Government Agency for Military Technology and Procurement on fire extinguishing foam compounds from multiple companies Dr. H. Hellmann, D. Muller 10/12/77, 3/7/80 Robust summary, Technical Awareness Report, final report ! 10 I FC-206A Acronyms: Physical/Chemical Properties Title None available Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-206A I Laboratory or Completion Author Date Type S Laboratory or Author 3M Env. Lab Completion Date 11/10/78 i) Type Robust summary, copies of data sheets Ecotoxlcity Elements Title FC-206A cc 785-22: Results of Aquatic 96-hr. LC50 Tests (bluegill sunfish)' Acute static toxicity of FC-206A to fathead minnow Acute flow-through toxicity of FC-206A to fathead minnow Acute toxicity of FC-206A to Daphnia magna Microbial inhibition (dehydrogenase activity) of FC-206A Acute toxicity of FC-206A to activated sludge mixed liquor Laboratory or Author 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab Completion Date 11/2/78 7/14/79 7/21/79 7/14/79 11/29/79 8/8/79 Type Robust summary, Technical Report Summary Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets FC-206C Acronyms:L-5439, 81-2/8, Lab Request Numbers; 6812S, 7625, 7736, 7737, 7738, 7903, Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type 4 I ! Environmental Fate and Transport Title Ready blodegradabillty (BOD/COD) of FC-206C Laboratory or Completion Author Date Numerous 1981-1982 Type Robust summary of several studies, copies of data sheets Ecotoxicity Elements Title Acute toxicity of FC-206C to activated sludge mixed liquor Laboratory or Author 3M Env. Lab Completion Date 7/1/81 Type Robust summary, copies of data sheets 11 000^)27 i Acute Toxicity of 81-2/8 to Fathead Minnow fPimephales oromelasl Acute Toxicity of a Surfactant Solution to the Mummichog /Fundulus heteroclitusi in a Flow-through System. (FC206C) EG&G Bionomics, Wareham, MA October, 1981 EG&G Bionomics, Pensacola, FL September, 1981 Algal Assay: Bottle Test (AA:BT), Toxicity Testing FC-206C 3M Env. Lab 6/23/81 Robust summary, final report Robust summary, final report Robust summary, Technical Report summary FC-206CE Acronyms: Lab Request Numberts: G1358-2, J 1884-2, H1480-2, H1480-4 Physical/Chomical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-206CE Ready biodegradability (OECD 301E) of FC-206CE Laboratory or Completion Author Date Type Pace Laboratories, Inc, Minneapolis, MN 3M Env. Lab 5/12/89 6/23/89 Robust summary, final report Robust summary, copies of data sheets Ecotoxicity Elements Title Laboratory or Completion Author Date Acute static toxicity of FC-206CE to Daphnia magna 3M Env. Lab 4/6/89 Acute static toxicity of FC-206CE to Daphnia magna Acute static-renewal toxicity or FC-206CE to fathead minnow Acute toxicity of FC-206CE to green algae, Setenastrum capricomutum 3M Env. Lab 3M Env. Lab 3M Env. Lab 5/13/89 5/15/89 5/28/89 Acute toxicity of FC-206CE to Microtox 3M Env. Lab 6/16/89 Acute toxicity of FC-206CE to activated sludge mixed liquor 3M Env. Lab 6/23/89 Acute toxicity of FC-206CE to activated sludge mixed liquor 3M Env. Lab Acute toxicity of FC-206CE + antifoamer to activated sludge mixed liquor 3M Env. Lab Static Acute Toxicity of FC-206CE to the Daphnid, Daphnia magna EnviroSystems Division of Resource Analysts Inc., Hampton, NH EnviroSystems Division of Resource Static Acute Toxicity of FC-206CE to the Alga, Selenastrum Analysts Inc., capricomutum Hampton, NH 3/23/90 3/23/90 June, 1991 July, 1991 Type Robust summary, copy of data sheet Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, final report - Robust summary, final report 12 000028 I i Summary Reports Title Environmental Effects of LIGHT WATER Brand AFFF and components - Robust summary for FC-206CE Laboratory or Author 3M Env. Lab Completion Date 4/1/91 Type Robust summary, Technical Report Summary FC-206CF Acronyms: FC-206CF-X Lab Request Numbers: J1884-4, J1885-2, K1905 Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability of FC-206CF (BOD/COD) Laboratory or Author Pace Incorporated, Minneapolis, MN Completion Date 7/2/91 Type Robust summary, final report Ecotoxicity Elements Static Acute Toxicity of FC 206CF to the Fathead Minnow, Pimephales promelas Static Acute Toxicity of FC-206CF to the Daphnid, Daphnia magna EnviroSystems Division Resource Analysts, Inc., Hampton, NH EnviroSystems Division Resource Analysts, Inc., Hampton, NH Acute toxicity of FC-206CF to Microtox Static Acute Toxicity of FC 206CF to the Alga, Selenastrum capricomutum Acute toxicity of FC-206CF-X to activated sludge mixed liquor 3M Env. Lab EnviroSystems Division Resource Analysts, Inc., Hampton, NH 3M Env. Lab June, 1991 Robust summary, final report June, 1991 7/19/91 Robust summary, final report Robust summary, copies of data sheets August, 1991 6/26/92 Robust summary, final report Robust summary, copies of data sheets FC-600 Acronyms: 3M-I Lab Request Numbers: 2874,8483,8873,8875,9063,9595, Physical/Chemical Properties Title None available Environmental Fate and Transport Laboratory or Completion Author Date Type j 13 0 0 0 0 2 9 Title Laboratory or Completion Author Date Type Summary of ready biodegradability studies on FC-600 Ecotoxicity Elements Title Acute static toxicity of FC-600 to fathead minnow Acute static toxicity of FC-600 to bluegill sunfish 3M Env. Lab 8/15/75, 10/27/82, Abbreviated robust summary,' 4/18/83, 7/9/84, copies of data sheets, Technical 10/4/88, Report Summaries 1 Laboratory or Author 3M Env. Lab 3M Env. Lab Completion Date 8/29/75 8/29/75 Type Robust summary, copies of data sheets Robust summary, copies of data sheets Acute static toxicity of FC-600 to Daphnia magna - first of 3 studies of effluent from an FC-600-exposed SCAS reactor 3M Env. Lab 8/10/77 Robust summary, copies of data sheets Acute static toxicity of FC-600 to Daphnia magna - second of 3 studies of effluent from an FC-600-exposed SCAS reactor (treated reactor after 4-hours of treatment) 3M Env. Lab 8/10/77 Robust summary, copies of data sheets Acute static toxicity of FC-600 to Daphnia magna - third of 3 studies of effluent from an FC-600-exposed SCAS reactor (blank control reactor after 4-hours of treatment) 3M Env. Lab Acute toxicity of FC-600 to activated sludge mixed liquor Acute toxicity of FC-600 (from Antwerp, Belgium) to activated sludge mixed liquor Range-finding study of acute toxicity of FC-600 (US) to fathead minnow Range-finding study of acute toxicity of FC-600 (Belgium) to fathead minnow Range-finding study of acute toxicity of FC-600 (US) to fathead minnow Range-finding study of acute toxicity of FC-600 (Belgium) to fathead minnow Dynamic Acute Toxicity of3M-l to Fathead Minnows 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab Analytical Bio- Chemistry Laboratories, Inc. Columbia, MO Aquatic Toxicity Testing: FC-600 (Belgium-AFFF) LR 9595 3M Env. Lab 8/10/77 2/1/83 2/1/83 2/10/83 2/10/83 2/10/83 2/10/83 Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets 3/29/83 7/21/83 Robust summary, final report Robust summary, Technical Report Summary i FX-601 Acronyms: Lab Request Number: B1684 Physlcal/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport i 14 0 0 0 0 3 0 Title None avialble Ecotoxicity Elements Title Acute static toxicity of FX-601 to fathead minnow Acute toxicity of FX-601 to activated sludge mixed liquor Laboratory or Completion Author Date Type Laboratory or Author 3M Env. Lab 3M Env. Lab Completion Date 6/15/84 6/20/84 Type Robust summary, copies of data sheets. Robust summary, copies of data sheets. FC-602 Acronyms: FC-602-X, FC-602-ATC, Lab Request Number: F1151 Physlcal/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-602 Laboratory or Completion Author Date Pace Laboratories, Inc. Minneapolis, MN 3/4/88 Type Robust summary, final report Ecotoxicity Elements Title Laboratory or Author Toxicity of FC-602 to Microtox 3M Env. Lab Acute static toxicity of FC-602-X to Daphnia magna 3M Env. Lab Acute static toxicity of FC-602-X to fathead minnow Acute Toxicity Test with the Marine Copepod Acadia tonsa (FC-602) Growth Inhibition Test with the Marine Alga Skeletonema costaturn FC-602) Acute Toxicity Sediment Test with the Marine Amphipod Corophium volutator (FC-602) 3M Env. Lab RF Rogaland Research, Stavanger, Norway RF Rogaland Research, Stavanger, Norway RF Rogaland Research, Stavanger, Norway Completion Date 1/28/88 3/17/88 3/25/88 1/7/00 1/7/00 1/7/00 Type Robust summary, copies o f data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, final report Robust summary, final report Robust summary, final report FC-603EF Acronyms: Lab Request Number: P2581 Physlcal/Chemical Properties 15 ! 000(j>3 Title None available Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-603EF Laboratory or Completion Author Date Type Laboratory or Author 3M Env. Lab i Completion Date Dec., 1996 Type Robust summary, copies of data sheets Ecotoxicity Elements Title Acute toxicity of FC-603EF to the Golden Orfe {Leuciscus idus) Acute toxicity of FC-603EF to the alga, Scenedesmus subspicatus Acute toxicity of FC-603EF to Daphnia magna Bacterial dehydrogenase activity of FC-603EF by the TTC method Toxicity of FC-603EF to activated sludge Laboratory or Author Hygiene-Institut des Ruhrgebiets, Gelsenkirchen, Germany Hygiene-Institut des Ruhrgebiets, Gelsenkirchen, Germany Hygiene-Institut des Ruhrgebiets, Gelsenkirchen, Germany Hygiene-Institut des Ruhrgebiets, Gelsenkirchen, Germany Hygiene-Institut des Ruhrgebiets, Gelsenkirchen, Germany Toxicity of FC-603EF to Microtox 3M Env. Lab Toxicity of FC-603EF to activated sludge mixed liquor Acute Toxicity of FC-603EF, Light Water (TM) ATC 3% ARAFFF to Daphnia magna 3M Env. Lab ASci Corporation, Duluth, MN Completion Date 9/26/96 9/26/96 9/26/96 9/26/96 9/26/96 10/22/96 10/23/96 11/7/96 Type Robust summary, Final report in the German language Robust summary, Final report in the German language Robust summary, Final report in the German language Robust summary, Final report in the German language Robust summary. Final report in the German language Robust summary, laboratory summary report, copies of data sheets Robust summary, copies of data sheets Robust summary, final report Growth Inhibition of FC-603EF, Light Water (TM) ATC 3%, AR-AFFF to Green Alga (Selenastmm capricomutum) ASci Corporation, Duluth, MN Acute Toxicity of FC-603EF, Light Water (TM) ATC 3% AR- ASci Corporation, AFFF to Fathead Minnow {Pimephales promelas) Duluth, MN Growth Inhibition Test with the Marine Alga Skeletonema costatum - FC-603EF RF Rogaland Research, Stavanger, Norway RF Rogaland Acute Toxicity Test with the Marine Copepod Acartia tonsa Research, FC-603EF Stavanger, Norway Acute Toxicity Sediment Test with the Marine Amphipod Corophium volutator - FC-603EF RF Rogaland Research, Stavanger, Norway 11/22/96 1/28/97 1/14/00 1/14/00 1/14/00 Robust summary, final report Robust summary, final report. Robust summary, final report Robust summary, final report Robust summary, final report 16 0 0 0 p 3 2 FC-603F Acronyms: Lab Request Number: M1655 Physical/Chemlcal Properties_________________ Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-603F Laboratory or Author Pace Inc., Minneapolis, MN Completion Date 5/10/94 Type Robust summaries, summary reports Ecotoxiclty Elements Title Acute static toxicity of FC-603F to fathead minnow Acute static toxicity of FC-603F to Selenastrum capricornutum Acute static toxicity of FC-603F to Daphnia magna Toxicity of FC-603F to Microtox Acute toxicity of FC-603F to activated sludge mixed liquor FC-780 Acronyms: Physical/Chemical Properties Title None available Laboratory or Author 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab Laboratory or Author Completion Date 5/27/94 10/13/95 5/27/94 5/20/94 5/10/94 Completion Date Type Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets , I Type Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-780 Laboratory or Completion Author Date Numerous 4/23/82 Type Robust summaries, summary reports Ecotoxiclty Elements Title Acute toxicity to Mummichog (Fundulus heteroclitusl Laboratory or Completion Author Date Type Naval Research Laboratory, Fire Supression Section, Washington, D.C. 6/11/82 Robust summary, summary report 17 0 0 0 0 3 3 FC-780B Acronyms: 7901, Sample 1-3, AFFF C, Lab Request Numbers: 4461, 4653, 4673, 5598, 6211 S 7685 Physical/Chemlcal Properties Title None available Environmental Fate and Transport Title Ready biodegradability of FC-780B (BOD/COD) Ready biodegradability of FC-780B (AFFF C) (OECD Closed Bottle Test) Ecotoxicity Elements Title 780B (lot 788-20): Results of Aquatic 96 Hr. LC50 Tests Acute Toxicity of 7901 to the Common Mummichog Dynamic 96-Hour Acute Toxicity of 3M Sample 1-3 to Fathead Minnows /Pimephales promelasl Laboratory or Completion Author Date Type Laboratory or Author Numerous 3M Env. Lab Completion Date Numerous 11/28/80 Type Abbreviated robust summary, copies of data sheets Robust summary, copies of data sheets Laboratory or Completion Author Date 3M Env. Lab EG&G Bionomics, Wareham, MA Analytical Bio Chemistry Laboratories, Inc. Columbia, MO 11/15/78 April, 1979 9/29/80 Type Robust summary, Technical Report Summary Robust summary, final report Robust summary, final report FC-783 Acronyms: 3M sample no. 6, Lab Request Number: 4896 Physical/Chemlcal Properties Title None available Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-783 Ecotoxicity Elements Title Acute Toxicity of 3M Sample No. 6 to Bluegill Sunfish Laboratory or Completion Author Date Type Laboratory or Author 3M Env. Lab Completion Date 6/8/79 Type Robust summary, copies of data, sheets Laboratory or Author Analytical Bio Chemistry Laboratories, Inc., Columbia, MO Completion Date 6/19/79 Type Robust summary, final report 18 0 0 0 0 3 4 1 Acute toxicity of FC-783 to activated sludge mixed liquor 3M Env. Lab 6/4/79 Robust summary, copies of data sheets i FC-787 Acronyms: FC-787-X. Lab Request Numbers: H1608, H1609 Physicol/Chomical Properties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradability of FC-787 (BOD/COD) Laboratory or Completion Author Date Type Serco Laboratories, 9/28/90,10/13/90, St Paul, MN 11/2/90 Robust summary, final report Ecotoxicity Elements Title Acute toxicity of FC-787 to Microtox Static Acute Toxicity of FC-787 to the Daphnid, Daphnia magna Flow Through Acute Toxicity of Fc-787 to the Fathead Minnow, Pimephales promelas Laboratory or Author 3M Env. Lab EnviroSystems Division Resource Analysts, Inc., Hampton, NH EnviroSystems Division Resource Analysts, Inc., Hampton, NH Completion Date 8/16/90 9/4/90 9/20/90 , Type Robust summary, copies of data sheets Robust summary, final report Robust summary, final report FC-3003 Acronyms: Lab Request Number: R1331 Physical/Chemical Properties Title None available Environmental Fate and Transport Title R1331 BOD Report for 3M Company Ecotoxicity Elements Title Toxicity of FC-3003 to Microtox Laboratory or Completion Author Date Type Laboratory or Author AScI Corporation, Duluth, MN Completion Date August, 1997 Type Robust summary, final report Laboratory or Author 3M Env. Lab . Completion Date 3/13/97 Type Robust summary, copies of data sheets 000035 i Toxicity of FC-3003 to activated sludge mixed liquor Acute Toxicity of R1331 to Daphnia magna Growth Inhibition of R1331 for Green alga (Selenastrum capricomutum) Acute static toxicity of FC-3003 to fathead minnow Acute Toxicity of R1331 to Fathead Minnow (Pimephalas promelas) 3M Env. Lab ASci Corporation, Duluth, MN ASci Corporation, Duluth, MN 3M Env. Lab ASci Corporation, Duluth, MN 3/21/97 3/27/97 4/3/97 . 4/18/97 6/26/97 Robust summary, copies of data sheets Robust summary, final report Robust summary, final report Robust summary and copies of data sheets Robust summary, final report FC-3017 Acronyms: Lab Request Numbers: N3188, N3688 Physlcal/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport_________________________________________________________________________________ j l Laboratory or Completion Title Author Date Type Biodegradation of "Light Water" Products in OECD Test 6/80 3M Env. Lab 6/30/80 Robust summary, technical report summary N3688 BOD Report for 3M Company ASci Corporation, Duluth, MN April, 1996 Robust summary, final report Ecotoxicity Elements Title Acute toxicity of FC-3017 to Microtox Acute static renewal toxicity of FC-3017 to fathead minnow Acute toxicity of FC-3017 to activated sludge mixed liquor Acute Toxicity of FC-3017 to Daphnia magna Acute toxicity of FC-3017 to Selenastmm capricomutum Laboratory or Author 3M Env. Lab 3M Env. Lab 3M Env. Lab ASci Corporation, Duluth, MN 3M Env. Lab Completion Date 9/26/95 9/29/95 9/29/95 12/23/95 1/16/96 4 Type Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, final report Robust summary, laboratory summary report, copies of data sheets Summary Reports Title Laboratory or Completion Author Date Type Summary for work performed for the German Government Agency for Military Technology and Procurement on fire extinguishing foam compounds from multiple companies Dr. H. Hellmann, D. Muller 10/12/77 Robust summary, Technical Awareness Report, final report FC-3031 20 0 0 0 0 3 6 i Acronyms: Lab Request Number: N3188 Physical/Chemical Properties Title None available Environmental Fate and Transport Title None available Ecotoxicity Elements Title Acute static toxicity of FC-3031 to fathead minnow Laboratory or Completion Author Date Laboratory or Completion Author Date Type Type ? Laboratory or Author 3M Env. Lab Completion Date 8/14/76 Type Robust summary, copies of data sheets FC-3041 Acronyms: Lab Request Number: 6508S Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FC-3041 Investigation for the Eco-toxicological Evaluation of the Fluoro-surfactant Base FC-3041. Aerobic Degradation. P a rtf Investigation for the Eco-toxicological Evaluation of the Fluoro-surfactant Base FC-3041. Anaerobic Degradation. Part g Laboratory or Author 3M Env. Lab Fraunhofer Institute for Environmental Chemistry and Eco- toxicology, Schmallenberg, Germany Fraunhofer Institute for Environmental Chemistry and Eco- toxicology, Schmallenberg, Germany Completion Date 3/5/81 December, 1993 December, 1993 } Type Robust summary, copies of data sheets Robust summary, final report Robust summary, final report Ecotoxicfty Elements Title Acute static toxicity of FC-3041 to fathead minnow Acute static toxicity of FC-3041 to Daphnia magna Acute toxicity of FC-3041 to activated sludge mixed liquor Laboratory or Completion Author Date 3M Env. Lab 2/13/81 3M Env. Lab 2/13/81 3M Env. Lab 3/6/81 Type Robust summary and copies of data sheets Robust summary and copies of data sheets Robust summary and copies of data sheets 21 000037 J\ FC-3052 Acronyms: Lab Request Number: W2039-2 Physical/Chemical Properties Title None available Environmental Fate and Transport Title None available Ecotoxicity Elements Title Acute Toxicity of FC-3052 to Rainbow Trout (Oncorhynchus mykiss) Laboratory or Completion Author Date Type Laboratory or Completion Author Date Type Laboratory or Author AScI Corporation, Duluth, MN Completion Date 7/19/99 Type Robust summary, final report FC-3072 Acronyms: Lab Request: M3597 Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type \ \ Environmental Fate and Transport Title None available Laboratory or Completion Author Date Type Ecotoxicity Elements Title Acute Toxicity of FC-3072 to Fathead Minnow (Pimephales Promelas) Laboratory or Author AScI Corporation, Duluth, MN Acute static toxicity of FC-3072 to Daphnia magna 3M Env. Lab Acute toxicity of FC-3072 to Microtox Acute toxicity of FC-3072 to activated sludge mixed liquor 3M Env. Lab 3M Env. Lab Completion Date Type 3/20/95 3/23/95 3/15/95 3/20/95 Robust summary, final report Robust summary, copy of data sheet Robust summary, copy of laboratory summary report, copies of raw data sheets Robust summary, copies of data sheets FX-3103 Acronyms: Lab Request Number: C 1 111-1 Physical/Chemical Properties 1 22 0 0 0 0 S Title None available Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FX-3103 Laboratory or Completion Author Date Type Laboratory or Author 3M Env. Lab i Completion Date 4/18/85 Type Robust summary, laboratory data summary Ecotoxlcity Elements Title Acute static toxicity of FX-3103 to fathead minnow Acute static toxicity of FX-3103 to Selenastrum capricomutum Acute static toxicity of FX-3103 to Daphnia magna Toxicity of FX-3103 to Microtox Acute toxicity of FX-3103 to activated sludge mixed liquor Laboratory or Completion Author Date 3M Env. Lab 2/8/85 3M Env. Lab 2/23/85 3M Env. Lab 2/8/85 3M Env. Lab 2/5/85 3M Env. Lab 2/20/85 Type Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets FX-3104 Acronyms: Lab Request Number: C1111-2 Physical/Chemlcal Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FX-3104 Ecotoxlcity Elements Title Acute static toxicity of FX-3104 to fathead minnow Acute static toxicity of FX-3104 to Selenastrum capricomutum Acute static toxicity of FX-3104 to Daphnia magna Toxicity of FX-3104 to Microtox Acute toxicity of FX-3104 to activated sludge mixed liquor Laboratory or Author 3M Env. Lab Completion Date 4/18/85 Type Robust summary, laboratory data summary <r Laboratory or Author 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab Completion Date 2/8/85 2/23/85 2/8/85 2/6/85 2/20/85 Type Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets 000033 FX-3106 Acronyms: Lab Request: C2282 Physical/Chemical Properties Title None available Laboratory or Completion Author Date Type Environmental Fate and Transport Title Ready biodegradability (BOD/COD) of FX-3106 Laboratory or Author 3M Env. Lab Completion Date 11/26/85 Type Robust summary, copies of data sheets Ecotoxicity Elements Title Acute static renewal toxicity of FX-3106 to fathead minnow Toxicity of FX-3106 to Microtox Laboratory or Author 3M Env. Lab 3M Env. Lab Completion Date 11/2/85 10/28/85 Type Robust summary, copies o f data sheets. Robust summary, copies of data sheets. L-4647 Acronyms: Lab Request Number: 5623S Physical/Chemical Properties Title None available Environmental Fate and Transport Title Ready biodegradabifity (BOD/COD) of L-4647 Ecotoxicity Elements Title Acute static toxicity of L-4647 to fathead minnow Miscellaneous Studies Title Summary for foaming studies done on vairous AFFF products Laboratory or Completion Author Date Type Laboratory or Author 3M Env. Lab Completion Date 5/21/80 Type Robust summary, copies of data sheets Laboratory or Author 3M Env. Lab Completion Date 6/28/80 Type Robust summary, copies of data sheets. i Laboratory or Author 3M Env. Lab Completion Date 8/15/79, 6/18/81, 3/15/82, 3/16/90, 8/19/92, 1/27/94, 3/20/95 Type Abbreviated robust summary, reports, copies of data sheets. J, 24 000040 BibliAogttraacphhmyeonRftPselutaobtelLidsehttetoedrPLFtoiOteCSr.aMAtuuirxeetruirndea3stMed's6/P2o8s/0se0ssion 1. A33R9e,vRieewseaorfcFhirCeoFntirgahcttionrg: FWoaRmcsptico,IEdnevnitrifoynPmreinortiAtiegsenfocry,EUQKS,D1e9v9e4lo. pment. R&D Note 2. DAenfseunlsCeoTmepchannyic.alFIinnafolrRmeaptoirotn: CEennvtierronNm00en1t7a3ll-y76Im-Cp-r0o2v9e5d, ADFecFeFm. bDeerpa1r3t,m1e9n9t7o. f 3. BNaasvsa,lCC.Mivi.l SEonigl itnreeaetrminegnLt aobfoArFatFoFry:.MTicMroNtoox. t8o0x-i5c4it-y14m.onSietpotr. e1v9a8l0u.ation: Phase 1. 4. tBlAihqaFrusoFsiuFd,g:CchPh.Mahro.s.DmaT.nahdDte,oigssfsoraeaitrlep,thaaotynridoaannce,dtfifUvtehanctetiesvdBeorecfscaiahrtqymbuooaennfobOuMisokifflciiallrhtmoeotrmofowxaritmt(oh1xi9nai8cgpi2ptf)yoe.anmmdoicn(eAistFoorFnaFhp)ipgalshicipattepiroafnosssremtsoance 5. BpfCorahaotamtcnae,ls(iDAsoenF.sB.FC.FeTnT)Mt-oexrAN,icosA.usuumMbgms-.t5aa14rn9-yc88e00o:.-f1Dp0ir,sopCgorisveaisllsEotonf gwdiaantseeteeorwninadgteeLrvaecblooonprtmaatioenrniynt,goNfaaqavlulaeAloCuFsFonfFislttmrreufacottmriomennintg 6. WECnhagetnienr,eGTerhuirnooqguiDngghepUaanVrdtmFPaehrnohtt,aoUnlygnsiiSvsheaarndsdimtyPahnoo.ftAoRcreaimztoaonlvyaat,ilcToOufcxTsiordanac,teiAoSnru.izroCfanhcateam8n5it7cfa2rl1o.&mEUnltvriarpounrmeental 7. HAmowereilcl,aRn .EDn.v, iarnodnmE.eEn.taTluLcakbeor.raRtoermyo1v2a(l1o9f9s6u)rf1a0c.tants from fire extinguishing foam. 8. MImopoadcyte, dCb.Ay.Fainred-FJ.iAgh. tFiniegldA. cDtivetiteyr,mEinnavtirioonnmofenPtearlflSucoireonccaerb&oxTyelcahtensoilnogGyr,oVuonld.w3a3t,eNr o. 16, (1999), pp. 2800-2806. 9. ESanagmin,eRer.inangdLPa.bRoraaktoorwys.kiT. MFiNreo.fig5h4t-i7n9g-1s4c.hJouonlew, a1s9t7e9t.reatment study. Naval Civil 000041